CN105819944A - Pest dispelling and killing component-containing granular fertilizer coating membrane paste and preparation method thereof - Google Patents

Pest dispelling and killing component-containing granular fertilizer coating membrane paste and preparation method thereof Download PDF

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Publication number
CN105819944A
CN105819944A CN201610122194.1A CN201610122194A CN105819944A CN 105819944 A CN105819944 A CN 105819944A CN 201610122194 A CN201610122194 A CN 201610122194A CN 105819944 A CN105819944 A CN 105819944A
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China
Prior art keywords
parts
cortex
granular fertilizer
paste
raw material
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Withdrawn
Application number
CN201610122194.1A
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Chinese (zh)
Inventor
朱斌
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Hexian Zhuhan Melon And Fruit Growing Family Farm
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Hexian Zhuhan Melon And Fruit Growing Family Farm
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Priority to CN201610122194.1A priority Critical patent/CN105819944A/en
Publication of CN105819944A publication Critical patent/CN105819944A/en
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    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/60—Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants
    • C—CHEMISTRY; METALLURGY
    • C05—FERTILISERS; MANUFACTURE THEREOF
    • C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G5/00—Fertilisers characterised by their form
    • C05G5/30—Layered or coated, e.g. dust-preventing coatings

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  • Life Sciences & Earth Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Plant Pathology (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Fertilizers (AREA)

Abstract

A pest dispelling and killing component-containing granular fertilizer coating membrane paste is prepared from 60-80 parts of diatomite, 20-30 parts of talcum powder, 3-5 parts of polyvinyl alcohol, 4-6 parts of copovidone, 8-10 parts of hydroxypropyl methylcellulose, 3-5 parts of magnesium stearate, 2-4 parts of tween, 2-4 parts of castor oil, 15-25 parts of hydroxypropyl-beta-cyclodextrin, 6-8 parts of stearic acid, 6-8 parts of glyceryl behenate, 7-9 parts of a bonding film forming agent, 3-5 parts of Cortex Meliae, 2-4 parts of castor beans, 2-4 parts of Fructus Viticis, 15-25 parts of sodium humate, 6-8 parts of Ailantus Endocuticle, 7-9 parts of babylon weeping willow root-bark, 2-4 parts of Longmiao, 5-7 parts of chalcanthite and 8-10 parts of realgar. The coating membrane paste prepared the invention has the advantages of simple components, easy industrialization and very good dissolving performance, and can be immediately dissolved when the paste meets water or moist air; and pest dispelling and killing components arranged in the paste can realize sterilization efficacy, so the paste adopting traditional Chinese medicines to dispel and kill pests has the advantages of no peculiar smell, low cost, and very good economic and social benefits.

