CN105815785A - Method for extracting preparing fat removing powder through tartronic acid extracted from cucumber - Google Patents
Method for extracting preparing fat removing powder through tartronic acid extracted from cucumber Download PDFInfo
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- CN105815785A CN105815785A CN201610195417.7A CN201610195417A CN105815785A CN 105815785 A CN105815785 A CN 105815785A CN 201610195417 A CN201610195417 A CN 201610195417A CN 105815785 A CN105815785 A CN 105815785A
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- cucumidis sativi
- fructus
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- cucumber
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- ROBFUDYVXSDBQM-UHFFFAOYSA-N hydroxymalonic acid Chemical compound OC(=O)C(O)C(O)=O ROBFUDYVXSDBQM-UHFFFAOYSA-N 0.000 title claims abstract description 82
- 235000010799 Cucumis sativus var sativus Nutrition 0.000 title claims abstract description 26
- 239000000843 powder Substances 0.000 title claims abstract description 24
- 238000000034 method Methods 0.000 title claims abstract description 20
- 244000299906 Cucumis sativus var. sativus Species 0.000 title 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 32
- 240000008067 Cucumis sativus Species 0.000 claims abstract description 25
- 235000013311 vegetables Nutrition 0.000 claims abstract description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 43
- 238000003756 stirring Methods 0.000 claims description 34
- 239000000203 mixture Substances 0.000 claims description 31
- 239000000706 filtrate Substances 0.000 claims description 30
- 239000000284 extract Substances 0.000 claims description 18
- 239000011812 mixed powder Substances 0.000 claims description 18
- 239000004519 grease Substances 0.000 claims description 17
- 230000010355 oscillation Effects 0.000 claims description 13
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 12
- 238000000855 fermentation Methods 0.000 claims description 12
- 230000004151 fermentation Effects 0.000 claims description 12
- 230000001954 sterilising effect Effects 0.000 claims description 12
- 238000010792 warming Methods 0.000 claims description 12
- 108091005804 Peptidases Proteins 0.000 claims description 7
- 239000004365 Protease Substances 0.000 claims description 7
- 239000000796 flavoring agent Substances 0.000 claims description 7
- 235000019634 flavors Nutrition 0.000 claims description 7
- 230000008569 process Effects 0.000 claims description 7
- 241000628997 Flos Species 0.000 claims description 6
- 238000006243 chemical reaction Methods 0.000 claims description 6
- 238000004140 cleaning Methods 0.000 claims description 6
- 238000001035 drying Methods 0.000 claims description 6
- 238000001914 filtration Methods 0.000 claims description 6
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
- 238000010298 pulverizing process Methods 0.000 claims description 6
- 210000002966 serum Anatomy 0.000 claims description 6
- 239000002893 slag Substances 0.000 claims description 6
- 239000002002 slurry Substances 0.000 claims description 6
- 239000011780 sodium chloride Substances 0.000 claims description 6
- 238000010025 steaming Methods 0.000 claims description 6
- 238000004659 sterilization and disinfection Methods 0.000 claims description 6
- 238000005406 washing Methods 0.000 claims description 6
- 235000011273 Benincasa Nutrition 0.000 claims description 3
- 102000035195 Peptidases Human genes 0.000 claims description 3
- 241001349593 Praecitrullus Species 0.000 claims description 3
- 238000001125 extrusion Methods 0.000 claims description 3
- 230000036541 health Effects 0.000 abstract description 8
- 235000013305 food Nutrition 0.000 abstract description 3
- 239000002994 raw material Substances 0.000 abstract description 3
- 239000000126 substance Substances 0.000 abstract description 2
- 235000019441 ethanol Nutrition 0.000 abstract 2
- 235000011274 Benincasa cerifera Nutrition 0.000 abstract 1
- 244000036905 Benincasa cerifera Species 0.000 abstract 1
- 235000009811 Momordica charantia Nutrition 0.000 abstract 1
- 244000078912 Trichosanthes cucumerina Species 0.000 abstract 1
- 235000008322 Trichosanthes cucumerina Nutrition 0.000 abstract 1
- 108010007119 flavourzyme Proteins 0.000 abstract 1
- 230000006378 damage Effects 0.000 description 7
- 239000003814 drug Substances 0.000 description 6
- 230000000694 effects Effects 0.000 description 5
- 102100037486 Reverse transcriptase/ribonuclease H Human genes 0.000 description 4
- 230000037396 body weight Effects 0.000 description 4
- 235000005911 diet Nutrition 0.000 description 4
