CN105816387A - Pure natural solution prepared from fleece flower roots, Chinese soapberry fruits and plant Chinese honeylocust fruits - Google Patents
Pure natural solution prepared from fleece flower roots, Chinese soapberry fruits and plant Chinese honeylocust fruits Download PDFInfo
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- CN105816387A CN105816387A CN201610301715.XA CN201610301715A CN105816387A CN 105816387 A CN105816387 A CN 105816387A CN 201610301715 A CN201610301715 A CN 201610301715A CN 105816387 A CN105816387 A CN 105816387A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/006—Antidandruff preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/008—Preparations for oily hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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Abstract
The invention discloses a pure natural solution prepared from fleece flower roots, Chinese soapberry fruits and plant Chinese honeylocust fruits. A preparing method comprises the following steps that firstly, fresh Chinese honeylocust fruits, fleece flower roots and Chinese soapberry fruits are harvested and dried in the shade, wherein the Chinese honeylocust fruits and the Chinese soapberry fruits are steamed for 1.5-2.5 h at 110-130 DEG C after being harvested and then dried in the shade; secondly, the Chinese honeylocust fruits dried in the shade, the fleece flower roots dried in the shade and the Chinese soapberry fruits dried in the shade are dried and ground and then pass through a 20-30-mesh screen, and fine powder is obtained; thirdly, the fine powder is subjected to heat reflux extraction with 70-80% ethyl alcohol for 2-4 times, each time of heat reflux extraction takes 1.5-2.5 h, filtering is carried out, and filter liquor is collected; fourthly, the filter liquor is subjected to vacuum concentration until the alcohol smell is eliminated, AB-8 type macropore adsorption resin is used for purification and enrichment, 10-20% ethyl alcohol is used for elution of 6-10 column volume, 70-80% ethyl alcohol is then used for elution of 12-16 column volume, and the 70-80% ethyl alcohol eluant is collected.
Description
Technical field
The invention belongs to household chemicals field, be specifically related to a kind of pure natural Radix Polygoni Multiflori soapberry Fructus Gleditsia liquid.
Background technology
Fructus Gleditsia shampoo is without any essence pigment and the shampoo of chemical substance pure natural.The Chinese nation the most just has soap
The natural plants such as angle, the Radix Polygoni Multiflori, camellia oleosa seed smash the tradition of hair washing hair care to pieces, and pitch-black dense, the chipless of hair is without itching.According to Compendium of Material Medica
Record: Fructus Gleditsia removing scurf and relieving itching, detumescence toxic removing；Radix Polygoni Multiflori benefit vim and vigour, black temples hair growth promoting, improving healthy complexion.
Radix Polygoni Multiflori, has another name called and spends more knotweed, purple crow rattan, Caulis Polygoni Multiflori etc..It is that Polygonaceae knotweed race Radix Polygoni Multiflori belongs to perennial winding liana,
Tuber is plump, oblong, pitchy.Raw mountain valley shrubbery, hillside sylvan life, ditch curb gap.Produce Southern Shaanxi, SOUTH OF GANSU,
East China, Central China, south China, Sichuan, Yunnan and Guizhou.Its tuber is used as medicine, and can calm the nerves, nourishes blood, active, removing toxic substances (preventing the attack (or recurrence) of malaria),
Eliminating carbuncle；Radix Polygoni Multiflori Preparata can tonification essence and blood, crow beard and hair, bone and muscle strengthening, invigorating the liver and kidney, be your detail medical material common.
Fructus Gleditsia i.e. Fructus Gleditsia, containing triterpenoid saponin (gledinin, gleditschiasaponin), tannin, ceryl alcohol, nonacosane, stigmasterol, sitosterol
Deng.The function have eliminating the phlegm, having one's ideas straightened out.Saponin element contained in Fructus Gleditsia is triterpene alkenes and oligosaccharide, have antiinflammatory, antiulcer,
Disease-resistant change effect, the most anticancer and improve the effect such as acquired immune deficiency syndrome (AIDS) immunity.
