CN105746511A - Attractant for ips typographus - Google Patents
Attractant for ips typographus Download PDFInfo
- Publication number
- CN105746511A CN105746511A CN201610183543.0A CN201610183543A CN105746511A CN 105746511 A CN105746511 A CN 105746511A CN 201610183543 A CN201610183543 A CN 201610183543A CN 105746511 A CN105746511 A CN 105746511A
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- CN
- China
- Prior art keywords
- attractant
- parts
- ips typographus
- cis
- verbenol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N31/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic oxygen or sulfur compounds
- A01N31/08—Oxygen or sulfur directly attached to an aromatic ring system
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N27/00—Biocides, pest repellants or attractants, or plant growth regulators containing hydrocarbons
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N31/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic oxygen or sulfur compounds
- A01N31/02—Acyclic compounds
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N31/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic oxygen or sulfur compounds
- A01N31/06—Oxygen or sulfur directly attached to a cycloaliphatic ring system
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- Life Sciences & Earth Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
An attractant for ips typographus is prepared from components in parts by weight as follows: 1.5-120 parts of cis-verbenol, 1.5-120 parts of 2-methyl-3-butene-2-ol, 1.5-120 parts of alpha-pinene(+25/-75), 0.001-0.02 parts of butylated hydroxytoluene and 0.001-0.02 parts of 2-hydroxy-4-methoxybenzophenone. A formula of the attractant capable of effectively improving the attraction effect on ips typographus is provided and used for improving the monitoring accuracy and the comprehensive control effect on ips typographus. The attractant has the advantages of low cost and high efficiency and is especially suitable for being used in large forest areas with complicated terrain.
Description
Technical field
The invention belongs to the technical field utilizing semiochemicals to carry out insect green prevention and control, be specifically related to a kind of application message
The attractant that ips typographus is monitored and prevents and treats by element.
Background technology
Ips typographus Ips typographus belongs to coleoptera bark beetle section tooth bark beetle and belongs to, and is distributed widely in global
52 countries and regions, extremely serious (http://www.eppo.org/) in the harm of the countries and regions of 12 low latitudes.
In China, it is distributed mainly on the ground such as Heilungkiang, Jilin, Sichuan, Qinghai and Xinjiang.Ips typographus main harm sky
So spruce forest (be generally into, overmature forest), condition is suitable or rampant occur in the case of can direct health risk standing tree,
And cause the large area of forest withered together with other bark beetles, cause huge loss to production of forestry and improvement of the ecological environment.
Ips typographus, because of the feature in the subcutaneous harm of host tree, brings the biggest difficulty to preventing and controlling.Use traditional
Chemical prevention and control method such as medicament smoked kill, the trunk spray method such as medicine, although achieve certain effect, but its cost accounting mistake
The side effects such as height, weak effect, killing natural enemy and pollution environment display the most simultaneously.And the monitoring of application message element and preventing and treating woods
Wood insect, will not be to Forest ecosystem because affecting less on the species diversity in forest ecosystem and ecosystem stability
Matter and energy flowing in system produces great change, complies fully with the target of the sustainable control of injurious forest-insect, so becoming
The advanced means of current injurious insect control.At present, the pheromones about ips typographus has produced (entitledWith), main component be all cis-verbenol (cV) and
2-methyl-3-buten-2-ol(MB).And host and Non-host volatiles have mixed synergistic effect with above-mentioned 2 kinds of compositions,
Appear in the newspapers, such as: (-)-Ipsdienol (Id) low concentration when, be used in mixed way with above two composition and just can rise
Synergistic effect.Inventor is in the patent (patent No.: ZL2008 1 0051469.2 and ZL 2,009 1 0101313.5) authorized
Have also discovered 2 kinds rise synergistic effects materials: cis-3-hexenyl-1-alcohol and trans-2-hexenyl-1-alcohol.Although these 2 kinds
The attractant effect of ips typographus attractant is well beyond other attractants, but it is not fully achieved applicant
Intended effect.