- 230000037213 diet Effects 0.000 description 4
- 230000003203 everyday effect Effects 0.000 description 4
- 238000000605 extraction Methods 0.000 description 4
- 229940079593 drug Drugs 0.000 description 3
- 239000013585 weight reducing agent Substances 0.000 description 3
- 208000008589 Obesity Diseases 0.000 description 2
- 230000009471 action Effects 0.000 description 2
- 235000013399 edible fruits Nutrition 0.000 description 2
- 235000016709 nutrition Nutrition 0.000 description 2
- 230000035764 nutrition Effects 0.000 description 2
- 235000020824 obesity Nutrition 0.000 description 2
- 241000282412 Homo Species 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 206010033307 Overweight Diseases 0.000 description 1
- 208000004880 Polyuria Diseases 0.000 description 1
- 238000000944 Soxhlet extraction Methods 0.000 description 1
- 208000027418 Wounds and injury Diseases 0.000 description 1
- 210000000577 adipose tissue Anatomy 0.000 description 1
- 230000003579 anti-obesity Effects 0.000 description 1
- 235000019789 appetite Nutrition 0.000 description 1
- 230000036528 appetite Effects 0.000 description 1
- 230000003796 beauty Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 150000001720 carbohydrates Chemical class 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 230000001413 cellular effect Effects 0.000 description 1
- 230000008602 contraction Effects 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 208000029078 coronary artery disease Diseases 0.000 description 1
- 201000010251 cutis laxa Diseases 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 230000035619 diuresis Effects 0.000 description 1
- 239000003651 drinking water Substances 0.000 description 1
- 235000020188 drinking water Nutrition 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 208000014674 injury Diseases 0.000 description 1
- 230000000968 intestinal effect Effects 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 235000012054 meals Nutrition 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 231100000957 no side effect Toxicity 0.000 description 1
- 235000021590 normal diet Nutrition 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 210000003296 saliva Anatomy 0.000 description 1
- 230000003867 tiredness Effects 0.000 description 1
- 208000016255 tiredness Diseases 0.000 description 1
- 239000003053 toxin Substances 0.000 description 1
- 231100000765 toxin Toxicity 0.000 description 1
- 230000004580 weight loss Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Coloring Foods And Improving Nutritive Qualities (AREA)
- Preparation Of Fruits And Vegetables (AREA)
Abstract
The invention discloses a method for preparing fat removing powder through tartronic acid extracted from cucumber, and belongs to the technical field of extracting and preparing.The method includes the steps that cucumber serves as a raw material, and is sliced and squeezed, ethyl alcohol and flavourzyme is added, then ethyl alcohol is removed in an ultrasonic oscillating mode and a cable-type extracting mode, the tartronic acid is extracted from the cucumber accordingly, diuretic-and-detoxifying food such as white gourds, bitter gourds and green vegetables are added and combined with the tartronic acid, and therefore the method for preparing fat removing powder through the tartronic acid extracted from the cucumber is obtained.An example shows that the method is easy to operate and conduct and low in cost, substances harming to the human body are not generated, the tartronic acid extracted from the cucumber is effectively used for losing weight, safety and health are achieved, and the fat removing rate is 80% or above.
Description
Technical field
The invention discloses a kind of method that grease removal powder prepared by extraction hydroxymalonic acid from Fructus Cucumidis sativi, belong to extraction preparing technical field.
Background technology
Hydroxymalonic acid is a kind of small molecular organic acid.It can suppress carbohydrate to be converted into fat in animal body.Modern pharmacology research shows in cucumber fruits containing hydroxymalonic acid, and body fat mass in human body can be stoped to pile up, and has fat-reducing and effect of prevention coronary heart disease.The astringent mouthfeel of Fructus Cucumidis sativi is essentially from the hydroxymalonic acid contained by Fructus Cucumidis sativi, and this is the composition that other general vegetable does not contains.Hydroxymalonic acid and saliva merge mouthfeel that can be the most astringent.It was found that contained hydroxymalonic acid has no side effect in Fructus Cucumidis sativi, it it is good natural diet food.
