CN105753453A - Selenium-rich porcelain veneer and selenium-rich porcelain preparation method - Google Patents
Selenium-rich porcelain veneer and selenium-rich porcelain preparation method Download PDFInfo
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- CN105753453A CN105753453A CN201610090407.7A CN201610090407A CN105753453A CN 105753453 A CN105753453 A CN 105753453A CN 201610090407 A CN201610090407 A CN 201610090407A CN 105753453 A CN105753453 A CN 105753453A
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- selenium
- porcelain
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- ceramic paster
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B37/00—Joining burned ceramic articles with other burned ceramic articles or other articles by heating
- C04B37/001—Joining burned ceramic articles with other burned ceramic articles or other articles by heating directly with other burned ceramic articles
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/349—Clays, e.g. bentonites, smectites such as montmorillonite, vermiculites or kaolines, e.g. illite, talc or sepiolite
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/42—Non metallic elements added as constituents or additives, e.g. sulfur, phosphor, selenium or tellurium
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Structural Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
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Abstract
The invention relates to a selenium-rich porcelain veneer and a selenium-rich porcelain preparation method. According to product requirements, a mud sheet is put into a mold; after 3 to 5 hours, the mud sheet is manufactured into a blank; stripping and drying are performed; the dried blank is taken; the blank is modified according to the pattern size; water replenishing is performed on the blank body by dripping water via sponge; pin holes and all bubbles in the surface of the blank body are modified, so that the blank surface is complete, smooth and clean; according to requirements, the enamel is firstly applied at the inner wall of the blank and is then applied at the outer wall of the blank, or enamel spraying and bottom stripping are performed, and drying is performed; the dried blank is taken and loaded into a kiln; the blank is sintered for 12 hours at 1350 DEG C into porcelain; the selenium-rich porcelain veneer with finished product selenium soil patterns is put into the sintered selenium-free porcelain incapable of dissolving out selenium, and is pasted to the bottom or the inner wall for drying; the porcelain with selenium soil patterns is put onto an electrical kiln at high temperature for 8 hours to prepare the finished product; the porcelain finished product can automatically dissolve out selenium elements in the use process; the selenium element can degrade the content of harmful elements such as arsenic, lead and cadmium in water; the effects of cancer prevention and cancer resistance are achieved; the preparation method is an economic substantial and fast-selenium-supplementing method.
Description
Technical field
The present invention relates to a kind of selenium-rich ceramic paster and the preparation method of selenium-rich pottery.
Background technology
Domestic ceramics includes tea set, drinking vessel and tableware etc., and its function is used only to contain tea or water, its function singleness, shows
In generation life, the arsenic in water, lead, the health to human body that exceeds standard of cadmium constitute invisible harm, and existing domestic ceramics cannot be fine
Ground solves this problem.
A few days ago, the preparation of domestic ceramics is mostly pottery slice and puts into base in mould, and disengagement is dried, and sinters porcelain into.
Not containing selenium and dissolution selenium according to the pottery that prior art provides, people mend selenium and are difficult in daily Drinking Water mend selenium, right
In conventional ceramic energy dissolution selenium element automatically to reach also not having of se complementary effect.
Summary of the invention
Its purpose of the present invention is that provides a kind of selenium-rich ceramic paster and the preparation method of selenium-rich pottery, solves existing
Ceramic in without selenium and the problem of dissolution selenium, ceramic product in use can dissolution selenium element automatically, plain selenium is permissible
The content of the harmful elements such as arsenic in degradation water, lead, cadmium, has effect of cancer-resisting, is a kind of economical and practical quick benefit selenium
Method.
The technical scheme realizing above-mentioned purpose and take includes,
The preparation method of a kind of selenium-rich ceramic paster, the ingredients by weight percentage of described selenium-rich ceramic paster is: kaolin 10-
20%, selenium 50-60%, glaze water 10-20%；The preparation method of selenium-rich ceramic paster includes step:
1) selenium that purity is 99.9999% is added stirring by 50-60% percentage by weight with kaolin 10-20% percentage by weight
Machine was through the stirring of 72 hours, and selenium and kaolin are completely combined and are prepared as selenium soil；
2) the selenium soil being stirred pours vacuum deairing machine into, is prepared as pottery selenium mud so that selenium is completely combined further with kaolin
Reach the effect of pottery mud；
3) pottery selenium mud being added the glaze water beater of 10-20% percentage by weight, to break into selenium slurry stand-by；
4) touch according to pattern pattern, be that selenium soil pattern printed by raw material with selenium slurry, be prepared as selenium-rich ceramic paster.
