CN105769704A - Skincare mask based on active ingredients of staminate flowers of eucommia ulmoides and preparation method of skincare mask - Google Patents
Skincare mask based on active ingredients of staminate flowers of eucommia ulmoides and preparation method of skincare mask Download PDFInfo
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- CN105769704A CN105769704A CN201610253114.6A CN201610253114A CN105769704A CN 105769704 A CN105769704 A CN 105769704A CN 201610253114 A CN201610253114 A CN 201610253114A CN 105769704 A CN105769704 A CN 105769704A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
Abstract
The invention discloses a skincare mask based on active ingredients of staminate flowers of eucommia ulmoides and a preparation method of the skincare mask, and belongs to the technical field of cosmetics. The skincare mask is composed of the following raw materials and auxiliary materials in parts by mass: 3.0-9.0 parts of an extract of staminate flowers of eucommia ulmoides, 5.0-15.0 parts of a water-soluble vegetable gum, 2.0-6.0 parts of a thickener, 2.0-6.0 parts of water-soluble collagen powder, 3.0-9.0 parts of glycerol, 0.6-1.8 parts of natural essential oil and the balance of deionized water to make up 100 parts. The skincare mask provided by the invention has the effects of accelerating the removal of skin impurities and free radicals, toughening collagen and elastic fibers in the skin and enhancing expansive force, and also can clean folliculus pili and deep skin, to make the pores finer, make the skin more delicate, more flat and more smooth, and play the roles of improving and protecting the skin.
Description
Technical field
The invention belongs to cosmetic technical field, particularly belong to a kind of skin cosmetic being raw material with galenical.
Background technology
Facial film is the cosmetics of a kind of novelty, and facial film as the carrier of nutrient substance, both effectiveness material, can be conducive to trophism or both effectiveness material to penetrate into the deep layer of skin, play the effect of protection beautifying skin.Especially the facial film being functional component with vegetalitas preparation, more by the favor of people.TCM in Ancient China document Thousand Golden Prescriptions just there is plant amedica such as utilizing plant Radix Angelicae Sinensis, the Radix Angelicae Dahuricae, CHUANSHAO to carry out the record of beauty therapeutic.
The Cortex Eucommiae (Eucommiaulmoides) is the medicinal plants that China is precious, rich in nutrient substance such as chlorogenic acid, aucubin, Geniposidic acid, Polyphenols, flavonoid, polysaccharide isoreactivity material and multiple mineral element, crude protein, vitamin and aminoacid in eucommia Bark male flower.Pharmacological testing shows, rat is had no side effect by eucommia Bark male flower, illustrate its have grade-safe (Du Hongyan etc. the food safety toxicology of eucommia ulmoides male flower tea, Sino-South African Forestry University of Science and Technology's journal, 2008.28 (2): 91-92), eucommia Bark male flower now has been developed that into the product-feed markets such as eucommia ulmoides male flower tea.But, relevant eucommia Bark male flower answers land used research then few in number on daily chemical products.
Another key technology prepared by facial film is film, and it is the carrier of medicine, i.e. " macromolecule sponge ", and it can carry and discharge medicine, reaches the effect for the treatment of, protection skin of face.The a lot of facial film of conventional filmogen is that ductility is poor using non-woven fabrics as carrier, it is impossible to well fit with face.More be used mostly synthetic material such as polrvinyl chloride, polyvinyl alcohol, acrylate etc at present, there is safety and sanitation problem in this type of material.Therefore, about the research of facial film also to All Pure Nature, safety, nuisanceless type, high-quality direction develop.
Summary of the invention
The object of the invention is just to provide a kind of facial treatment mask based on eucommia Bark male flower active component, and this facial film can accelerate to remove skin impurities, free radical, plays the effect improved and protect skin.
The preparation method that another object of the present invention is to provide a kind of facial treatment mask based on eucommia Bark male flower active component.
It is an object of the invention to be achieved through the following technical solutions.
A kind of facial treatment mask based on eucommia Bark male flower active component, it is characterised in that be made up of following masses proportioning part supplementary material:
Eucommia Bark male flower extract 3.0～9.0 parts,
5.0～15.0 parts of water-soluble plant glue,
Thickening agent 2.0～6.0 parts,
2.0～6.0 parts of water-solubility collagen powder,
Glycerol 3.0～9.0 parts,
Natural essential oil 0.6～1.8 part,
Balance deionized water supplies 100 parts.
