CN105802477A - Environment-friendly waterborne paint and preparation method thereof - Google Patents
Environment-friendly waterborne paint and preparation method thereof Download PDFInfo
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- CN105802477A CN105802477A CN201610371124.XA CN201610371124A CN105802477A CN 105802477 A CN105802477 A CN 105802477A CN 201610371124 A CN201610371124 A CN 201610371124A CN 105802477 A CN105802477 A CN 105802477A
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
- C09D175/04—Polyurethanes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/70—Additives characterised by shape, e.g. fibres, flakes or microspheres
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/02—Flame or fire retardant/resistant
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Paints Or Removers (AREA)
- Application Of Or Painting With Fluid Materials (AREA)
Abstract
The invention belongs to the field of paint preparation, and particularly relates to environment-friendly waterborne paint and a preparation method thereof.The environment-friendly waterborne paint is composed of, by weight, 50-60 parts of waterborne polyurethane dispersoid, 15-20 parts of acrylate solution, 20-35 parts of purified water, 5-8 parts of an auxiliary, 10-15 parts of modified carbon nano fiber, 5-7 parts of hydroxypropyl starch, 3-5 parts of modified tea steam powder and 5-10 parts of waterborne pigment.The modified carbon nano fiber is added, so that wear resistance of the waterborne paint is improved; the hydroxypropyl starch is added, so that the waterborne paint has certain flame retardancy; the modified tea stem powder is added, so that improving of adhesion of the waterborne paint is facilitated; the waterborne paint prepared by the method is environment-friendly, good in film forming performance, wear resistance and glossiness and suitable for Christmas ball painting.
Description
Technical field
The invention belongs to coating preparation field, be specifically related to a kind of environment-friendly water-based paint and preparation method thereof.
Background technology
Christmas ball is usually and uses polystyrene resin is that primary raw material is fabricated to spheroid, the most again spheroid is carried out baking vanish, colouring, is allowed to present various color.During existing Christmas ball baking vanish, finish paint uses acrylic lacquer, is made up of acrylic resin and various volatile organic solvent, has certain pollution to air, and the most inflammable.Priming paint then be alkyd varnish, be made up of alkyd resin and organic solvent, water body and air can be polluted；And inflammable, its steam and air are easily formed explosive mixture, meet high heat, and naked light, strong oxidizer easily causes burning.
Although traditional water paint environmental protection, but filming performance is poor, gloss difference, wear no resistance, froth breaking difficulty.
Summary of the invention
Present invention aims to the deficiency of existing water paint, it is provided that a kind of environment-friendly water-based paint and preparation method thereof.This water paint filming performance, wearability are good, have preferable glossiness, are suitable for Christmas ball japanning.
For achieving the above object, the present invention adopts the following technical scheme that
A kind of environment-friendly water-based paint, its raw material composition is calculated as by weight, aqueous pu dispersions 50-60 part, acrylic acid ester emulsion 15-20 part, pure water 30-35 part, auxiliary agent 5-8 part, modified carbon nano tube fiber 10-15 part, hydroxypropyl starch 5-7 part, modified stalky tea powder 3-5 part, water dispersible pigment 5-10 part.
Preferably, its raw material of environment-friendly water-based paint composition is calculated as by weight, aqueous pu dispersions 58 parts, acrylic acid ester emulsion 17 parts, pure water 35 parts, auxiliary agent 8 parts, modified carbon nano tube fiber 13 parts, hydroxypropyl starch 6 parts, modified 4 parts of stalky tea powder, water dispersible pigment 7 parts.
The preparation method of described modified carbon nano tube fiber is: be dissolved in 40-50 ml pure water by the cetomacrogol 1000-1500 of 0.4-0.6 g, ultrasonic disperse 15-20 min so that it is be uniformly dispersed to obtain dispersion liquid；In dispersion liquid, add 0.3-0.5 g carbon nano-fiber, stirring mixing 12 h subsequently, make Polyethylene Glycol be substantially adhered to carbon nano-fiber surface, prepare modified carbon nano tube fiber.