Fructus Sapindi Mukouossi is rich in saponin, and its soap breast foaming abundancy, feel is fine and smooth, and strong detergency can improve skin quality so that it is fine and smooth
Gloss, high resilience.The effects such as the most antibacterial, antiinflammatory, oxidation and removing free radicals, anticoagulation.Fruit in Fructus Sapindi Mukouossi
Acid helps skin removed to be deposited in the aging cutin of outer layer, accelerates skin renewal, help improve skin comedo, black speck, wrinkle,
Xerosis cutis, the skin problem such as coarse.For hair washing also can pre-anti-dandruff anti-dandruff and itching-relieving efficacies, its pH value 5～7 it
Between, in natural acidity, the interfacial agent of pure natural, body of not hurting sb.'s feelings, the not characteristic of polluted source.
Summary of the invention
It is an object of the invention to provide a kind of pure natural Radix Polygoni Multiflori soapberry Fructus Gleditsia liquid with preventing and treating alopecia function.
The above-mentioned purpose of the present invention is achieved by techniques below scheme:
A kind of pure natural Radix Polygoni Multiflori soapberry Fructus Gleditsia liquid, is made by the raw material of following weight portion: Fructus Gleditsia, 45～55 parts；What
The Radix Polygoni Multiflori, 35～45 parts；Fructus Sapindi Mukouossi, 50～60 parts；Water, 25～35 parts；Preparation method comprises the steps:
Step S1, gathers in fresh Fructus Gleditsia, Radix Polygoni Multiflori and Fructus Sapindi Mukouossi and dries in the shade；Wherein, elder generation's warp after Fructus Gleditsia and Fructus Sapindi Mukouossi gather in
110～130 DEG C steam 1.5～2.5 hours, then dry in the shade；
Step S2, dries the Fructus Gleditsia dried in the shade, Radix Polygoni Multiflori and Fructus Sapindi Mukouossi, pulverized 20～30 mesh sieves, and obtained fine powder；
Step S3, by fine powder with 70～80% alcohol heat reflux extract 2～4 times, each 1.5～2.5 hours, filtrate is collected by filtration；
Step S4, filtrate reduced in volume is to without alcohol taste, with the enrichment of AB-8 type purification with macroreticular resin, first with 10～the second of 20%
Alcohol eluting 6～10 column volumes, then with 70～80% ethanol elution 12～16 column volumes, collect 70～80% ethanol elution；
Step S5,70～80% ethanol elution concentrating under reduced pressure, it is spray-dried, obtains the extract of powdered；
Step S6, redissolves the extract of above-mentioned powdered and get final product with water.
Further, described pure natural Radix Polygoni Multiflori soapberry Fructus Gleditsia liquid is made by the raw material of following weight portion: Fructus Gleditsia, and 50
Part；Radix Polygoni Multiflori, 40 parts；Fructus Sapindi Mukouossi, 55 parts；Water, 30 parts；Preparation method is as follows:
Step S1, gathers in fresh Fructus Gleditsia, Radix Polygoni Multiflori and Fructus Sapindi Mukouossi and dries in the shade；Wherein, first through 120 DEG C after Fructus Gleditsia and Fructus Sapindi Mukouossi gather in
Steam 2 hours, then dry in the shade；
Step S2, dries the Fructus Gleditsia dried in the shade, Radix Polygoni Multiflori and Fructus Sapindi Mukouossi, pulverized 20 mesh sieves, and obtained fine powder；
Step S3, extracts fine powder 3 times with 75% alcohol heat reflux, each 2 hours, filtrate is collected by filtration；
Step S4, filtrate reduced in volume is to without alcohol taste, with the enrichment of AB-8 type purification with macroreticular resin, first with 15% ethanol
8 column volumes of eluting, then with 14 column volumes of 75% ethanol elution, collect 75% ethanol elution；
Step S5,75% ethanol elution concentrating under reduced pressure, it is spray-dried, obtains the extract of powdered；
Step S6, redissolves the extract of above-mentioned powdered and get final product with water.