Optimizing, described facial treatment mask is made up of following masses proportioning part supplementary material:
Eucommia Bark male flower extract 6.0 parts,
10.0 parts of water-soluble plant glue,
Thickening agent 4.0 parts,
4.0 parts of water-solubility collagen powder,
Glycerol 6.0 parts,
Natural essential oil 1.2 parts,
Balance deionized water supplies 100 parts.
Described eucommia Bark male flower extract, it is the male flower with the famous and precious medicinal plants Cortex Eucommiae Xiong Shu of China through pre-treatment, extracts the extract with skin care activity functional component being isolated, rich in nutrient substance such as iridoids, chlorogenic acid, aucubin, Geniposidic acid, Polyphenols, flavonoid, polysaccharide isoreactivity material and multiple mineral element, crude protein, vitamin and aminoacid.
Described water-soluble plant glue, is the plant gum that is made up of galactomannan of a class, mean molecule quantity 20～300,000 dalton.Easily it is dispersed in hot water or cold water and forms the fluid with certain viscosity, other electrolyte are had good compatibility.Tool cis ortho position dihydroxy, can form gel, have fabulous water holding and adhesive ability after crosslinking.Water-soluble plant glue described in this formula in tracasol, guar gum (Guargum), sesbania gum, the trigonella bean gum one or more.
Described thickening agent, be chosen among plant cellulose derivant carboxymethyl cellulose, ethyl cellulose, hydroxyethyl cellulose, hydroxypropyl cellulose and hydroxypropyl methyl cellulose one or more.
Described natural essential oil, be chosen from natural plants Herba Lysimachiae foenum-graeci quintessence oil, Flos Rosae Rugosae quintessence oil, Radix Cymbopogonis Citrati quintessence oil, rosemary ethereal oil, Peppermint essential oil, Flos Jasmini Sambac quintessence oil, Salvia Sclare L. quintessence oil one or more.
The preparation method of a kind of facial treatment mask based on eucommia Bark male flower active component, is characterized in that, adopts following steps to complete:
1, the preparation method of eucommia Bark male flower extract: the eucommia Bark male flower flower bud gathered after selecting remove impurity, then the 40～60s that completes in steam；In microwave oven, under 560W power, it is dried to moisture≤8.0%；Pulverizing 40 orders, with 50% ethanol of material 10 times amount (W/V) for solvent, supersound extraction, ultrasonic power is 60kw, extracts 2 times, each 60min under room temperature；After the recovered ethanol of extract filtrate, at vacuum 0.85～0.95Mpa, 60～70 DEG C are evaporated to relative density and are 1.1～1.25(50 DEG C) extractum；At vacuum 0.85～0.95Mpa, dry moisture≤5.0%, pulverized 100 mesh sieve holes standby for 60～70 DEG C；Extract yield is more than 8.2%, and extract total phenol content is more than 86.0mg.g-1, total flavones is more than 17.0mg.g-1, extract sanitary index should meet country Ministry of Foreign Trade and Economic Cooperation WM2-2001 " green industry standard imported and exported by medicinal plants and preparation "；
2, configuration technological operation step: another water-soluble plant gum, thickening agent suitable quantity of water mix pasty state, add after soaking 24h
Appropriate amount of deionized water, is sequentially added into eucommia Bark male flower extract under stirring at 60～70 DEG C, water-solubility collagen powder, glycerol make it be uniformly dispersed；Stirring drops to room temperature, adds natural essential oil, adds deionized water；Stir, obtain emulsion, fill, steam high-voltage sterilizing and get final product.
Using method: cleaned up by face, is applied to face by above-mentioned facial film emulsion Direct Uniform, or facial film emulsion is applied on face paper (cloth), be pasted on face, after 1～3h, remove.
3, facial mask shaping technique: poured into by emulsion in facial film mould, places 18～24 hours, and then logical 50～60 DEG C of hot-air dewaterings molding in 40～60 minutes in hot blast cabinet, then at-10 DEG C～-15 DEG C freezings 2～3 days；The product thaw at RT demoulding, uses composite plastic film gas flush packaging, isotope sterilizing, thus obtaining the product.Molding facial film directly against spreading on face, after 1～3h, can remove.