A kind of method using selenium-rich ceramic paster to prepare selenium-rich pottery, including step:
1) being put in mould after 3-5 hour makes base by slice by product requirement, disengagement is dried；
2) take and dry base, according to pattern magnitude repaired biscuit and dip in water with sponge and carry out moisturizing on base substrate, study for a second time courses one has flunked the pin on idiosome surface
Hole and each bubble so that the surface of embryo is the brightest and the cleanest；
3) the most first execute base inwall and execute the outer glaze of wall again or glaze spraying takes off the end, dry；
4) take the dry blank kiln loading that dries in the air, sinter porcelain into through 1350 DEG C of high temperature 12 hours；
5) the selenium-rich ceramic paster of the finished product selenium soil pattern containing selenium element is placed in burned porcelain, is attached to the end of porcelain
Portion or inwall, dry；
6) high temperature that the porcelain added with selenium-rich ceramic paster was put in electrical kiln through 8 hours prepares finished product, wherein, and 100-200
When spending, 1 hour used time was incubated 20 minutes；Stop when 450 degree heating and being incubated 10 minutes；Stop when 600 degree heating and being incubated 35 points
Clock；Burned unlimited wicket cooling when 680 degree, temperature closes wicket when declining 300 degree.
Beneficial effect
Compared with prior art the present invention has the following advantages.
During use can dissolution selenium element automatically, selenium is a kind of life trace element, can be with the arsenic in degradation water, lead, cadmium
Deng harmful element, having effect of cancer-resisting, preparation method is simple, is a kind of method of economical and practical quick benefit selenium.
Detailed description of the invention
The preparation method of a kind of selenium-rich ceramic paster, the ingredients by weight percentage of described selenium-rich ceramic paster is: kaolin
10-20%, selenium 50-60%, glaze water 10-20%；The preparation method of selenium-rich ceramic paster includes step:
1) selenium that purity is 99.9999% is added stirring by 50-60% percentage by weight with kaolin 10-20% percentage by weight
Machine was through the stirring of 72 hours, and selenium and kaolin are completely combined and are prepared as selenium soil；
2) the selenium soil being stirred pours vacuum deairing machine into, is prepared as pottery selenium mud so that selenium is completely combined further with kaolin
Reach the effect of pottery mud；
3) pottery selenium mud being added the glaze water beater of 10-20% percentage by weight, to break into selenium slurry stand-by；
4) touch according to pattern pattern, be that selenium soil pattern printed by raw material with selenium slurry, be prepared as selenium-rich ceramic paster.
A kind of method using selenium-rich ceramic paster to prepare selenium-rich pottery, including step:
1) being put in mould after 3-5 hour makes base by slice by product requirement, disengagement is dried；
2) take and dry base, according to pattern magnitude repaired biscuit and dip in water with sponge and carry out moisturizing on base substrate, study for a second time courses one has flunked the pin on idiosome surface
Hole and each bubble so that the surface of embryo is the brightest and the cleanest；
3) the most first execute base inwall and execute the outer glaze of wall again or glaze spraying takes off the end, dry；
4) take the dry blank kiln loading that dries in the air, sinter porcelain into through 1350 DEG C of high temperature 12 hours；
5) the selenium-rich ceramic paster of the finished product selenium soil pattern containing selenium element is placed in burned porcelain, is attached to the end of porcelain
Portion or inwall, dry；
6) high temperature that the porcelain added with selenium-rich ceramic paster was put in electrical kiln through 8 hours prepares finished product, wherein, and 100-200
When spending, 1 hour used time was incubated 20 minutes；Stop when 450 degree heating and being incubated 10 minutes；Stop when 600 degree heating and being incubated 35 points
Clock；Burned unlimited wicket cooling when 680 degree, temperature closes wicket when declining 300 degree.