Further, described pure natural Radix Polygoni Multiflori soapberry Fructus Gleditsia liquid is made by the raw material of following weight portion: Fructus Gleditsia, and 45
Part；Radix Polygoni Multiflori, 35 parts；Fructus Sapindi Mukouossi, 50 parts；Water, 25 parts；Preparation method is as follows:
Step S1, gathers in fresh Fructus Gleditsia, Radix Polygoni Multiflori and Fructus Sapindi Mukouossi and dries in the shade；Wherein, first through 120 DEG C after Fructus Gleditsia and Fructus Sapindi Mukouossi gather in
Steam 2 hours, then dry in the shade；
Step S2, dries the Fructus Gleditsia dried in the shade, Radix Polygoni Multiflori and Fructus Sapindi Mukouossi, pulverized 20 mesh sieves, and obtained fine powder；
Step S3, extracts fine powder 3 times with 75% alcohol heat reflux, each 2 hours, filtrate is collected by filtration；
Step S4, filtrate reduced in volume is to without alcohol taste, with the enrichment of AB-8 type purification with macroreticular resin, first with 15% ethanol
8 column volumes of eluting, then with 14 column volumes of 75% ethanol elution, collect 75% ethanol elution；
Step S5,75% ethanol elution concentrating under reduced pressure, it is spray-dried, obtains the extract of powdered；
Step S6, redissolves the extract of above-mentioned powdered and get final product with water.
Further, described pure natural Radix Polygoni Multiflori soapberry Fructus Gleditsia liquid is made by the raw material of following weight portion: Fructus Gleditsia, and 55
Part；Radix Polygoni Multiflori, 45 parts；Fructus Sapindi Mukouossi, 60 parts；Water, 35 parts；Preparation method is as follows:
Step S1, gathers in fresh Fructus Gleditsia, Radix Polygoni Multiflori and Fructus Sapindi Mukouossi and dries in the shade；Wherein, first through 120 DEG C after Fructus Gleditsia and Fructus Sapindi Mukouossi gather in
Steam 2 hours, then dry in the shade；
Step S2, dries the Fructus Gleditsia dried in the shade, Radix Polygoni Multiflori and Fructus Sapindi Mukouossi, pulverized 20 mesh sieves, and obtained fine powder；
Step S3, extracts fine powder 3 times with 75% alcohol heat reflux, each 2 hours, filtrate is collected by filtration；
Step S4, filtrate reduced in volume is to without alcohol taste, with the enrichment of AB-8 type purification with macroreticular resin, first with 15% ethanol
8 column volumes of eluting, then with 14 column volumes of 75% ethanol elution, collect 75% ethanol elution；
Step S5,75% ethanol elution concentrating under reduced pressure, it is spray-dried, obtains the extract of powdered；
Step S6, redissolves the extract of above-mentioned powdered and get final product with water.
Advantages of the present invention:
The pure natural Radix Polygoni Multiflori soapberry Fructus Gleditsia liquid that the present invention provides has anticreep, controls oily, anti-dandruff, antipruritic effect, preventing and treating
The effect of alopecia whether may first pass through after gathering in Fructus Gleditsia and Fructus Sapindi Mukouossi steam relevant.
Detailed description of the invention
Further illustrate the essentiality content of the present invention below in conjunction with embodiment, but do not limit scope with this.To the greatest extent
The present invention is explained in detail by pipe with reference to preferred embodiment, it will be understood by those within the art that, can be to the present invention
Technical scheme modify or equivalent, without deviating from the spirit and scope of technical solution of the present invention.
Embodiment 1: the preparation of pure natural Radix Polygoni Multiflori soapberry Fructus Gleditsia liquid
Parts by weight of raw materials compares:
Fresh Fructus Gleditsia, 50 parts；New fresh Radix Polygoni Multiflori, 40 parts；Fresh Fructus Sapindi Mukouossi, 55 parts；Water, 30 parts.
Preparation method:
Step S1, gathers in fresh Fructus Gleditsia, Radix Polygoni Multiflori and Fructus Sapindi Mukouossi and dries in the shade；Wherein, first through 120 DEG C after Fructus Gleditsia and Fructus Sapindi Mukouossi gather in
Steam 2 hours, then dry in the shade；
Step S2, dries the Fructus Gleditsia dried in the shade, Radix Polygoni Multiflori and Fructus Sapindi Mukouossi, pulverized 20 mesh sieves, and obtained fine powder；
Step S3, extracts fine powder 3 times with 75% alcohol heat reflux, each 2 hours, filtrate is collected by filtration；
Step S4, filtrate reduced in volume is to without alcohol taste, with the enrichment of AB-8 type purification with macroreticular resin, first with 15% ethanol
8 column volumes of eluting, then with 14 column volumes of 75% ethanol elution, collect 75% ethanol elution；
Step S5,75% ethanol elution concentrating under reduced pressure, it is spray-dried, obtains the extract of powdered；
Step S6, redissolves the extract of above-mentioned powdered and get final product with water.