Owing to lacking the reasons such as motion, irregular eating, nutrition is unbalanced, increasing body weight for humans exceeds standard, and according to statistics, the current whole world there are about 2,000,000,000 population considered overweight or obesity, loses weight and has become as a global topic.Ways of preventing obesity mainly has: keep fit through sport, fat-reducing of going on a diet, weight reduction with drugs, Chinese medicine defatting, lipposuction, pantry fat-reducing and generation meal fat-reducing.
Keeping fit through sport is the method for weight-reducing of a kind of health, but most people is due to busy, does not has time enough to take exercises；Go on a diet fat-reducing, be a kind of method of weight-reducing got instant result, but this fat-reducing is very big to the injury of health, weight loss procedures there will be the side effect such as immunity degradation, cutis laxa, intestinal discomfort, and once recovering normal diet, body weight can rise again, the even more than body weight before fat-reducing；Weight reduction with drugs, being to have the medicine of antiobesity action by use to reduce human body excess fat, body weight, its action principle is to go constrain appetite by medicine, stops health to absorb nutrition and fat, large quantity of moisture is excreted, weight reduction with drugs instant effect and notable, need not go on a diet and move, but health also can be had side effects by it, such as skin becomes unglazed, cellular contraction in health, mobility is substantially reduced, and affects physical and healthy.
Hydroxymalonic acid content difference in the cucumber fruits of different cultivars is bigger.Having much about the communications and reports containing hydroxymalonic acid in Fructus Cucumidis sativi at present, but do not have in Fructus Cucumidis sativi to do after the extraction of hydroxymalonic acid grease removal powder, research still belongs to blank both at home and abroad in this respect.
In view of the fat-reducing of hydroxymalonic acid and beauty functions and Fructus Cucumidis sativi importance on people's dining table, it is contemplated that the research in this field will gain great popularity.
Summary of the invention
The technical problem that present invention mainly solves: for the most conventional method of weight-reducing, although the effect of fat-reducing can be played, but it is the most thorough to there is fat-reducing, easily bounce-back, body metabolism rate reduces and the drawback of the problem of tiredness after fat-reducing, provide a kind of with Fructus Cucumidis sativi as raw material, first cut into slices and squeezed, and add ethanol and flavor protease, ethanol is removed the most again by sonic oscillation and Soxhlet extraction, hydroxymalonic acid is extracted from Fructus Cucumidis sativi, followed by adding Fructus Benincasae, Fructus Momordicae charantiae, the food of these diuresis toxin expellings of green vegetable is combined with hydroxymalonic acid, thus obtain extracting from Fructus Cucumidis sativi the method that grease removal powder prepared by hydroxymalonic acid.Not only operation is simple for the method, low cost, and the material of the human body that is safe from harm produces, and effectively utilize the hydroxymalonic acid extracted in Fructus Cucumidis sativi and lose weight, and safety and Health, grease removal rate reaches more than 80%.
In order to solve above-mentioned technical problem, the technical solution adopted in the present invention is:
(1) take the fresh cucumber of 2～3kg, put in 5～6L clear water, backward clear water in add 50～80g sodium chloride, after stirring, repeatedly wash Fructus Cucumidis sativi surface by rubbing with the hands, go dirt and the spinule of skim-coat；