Embodiment 1
A kind of method using selenium-rich ceramic paster to prepare selenium-rich pottery, this preparation method and step are as follows:
Step one: being put into by the slice bought by product requirement after making base after 3-5 hour in mould, disengagement is dried；
Step 2: take and dry base, according to pattern magnitude repaired biscuit and dip in water with sponge and carry out moisturizing on base substrate, studies for a second time courses one has flunked idiosome surface
Pin hole and each bubble so that the surface of embryo is the brightest and the cleanest；
Step 3: the most first execute base inwall and execute the outer glaze of wall again or glaze spraying takes off the end, dry；
Step 4: take the dry blank kiln loading that dries in the air, sinters porcelain into through 1350 DEG C of high temperature 12 hours；
Step 5: the selenium-rich ceramic paster of the finished product selenium soil pattern containing selenium element is placed in burned porcelain, is attached to the end
Portion or inwall, dry；
Step 6: the high temperature that the porcelain added with selenium-rich ceramic paster was put in electrical kiln through 8 hours prepares finished product, owing to selenium exists
Can run off under high temperature, so kiln temperature have to be controlled.Wherein, when 100-200 spends, 1 hour used time was incubated 20 minutes；450 degree
Time temperature control to be stopped 10 minutes；Temperature control to be stopped 35 minutes when 600 degree；The burned wicket that can open wide when 680 degree, temperature declines
Wicket can be closed when 300 degree.
In the present embodiment, the preparation method of selenium-rich ceramic paster, the proportion scale of selenium-rich ceramic paster is: kaolin 10%
Percentage by weight, selenium 50% percentage by weight, glaze water 10% percentage by weight.
The preparation method of selenium-rich ceramic paster:
1) selenium 50% percentage by weight and kaolin 10% percentage by weight that purity is 99.9999% are added mixer through 72
Hour high-speed stirred, selenium and kaolin are completely combined；
2) the selenium soil being stirred pours vacuum deairing machine into so that selenium and kaolin are completely combined the effect reaching pottery mud further
Really；
3) pottery selenium mud being added the glaze water beater of 10% percentage by weight, to break into selenium slurry stand-by；
4) touch according to pattern pattern, be that selenium soil pattern printed by raw material with selenium slurry.
Embodiment 2
A kind of method using selenium-rich ceramic paster to prepare selenium-rich pottery, this preparation method and step are with embodiment 1.
In the present embodiment, the preparation method of selenium-rich ceramic paster, the proportion scale of selenium-rich ceramic paster is: kaolin 15%
Percentage by weight, selenium 60% percentage by weight, glaze water 15% percentage by weight.
The preparation method of selenium-rich ceramic paster:
1) selenium 60% percentage by weight and kaolin 15% percentage by weight that purity is 99.9999% are added mixer through 72
Hour high-speed stirred, selenium and kaolin are completely combined；
2) the selenium soil being stirred pours vacuum deairing machine into so that selenium and kaolin are completely combined the effect reaching pottery mud further
Really；
3) pottery selenium mud being added the glaze water beater of 15% percentage by weight, to break into selenium slurry stand-by；
4) touch according to pattern pattern, be that selenium soil pattern printed by raw material with selenium slurry.
Embodiment 3
A kind of method using selenium-rich ceramic paster to prepare selenium-rich pottery, this preparation method and step are with embodiment one.
In the present embodiment, the preparation method of selenium-rich ceramic paster, the proportion scale of selenium-rich ceramic paster is: kaolin 20%
Percentage by weight, selenium 60% percentage by weight, glaze water 20% percentage by weight.
The preparation method of selenium-rich ceramic paster:
1) selenium 60% percentage by weight and kaolin 20% percentage by weight that purity is 99.9999% are added mixer through 72
Hour high-speed stirred, selenium and kaolin are completely combined；
2) the selenium soil being stirred pours vacuum deairing machine into so that selenium and kaolin are completely combined the effect reaching pottery mud further
Really；
3) pottery selenium mud being added the glaze water beater of 20% percentage by weight, to break into selenium slurry stand-by；
Touch according to pattern pattern, be that selenium soil pattern printed by raw material with selenium slurry.
Claims (2)
1. the preparation method of a selenium-rich ceramic paster, it is characterised in that the ingredients by weight percentage of described selenium-rich ceramic paster
For: kaolin 10-20%, selenium 50-60%, glaze water 10-20%；The preparation method of selenium-rich ceramic paster includes step:
The selenium that purity is 99.9999% is added mixer by 50-60% percentage by weight with kaolin 10-20% percentage by weight
It is completely combined through the stirring of 72 hours, selenium and kaolin and is prepared as selenium soil；
The selenium soil being stirred pours vacuum deairing machine into, is prepared as pottery selenium mud so that selenium is completely combined further with kaolin and reaches
Effect to pottery mud；
It is stand-by that the glaze water beater that ceramic selenium mud is added 10-20% percentage by weight breaks into selenium slurry；
Touch according to pattern pattern, be that selenium soil pattern printed by raw material with selenium slurry, be prepared as selenium-rich ceramic paster.