The preparation method of described modified stalky tea powder is: adds in high-speed mixer by dry stalky tea powder, is stirred at 80-90 DEG C, adds the coupling agent of stalky tea grain weight amount 1-2%, stirs 5-6min, obtains the stalky tea powder after activation.
A kind of method preparing environment-friendly water-based paint as above, concretely comprises the following steps:
1) aqueous pu dispersions, acrylic acid ester emulsion and portion of pure water being put in blender, mixing speed is 500-700r/min, stirs 10-15min；
2) under 500-700r/min state, add auxiliary agent, hydroxypropyl starch, stir 12-15min；
3) then proceed to add modified carbon nano tube fiber, modified stalky tea powder and water dispersible pigment, disperse 20-30min at 1200-1500r/min；
4) it is eventually adding residue pure water, stirs 10-15min with 500-700r/min；Then censorship, packaging.
The application of a kind of environment-friendly water-based paint as above: for Christmas ball japanning.
The beneficial effects of the present invention is:
1) present invention is by adding modified carbon nano tube fiber, adds the wearability of water paint；The addition of hydroxypropyl starch so that water paint has certain anti-flammability；The addition of modified stalky tea powder, is conducive to increasing the adhesive force of water paint, the formaldehyde in absorption air；Obtained water paint environmental protection, filming performance, wearability are good, have preferable glossiness, are suitable for Christmas ball japanning；
2) one-dimentional structure, physics and chemical property that carbon nano-fiber is unique are utilized so that it is jointly act on hydroxypropyl starch, modified stalky tea powder, aqueous pu dispersions and acrylic acid ester emulsion, produce synergistic function；Environment protecting adhesive force prominent, on Christmas ball is strong, wear-resisting, and decorative effect is good.
Detailed description of the invention
In order to make content of the present invention easily facilitate understanding, below in conjunction with detailed description of the invention, technical solutions according to the invention are described further, but the present invention is not limited only to this.
Embodiment
1
A kind of environment-friendly water-based paint, its raw material composition is calculated as by weight, aqueous pu dispersions 50 parts, acrylic acid ester emulsion 20 parts, pure water 30 parts, auxiliary agent 8 parts, modified carbon nano tube fiber 10 parts, hydroxypropyl starch 7 parts, modified 3 parts of stalky tea powder, water dispersible pigment 10 parts.
The preparation method of described modified carbon nano tube fiber is: be dissolved in by the cetomacrogol 1000 of 0.5 g in 45 ml pure water, ultrasonic disperse 17 min so that it is be uniformly dispersed to obtain dispersion liquid；In dispersion liquid, add 0.4 g carbon nano-fiber, stirring mixing 12 h subsequently, make Polyethylene Glycol be substantially adhered to carbon nano-fiber surface, prepare modified carbon nano tube fiber.
The preparation method of described modified stalky tea powder is: adds in high-speed mixer by dry stalky tea powder, is stirred at 85 DEG C, adds the coupling agent of stalky tea grain weight amount 1%, stirs 5min, obtains the stalky tea powder after activation.
A kind of method preparing environment-friendly water-based paint as above, concretely comprises the following steps:
1) aqueous pu dispersions, acrylic acid ester emulsion and portion of pure water being put in blender, mixing speed is 600r/min, stirs 12min；
2) under 700r/min state, add auxiliary agent, hydroxypropyl starch, stir 14min；
3) then proceed to add modified carbon nano tube fiber, modified stalky tea powder and water dispersible pigment, disperse 30min at 1200r/min；
4) it is eventually adding residue pure water, stirs 13min with 600r/min；Then censorship, packaging.
The application of a kind of environment-friendly water-based paint as above: for Christmas ball japanning.