(2) after cleaning, Fructus Cucumidis sativi after washing is cut into the lamellar that thickness is 1～1.5cm, it is positioned in the Fructus Ananadis comosi sieve being paved with gauze, ted 3～6L in the sun, wherein tedding once every 2h, until cucumber slice water content is 25～30%, the cucumber slice after shining afterwards is put in squeezer and is squeezed the juice, squeezing 15～20min, obtains Sucus Cucumidis sativi；
(3) slag inclusion 5 squeezing obtained～the Sucus Cucumidis sativi of 8% are put in reactor, regulation temperature is 15～20 DEG C, and it is added thereto to Sucus Cucumidis sativi quality 1～2 times of mass concentrations are 8% ethanol solution and 6～8U flavor proteases, regulation pH is 5.0～6.2, and stir 10～15min with the rotating speed of 300～400r/min, to be mixed complete, then it is warming up to 40～50 DEG C with the speed program of 5～6 DEG C/min, obtain Fructus Cucumidis sativi mixed liquor；
(4) wait to heat up complete, the mixed liquor after above-mentioned intensification is positioned in sonic oscillation instrument, sonic oscillation reaction 1～3h, arranging supersonic frequency is 25～30KHz, and ultrasonic power is 100～150W, filters afterwards, remove filtering residue, obtain filtrate, and filtrate is stood 40～50min；
(5) filtrate after above-mentioned standing is put in Soxhlet extractor, extract 45～60min, collect filtrate extract, then move it in fermentation tank, it is warming up to 100～115 DEG C, and is stirred continuously 10～15min with the speed of 150～200r/min, remove wherein ethanol；
(6) it is kept stirring for state, during until filtrate extract volume is original volume 1/4 in fermentation tank, stops stirring, stand 1～2h so that it is naturally cool to room temperature, hydroxymalonic acid can be extracted from Fructus Cucumidis sativi；
(7) take 200～300g Fructus Benincasaes, 250～400g Fructus Momordicae charantiae, 220～320g green vegetable and put into steaming and decocting 20～30min in the water of 60～80 DEG C, take out afterwards, put in filter bag, extrusion excessive moisture, mixture after squeezing afterwards is positioned in screen 1～2h, drain excessive moisture so that water content is 15～20%；
(8) mixture after draining takes out, and puts in baking oven machine, and regulation oven temperature is 55～60 DEG C, being dried to mixture water content be kept to when 2～3% stop baking, dislocation carries out pulverization process in pulverizer, pulverizes 5～8min, cross 110～120 mesh sieves, obtain mix powder；
(9) mixed-powder obtained above will add 80～100g Flos Camelliae Japonicae nectar, after mix homogeneously, high-speed stirred 10～15min under the rotating speed of 500～600r/min, the hydroxymalonic acid extracted in the Fructus Cucumidis sativi that will obtain in above-mentioned steps (6) the most again is added thereto, it is kept stirring for state 5～7min, stand subsequently, thickness mixed serum must be mixed；
(10) above-mentioned prepared mixing thick slurry is placed in drying machine, dried 20～35min at 100～120 DEG C, obtain mixed-powder, afterwards the mixed-powder obtained is placed under uviol lamp and carries out sterilization treatment, sterilizing 45～55min, i.e. can obtain the grease removal powder prepared with the hydroxymalonic acid extracted in Fructus Cucumidis sativi.
The application process of the present invention is: time edible, take the grease removal powder that the 10～15g present invention prepare and put in cup, and add 200～250mL warm water, stir i.e. edible, it is proposed that eat every day 1～3 time, drinking-water 200～300mL after eating, the most edible 10～18 days, can easily lose weight 5～8 kilograms, and will not rebound, any harm is not had for human body.
The invention has the beneficial effects as follows:
(1) raw material is simple and easy to get, reduces cost, and without chemical substance in preparation process, is safe from harm human body；
(2) taking full advantage of Fructus Cucumidis sativi resource, and the hydroxymalonic acid extracted is lost weight, safety and Health, grease removal rate reaches more than 80%.