Description

A kind of granular fertilizer coating membrane cream containing expelling worm composition and preparation method thereof
Technical field
The present invention relates to technical field of fertilizers, be specifically related to a kind of granular fertilizer coating containing expelling worm composition Film cream and preparation method thereof.
Background technology
Coating is most important in modern science and technology, is also one of the technique of forefront, and it is at specific equipment In, by specific technique, the material of film forming is coated in the outer surface of granular solids preparation so that it is dried Become and be adhered tightly to one or more layers different thickness on surface, different elastic Multifunctional protective sheath, this Individual Multifunctional protective sheath is just called coating.
Fertilizer, is indispensable nutrition material in current agricultural planting, and it is permissible in normal application Ensureing increasing rapidly of crops, promote that crop yield is high, being to provide one or more plants must The nutrient needed, improves a class material of soil property, level of increasing soil fertility, and fertilizer type is numerous Many, there is a foliage fertilizer, powder is fertile, granular fertilizer etc., and most often granular fertilizer on market, it is due to system Standby simple, resistance to and storage, the most well utilized.
Along with improving constantly of people's agricultural planting technique, traditional fertilizer is carried out by technical staff Certain technological transformation, in recent years, medicine fertilizer the most gradually enters the people visual field, and medicine fertilizer not only possesses former Have provides trophic function to crops, the most also has the functions such as sterilization anthelmintic concurrently, but traditional medicine Fertilizer, when it is prepared, technique is the simplest and the crudest, simply through common crushing, stirring, mixing, so process After fertilizer not only nutrient to fertilizer cause part to run off, and drug effect is also greatly affected
Summary of the invention
The technical problem to be solved is to provide a kind of formula reasonable, and preparation method is simple, makes Granular fertilizer coating membrane cream significantly containing expelling worm composition by effect and preparation method thereof.
The technical problem to be solved realizes by the following technical solutions:
A kind of granular fertilizer coating membrane cream containing expelling worm composition, it is characterised in that: former by following components Material is made:
Kieselguhr 60-80 part, Pulvis Talci 20-30 part, polyvinyl alcohol 3-5 part, copolyvidone 4-6 part, hydroxyl Third methylcellulose 8-10 part, magnesium stearate 3-5 part, tween 2-4 part, Oleum Ricini 2-4 part, hydroxy propyl-Beta- Cyclodextrin 15-25 part, stearic acid 6-8 part, Glyceryl Behenate 6-8 part, it is bonded to membrane 7-9 part, hardship Chinaberry skin 3-5 part, Semen Ricini 2-4 part, Fructus Viticis 2-4 part, sodium humate 15-25 part, Cortex toonae sinensis radicis 6-8 part, Cortex Salicis Babylonicae Radicis 7-9 part, dragon Seedling 2-4 part, Chalcanthitum 5-7 part, Realgar 8-10 part.
The preferred ingredient of each raw material is: 70 parts of kieselguhr, Pulvis Talci 25 parts, polyvinyl alcohol 4 parts, copolymerization dimension Ketone 5 parts, hypromellose 9 parts, magnesium stearate 4 parts, tween 3 parts, Oleum Ricini 3 parts, hydroxy propyl-Beta- Cyclodextrin 20 parts, stearic acid 7 parts, Glyceryl Behenate 7 parts, be bonded to membrane 8 parts, Cortex Meliae 4 parts, Semen Ricini 3 parts, Fructus Viticis 3 parts, sodium humate 20 parts, Cortex toonae sinensis radicis 7 parts, Cortex Salicis Babylonicae Radicis 8 parts, dragon Seedling 3 parts, 6 parts of Chalcanthitum, Realgar 9 parts.
Described bonding film former is entered by chitosan 3 parts, polyvinyl alcohol 4 parts, glycerol 6 parts and gibberellins 6 parts Row is compounding to be made.
It is a further object of the present invention to provide a kind of granular fertilizer coating membrane cream preparation side containing expelling worm composition Method, step is as follows,
1) by the kieselguhr in raw material, Pulvis Talci, polyvinyl alcohol, copolyvidone, hypromellose, Magnesium stearate, tween, Oleum Ricini, HP-β-CD, stearic acid, Glyceryl Behenate and viscous Form membrane and put in reactor, be subsequently adding the clear water of total amount 2 times, be heated to while stirring 180-200℃；
2) by the Cortex Meliae in raw material, Semen Ricini, Fructus Viticis, sodium humate, Cortex toonae sinensis radicis, Cortex Salicis Babylonicae Radicis, Long Miao, Chalcanthitum, Realgar are put into and turn over companion in pot is 2-5% to total moisture content, then takes out, carries out after cooling Grind to form mixed powder；