Embodiment
2
A kind of environment-friendly water-based paint, its raw material composition is calculated as by weight, aqueous pu dispersions 58 parts, acrylic acid ester emulsion 17 parts, pure water 35 parts, auxiliary agent 8 parts, modified carbon nano tube fiber 13 parts, hydroxypropyl starch 6 parts, modified 4 parts of stalky tea powder, water dispersible pigment 7 parts.
The preparation method of described modified carbon nano tube fiber is: be dissolved in by the polyethylene glycol 1500 of 0.4 g in 50 ml pure water, ultrasonic disperse 20 min so that it is be uniformly dispersed to obtain dispersion liquid；In dispersion liquid, add 0.3 g carbon nano-fiber, stirring mixing 12 h subsequently, make Polyethylene Glycol be substantially adhered to carbon nano-fiber surface, prepare modified carbon nano tube fiber.
The preparation method of described modified stalky tea powder is: adds in high-speed mixer by dry stalky tea powder, is stirred at 90 DEG C, adds the coupling agent of stalky tea grain weight amount 1%, stirs 6min, obtains the stalky tea powder after activation.
A kind of method preparing environment-friendly water-based paint as above, concretely comprises the following steps:
1) aqueous pu dispersions, acrylic acid ester emulsion and portion of pure water being put in blender, mixing speed is 500r/min, stirs 15min；
2) under 500r/min state, add auxiliary agent, hydroxypropyl starch, stir 15min；
3) then proceed to add modified carbon nano tube fiber, modified stalky tea powder and water dispersible pigment, disperse 20min at 1500r/min；
4) it is eventually adding residue pure water, stirs 10min with 700r/min；Then censorship, packaging.
The application of a kind of environment-friendly water-based paint as above: for Christmas ball japanning.
Embodiment
3
A kind of environment-friendly water-based paint, its raw material composition is calculated as by weight, aqueous pu dispersions 60 parts, acrylic acid ester emulsion 15 parts, pure water 35 parts, auxiliary agent 5 parts, modified carbon nano tube fiber 15 parts, hydroxypropyl starch 5 parts, modified 5 parts of stalky tea powder, water dispersible pigment 5 parts.
The preparation method of described modified carbon nano tube fiber is: be dissolved in by the polyethylene glycol 1500 of 0.6 g in 50 ml pure water, ultrasonic disperse 20 min so that it is be uniformly dispersed to obtain dispersion liquid；In dispersion liquid, add 0.5 g carbon nano-fiber, stirring mixing 12 h subsequently, make Polyethylene Glycol be substantially adhered to carbon nano-fiber surface, prepare modified carbon nano tube fiber.
The preparation method of described modified stalky tea powder is: adds in high-speed mixer by dry stalky tea powder, is stirred at 80 DEG C, adds the coupling agent of stalky tea grain weight amount 2%, stirs 6min, obtains the stalky tea powder after activation.
A kind of method preparing environment-friendly water-based paint as above, concretely comprises the following steps:
1) aqueous pu dispersions, acrylic acid ester emulsion and portion of pure water being put in blender, mixing speed is 700r/min, stirs 10-15min；
2) under 700r/min state, add auxiliary agent, hydroxypropyl starch, stir 12min；
3) then proceed to add modified carbon nano tube fiber, modified stalky tea powder and water dispersible pigment, disperse 20min at 1500r/min；
4) it is eventually adding residue pure water, stirs 10min with 700r/min；Then censorship, packaging.
The application of a kind of environment-friendly water-based paint as above: for Christmas ball japanning.
The foregoing is only presently preferred embodiments of the present invention, all impartial changes done according to scope of the present invention patent and modification, all should belong to the covering scope of the present invention.
Claims (6)
1. an environment-friendly water-based paint, it is characterized in that: its raw material composition is calculated as by weight, aqueous pu dispersions 50-60 part, acrylic acid ester emulsion 15-20 part, pure water 30-35 part, auxiliary agent 5-8 part, modified carbon nano tube fiber 10-15 part, hydroxypropyl starch 5-7 part, modified stalky tea powder 3-5 part, water dispersible pigment 5-10 part.