The invention has the beneficial effects as follows: eucommia Bark male flower extract of the present invention preparation adopts Cortex Eucommiae extract rich in natural antioxidation, fungicide active ingredients such as eucommia Bark male flower flavone, phenols.There is acceleration and remove skin impurities, free radical; make that collagen elastic fibers in epidermis is tough and tensile, expansive force strengthens, hair follicle and deep skin can be cleaned again, make pore more tiny; so that allowing skin seem finer and smoother more smooth lubricious, play the good effects improved and protect skin.The present invention utilizes natural plant as effective ingredient carrier first, has extraordinary film property, and the film toughness formed is strong, ductility good, particularly has good adhesiveness, can be intimately associated with skin, reaches intended cleaning effect.Water-soluble plant glue is a kind of pure plant source active substance, and skin is non-stimulated, has no side effect, degradable in nature, be manufacture facial film preferably, environmentally friendly natural biologic material.The eucommia Bark male flower extract skin care activity composition facial film of preparation.Avoid the safety and sanitation problem because using synthesizing polyvinyl chloride, polyvinyl alcohol, acrylate etc material to cause, make cosmetics facial film realize effective, pure natural and environmental protection.The formula material of the present invention and preparation method uniqueness are novel.
Detailed description of the invention
But the explanation of specific examples below is not limitation of the present invention, the technology of the present invention content is also not limited to following citing.The art person skilled, in the essential scope of the present invention, change, change, interpolation or the replacement made all should belong to protection scope of the present invention.
Embodiment 1.
(1) formula composition: (preparation 1000g).
Eucommia Bark male flower extract 60g, water-soluble plant glue 100g, thickening agent 40g.Water solublity collagen egg 40g, glycerol 60g, natural essential oil 12g.
(2) preparation technology.
1) preparation method of eucommia Bark male flower extract: the eucommia Bark male flower flower bud gathered after selecting remove impurity, then the 40～60s that completes in steam.In microwave oven, under 560W power, it is dried to moisture≤8.0%.Pulverize 40 orders, take 1000g, with 50% ethanol of 10L for solvent, lower 2 times of the ultrasonic room temperature of 60kw, each 60min.After the recovered ethanol of extract filtrate, at vacuum 0.85～0.95Mpa, 60～70 DEG C are evaporated to relative density and are 1.1～1.25(50 DEG C) extractum.At vacuum 0.85～0.95Mpa, drying moisture≤5.0% for 60～70 DEG C, obtaining extract 86g, to pulverize 100 mesh sieve holes standby.Extract total phenol content 88.0mg.g-1, total flavones 19.0mg.g-1.Extract sanitary index should meet country Ministry of Foreign Trade and Economic Cooperation WM2-2001 " green industry standard imported and exported by medicinal plants and preparation ".
2) configuration technological operation step: weigh water-soluble plant glue 100g, thickening agent 40g suitable quantity of water mixes pasty state, soak after 24h and add appropriate amount of deionized water, be sequentially added into eucommia Bark male flower extract 60g under stirring at 60～70 DEG C, water-solubility collagen powder 40g, glycerol 60g make it be uniformly dispersed.Stirring drops to room temperature, adds natural essential oil 12g and adds deionized water and makes it become 1000g, stirs, and obtains emulsion, deaeration, fill, steam high-voltage sterilizing and get final product.
Using method: cleaned up by face, is applied to face by above-mentioned facial film emulsion Direct Uniform, or facial film emulsion is applied on face paper (cloth), be pasted on face, after 1～3h, remove.
3) facial mask shaping technique: poured into by emulsion in facial film mould, places 18～24 hours, and then logical 50～60 DEG C of hot-air dewaterings molding in 40～60 minutes in hot blast cabinet, then at-10 DEG C～-15 DEG C freezings 2～3 days；The product thaw at RT demoulding, by composite membrane plastic bag gas flush packaging, isotope sterilizing, thus obtaining the product.Molding facial film directly against spreading on face, after 1～3h, can remove.
Embodiment 2.
(1) formula composition: (preparation 1000g).
Eucommia Bark male flower extract 30g, water-soluble plant glue 50g, thickening agent 20g.Water solublity collagen egg 20g, glycerol 30g, natural essential oil 6.0g.
(2) preparation technology.
1) preparation method of eucommia Bark male flower extract: the eucommia Bark male flower flower bud gathered after selecting remove impurity, then the 40～60s that completes in steam.In microwave oven, under 560W power, it is dried to moisture≤8.0%.Pulverize 40 orders, take 500g, with 50% ethanol of 0.5L for solvent, lower 2 times of the ultrasonic room temperature of 60kw, each 60min.After the recovered ethanol of extract filtrate, at vacuum 0.85～0.95Mpa, 60～70 DEG C are evaporated to relative density and are 1.1～1.25(50 DEG C) extractum.At vacuum 0.85～0.95Mpa, drying moisture≤5.0% for 60～70 DEG C, obtaining extract 41.5g, to pulverize 100 mesh sieve holes standby.Total phenol content 87.0mg.g in extract-1, total flavones 18.0mg.g-1.Extract sanitary index should meet country Ministry of Foreign Trade and Economic Cooperation WM2-2001 " green industry standard imported and exported by medicinal plants and preparation ".