Embodiment 2: comparative example, without steaming after Fructus Gleditsia harvesting
Parts by weight of raw materials compares:
Fresh Fructus Gleditsia, 50 parts；New fresh Radix Polygoni Multiflori, 40 parts；Fresh Fructus Sapindi Mukouossi, 55 parts；Water, 30 parts.
Preparation method:
Step S1, gathers in fresh Fructus Gleditsia, Radix Polygoni Multiflori and Fructus Sapindi Mukouossi and dries in the shade；Wherein, first steam through 120 DEG C after Fructus Sapindi Mukouossi harvesting
2 hours, then dry in the shade；
Step S2, dries the Fructus Gleditsia dried in the shade, Radix Polygoni Multiflori and Fructus Sapindi Mukouossi, pulverized 20 mesh sieves, and obtained fine powder；
Step S3, extracts fine powder 3 times with 75% alcohol heat reflux, each 2 hours, filtrate is collected by filtration；
Step S4, filtrate reduced in volume is to without alcohol taste, with the enrichment of AB-8 type purification with macroreticular resin, first with 15% ethanol
8 column volumes of eluting, then with 14 column volumes of 75% ethanol elution, collect 75% ethanol elution；
Step S5,75% ethanol elution concentrating under reduced pressure, it is spray-dried, obtains the extract of powdered；
Step S6, redissolves the extract of above-mentioned powdered and get final product with water.
Embodiment 3: comparative example, without steaming after Fructus Sapindi Mukouossi harvesting
Parts by weight of raw materials compares:
Fresh Fructus Gleditsia, 50 parts；New fresh Radix Polygoni Multiflori, 40 parts；Fresh Fructus Sapindi Mukouossi, 55 parts；Water, 30 parts.
Preparation method:
Step S1, gathers in fresh Fructus Gleditsia, Radix Polygoni Multiflori and Fructus Sapindi Mukouossi and dries in the shade；Wherein, first 2 are steamed through 120 DEG C after Fructus Gleditsia harvesting
Hour, then dry in the shade；
Step S2, dries the Fructus Gleditsia dried in the shade, Radix Polygoni Multiflori and Fructus Sapindi Mukouossi, pulverized 20 mesh sieves, and obtained fine powder；
Step S3, extracts fine powder 3 times with 75% alcohol heat reflux, each 2 hours, filtrate is collected by filtration；
Step S4, filtrate reduced in volume is to without alcohol taste, with the enrichment of AB-8 type purification with macroreticular resin, first with 15% ethanol
8 column volumes of eluting, then with 14 column volumes of 75% ethanol elution, collect 75% ethanol elution；
Step S5,75% ethanol elution concentrating under reduced pressure, it is spray-dried, obtains the extract of powdered；
Step S6, redissolves the extract of above-mentioned powdered and get final product with water.
Embodiment 4: effect example, prevents and treats alopecia
1, materials and methods
1.1 animal
SPF level, male C57BL/6 mice, weight 18～20g, Shanghai Slac Experimental Animal Co., Ltd..Feeding environment:
Room temperature controls at 24～26 DEG C, light every 12h light and shade alternately, ad lib, the next day change bedding and padding.
1.2 reagent and sample
Fructus Gleditsia liquid 1～3 is prepared respectively according to the method for embodiment 1～3.Cyclophosphamide (Hengrui Medicine Co., Ltd., Jiangsu Prov.).
CBA detection kit (U.S., BD company), CD4 detection kit (Shanghai Ying Xin laboratory equlpment company limited), CD8
Detection kit (Shanghai Ying Xin laboratory equlpment company limited).
1.3 instrument
JEM-1010 type Electronic Speculum (Japan, NEC company), C6 type flow cytometer (U.S., BD company), MK3
Type microplate reader (U.S., Thermo company).
Prepared by 1.4 mice group and model
C57BL/6 mice anesthetic machine is anaesthetized.After anesthesia, Colophonium and paraffin are melted in the ratio Hybrid Heating of 1: 1, and all
Even be applied in a back, solidify hardening after throw off, induced growth phase hair, every mice depilation area is about 2.0cm × 2.0cm.
It is careful not to burned mouse skin.Lose hair or feathers latter 9 days (generation of mouse back skin induced growth phase hair follicle), according to table of random number,
Mice is divided into 4 groups, and often group 20, is blank group, Fructus Gleditsia liquid 1 group, Fructus Gleditsia liquid 2 groups, Fructus Gleditsia liquid 3 groups respectively.