3) raw material in step 2 is added in the reactor in step 1, continue stirring, lower the temperature while stirring To room temperature, then the most available after discharging.
The invention has the beneficial effects as follows: instant component is simple, it is easy to industrialization, the coating membrane cream of preparation There is good solubility property, run into water or malaria, just can dissolve immediately, internal implantation Group's insecticidal constituent can realize biocidal efficacies, Chinese medicine expelling worm, free from extraneous odour, low cost, have very Good economic benefit and social benefit.
Detailed description of the invention
For the technological means making the present invention realize, creation characteristic, reach purpose and effect and be readily apparent from Solve, below in conjunction with specific embodiment, the present invention is expanded on further.
Embodiment 1
Weigh: kieselguhr 60kg, Pulvis Talci 20kg, polyvinyl alcohol 3kg, copolyvidone 4kg, hydroxypropyl first Cellulose 8kg, magnesium stearate 3kg, tween 2kg, Oleum Ricini 2kg, HP-β-CD 15kg, Stearic acid 6kg, Glyceryl Behenate 6kg, it is bonded to membrane 7kg, Cortex Meliae 3kg, Semen Ricini 2kg, climing Fructus Vitics Simplicifoliae 2kg, sodium humate 15kg, Cortex toonae sinensis radicis 6kg, Cortex Salicis Babylonicae Radicis 7kg, dragon Seedling 2kg, Chalcanthitum 5kg, Realgar 8kg。
Embodiment 2
Weigh: kieselguhr 80kg, Pulvis Talci 30kg, polyvinyl alcohol 5kg, copolyvidone 6kg, hydroxypropyl first Cellulose 10kg, magnesium stearate 5kg, tween 4kg, Oleum Ricini 4kg, HP-β-CD 25kg, Stearic acid 8kg, Glyceryl Behenate 8kg, it is bonded to membrane 9kg, Cortex Meliae 5kg, Semen Ricini 4kg, climing Fructus Vitics Simplicifoliae 4kg, sodium humate 25kg, Cortex toonae sinensis radicis 8kg, Cortex Salicis Babylonicae Radicis 9kg, dragon Seedling 4kg, Chalcanthitum 7kg, Realgar 10kg。
Embodiment 3
Weigh: kieselguhr 70kg, Pulvis Talci 25kg, polyvinyl alcohol 4kg, copolyvidone 5kg, hydroxypropyl first Cellulose 9kg, magnesium stearate 4kg, tween 3kg, Oleum Ricini 3kg, HP-β-CD 20kg, Stearic acid 7kg, Glyceryl Behenate 7kg, it is bonded to membrane 8kg, Cortex Meliae 4kg, Semen Ricini 3kg, climing Fructus Vitics Simplicifoliae 3kg, sodium humate 20kg, Cortex toonae sinensis radicis 7kg, Cortex Salicis Babylonicae Radicis 8kg, dragon Seedling 3kg, Chalcanthitum 6kg, Realgar 9kg。
The method of preparation embodiment 1,2 or 3, comprises the following steps:
1) by the kieselguhr in raw material, Pulvis Talci, polyvinyl alcohol, copolyvidone, hypromellose, Magnesium stearate, tween, Oleum Ricini, HP-β-CD, stearic acid, Glyceryl Behenate and viscous Form membrane and put in reactor, be subsequently adding the clear water of total amount 2 times, be heated to while stirring 180-200℃；
2) by the Cortex Meliae in raw material, Semen Ricini, Fructus Viticis, sodium humate, Cortex toonae sinensis radicis, Cortex Salicis Babylonicae Radicis, Long Miao, Chalcanthitum, Realgar are put into and turn over companion in pot is 2-5% to total moisture content, then takes out, carries out after cooling Grind to form mixed powder；
3) raw material in step 2 is added in the reactor in step 1, continue stirring, lower the temperature while stirring To room temperature, then the most available after discharging.
Below by the wheatland under two blocks, North Huaihe River Area of Anhui Province equal conditions environment, the experiment carried out is right Than parameter list:
A field: use tradition coated granule fertile, normally apply fertilizer；
B field: the granular fertilizer using this product coating membrane cream to be coated, normally applies fertilizer；
Test: A field and B field use tradition coated fertilizer and this product coated fertilizer respectively, apply fertilizer latter 3 days, Insect substantially quantity in plot；Unit (individual)
Gold ant Bend over worm Red spider Caterpillar Borer Weave silk worm Tooth worm Dou Tiane
A field 120 330 210 210 250 350 340 320
B field 80 10 20 30 25 25 15 30
As can be seen from the above table, this product coating is used to carry out granular fertilizer making, the tradition that compares coated granule Fertilizer, has obvious advantage killing and expelling on insect.
The ultimate principle of the present invention and principal character and advantages of the present invention have more than been shown and described.One's own profession Skilled person will appreciate that of industry, the present invention is not restricted to the described embodiments, above-described embodiment and explanation The principle that the present invention is simply described described in book, without departing from the spirit and scope of the present invention, The present invention also has various changes and modifications, and these changes and improvements both fall within claimed invention model In enclosing.Claimed scope is defined by appending claims and equivalent thereof.