Detailed description of the invention
Take the fresh cucumber of 2～3kg, put in 5～6L clear water, backward clear water in add 50～80g sodium chloride, after stirring, repeatedly wash Fructus Cucumidis sativi surface by rubbing with the hands, go dirt and the spinule of skim-coat；After cleaning, Fructus Cucumidis sativi after washing is cut into the lamellar that thickness is 1～1.5cm, it is positioned in the Fructus Ananadis comosi sieve being paved with gauze, ted 3～6L in the sun, wherein tedding once every 2h, until cucumber slice water content is 25～30%, the cucumber slice after shining afterwards is put in squeezer and is squeezed the juice, squeezing 15～20min, obtains Sucus Cucumidis sativi；The slag inclusion 5 squeezing obtained～the Sucus Cucumidis sativi of 8% are put in reactor, regulation temperature is 15～20 DEG C, and it is added thereto to Sucus Cucumidis sativi quality 1～2 times of mass concentrations are 8% ethanol solution and 6～8U flavor proteases, regulation pH is 5.0～6.2, and stir 10～15min with the rotating speed of 300～400r/min, to be mixed complete, then it is warming up to 40～50 DEG C with the speed program of 5～6 DEG C/min, obtain Fructus Cucumidis sativi mixed liquor；Wait to heat up complete, the mixed liquor after above-mentioned intensification is positioned in sonic oscillation instrument, sonic oscillation reaction 1～3h, arranging supersonic frequency is 25～30KHz, and ultrasonic power is 100～150W, filters afterwards, remove filtering residue, obtain filtrate, and filtrate is stood 40～50min；Filtrate after above-mentioned standing is put in Soxhlet extractor, extracts 45～60min, collect filtrate extract, then move it in fermentation tank, be warming up to 100～115 DEG C, and be stirred continuously 10～15min with the speed of 150～200r/min, remove wherein ethanol；It is kept stirring for state, during until filtrate extract volume is original volume 1/4 in fermentation tank, stops stirring, stand 1～2h so that it is naturally cool to room temperature, hydroxymalonic acid can be extracted from Fructus Cucumidis sativi；Take 200～300g Fructus Benincasaes, 250～400g Fructus Momordicae charantiae, 220～320g green vegetable and put into steaming and decocting 20～30min in the water of 60～80 DEG C, take out afterwards, put in filter bag, extrusion excessive moisture, mixture after squeezing afterwards is positioned in screen 1～2h, drains excessive moisture so that water content is 15～20%；Mixture after draining takes out, and puts in baking oven machine, and regulation oven temperature is 55～60 DEG C, being dried to mixture water content be kept to when 2～3% stop baking, dislocation carries out pulverization process in pulverizer, pulverizes 5～8min, cross 110～120 mesh sieves, obtain mix powder；Mixed-powder obtained above will add 80～100g Flos Camelliae Japonicae nectar, after mix homogeneously, high-speed stirred 10～15min under the rotating speed of 500～600r/min, the hydroxymalonic acid extracted in Fructus Cucumidis sativi the most obtained above is added thereto, it is kept stirring for state 5～7min, stand subsequently, thickness mixed serum must be mixed；Finally above-mentioned prepared mixing thick slurry is placed in drying machine, dried 20～35min at 100～120 DEG C, obtain mixed-powder, afterwards the mixed-powder obtained is placed under uviol lamp and carries out sterilization treatment, sterilizing 45～55min, i.e. can obtain the grease removal powder prepared with the hydroxymalonic acid extracted in Fructus Cucumidis sativi.
Example 1
Take the fresh cucumber of 2kg, put in 5L clear water, backward clear water in add 50g sodium chloride, after stirring, repeatedly wash Fructus Cucumidis sativi surface by rubbing with the hands, go dirt and the spinule of skim-coat；After cleaning, Fructus Cucumidis sativi after washing is cut into the lamellar that thickness is 1cm, it is positioned in the Fructus Ananadis comosi sieve being paved with gauze, ted 3L in the sun, wherein tedding once every 2h, until cucumber slice water content is 25%, the cucumber slice after shining afterwards is put in squeezer and is squeezed the juice, squeezing 15min, obtains Sucus Cucumidis sativi；The Sucus Cucumidis sativi of the slag inclusion 5% squeezing obtained is put in reactor, regulation temperature is 15 DEG C, and to be added thereto to 1 times of mass concentration of Sucus Cucumidis sativi quality be 8% ethanol solution and 6U flavor protease, regulation pH is 5.0, and stir 10min with the rotating speed of 300r/min, to be mixed complete, then it is warming up to 40 DEG C with the speed program of 5 DEG C/min, obtain Fructus Cucumidis sativi mixed liquor；Waiting to heat up complete, be positioned in sonic oscillation instrument by the mixed liquor after above-mentioned intensification, sonic oscillation reaction 1h, arranging supersonic frequency is 25KHz, and ultrasonic power is 100W, filters afterwards, removes filtering residue, obtains filtrate, and filtrate is stood 40min；Filtrate after above-mentioned standing is put in Soxhlet extractor, extracts 45min, collect filtrate extract, then move it in fermentation tank, be warming up to 100 DEG C, and be stirred continuously 10min with the speed of 150r/min, remove wherein ethanol；It is kept stirring for state, during until filtrate extract volume is original volume 1/4 in