After all mices depilation district subcutaneous injection CTX150mg/kg, model group gives free rein to growth, and blank group is smeared in depilation district
Deionized water, Fructus Gleditsia liquid 1～3 groups smear Fructus Gleditsia liquid 1～3 in depilation district, and smearing dosage is each 1ml/cm2, once-a-day, hold
Continue and smear 8 weeks.
2, experimental result (changes of body mass and hair growth situation)
Mice is terminated to experiment through CTX induction depilation, each group Mice Body quality no significant difference (P ＞ 0.05).Fructus Gleditsia liquid 1 group
Depilation mice is after Fructus Gleditsia liquid 1 smears 1～2 week, and depilation district local skin is gradually transformed into grey black, mice depilation district by pink colour
Skin grey black region is substantially big than blank group and Fructus Gleditsia liquid 2～3 groups；Smearing to 4～8 weeks, 1 group of mice of Fructus Gleditsia liquid takes off
Hair-fields is black, and has hair gradually to grow, extends, and is substantially better than blank group and Fructus Gleditsia liquid 2～3 groups.
The depilation the most frequently used laboratory animal of model is C57BL/6 mice, and owing to it is coloured kind, skin color is with the growth of hair follicle
And show different colors, it is research hair follicle development and a kind of well laboratory animal of regeneration.
Above-mentioned result of the test shows, the pure natural Radix Polygoni Multiflori soapberry Fructus Gleditsia liquid that the present invention provides has the effect of preventing and treating alopecia,
The effect of preventing and treating alopecia whether may first pass through after gathering in Fructus Gleditsia and Fructus Sapindi Mukouossi steam relevant.
The pure natural Radix Polygoni Multiflori soapberry Fructus Gleditsia liquid that the present invention provides has anticreep, controls oily, anti-dandruff, antipruritic effect.
The effect of above-described embodiment indicates that the essentiality content of the present invention, but does not limit protection scope of the present invention with this.
It will be understood by those within the art that, technical scheme can be modified or equivalent, and not take off
Essence and protection domain from technical solution of the present invention.
Claims (4)
1. a pure natural Radix Polygoni Multiflori soapberry Fructus Gleditsia liquid, it is characterised in that made by the raw material of following weight portion: Fructus Gleditsia,
45～55 parts；Radix Polygoni Multiflori, 35～45 parts；Fructus Sapindi Mukouossi, 50～60 parts；Water, 25～35 parts；Preparation method comprises the steps:
Step S1, gathers in fresh Fructus Gleditsia, Radix Polygoni Multiflori and Fructus Sapindi Mukouossi and dries in the shade；Wherein, elder generation's warp after Fructus Gleditsia and Fructus Sapindi Mukouossi gather in
110～130 DEG C steam 1.5～2.5 hours, then dry in the shade；
Step S2, dries the Fructus Gleditsia dried in the shade, Radix Polygoni Multiflori and Fructus Sapindi Mukouossi, pulverized 20～30 mesh sieves, and obtained fine powder；
Step S3, by fine powder with 70～80% alcohol heat reflux extract 2～4 times, each 1.5～2.5 hours, filtrate is collected by filtration；
Step S4, filtrate reduced in volume is to without alcohol taste, with the enrichment of AB-8 type purification with macroreticular resin, first with 10～the second of 20%
Alcohol eluting 6～10 column volumes, then with 70～80% ethanol elution 12～16 column volumes, collect 70～80% ethanol elution；
Step S5,70～80% ethanol elution concentrating under reduced pressure, it is spray-dried, obtains the extract of powdered；
Step S6, redissolves the extract of above-mentioned powdered and get final product with water.
