CN105768218A - Cigarette purifying agent containing squid bones as well as preparation method and application of cigarette purifying agent - Google Patents
Cigarette purifying agent containing squid bones as well as preparation method and application of cigarette purifying agent Download PDFInfo
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- CN105768218A CN105768218A CN201610174798.0A CN201610174798A CN105768218A CN 105768218 A CN105768218 A CN 105768218A CN 201610174798 A CN201610174798 A CN 201610174798A CN 105768218 A CN105768218 A CN 105768218A
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- Prior art keywords
- squid bone
- cleanser
- squid
- purifying agent
- medicated cigarette
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/08—Use of materials for tobacco smoke filters of organic materials as carrier or major constituent
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The invention relates to a cigarette purifying agent containing squid bones as well as a preparation method and an application of the cigarette purifying agent. The cigarette purifying agent is prepared from raw materials in percentage by mass as follows: 60%-90% of the squid bone meal, 0.4%-1.2% of xanthan gum, 1%-1.5% of organic acid matters, 1%-1.5% of ester compounds and 10%-20% of activated carbon, wherein the squid bone meal is treated; the organic acid matters are a mixture of malic acid and citric acid; the ester compounds is one of or a mixture of ethyl formate, ethyl acetate and ethyl propionate. The cigarette purifying agent has the characteristics of high safety, low production cost and the like; the cigarette purifying agent prepared with the method and a filter tip containing the purifying agent can remarkably reduce the content of harmful gas such as aldehydes materials and the like produced in the burning process of cigarettes, and the purpose of protecting health of human bodies is achieved.
Description
Technical field
The present invention relates to technical field of cigarettes, particularly relate to a kind of squid bone Medicated cigarette cleanser and preparation method thereof and the application on cigarette holder of this cleanser.
Background technology
Medicated cigarette is the common consumer product that consumer is important, also it is the important source of paying taxes of country, but in the flue gas that Medicated cigarette produces containing a large amount of with aldehyde material be representative to the poisonous and hazardous chemical substance of human body, tobacco industry covers, typically via adding spiced perfume compounding method, the harmful gas that human body has relatively strong and stimulating, although existing scholar reduces harmful gas content by adding the methods such as activated carbon in prolongation filter length, change filter plug material, filter plug at present, but aldehyde matter content reducing effect is extremely limited by these methods.
Squid bone is some transparent hoses in squid trunk, and its main component is chitin, and along with China's squid amount of fishing rises year by year, the comprehensive utilization of squid cartilage also becomes current processing of aquatic products industry important topic.The present invention with Peru squid cartilage for raw material, prepare into after processing can the cleanser of the aldehyde material such as efficient absorption formaldehyde, acetaldehyde, add in filter plug, to realize reducing the purpose of aldehyde matter content in flue gas.
Summary of the invention
The present invention provides a kind of squid bone Medicated cigarette cleanser and its preparation method and application, efficiently solves the direct of the aldehyde like harmful substance confrontation human body in Medicated cigarette and injures.
Technical scheme is as follows:
A kind of squid bone Medicated cigarette cleanser, it is characterised in that: with raw materials quality than calculating, its raw material composition include 60～90% squid bone meal, 0.4～1.2% xanthan gum, 1～1.5% organic acid substance, 1～1.5% ester type compound and 10～20% activated carbon.
The preparation method of a kind of squid bone Medicated cigarette cleanser, it is characterised in that comprise the following steps:
1) organic Halogenated-hydrocarbons is dissolved in the water, makes mixed solution A；
2) by squid bone meal and activated carbon Homogeneous phase mixing in proportion, with solution A Homogeneous phase mixing after carry out lyophilization, obtain pressed powder B；
3) xanthan gum is dissolved in the water, is configured to the solution C of 0.4～1.2% mass concentration, during configuration, want continuous uniform stirring；
4) by step 2) in the pressed powder B that obtains mix with xanthan gum solution C after carry out lyophilization again, obtain fume-clarifying agent powder；
The mass percent of the wherein said squid bone each raw material of Medicated cigarette cleanser is: squid bone meal 60～90%, xanthan gum 0.4～1.2%, organic acid substance 1～1.5%, ester type compound 1～1.5% and activated carbon 10～20%, all the other are water.
As preferably, the organic acid substance described in step 1) is the mixture of malic acid and citric acid；Described ester type compound is the mixture of one or more of Ethyl formate, ethyl acetate and ethyl propionate.
As preferably, step 2) described in squid bone meal be treated squid bone meal, the concrete technique that processes is: weigh a certain amount of squid cartilage, clear water is cleaned, naturally dry and be placed in plastic packaging bag, it is positioned in ultra cold storage freezer, cryogenic temperature is-65～-80 DEG C, process time 24～36h, squid bone after process takes out at once and carries out tissue pulverizer pulverizing, grinding particle size required 80 mesh sieves, namely coarse powder is obtained, coarse powder is placed in closing crucible, calcine in Muffle furnace, calcining heat 300～500 DEG C, time 1.5～3h, rear taking-up is placed in slow cooling in 60 DEG C of baking ovens, finally it is placed in drying basin standby.