fermentation tank, stops stirring, stand 1h so that it is naturally cool to room temperature, hydroxymalonic acid can be extracted from Fructus Cucumidis sativi；Take 200g Fructus Benincasae, steaming and decocting 20min in the water of 60 DEG C put into by 250g Fructus Momordicae charantiae, 220g green vegetable, takes out afterwards, puts in filter bag, extrudes excessive moisture, and the mixture after squeezing afterwards is positioned over 1h in screen, drains excessive moisture so that water content is 15%；Mixture after draining takes out, and puts in baking oven machine, and regulation oven temperature is 55 DEG C, is dried to mixture water content and is kept to when 2% stop baking, and dislocation carries out pulverization process in pulverizer, pulverizes 5min, crosses 110 mesh sieves, obtains mix powder；Mixed-powder obtained above will add 80g Flos Camelliae Japonicae nectar, after mix homogeneously, high-speed stirred 10min under the rotating speed of 500r/min, the hydroxymalonic acid extracted in Fructus Cucumidis sativi the most obtained above is added thereto, it is kept stirring for state 5min, stands subsequently, thickness mixed serum must be mixed；Finally above-mentioned prepared mixing thick slurry is placed in drying machine, dried 20min at 100 DEG C, obtains mixed-powder, is placed under uviol lamp by the mixed-powder obtained afterwards and carries out sterilization treatment, sterilizing 45min, i.e. can obtain the grease removal powder prepared with the hydroxymalonic acid extracted in Fructus Cucumidis sativi.
This example operation is simple, time edible, take the grease removal powder that the 10g present invention prepares to put in cup, and add 200mL warm water, stir i.e. edible, suggestion eats 1 time every day, drink water after Shi Yong 200mL, the most edible 10 days, can easily lose weight 5 kilograms, and will not rebound, any harm is not had for human body.
Example 2
Take the fresh cucumber of 2.5kg, put in 5.5L clear water, backward clear water in add 65g sodium chloride, after stirring, repeatedly wash Fructus Cucumidis sativi surface by rubbing with the hands, go dirt and the spinule of skim-coat；After cleaning, Fructus Cucumidis sativi after washing is cut into the lamellar that thickness is 1.3cm, it is positioned in the Fructus Ananadis comosi sieve being paved with gauze, ted 5L in the sun, wherein tedding once every 2h, until cucumber slice water content is 28%, the cucumber slice after shining afterwards is put in squeezer and is squeezed the juice, squeezing 18min, obtains Sucus Cucumidis sativi；The Sucus Cucumidis sativi of the slag inclusion 6% squeezing obtained is put in reactor, regulation temperature is 17 DEG C, and to be added thereto to 1.5 times of mass concentrations of Sucus Cucumidis sativi quality be 8% ethanol solution and 7U flavor protease, regulation pH is 5.8, and stir 13min with the rotating speed of 350r/min, to be mixed complete, then it is warming up to 45 DEG C with the speed program of 5.5 DEG C/min, obtain Fructus Cucumidis sativi mixed liquor；Waiting to heat up complete, be positioned in sonic oscillation instrument by the mixed liquor after above-mentioned intensification, sonic oscillation reaction 2h, arranging supersonic frequency is 28KHz, and ultrasonic power is 130W, filters afterwards, removes filtering residue, obtains filtrate, and filtrate is stood 45min；Filtrate after above-mentioned standing is put in Soxhlet extractor, extracts 55min, collect filtrate extract, then move it in fermentation tank, be warming up to 110 DEG C, and be stirred continuously 13min with the speed of 180r/min, remove wherein ethanol；It is kept stirring for state, during until filtrate extract volume is original volume 1/4 in fermentation tank, stops stirring, stand 1.5h so that it is naturally cool to room temperature, hydroxymalonic acid can be extracted from Fructus Cucumidis sativi；Take 250g Fructus Benincasae, steaming and decocting 25min in the water of 70 DEG C put into by 350g Fructus Momordicae charantiae, 280g green vegetable, takes out afterwards, puts in filter bag, extrudes excessive moisture, and the mixture after squeezing afterwards is positioned over 1.5h in screen, drains excessive moisture so that water content is 18%；Mixture after draining takes out, and puts in baking oven machine, and regulation oven temperature is 58 DEG C, is dried to mixture water content and is kept to when 2.5% stop baking, and dislocation carries out pulverization process in pulverizer, pulverizes 7min, crosses 115 mesh sieves, obtains mix powder；Mixed-powder obtained above will add 90g Flos Camelliae Japonicae nectar, after mix homogeneously, high-speed stirred 13min under the rotating speed of 550r/min, the hydroxymalonic acid extracted in Fructus Cucumidis sativi the most obtained above is added thereto, it is kept stirring for state 6min, stands subsequently, thickness mixed serum must be mixed；Finally above-mentioned prepared mixing thick slurry is placed in drying machine, dried 30min at 110 DEG C, obtains mixed-powder, is placed under uviol lamp by the mixed-powder obtained afterwards and carries out sterilization treatment, sterilizing 50min, i.e. can obtain the grease removal powder prepared with the hydroxymalonic acid extracted in Fructus Cucumidis sativi.