Environment-friendly water-based paint the most according to claim 1, it is characterized in that: its raw material composition is calculated as by weight, aqueous pu dispersions 58 parts, acrylic acid ester emulsion 17 parts, pure water 35 parts, auxiliary agent 8 parts, modified carbon nano tube fiber 13 parts, hydroxypropyl starch 6 parts, modified 4 parts of stalky tea powder, water dispersible pigment 7 parts.
Environment-friendly water-based paint the most according to claim 1 and 2, it is characterized in that: the preparation method of described modified carbon nano tube fiber is: the cetomacrogol 1000-1500 of 0.4-0.6 g is dissolved in 40-50 ml pure water, ultrasonic disperse 15-20 min so that it is be uniformly dispersed to obtain dispersion liquid；In dispersion liquid, add 0.3-0.5 g carbon nano-fiber, stirring mixing 12 h subsequently, make Polyethylene Glycol be substantially adhered to carbon nano-fiber surface, prepare modified carbon nano tube fiber.
Environment-friendly water-based paint the most according to claim 1 and 2, it is characterized in that: the preparation method of described modified stalky tea powder is: add in high-speed mixer by dry stalky tea powder, it is stirred at 80-90 DEG C, add the coupling agent of stalky tea grain weight amount 1-2%, stirring 5-6min, obtains the stalky tea powder after activation.
5. the method for the environment-friendly water-based paint prepared as described in any one of claim 1-2, it is characterised in that: concretely comprise the following steps:
1) aqueous pu dispersions, acrylic acid ester emulsion and portion of pure water being put in blender, mixing speed is 500-700r/min, stirs 10-15min；
2) under 500-700r/min state, add auxiliary agent, hydroxypropyl starch, stir 12-15min；
3) then proceed to add modified carbon nano tube fiber, modified stalky tea powder and water dispersible pigment, disperse 20-30min at 1200-1500r/min；
4) it is eventually adding residue pure water, stirs 10-15min with 500-700r/min；Then censorship, packaging.
6. the application of the environment-friendly water-based paint as described in any one of claim 1-2, it is characterised in that: for Christmas ball japanning.
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| CN201610371124.XA CN105802477B (en) | 2016-05-31 | 2016-05-31 | A kind of environment-friendly water-based paint and preparation method thereof |
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| CN201610371124.XA CN105802477B (en) | 2016-05-31 | 2016-05-31 | A kind of environment-friendly water-based paint and preparation method thereof |
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| CN105802477B CN105802477B (en) | 2018-05-04 |
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Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106243964A (en) * | 2016-08-25 | 2016-12-21 | 阜阳富瑞雪化工科技有限公司 | A kind of furniture water paint with refreshment effect |
| CN106280951A (en) * | 2016-08-25 | 2017-01-04 | 阜阳富瑞雪化工科技有限公司 | A kind of high-quality furniture water paint |
| CN106833344A (en) * | 2016-12-13 | 2017-06-13 | 苏州赛斯德工程设备有限公司 | A kind of water nano anticorrosive paint and preparation method thereof |
| CN107384083A (en) * | 2017-09-05 | 2017-11-24 | 东莞市长安沃土装饰材料店 | Wear-resisting type emulsion paint |
| CN107722689A (en) * | 2017-10-11 | 2018-02-23 | 阜南县大自然工艺品有限公司 | A kind of anti-fouling paint for wicker products |
| CN109096900A (en) * | 2018-07-20 | 2018-12-28 | 张军 | A kind of environment-friendly water-based woodcare paint |
| CN109666352A (en) * | 2018-11-22 | 2019-04-23 | 河北晨阳工贸集团有限公司 | A kind of water paint and preparation method thereof for door and window |