Summary of the invention
The problem existed for prior art, it is an object of the invention to: provide one can be effectively improved ips typographus
The attractant formula of gathering effect, to improve the monitoring accuracy to ips typographus and integrated control effect.This attractant
There is low cost, advantage that efficiency is high, be particularly suitable for the forest zone that occurring area is big, landform, physical features are complicated and use.
A kind of ips typographus attractant, including following components in parts by weight:
Cis-verbenol 1.5-120 part
2-M3BOL 1.5-120 part
Australene (+25/-75) 1.5-120 part
BHT 0.001-0.02 part
ESCALOL 567 0.001-0.02 part.
Described a kind of ips typographus attractant, including following components in parts by weight:
Cis-verbenol 15-120 part
2-M3BOL 15-120 part
Australene (+25/-75) 15-120 part
BHT 0.001-0.02 part
ESCALOL 567 0.001-0.02 part.
Described a kind of ips typographus attractant, including following components in parts by weight:
Cis-verbenol 1.5-60 part
2-M3BOL 1.5-60 part
Australene (+25/-75) 1.5-60 part
BHT 0.005-0.01 part
ESCALOL 567 0.005-0.01 part.
Described a kind of ips typographus attractant, including following components in parts by weight:
Cis-verbenol 60-120 part
2-M3BOL 60-120 part
Australene (+25/-75) 60-120 part
BHT 0.01-0.02 part
ESCALOL 567 0.01-0.02 part.
Described a kind of ips typographus attractant, including following components in parts by weight:
Cis-verbenol 1.5-12 part
2-M3BOL 1.5-12 part
Australene (+25/-75) 1.5-12 part
BHT 0.002-0.012 part
ESCALOL 567 0.002-0.012 part.
The preparation technology of described a kind of ips typographus attractant lure specifically comprises the following steps that
1) preparation of bottle it is sustained: polyethylene is sustained bottle (purchased from Pherobio Technology Co., Ltd.) at ethanol
After middle immersion 5-10 days, with distilled water flushing lure carrier, till without ethanol taste, after drying, pack seals standby;
2) preparation of attractant: in formula, the number of active ingredient accurately weighs respectively in units of milligram, then at homogeneous
On instrument, low speed concussion mixing, standby;
3) by step 2) prepare attractant drop to step 1) prepare lure carrier in, then in lure carrier drip
The dichloromethane 50-300 each lure of μ L/, i.e. prepares ips typographus attractant lure.
2-M3BOL of the present invention and cis-verbenol are the main component of attractant;Described α-
Firpene (+25/-75) is the synergistic component of attractant;Described BHT and 2-hydroxyl-4-methoxyl group two
Benzophenone is respectively antioxidant and ultraviolet light adsorbent, is the auxiliary element of attractant;Described dichloromethane is dispersant,
Help each component of attractant dispersed.
Above-mentioned ips typographus attractant, compatibility is reasonable, and the present invention is to be not added with α to the gathering effect of ips typographus
2.37 times of-firpene (+25/-75) attractant, with add ipsdienol (-)-Ipsdienol, cis-3-hexenyl-1-
All there were significant differences for alcohol cis-3-hexen-1-ol or trans-2-hexenyl-1-alcohol E-2-hexen-1-ol.The present invention is aobvious
Write while improving gathering effect, reduce again production cost.The attractant lasting period of the present invention is up to 30-50 days, available
In monitoring ips typographus population occurrence dynamics, trap and kill and carry out the many aspects such as large area control, can be by little for dragon spruce octadentate
The loss that forest is caused by moth-eaten harm is minimized, and has obvious economy, society and ecological benefits.Due to more warp of filling a prescription
Ji effectively, is particularly suitable for carrying out woodland popularization and application, has wide industrialization prospect.
Detailed description of the invention
The present invention is further illustrated below in conjunction with embodiment.