This example operation is simple, time edible, take the grease removal powder that the 13g present invention prepares to put in cup, and add 230mL warm water, stir i.e. edible, suggestion eats 2 times every day, drink water after Shi Yong 250mL, the most edible 15 days, can easily lose weight 7 kilograms, and will not rebound, any harm is not had for human body.
Example 3
Take the fresh cucumber of 3kg, put in 6L clear water, backward clear water in add 80g sodium chloride, after stirring, repeatedly wash Fructus Cucumidis sativi surface by rubbing with the hands, go dirt and the spinule of skim-coat；After cleaning, Fructus Cucumidis sativi after washing is cut into the lamellar that thickness is 1.5cm, it is positioned in the Fructus Ananadis comosi sieve being paved with gauze, ted 6L in the sun, wherein tedding once every 2h, until cucumber slice water content is 30%, the cucumber slice after shining afterwards is put in squeezer and is squeezed the juice, squeezing 20min, obtains Sucus Cucumidis sativi；The Sucus Cucumidis sativi of the slag inclusion 8% squeezing obtained is put in reactor, regulation temperature is 20 DEG C, and to be added thereto to 2 times of mass concentrations of Sucus Cucumidis sativi quality be 8% ethanol solution and 8U flavor protease, regulation pH is 6.2, and stir 15min with the rotating speed of 400r/min, to be mixed complete, then it is warming up to 50 DEG C with the speed program of 6 DEG C/min, obtain Fructus Cucumidis sativi mixed liquor；Waiting to heat up complete, be positioned in sonic oscillation instrument by the mixed liquor after above-mentioned intensification, sonic oscillation reaction 3h, arranging supersonic frequency is 30KHz, and ultrasonic power is 150W, filters afterwards, removes filtering residue, obtains filtrate, and filtrate is stood 50min；Filtrate after above-mentioned standing is put in Soxhlet extractor, extracts 60min, collect filtrate extract, then move it in fermentation tank, be warming up to 115 DEG C, and be stirred continuously 15min with the speed of 200r/min, remove wherein ethanol；It is kept stirring for state, during until filtrate extract volume is original volume 1/4 in fermentation tank, stops stirring, stand 2h so that it is naturally cool to room temperature, hydroxymalonic acid can be extracted from Fructus Cucumidis sativi；Take 300g Fructus Benincasae, steaming and decocting 30min in the water of 80 DEG C put into by 400g Fructus Momordicae charantiae, 320g green vegetable, takes out afterwards, puts in filter bag, extrudes excessive moisture, and the mixture after squeezing afterwards is positioned over 2h in screen, drains excessive moisture so that water content is 20%；Mixture after draining takes out, and puts in baking oven machine, and regulation oven temperature is 60 DEG C, is dried to mixture water content and is kept to when 3% stop baking, and dislocation carries out pulverization process in pulverizer, pulverizes 8min, crosses 120 mesh sieves, obtains mix powder；Mixed-powder obtained above will add 100g Flos Camelliae Japonicae nectar, after mix homogeneously, high-speed stirred 15min under the rotating speed of 600r/min, the hydroxymalonic acid extracted in Fructus Cucumidis sativi the most obtained above is added thereto, it is kept stirring for state 7min, stands subsequently, thickness mixed serum must be mixed；Finally above-mentioned prepared mixing thick slurry is placed in drying machine, dried 35min at 120 DEG C, obtains mixed-powder, is placed under uviol lamp by the mixed-powder obtained afterwards and carries out sterilization treatment, sterilizing 55min, i.e. can obtain the grease removal powder prepared with the hydroxymalonic acid extracted in Fructus Cucumidis sativi.