One squid bone Medicated cigarette cleanser of the present invention is employed on filter tip, and described cleanser content is 1.0mg/mm～1.6mg/mm.
Compared with prior art, the ownership of the present invention has the features such as safety height, production cost be low for raw material；The Medicated cigarette cleanser that prepared by the method for the invention and the filter plug containing cleanser, can be significantly reduced the harmful gas content such as the aldehyde material that contains in the flue gas that cigarette burning process produces, reach the target of protection health.
Accompanying drawing explanation
Fig. 1: embodiment 1 squid bone Medicated cigarette cleanser purification efficiency table；
Fig. 2: embodiment 2 squid bone Medicated cigarette cleanser purification efficiency table.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described in further detail.
The Medicated cigarette cleanser of the present invention is made up of the composition of following weight ratio: the squid bone meal 60～90% after xanthan gum 0.4～1.2%, process, organic acid substance 1～1.5%, ester type compound 1～1.5%, activated carbon 10～20%.
Wherein, described squid bone meal is treated squid bone meal, the concrete technique that processes is: weigh a certain amount of squid cartilage, clear water is cleaned, naturally dry and be placed in plastic packaging bag, it is positioned in ultra cold storage freezer, cryogenic temperature is-65～-80 DEG C, process time 24～36h, squid bone after process takes out at once and carries out tissue pulverizer pulverizing, grinding particle size required 80 mesh sieves, namely coarse powder is obtained, coarse powder is placed in closing crucible, calcine in Muffle furnace, calcining heat 300～500 DEG C, time 1.5～3h, rear taking-up is placed in slow cooling in 60 DEG C of baking ovens, finally it is placed in drying basin standby；Wherein, described organic acid substance is the mixture of malic acid and citric acid；Wherein, described ester type compound is the mixture of one or more of Ethyl formate, ethyl acetate and ethyl propionate.
During preparation, organic Halogenated-hydrocarbons is dissolved in the water, prepare into solution A, again the squid bone meal after process and activated carbon are mixed according to a certain percentage, then with solution A Homogeneous phase mixing, lyophilization, pressed powder is obtained in the xanthan gum solution that concentration is 0.4～1.2% Homogeneous phase mixing again, lyophilization again, namely obtains squid bone Medicated cigarette cleanser.
Embodiment 1:
1) by 0.5g malic acid, 0.5g citric acid and 0.75g Ethyl formate, 0.5g acetic acid ethyl dissolution in 100mL water, solution A is obtained；
2) take squid bone meal, 17g activated carbon that 80g processed, and after solution A Homogeneous phase mixing, carry out lyophilization, obtain pressed powder B；
3) the lyophilized solid powder B obtained is carried out lyophilization after the xanthan gum solution Homogeneous phase mixing that concentration is 0.4%, obtain the squid bone Medicated cigarette cleanser of the present invention.
Implementation result: take commercially available 7.5 yuan of Hongta flue-cured tobaccos 2 parts, a flue-cured tobacco filter plug adds cleanser of the present invention, content is 1.0mg/mm, portion is added without cleanser of the present invention, after 2 parts of flue-cured tobaccos are lighted, collect flue gas, with reference to GB/T18204.26-2000 " public place method for determining formaldehyde in air ", adopt aldehyde matter content in colorimetric method for determining main flume, measurement result is shown in Fig. 1, reduction rate=(107.18-79.31)/107.18=26%, as shown in Figure 1, after adding squid bone Medicated cigarette cleanser of the present invention, formaldehyde, harmful aldehyde matter content such as acetaldehyde and crotonic aldehyde reduces 26%, the cleanser that embodiment 1 prepares has the effect significantly reducing harmful substance.
Embodiment 2:
1) 0.75g malic acid, 0.75g citric acid and 0.5g Ethyl formate, 0.5g ethyl acetate, 0.5g ethyl propionate are dissolved in 100mL water, obtain solution A；
2) take squid bone meal, 6g activated carbon that 90g processed, and after solution A Homogeneous phase mixing, carry out lyophilization, obtain pressed powder B；
3) by the lyophilized solid powder obtained and concentration be 0.8% xanthan gum solution Homogeneous phase mixing after carry out lyophilization, obtain fume-clarifying agent.
Implementation result: take commercially available 7.5 yuan of Hongta flue-cured tobaccos 2 parts, a flue-cured tobacco filter plug adds fume-clarifying agent, content is 1.2mg/mm, portion is added without above-mentioned cleanser, after 2 parts of flue-cured tobaccos are lighted, collect flue gas, with reference to GB/T18204.26-2000 " public place method for determining formaldehyde in air ", adopt aldehyde matter content in colorimetric method for determining main flume, measurement result is shown in Fig. 2, reduction rate=(110.28-79.31)/110.28=28%, as shown in Figure 2, after adding fume-clarifying agent, formaldehyde, harmful aldehyde matter content such as acetaldehyde and crotonic aldehyde reduces 39.05%, the fume-clarifying agent that embodiment 2 prepares has the effect significantly reducing harmful substance.