Embodiment 1: the preparation (weight portion) of ips typographus attractant
Weigh cis-verbenol 1.5 parts, 2-M3BOL 1.5 parts, australene (+25/-75) 1.5 parts,
BHT 0.001 part, ESCALOL 567 0.001 part, oscillator mixes,
I.e. prepare ips typographus imago attractant.
Embodiment 2: the preparation (weight portion) of ips typographus attractant
Weigh cis-verbenol 5 parts, 2-M3BOL 5 parts, australene (+25/-75) 5 parts, 2,
6-BHT 0.02 part and ESCALOL 567 0.02 part, oscillator mixes, i.e.
Prepare ips typographus imago attractant.
Embodiment 3: the preparation (weight portion) of ips typographus attractant
Weigh cis-verbenol 10 parts, 2-M3BOL 10 parts, australene (+25/-75) 10 parts, 2,
6-BHT 0.01 part and ESCALOL 567 0.01 part, oscillator mixes, i.e.
Prepare ips typographus imago attractant.
Embodiment 4: the preparation (weight portion) of ips typographus attractant
Weigh cis-verbenol 20 parts, 2-M3BOL 20 parts, australene (+25/-75) 10 parts, 2,
6-BHT 0.015 part and ESCALOL 567 0.015 part, oscillator mixes,
I.e. prepare ips typographus imago attractant.
Embodiment 5: the preparation (weight portion) of ips typographus attractant
Weigh cis-verbenol 30 parts, 2-M3BOL 30 parts, australene (+25/-75) 90 parts, 2,
6-BHT 0.005 part, ESCALOL 567 0.005 part, oscillator mixes,
I.e. prepare ips typographus imago attractant.
Embodiment 6: the preparation (weight portion) of ips typographus attractant
Weigh cis-verbenol 60 parts, 2-M3BOL 60 parts, australene (+25/-75) 60 parts, 2,
6-BHT 0.02 part and ESCALOL 567 0.02 part, oscillator mixes, i.e.
Prepare ips typographus imago attractant.
Embodiment 7: the preparation (weight portion) of ips typographus attractant
Weigh cis-verbenol 60 parts, 2-M3BOL 60 parts, australene (+25/-75) 120 parts,
BHT 0.02 part and ESCALOL 567 0.02 part, oscillator mixes,
I.e. prepare ips typographus imago attractant.
Embodiment 8: the preparation (weight portion) of ips typographus attractant
Weigh cis-verbenol 120 parts, 2-M3BOL 120 parts, australene (+25/-75) 100 parts,
BHT 0.001 part and ESCALOL 567 0.001 part, oscillator mixes,
I.e. prepare ips typographus imago attractant.
Test example 1: the ips typographus attractant using embodiment 1 to prepare, accurately measure attractant 10 μ l be added drop-wise to through
Cross in the sleeve formula silicon rubber carrier processed, and drip dichloromethane 2 μ L/ lure.Field intercepts the band of 5 80cm length and invades
The juggle in hole, indoor are positioned over the acrylic case kind of 100cm × 100cm × 100cm, take out at once, with tree after adult eclosion
Skin is single in culture dish only to be fed 15 days, treats sexal maturity laggard row behaviour bioassay, hungry 3h before test.Test result shows,
The new existing patent formulation (ZL2008 1 0051469.2 and ZL 2,009 1 0101313.5) of formula contrast has and significantly draws
Lure effect.The results detailed in Table 1-2.
The attractant effect that table 1 is newly filled a prescription with existing patent formulation (ZL2008 1 0051469.2) compares (Y-shaped smell sensing apparatus)
χ2-test:*P<0.05;**P<0.005;n.s.,P>0.05.
The attractant effect that table 2 is newly filled a prescription with existing patent formulation (ZL 2,009 1 0101313.5) compares (Y-shaped smell sensing apparatus)
χ2-test:*P<0.05;**P<0.005;n.s.,P>0.05.