A kind of method using selenium-rich ceramic paster to prepare selenium-rich pottery the most according to claim 1, it is characterised in that bag
Include step:
1) being put in mould after 3-5 hour makes base by slice by product requirement, disengagement is dried；
2) take and dry base, according to pattern magnitude repaired biscuit and dip in water with sponge and carry out moisturizing on base substrate, study for a second time courses one has flunked the pin on idiosome surface
Hole and each bubble so that the surface of embryo is the brightest and the cleanest；
3) the most first execute base inwall and execute the outer glaze of wall again or glaze spraying takes off the end, dry；
4) take the dry blank kiln loading that dries in the air, sinter porcelain into through 1350 DEG C of high temperature 12 hours；
5) the selenium-rich ceramic paster of the finished product selenium soil pattern containing selenium element is placed in burned porcelain, is attached to the end of porcelain
Portion or inwall, dry；
6) high temperature that the porcelain added with selenium-rich ceramic paster was put in electrical kiln through 8 hours prepares finished product, wherein, and 100-200
When spending, 1 hour used time was incubated 20 minutes；Stop when 450 degree heating and being incubated 10 minutes；Stop when 600 degree heating and being incubated 35 points
Clock；Burned unlimited wicket cooling when 680 degree, temperature closes wicket when declining 300 degree.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610090407.7A CN105753453A (en) | 2016-02-18 | 2016-02-18 | Selenium-rich porcelain veneer and selenium-rich porcelain preparation method |
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| CN201610090407.7A CN105753453A (en) | 2016-02-18 | 2016-02-18 | Selenium-rich porcelain veneer and selenium-rich porcelain preparation method |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106630624A (en) * | 2017-01-11 | 2017-05-10 | 余安平 | Preparation method of selenium-earth pattern and preparation method of selenium-enriched container |
| CN110683829A (en) * | 2019-11-20 | 2020-01-14 | 西北大学 | Preparation method of natural selenium-rich pottery |
| CN113105267A (en) * | 2021-04-13 | 2021-07-13 | 景德镇陶瓷大学 | Ceramic stained paper additive, ceramic stained paper, selenium-rich ceramic and preparation method |
| CN116396057A (en) * | 2023-03-23 | 2023-07-07 | 四川美术学院 | Selenium-rich ceramic and preparation method thereof |
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| CN2392463Y (en) * | 1999-10-24 | 2000-08-23 | 江苏三乐特种炊具厂 | Selenium-rich composite ceramic cooker |
| CN1416762A (en) * | 2002-12-08 | 2003-05-14 | 崔江大 | Selenium-rich china tableware and its production process |
| CN201365765Y (en) * | 2009-02-04 | 2009-12-23 | 斯达高瓷艺发展（深圳）有限公司 | Ceramic dining container with functions of health care and disease prevention |
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2016
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|---|---|---|---|---|
| CN2392463Y (en) * | 1999-10-24 | 2000-08-23 | 江苏三乐特种炊具厂 | Selenium-rich composite ceramic cooker |
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| CN201365765Y (en) * | 2009-02-04 | 2009-12-23 | 斯达高瓷艺发展（深圳）有限公司 | Ceramic dining container with functions of health care and disease prevention |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106630624A (en) * | 2017-01-11 | 2017-05-10 | 余安平 | Preparation method of selenium-earth pattern and preparation method of selenium-enriched container |
| CN106630624B (en) * | 2017-01-11 | 2019-08-20 | 余安平 | A kind of preparation method of selenium soil pattern and the preparation method of selenium-rich container |
| CN110683829A (en) * | 2019-11-20 | 2020-01-14 | 西北大学 | Preparation method of natural selenium-rich pottery |
| CN113105267A (en) * | 2021-04-13 | 2021-07-13 | 景德镇陶瓷大学 | Ceramic stained paper additive, ceramic stained paper, selenium-rich ceramic and preparation method |
| CN116396057A (en) * | 2023-03-23 | 2023-07-07 | 四川美术学院 | Selenium-rich ceramic and preparation method thereof |
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Application publication date: 20160713 |
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