Claims (4)

1. the granular fertilizer coating membrane cream containing expelling worm composition, it is characterised in that: by following components Raw material is made:
Kieselguhr 60-80 part, Pulvis Talci 20-30 part, polyvinyl alcohol 3-5 part, copolyvidone 4-6 part, hydroxyl Third methylcellulose 8-10 part, magnesium stearate 3-5 part, tween 2-4 part, Oleum Ricini 2-4 part, hydroxy propyl-Beta- Cyclodextrin 15-25 part, stearic acid 6-8 part, Glyceryl Behenate 6-8 part, it is bonded to membrane 7-9 part, hardship Chinaberry skin 3-5 part, Semen Ricini 2-4 part, Fructus Viticis 2-4 part, sodium humate 15-25 part, Cortex toonae sinensis radicis 6-8 part, Cortex Salicis Babylonicae Radicis 7-9 part, dragon Seedling 2-4 part, Chalcanthitum 5-7 part, Realgar 8-10 part.
A kind of granular fertilizer coating membrane cream containing expelling worm composition the most according to claim 1, it is special Levy and be: the preferred ingredient of each raw material is: 70 parts of kieselguhr, Pulvis Talci 25 parts, polyvinyl alcohol 4 parts, altogether Polyvidone 5 parts, hypromellose 9 parts, magnesium stearate 4 parts, tween 3 parts, Oleum Ricini 3 parts, hydroxypropyl -beta-schardinger dextrin-20 parts, stearic acid 7 parts, Glyceryl Behenate 7 parts, it is bonded to membrane 8 parts, Cortex Meliae 4 Part, Semen Ricini 3 parts, Fructus Viticis 3 parts, sodium humate 20 parts, Cortex toonae sinensis radicis 7 parts, Cortex Salicis Babylonicae Radicis 8 parts, dragon Seedling 3 Part, 6 parts of Chalcanthitum, Realgar 9 parts.
A kind of granular fertilizer coating membrane cream containing expelling worm composition the most according to claim 1, it is special Levy and be: described bonding film former is by chitosan 3 parts, polyvinyl alcohol 4 parts, glycerol 6 parts and gibberellins 6 Part carries out compounding making.
4. prepare a kind of granular fertilizer coating containing expelling worm composition described in any one of claim 1 and 2 for one kind The method of film cream, it is characterised in that: step is as follows,
1) by the kieselguhr in raw material, Pulvis Talci, polyvinyl alcohol, copolyvidone, hypromellose, Magnesium stearate, tween, Oleum Ricini, HP-β-CD, stearic acid, Glyceryl Behenate and viscous Form membrane and put in reactor, be subsequently adding the clear water of total amount 2 times, be heated to 180-200 DEG C while stirring；
2) by the Cortex Meliae in raw material, Semen Ricini, Fructus Viticis, sodium humate, Cortex toonae sinensis radicis, Cortex Salicis Babylonicae Radicis, Long Miao, Chalcanthitum, Realgar are put into and turn over companion in pot is 2-5% to total moisture content, then takes out, carries out after cooling Grind to form mixed powder；
3) raw material in step 2 is added in the reactor in step 1, continue stirring, lower the temperature while stirring To room temperature, then the most available after discharging.
CN201610122194.1A 2016-03-03 2016-03-03 Pest dispelling and killing component-containing granular fertilizer coating membrane paste and preparation method thereof Withdrawn CN105819944A (en)

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CN201610122194.1A CN105819944A (en) 2016-03-03 2016-03-03 Pest dispelling and killing component-containing granular fertilizer coating membrane paste and preparation method thereof

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Application Number Priority Date Filing Date Title
CN201610122194.1A CN105819944A (en) 2016-03-03 2016-03-03 Pest dispelling and killing component-containing granular fertilizer coating membrane paste and preparation method thereof

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110463725A (en) * 2019-09-04 2019-11-19 淮北师范大学 A kind of environment-friendly type coating agent for seed and preparation method

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101962306A (en) * 2010-07-13 2011-02-02 北京市农林科学院 Photodegradable mulch resin coated fertilizer and preparation method thereof
CN102951972A (en) * 2012-12-03 2013-03-06 河南好年景生物发展有限公司 Controlled release fertilizer with natural insecticide efficacy
CN103964971A (en) * 2014-05-29 2014-08-06 济南巴顿化肥有限公司 Fertilizer specially used for rice and preparation method thereof
CN104355839A (en) * 2014-11-11 2015-02-18 合肥不老传奇保健科技有限公司 Strawberry coated fertilizer with sterilizing effect and preparation method thereof
CN104446853A (en) * 2013-09-21 2015-03-25 山东恩宝生物科技有限公司 Coating organic efficient granule fertilizer
CN104725135A (en) * 2015-03-18 2015-06-24 陈广田 Illite coating and application thereof

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101962306A (en) * 2010-07-13 2011-02-02 北京市农林科学院 Photodegradable mulch resin coated fertilizer and preparation method thereof
CN102951972A (en) * 2012-12-03 2013-03-06 河南好年景生物发展有限公司 Controlled release fertilizer with natural insecticide efficacy
CN104446853A (en) * 2013-09-21 2015-03-25 山东恩宝生物科技有限公司 Coating organic efficient granule fertilizer
CN103964971A (en) * 2014-05-29 2014-08-06 济南巴顿化肥有限公司 Fertilizer specially used for rice and preparation method thereof
CN104355839A (en) * 2014-11-11 2015-02-18 合肥不老传奇保健科技有限公司 Strawberry coated fertilizer with sterilizing effect and preparation method thereof
CN104725135A (en) * 2015-03-18 2015-06-24 陈广田 Illite coating and application thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110463725A (en) * 2019-09-04 2019-11-19 淮北师范大学 A kind of environment-friendly type coating agent for seed and preparation method

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Application publication date: 20160803