This example operation is simple, time edible, take the grease removal powder that the 15g present invention prepares to put in cup, and add 250mL warm water, stir i.e. edible, suggestion eats 1～3 time every day, drink water after Shi Yong 300mL, the most edible 18 days, can easily lose weight 8 kilograms, and will not rebound, any harm is not had for human body.
Claims (1)
1. one kind is extracted the method that grease removal powder prepared by hydroxymalonic acid from Fructus Cucumidis sativi, it is characterised in that concrete operation step is:
(1) take the fresh cucumber of 2～3kg, put in 5～6L clear water, backward clear water in add 50～80g sodium chloride, after stirring, repeatedly wash Fructus Cucumidis sativi surface by rubbing with the hands, go dirt and the spinule of skim-coat；
(2) after cleaning, Fructus Cucumidis sativi after washing is cut into the lamellar that thickness is 1～1.5cm, it is positioned in the Fructus Ananadis comosi sieve being paved with gauze, ted 3～6L in the sun, wherein tedding once every 2h, until cucumber slice water content is 25～30%, the cucumber slice after shining afterwards is put in squeezer and is squeezed the juice, squeezing 15～20min, obtains Sucus Cucumidis sativi；
(3) slag inclusion 5 squeezing obtained～the Sucus Cucumidis sativi of 8% are put in reactor, regulation temperature is 15～20 DEG C, and it is added thereto to Sucus Cucumidis sativi quality 1～2 times of mass concentrations are 8% ethanol solution and 6～8U flavor proteases, regulation pH is 5.0～6.2, and stir 10～15min with the rotating speed of 300～400r/min, to be mixed complete, then it is warming up to 40～50 DEG C with the speed program of 5～6 DEG C/min, obtain Fructus Cucumidis sativi mixed liquor；
(4) wait to heat up complete, the mixed liquor after above-mentioned intensification is positioned in sonic oscillation instrument, sonic oscillation reaction 1～3h, arranging supersonic frequency is 25～30KHz, and ultrasonic power is 100～150W, filters afterwards, remove filtering residue, obtain filtrate, and filtrate is stood 40～50min；
(5) filtrate after above-mentioned standing is put in Soxhlet extractor, extract 45～60min, collect filtrate extract, then move it in fermentation tank, it is warming up to 100～115 DEG C, and is stirred continuously 10～15min with the speed of 150～200r/min, remove wherein ethanol；
(6) it is kept stirring for state, during until filtrate extract volume is original volume 1/4 in fermentation tank, stops stirring, stand 1～2h so that it is naturally cool to room temperature, hydroxymalonic acid can be extracted from Fructus Cucumidis sativi；
(7) take 200～300g Fructus Benincasaes, 250～400g Fructus Momordicae charantiae, 220～320g green vegetable and put into steaming and decocting 20～30min in the water of 60～80 DEG C, take out afterwards, put in filter bag, extrusion excessive moisture, mixture after squeezing afterwards is positioned in screen 1～2h, drain excessive moisture so that water content is 15～20%；
(8) mixture after draining takes out, and puts in baking oven machine, and regulation oven temperature is 55～60 DEG C, being dried to mixture water content be kept to when 2～3% stop baking, dislocation carries out pulverization process in pulverizer, pulverizes 5～8min, cross 110～120 mesh sieves, obtain mix powder；
(9) mixed-powder obtained above will add 80～100g Flos Camelliae Japonicae nectar, after mix homogeneously, high-speed stirred 10～15min under the rotating speed of 500～600r/min, the hydroxymalonic acid extracted in the Fructus Cucumidis sativi that will obtain in above-mentioned steps (6) the most again is added thereto, it is kept stirring for state 5～7min, stand subsequently, thickness mixed serum must be mixed；
(10) above-mentioned prepared mixing thick slurry is placed in drying machine, dried 20～35min at 100～120 DEG C, obtain mixed-powder, afterwards the mixed-powder obtained is placed under uviol lamp and carries out sterilization treatment, sterilizing 45～55min, i.e. can obtain the grease removal powder prepared with the hydroxymalonic acid extracted in Fructus Cucumidis sativi.
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