Test example 2: the ips typographus male imago attractant using embodiment 3 to prepare, accurately measures attractant 10 μ l and drips
It is added in treated sleeve formula silicon rubber carrier, and drips dichloromethane 2 μ L/ lure.Field intercepts 5 80cm length
Band invades the juggle in hole, and indoor are positioned over the acrylic case kind of 100cm × 100cm × 100cm, take out at once after adult eclosion,
Only feed 15 days with bark is single in culture dish, treat sexal maturity laggard row behaviour bioassay, hungry 3h before test.Test result
Showing, new formula is compared existing patent formulation and is had significant attracting action.The results detailed in Table 3-4.
The attractant effect that table 3 is newly filled a prescription with existing patent formulation (ZL2008 1 0051469.2) compares (Y-shaped smell sensing apparatus)
χ2-test:*P<0.05;**P<0.005;n.s.,P>0.05.
The attractant effect that table 4 is newly filled a prescription with existing patent formulation (ZL 2,009 1 0101313.5) compares (Y-shaped smell sensing apparatus)
χ2-test:*P<0.05;**P<0.005;n.s.,P>0.05.
Test example 3: the ips typographus male imago attractant using embodiment 5 to prepare, accurately measures attractant 10 μ l and drips
It is added in treated sleeve formula silicon rubber carrier, and drips dichloromethane 2 μ L/ lure.Field intercepts 5 80cm length
Band invades the juggle in hole, and indoor are positioned over the acrylic case kind of 100cm × 100cm × 100cm, take out at once after adult eclosion,
Only feed 15 days with bark is single in culture dish, treat sexal maturity laggard row behaviour bioassay, hungry 3h before test.Test result
Showing, newly filling a prescription has significant attracting action compared with commercialization lure.The results detailed in Table 5.
Table 5 attractant effect with commercialization lure of newly filling a prescription compares (Y-shaped smell sensing apparatus)
χ2-test:*P<0.05;**P<0.005;n.s.,P>0.05.
Test example 4: the ips typographus male imago attractant using embodiment 6 to prepare, accurately measures attractant 10 μ l and drips
It is added in treated sleeve formula silicon rubber carrier, and drips dichloromethane 2 μ L/ lure.Field intercepts 5 80cm length
Band invades the juggle in hole, and indoor are positioned over the acrylic case kind of 100cm × 100cm × 100cm, take out at once after adult eclosion,
Only feed 15 days with bark is single in culture dish, treat sexal maturity laggard row behaviour bioassay, hungry 3h before test.Test result
Showing, new formula is compared commercialization lure and is had significant attracting action.The results detailed in Table 3-4.
Table 6 attractant effect with commercialization lure of newly filling a prescription compares (Y-shaped smell sensing apparatus)
χ2-test:*P<0.05;**P<0.005;n.s.,P>0.05.
Test example 5: use the ips typographus attractant that embodiment 8 prepares, attractant is at field and funnel type trapper
It is used in combination, collection cups is contained below trapper 4/5 glass of liquid soap.Group distance 100m when trapper hangs, group inner distance
50m, each process and repetition random distribution are wherein.Trapper hangs up height for about 2m between Liang Shu, the trapper bottom away from
Ground is maintained at more than 10m at about 50cm, trapper with the spacing of host tree, to prevent the bark beetle danger luring collection to arrive
Trees near evil trapper.Before adult eclosion (Jilin Province is typically in mid or late April) hang up complete, weekly investigation lure
Catching the ips typographus adult quantity in device collection cups, emptying collection cups, in order to avoid affecting gathering effect simultaneously.Data Collection
Raise to second time ips typographus and fly to terminate (Jilin Province is that 8 the end of month are at the beginning of 9 months).Each process 9 repetition.Data
Analyzing and use one-way analysis of variance method, Deng Kenshi multipole difference is test.