Claims (5)
1. a squid bone Medicated cigarette cleanser, it is characterized in that: with raw materials quality than calculate, its raw material composition include 60～90% squid bone meal, 0.4～1.2% xanthan gum, 1～1.5% organic acid substance, 1～1.5% ester type compound and 10～20% activated carbon.
2. the preparation method of a squid bone Medicated cigarette cleanser, it is characterised in that comprise the following steps:
1) organic Halogenated-hydrocarbons is dissolved in the water, makes mixed solution A；
2) by squid bone meal and activated carbon Homogeneous phase mixing in proportion, then with solution A Homogeneous phase mixing after carry out lyophilization, obtain pressed powder B；
3) xanthan gum is dissolved in the water, is configured to the solution C of 0.4～1.2% mass concentration, during configuration, want continuous uniform stirring；
4) by step 2) in the pressed powder B that obtains mix with xanthan gum solution C after carry out lyophilization again, obtain Medicated cigarette cleanser powder；
The mass percent of the wherein said squid bone each raw material of Medicated cigarette cleanser is: squid bone meal 60～90%, xanthan gum 0.4～1.2%, organic acid substance 1～1.5%, ester type compound 1～1.5% and activated carbon 10～20%, all the other are water.
3. the preparation method of a kind of squid bone Medicated cigarette cleanser according to claim 2, it is characterised in that: the organic acid substance described in step 1) is the mixture of malic acid and citric acid；Described ester type compound is the mixture of one or more of Ethyl formate, ethyl acetate and ethyl propionate.
4. the preparation method of a kind of squid bone Medicated cigarette cleanser according to claim 2, it is characterized in that: step 2) described in squid bone meal be treated squid bone meal, the concrete technique that processes is: weigh a certain amount of squid cartilage, clear water is cleaned, naturally dry and be placed in plastic packaging bag, it is positioned in ultra cold storage freezer, cryogenic temperature is-65～-80 DEG C, process time 24～36h, squid bone after process takes out at once and carries out tissue pulverizer pulverizing, grinding particle size required 80 mesh sieves, namely coarse powder is obtained, coarse powder is placed in closing crucible, calcine in Muffle furnace, calcining heat 300～500 DEG C, time 1.5～3h, rear taking-up is placed in slow cooling in 60 DEG C of baking ovens, finally it is placed in drying basin standby.
5. a kind of squid bone Medicated cigarette cleanser according to claim 1 is employed on filter tip, and described cleanser content is 1.0mg/mm～1.6mg/mm.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610174798.0A CN105768218A (en) | 2016-03-25 | 2016-03-25 | Cigarette purifying agent containing squid bones as well as preparation method and application of cigarette purifying agent |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610174798.0A CN105768218A (en) | 2016-03-25 | 2016-03-25 | Cigarette purifying agent containing squid bones as well as preparation method and application of cigarette purifying agent |
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| CN105768218A true CN105768218A (en) | 2016-07-20 |
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| CN201610174798.0A Pending CN105768218A (en) | 2016-03-25 | 2016-03-25 | Cigarette purifying agent containing squid bones as well as preparation method and application of cigarette purifying agent |
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| CN103801180A (en) * | 2012-11-12 | 2014-05-21 | 镇江新元素医药科技有限公司 | Air purifier |
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| CN104432507A (en) * | 2014-12-15 | 2015-03-25 | 湖南中烟工业有限责任公司 | Cigarette filter tip additive removing aldehydes in cigarette mainstream smoke and preparation method and application thereof |
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2016
- 2016-03-25 CN CN201610174798.0A patent/CN105768218A/en active Pending
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| US20080003270A1 (en) * | 2006-07-03 | 2008-01-03 | Garcia Martinez Ion I | Chewable and/or Edible Product for Pets and Other Animals |
| CN101716360A (en) * | 2009-12-18 | 2010-06-02 | 南通市建筑工程质量检测中心 | Method for production of chitosan/nanometer titanium dioxide complex air-purifying agent |
| CN103801180A (en) * | 2012-11-12 | 2014-05-21 | 镇江新元素医药科技有限公司 | Air purifier |
| CN103271440A (en) * | 2013-05-31 | 2013-09-04 | 广东中烟工业有限责任公司 | Cigarette purifying and harm-reducing reagent and particles and preparation method of cigarette and particles |
| CN104307468A (en) * | 2014-09-15 | 2015-01-28 | 明光市嘉益电控科技有限公司 | Aperture-developed high-strength durable active carbon filter material for air conditioner and preparation method thereof |
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Application publication date: 20160720 |