2) configuration technological operation step: weigh water-soluble plant glue 50g, thickening agent 20g suitable quantity of water mixes pasty state, soak after 24h and add appropriate amount of deionized water, be sequentially added into eucommia Bark male flower extract 30g under stirring at 60～70 DEG C, water-solubility collagen powder 20g, glycerol 30g make it be uniformly dispersed.Stirring drops to room temperature, adds natural essential oil 6.0g and adds deionized water and makes it become 1000g, stirs, and obtains emulsion, deaeration, fill, steam high-voltage sterilizing and get final product.
Using method: with example 1.
3) facial mask shaping technique: with example 1.
Embodiment 3.
(1) formula composition: (preparation 1000g).
Eucommia Bark male flower extract 90g, water-soluble plant glue 150g, thickening agent 60g.Water solublity collagen egg 60g, glycerol 90g, natural essential oil 18g.
(2) preparation technology.
1) preparation method of eucommia Bark male flower extract: the eucommia Bark male flower flower bud gathered after selecting remove impurity, then the 40～60s that completes in steam.In microwave oven, under 560W power, it is dried to moisture≤8.0%.Pulverize 40 orders, take 1500g, with 50% ethanol of 15L for solvent, lower 2 times of the ultrasonic room temperature of 60kw, each 60min.After the recovered ethanol of extract filtrate, at vacuum 0.85～0.95Mpa, 60～70 DEG C are evaporated to relative density and are 1.1～1.25(50 DEG C) extractum.At vacuum 0.85～0.95Mpa, drying moisture≤5.0% for 60～70 DEG C, obtaining extract 125g, to pulverize 100 mesh sieve holes standby.This extract total phenol content 87.0mg.g-1, total flavones 17.0mg.g-1, sanitary index should meet country Ministry of Foreign Trade and Economic Cooperation WM2-2001 " green industry standard imported and exported by medicinal plants and preparation ".
2) configuration technological operation step: weigh water-soluble plant glue 150g, thickening agent 60g suitable quantity of water mixes pasty state, soak after 24h and add appropriate amount of deionized water, be sequentially added into eucommia Bark male flower extract 90g under stirring at 60～70 DEG C, water-solubility collagen powder 60g, glycerol 90g make it be uniformly dispersed.Stirring drops to room temperature, adds natural essential oil 18g and adds deionized water and makes it become 1000g, stirs, and obtains emulsion, deaeration, fill, steam high-voltage sterilizing and get final product.
Using method: with example 1.
3) facial mask shaping technique: with example 1.
Three batches of embodiment product indices reach following standard-required:
(1) product (emulsion) appearance character and stability: meet table 1.
Table 1 product appearance, character and stability.
(2) product (emulsion) sanitary index: in Table 2.
Table 2 product sanitary index.
(3) product (emulsion) skin irritation test: table 3 requirement should be met.
Table 3 skin irritation test result.
(4) evaluation of product result of use:
With 100 aspiration eucommia Bark male flower facial treatment mask on probation, to follow up a case by regular visits to evaluation number for index, result is as shown in table 4.
The evaluation table of table 4 product result of use.
Through follow up survey, volunteer uses this facial film of reaction without allergy, non-stimulated and greasy feeling；Thinking that eucommia Bark male flower facial treatment mask clearly can keep moisture of skin, high resilience soft and moist with rear skin, whitening effect is notable, and spot also can be effectively improved.
Claims (7)
1. the facial treatment mask based on eucommia Bark male flower active component, it is characterised in that: it is made up of the component of following masses part: eucommia Bark male flower extract 3.0～9.0 parts, 5.0～15.0 parts of water-soluble plant glue, thickening agent 2.0～6.0 parts, 2.0～6.0 parts of water-solubility collagen powder, glycerol 3.0～9.0 parts, natural essential oil 0.6～1.8 part and deionized water supply 100 parts.