| CN110982321A (en) * | 2019-12-02 | 2020-04-10 | 中山市恒美油墨涂料有限公司 | Water-based two-component automotive interior paint |
| CN111100215A (en) * | 2019-12-30 | 2020-05-05 | 河南新孚望新材料科技有限公司 | Preparation method of hydroxypropyl high amylose starch for water-based paint |
| CN111393929A (en) * | 2020-04-01 | 2020-07-10 | 郑州熙虎科技有限公司 | Environment-friendly water-based paint for historic building |
| CN112343262A (en) * | 2020-07-14 | 2021-02-09 | 青岛悦浪建筑技术有限责任公司 | Self-repairing waterproof coiled material connecting part structure and interface waterproof adhesive coating for connection of self-repairing waterproof coiled material connecting part structure |
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Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106243964A (en) * | 2016-08-25 | 2016-12-21 | 阜阳富瑞雪化工科技有限公司 | A kind of furniture water paint with refreshment effect |
| CN106280951A (en) * | 2016-08-25 | 2017-01-04 | 阜阳富瑞雪化工科技有限公司 | A kind of high-quality furniture water paint |
| CN106280951B (en) * | 2016-08-25 | 2017-10-03 | 阜阳富瑞雪化工科技有限公司 | A kind of high-quality furniture water paint |
| CN106833344A (en) * | 2016-12-13 | 2017-06-13 | 苏州赛斯德工程设备有限公司 | A kind of water nano anticorrosive paint and preparation method thereof |
| CN107384083A (en) * | 2017-09-05 | 2017-11-24 | 东莞市长安沃土装饰材料店 | Wear-resisting type emulsion paint |
| CN107722689A (en) * | 2017-10-11 | 2018-02-23 | 阜南县大自然工艺品有限公司 | A kind of anti-fouling paint for wicker products |
| CN109096900A (en) * | 2018-07-20 | 2018-12-28 | 张军 | A kind of environment-friendly water-based woodcare paint |
| CN109666352A (en) * | 2018-11-22 | 2019-04-23 | 河北晨阳工贸集团有限公司 | A kind of water paint and preparation method thereof for door and window |
| CN110982321A (en) * | 2019-12-02 | 2020-04-10 | 中山市恒美油墨涂料有限公司 | Water-based two-component automotive interior paint |
| CN111100215A (en) * | 2019-12-30 | 2020-05-05 | 河南新孚望新材料科技有限公司 | Preparation method of hydroxypropyl high amylose starch for water-based paint |
| CN111393929A (en) * | 2020-04-01 | 2020-07-10 | 郑州熙虎科技有限公司 | Environment-friendly water-based paint for historic building |
| CN112343262A (en) * | 2020-07-14 | 2021-02-09 | 青岛悦浪建筑技术有限责任公司 | Self-repairing waterproof coiled material connecting part structure and interface waterproof adhesive coating for connection of self-repairing waterproof coiled material connecting part structure |
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| Publication number | Publication date |
|---|---|
| CN105802477B (en) | 2018-05-04 |
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Address after: 355200 Shuangyue Road, Shuangyue Industrial Park, Fuding City, Ningde City, Fujian Province Patentee after: FUJIAN YINGHAO CULTURAL AND CREATIVE Co.,Ltd. Address before: 355200 E-5, Shuangyue Industrial Concentration Zone, Lantian Mountain Front, Fuding City, Ningde City, Fujian Province Patentee before: FUJIAN YINGHAO CRAFT PRODUCTS Co.,Ltd. |
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Denomination of invention: An environmentally friendly waterborne paint and its preparation method Effective date of registration: 20201112 Granted publication date: 20180504 Pledgee: China Co. truction Bank Corp Fuding branch Pledgor: FUJIAN YINGHAO CULTURAL AND CREATIVE Co.,Ltd. Registration number: Y2020350000133 |
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Date of cancellation: 20230908 Granted publication date: 20180504 Pledgee: China Co. truction Bank Corp Fuding branch Pledgor: FUJIAN YINGHAO CULTURAL AND CREATIVE Co.,Ltd. Registration number: Y2020350000133 |
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