Survey data from table 7 is it can be seen that the collection ability that lures of lure of the present invention is the 2.37 of commercialization lure (MB+cV)
Times, also there were significant differences compared with the attractant (MB+cV+Id) adding ipsdienol.The α that the present invention is added
-pinene ((+75/-25) gathering effect be significantly higher than add α-pinene other isomers (+50/-50),
(+90/-10)、(+75/-25)。
The gathering effect of forest farm, forestry bureau Jin Gou ridge, table 7:2014 Wangqing each lure combination compares
Lure composition | Lure collection amount ± standard error | The significance of difference |
MB+cV | 838.17±162.99 | bc |
MB+cV+α-pinene(+50/-50) | 537.17±91.66 | c |
MB+cV+α-pinene(+90/-10) | 558.86±98.18 | c |
MB+cV+α-pinene(+25/-75) | 1369.3±139.48 | a |
MB+cV+α-pinene(+75/-25) | 656.67±89.93 | bc |
MB+cV+Id | 869.80±80.98 | b |
Blank | 0.20±0.13 | d |
Note: different letters represent significant difference in 0.05 level.
Claims (5)
1. an ips typographus attractant, it is characterised in that include following components in parts by weight:
Cis-verbenol 1.5-120 part;
2-M3BOL 1.5-120 part;
Australene (+25/-75) 1.5-120 part;
BHT 0.001-0.02 part;
ESCALOL 567 0.001-0.02 part.
2. ips typographus attractant as claimed in claim 1 a kind of, it is characterised in that include following components in parts by weight:
Cis-verbenol 15-120 part;
2-M3BOL 15-120 part;
Australene (+25/-75) 15-120 part;
BHT 0.001-0.02 part;
ESCALOL 567 0.001-0.02 part.
3. ips typographus attractant as claimed in claim 1 a kind of, it is characterised in that include following components in parts by weight:
Cis-verbenol 1.5-60 part;
2-M3BOL 1.5-60 part;
Australene (+25/-75) 1.5-60 part;
BHT 0.005-0.01 part;
ESCALOL 567 0.005-0.01 part.
4. ips typographus attractant as claimed in claim 1 a kind of, it is characterised in that include following components in parts by weight:
Cis-verbenol 60-120 part;
2-M3BOL 60-120 part;
Australene (+25/-75) 60-120 part;
BHT 0.01-0.02 part;
ESCALOL 567 0.01-0.02 part.
5. ips typographus attractant as claimed in claim 1 a kind of, it is characterised in that include following components in parts by weight:
Cis-verbenol 1.5-12 part;
2-M3BOL 1.5-12 part;
Australene (+25/-75) 1.5-12 part;
BHT 0.002-0.012 part;
ESCALOL 567 0.002-0.012 part.
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN113661983A (en) * | 2021-08-20 | 2021-11-19 | 吉林省林业科学研究院 | Attractant for adult Honxiongguoshi |
CN114946846A (en) * | 2022-06-20 | 2022-08-30 | 吉林省林业科学研究院(吉林省林业生物防治中心站) | Method for treating ips typographus by applying push-pull strategy |
CN115176803A (en) * | 2022-08-01 | 2022-10-14 | 青海省森林病虫害防治检疫总站((青海省野生动物疫源疫病监测总站)) | Ips typographus attractant and application thereof, attracting core and preparation method and application thereof |
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Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN113661983A (en) * | 2021-08-20 | 2021-11-19 | 吉林省林业科学研究院 | Attractant for adult Honxiongguoshi |
CN113661983B (en) * | 2021-08-20 | 2022-07-08 | 吉林省林业科学研究院 | Attractant for adult Honxiongguoshi |
CN114946846A (en) * | 2022-06-20 | 2022-08-30 | 吉林省林业科学研究院(吉林省林业生物防治中心站) | Method for treating ips typographus by applying push-pull strategy |
CN115176803A (en) * | 2022-08-01 | 2022-10-14 | 青海省森林病虫害防治检疫总站((青海省野生动物疫源疫病监测总站)) | Ips typographus attractant and application thereof, attracting core and preparation method and application thereof |
CN115176803B (en) * | 2022-08-01 | 2024-02-23 | 青海省森林病虫害防治检疫总站((青海省野生动物疫源疫病监测总站)) | Cornus spruce bark beetle attractant and application thereof, lure core and preparation method and application thereof |
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