2. a kind of facial treatment mask based on eucommia Bark male flower active component according to claim 1, it is characterised in that: it is made up of following masses proportioning part supplementary material: eucommia Bark male flower extract 6.0 parts, 10.0 parts of water-soluble plant glue, thickening agent 4.0 parts, 4.0 parts of water-solubility collagen powder, glycerol 6.0 parts, natural essential oil 1.2 parts, deionized water supply 100 parts.
3. a kind of facial treatment mask based on eucommia Bark male flower active component according to claim 1, it is characterised in that: described water-soluble plant glue, is the plant gum that is made up of galactomannan of a class, mean molecule quantity 20～300,000 dalton；In tracasol, guar gum, sesbania gum, trigonella bean gum one or more.
4. a kind of facial treatment mask based on eucommia Bark male flower active component according to claim 1, it is characterised in that: described thickening agent is selected from one or more among plant cellulose derivant carboxymethyl cellulose, ethyl cellulose, hydroxyethyl cellulose, hydroxypropyl cellulose and hydroxypropyl methyl cellulose.
5. a kind of facial treatment mask based on eucommia Bark male flower active component according to claim 1, it is characterised in that: described natural essential oil selected from natural plants Herba Lysimachiae foenum-graeci quintessence oil, Flos Rosae Rugosae quintessence oil, Radix Cymbopogonis Citrati quintessence oil, rosemary ethereal oil, Peppermint essential oil, Flos Jasmini Sambac quintessence oil, Salvia Sclare L. quintessence oil one or more.
6. the preparation method of a kind of facial treatment mask based on eucommia Bark male flower active component described in claim 1, it is characterised in that: adopt following steps:
(1) preparation method of eucommia Bark male flower extract: the eucommia Bark male flower flower bud gathered after selecting remove impurity, complete 40～60s again in steam, in microwave oven, it is dried to moisture≤8.0% under 560W power, pulverized 40 orders, with material 10 times amount, W/V, 50% ethanol be solvent, supersound extraction, ultrasonic power is 60kw, extract 2 times under room temperature, each 60min, after the recovered ethanol of extract filtrate, at vacuum 0.85～0.95Mpa, 60～70 DEG C are evaporated to relative density is 1.1～1.25, the extractum of 50 DEG C, at vacuum 0.85～0.95Mpa, dry moisture≤5.0% for 60～70 DEG C, pulverized 100 mesh sieve holes standby；Extract yield more than 8.2%, total phenol content is more than 86.0mg.g-1, total flavones is more than 17.0mg.g-1, extract sanitary index should meet country Ministry of Foreign Trade and Economic Cooperation WM2-2001 " green industry standard imported and exported by medicinal plants and preparation "；
Configuration technological operation step: take formula ratio water-soluble plant glue, thickening agent suitable quantity of water mixes pasty state, soaks 24h
After add appropriate amount of deionized water, be sequentially added into formula ratio eucommia Bark male flower extract under stirring at 60～70 DEG C, water-solubility collagen powder, glycerol make it be uniformly dispersed；Stirring drops to room temperature, adds natural essential oil, adds deionized water, stir, obtain emulsion, fill, sterilizing, thus obtaining the product.
7. the preparation method of a kind of facial treatment mask based on eucommia Bark male flower active component according to claim 6, it is characterized in that: in described step (2), emulsion can carry out facial mask shaping technique: emulsion is poured in facial film mould, place 20～24 hours, then logical 50～60 DEG C of hot blasts molding in 40～60 minutes in hot blast cabinet, then at-10 DEG C～-15 DEG C freezings 2～3 days；The product thaw at RT demoulding, by composite plastic film bag gas flush packaging, isotope sterilizing, thus obtaining the product.
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| CN201610253114.6A CN105769704A (en) | 2016-04-22 | 2016-04-22 | Skincare mask based on active ingredients of staminate flowers of eucommia ulmoides and preparation method of skincare mask |
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| CN107823009A (en) * | 2017-12-13 | 2018-03-23 | 国家林业局泡桐研究开发中心 | A kind of bark of eucommia Chinese medicine hydrogel mask sheet and preparation method and application |
| CN113368020A (en) * | 2021-05-11 | 2021-09-10 | 上海游春生物科技有限公司 | All natural cucurbitaceae plant water beauty lotion |
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| CN107823009A (en) * | 2017-12-13 | 2018-03-23 | 国家林业局泡桐研究开发中心 | A kind of bark of eucommia Chinese medicine hydrogel mask sheet and preparation method and application |
| CN113368020A (en) * | 2021-05-11 | 2021-09-10 | 上海游春生物科技有限公司 | All natural cucurbitaceae plant water beauty lotion |
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