Pure natural Radix Polygoni Multiflori soapberry Fructus Gleditsia liquid the most according to claim 1, it is characterised in that by following weight portion
Raw material make: Fructus Gleditsia, 50 parts；Radix Polygoni Multiflori, 40 parts；Fructus Sapindi Mukouossi, 55 parts；Water, 30 parts；Preparation method is as follows:
Step S1, gathers in fresh Fructus Gleditsia, Radix Polygoni Multiflori and Fructus Sapindi Mukouossi and dries in the shade；Wherein, first through 120 DEG C after Fructus Gleditsia and Fructus Sapindi Mukouossi gather in
Steam 2 hours, then dry in the shade；
Step S2, dries the Fructus Gleditsia dried in the shade, Radix Polygoni Multiflori and Fructus Sapindi Mukouossi, pulverized 20 mesh sieves, and obtained fine powder；
Step S3, extracts fine powder 3 times with 75% alcohol heat reflux, each 2 hours, filtrate is collected by filtration；
Step S4, filtrate reduced in volume is to without alcohol taste, with the enrichment of AB-8 type purification with macroreticular resin, first with 15% ethanol
8 column volumes of eluting, then with 14 column volumes of 75% ethanol elution, collect 75% ethanol elution；
Step S5,75% ethanol elution concentrating under reduced pressure, it is spray-dried, obtains the extract of powdered；
Step S6, redissolves the extract of above-mentioned powdered and get final product with water.
Pure natural Radix Polygoni Multiflori soapberry Fructus Gleditsia liquid the most according to claim 1, it is characterised in that by following weight portion
Raw material make: Fructus Gleditsia, 45 parts；Radix Polygoni Multiflori, 35 parts；Fructus Sapindi Mukouossi, 50 parts；Water, 25 parts；Preparation method is as follows:
Step S1, gathers in fresh Fructus Gleditsia, Radix Polygoni Multiflori and Fructus Sapindi Mukouossi and dries in the shade；Wherein, first through 120 DEG C after Fructus Gleditsia and Fructus Sapindi Mukouossi gather in
Steam 2 hours, then dry in the shade；
Step S2, dries the Fructus Gleditsia dried in the shade, Radix Polygoni Multiflori and Fructus Sapindi Mukouossi, pulverized 20 mesh sieves, and obtained fine powder；
Step S3, extracts fine powder 3 times with 75% alcohol heat reflux, each 2 hours, filtrate is collected by filtration；
Step S4, filtrate reduced in volume is to without alcohol taste, with the enrichment of AB-8 type purification with macroreticular resin, first with 15% ethanol
8 column volumes of eluting, then with 14 column volumes of 75% ethanol elution, collect 75% ethanol elution；
Step S5,75% ethanol elution concentrating under reduced pressure, it is spray-dried, obtains the extract of powdered；
Step S6, redissolves the extract of above-mentioned powdered and get final product with water.
Pure natural Radix Polygoni Multiflori soapberry Fructus Gleditsia liquid the most according to claim 1, it is characterised in that by following weight portion
Raw material make: Fructus Gleditsia, 55 parts；Radix Polygoni Multiflori, 45 parts；Fructus Sapindi Mukouossi, 60 parts；Water, 35 parts；Preparation method is as follows:
Step S1, gathers in fresh Fructus Gleditsia, Radix Polygoni Multiflori and Fructus Sapindi Mukouossi and dries in the shade；Wherein, first through 120 DEG C after Fructus Gleditsia and Fructus Sapindi Mukouossi gather in
Steam 2 hours, then dry in the shade；
Step S2, dries the Fructus Gleditsia dried in the shade, Radix Polygoni Multiflori and Fructus Sapindi Mukouossi, pulverized 20 mesh sieves, and obtained fine powder；
Step S3, extracts fine powder 3 times with 75% alcohol heat reflux, each 2 hours, filtrate is collected by filtration；
Step S4, filtrate reduced in volume is to without alcohol taste, with the enrichment of AB-8 type purification with macroreticular resin, first with 15% ethanol
8 column volumes of eluting, then with 14 column volumes of 75% ethanol elution, collect 75% ethanol elution；
Step S5,75% ethanol elution concentrating under reduced pressure, it is spray-dried, obtains the extract of powdered；
Step S6, redissolves the extract of above-mentioned powdered and get final product with water.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106727137A (en) * | 2016-12-27 | 2017-05-31 | 成都天威保健品有限公司 | A kind of hair tonic preparation and preparation method with hair-washing hair-care function |
| CN113956927A (en) * | 2021-11-18 | 2022-01-21 | 江西维客泰美实业有限公司 | Plant extraction strong decontamination cleaning agent and preparation method thereof |
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| CN113956927A (en) * | 2021-11-18 | 2022-01-21 | 江西维客泰美实业有限公司 | Plant extraction strong decontamination cleaning agent and preparation method thereof |
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| Publication number | Publication date |
|---|---|
| CN105816387B (en) | 2018-08-07 |
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