CN105733696A - Non-toxic epoxy resin-soybean protein plant fuel oil and preparation method thereof - Google Patents

Non-toxic epoxy resin-soybean protein plant fuel oil and preparation method thereof Download PDF

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Publication number
CN105733696A
CN105733696A CN201610111579.8A CN201610111579A CN105733696A CN 105733696 A CN105733696 A CN 105733696A CN 201610111579 A CN201610111579 A CN 201610111579A CN 105733696 A CN105733696 A CN 105733696A
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China
Prior art keywords
parts
radix
soybean protein
fuel oil
oil
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CN201610111579.8A
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Chinese (zh)
Inventor
黄帮义
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Anhui Haydite Oil Chemical Co Ltd
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Anhui Haydite Oil Chemical Co Ltd
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Priority to CN201610111579.8A priority Critical patent/CN105733696A/en
Publication of CN105733696A publication Critical patent/CN105733696A/en
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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/02—Liquid carbonaceous fuels essentially based on components consisting of carbon, hydrogen, and oxygen only
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/10—Liquid carbonaceous fuels containing additives
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/10—Liquid carbonaceous fuels containing additives
    • C10L1/12—Inorganic compounds
    • C10L1/1233—Inorganic compounds oxygen containing compounds, e.g. oxides, hydroxides, acids and salts thereof
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/10—Liquid carbonaceous fuels containing additives
    • C10L1/14—Organic compounds
    • C10L1/18—Organic compounds containing oxygen
    • C10L1/185—Ethers; Acetals; Ketals; Aldehydes; Ketones
    • C10L1/1852—Ethers; Acetals; Ketals; Orthoesters
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/10—Liquid carbonaceous fuels containing additives
    • C10L1/14—Organic compounds
    • C10L1/24—Organic compounds containing sulfur, selenium and/or tellurium
    • C10L1/2443—Organic compounds containing sulfur, selenium and/or tellurium heterocyclic compounds
    • C10L1/245—Organic compounds containing sulfur, selenium and/or tellurium heterocyclic compounds only sulfur as hetero atom
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/10—Liquid carbonaceous fuels containing additives
    • C10L1/14—Organic compounds
    • C10L1/30—Organic compounds compounds not mentioned before (complexes)
    • C10L1/305—Organic compounds compounds not mentioned before (complexes) organo-metallic compounds (containing a metal to carbon bond)
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L2200/00—Components of fuel compositions
    • C10L2200/04—Organic compounds
    • C10L2200/0461—Fractions defined by their origin
    • C10L2200/0469—Renewables or materials of biological origin
    • C10L2200/0484—Vegetable or animal oils

Abstract

The invention relates to non-toxic epoxy resin-soybean protein plant fuel oil and a preparation method thereof. The fuel oil is prepared from 36-44 parts of corn oil, 4-6 parts of potassium permanganate, 9-11 parts of methanol, 9-11 parts of glycol, 4-6 parts of pentaerythritol, 9-11 parts of sulfolane, 19-21 parts of zinc naphthenate,5-15 parts of modified additives, and 6-10 parts of lower ether, and further comprises 100-120 parts of soybean protein, 10-15 parts of herba lysimachiae, 10-15 parts of spora lygodii, 10-15 parts of chicken's gizzard membrane, 10-12 parts of Chinese thorowax roots, 8-10 parts of immature bitter orange, 10-12 parts of pinellia tubers, 10-12 parts of rheum officinale, 10-12 parts of radix paeoniae alba, 5-8 parts of liquorice, 4-5 parts of scented tea, 1-2 parts of carbon tetrachloride, 2-5 parts of pentachlorophenol, 10-20 parts of floral water, 0.5-1 part of fructus forsythiae, 1-2 parts of indigowoad roots and 1-2 parts of indigowoad leaves. The fuel oil prepared in the invention has the advantages that the preparation process is simple and convenient, the quality of the fuel oil is high, the energy conservation is good, and no impurities exist after combustion; meanwhile, the combustion process is free of black smoke and pollution, not pungent, and environment-friendly; besides, during application, compared with common plant oil, the combustion time of the fuel oil is 20% longer, the adhesive force is strong, and the use effect is remarkable.

Description

A kind of non-toxic epoxy-soybean protein plant fuel oil and preparation method thereof
Technical field:
The present invention relates to industrial chemicals preparing technical field, be specifically related to a kind of non-toxic epoxy-Semen sojae atricolor egg White matter plant fuel oil and preparation method thereof.
Background technology:
Plant fuel its indices of oil is all close with diesel oil, even taller than diesel combustion value.Plant Fuel oil is made up of three parts: one is the vegetable oil of about 50%；Two is the ethanol of about 10%；Three is 40% The adjuvant of left and right.According to a certain percentage, develop through strict technique, this product also with diesel oil one Sample can be divided into-30# ,-20# ,-10#, 0#, and product has good sprayability, and it is excellent that calorific value high price is low etc. Point, with the plant fuel oil of technical grade Oleum Glycines preparation, cost price is only 4000 yuan of left and right per ton, produces in the future After product appear on the market, price will be less than 50 100 yuan per ton of diesel-fuel price on market.Vegetable oil is configured to fuel oil Ratio be that 4000 tons of vegetable oil are than adjuvants such as 1 ton of additives；This production engine is used easily to start, power Greatly, oil consumption is identical with oil product, life-time service not carbon deposit and colloid, and mechanical wear is little, and tail gas is harmful to Thing discharge less than national standard, is a kind of for any Diesel engine and the fuel oil of diesel burning systems.
Summary of the invention:
The technical problem to be solved is to overcome the defect of prior art, it is provided that a kind of without poison ring Epoxy resins-soybean protein plant fuel oil and preparation method thereof.
The technical problem to be solved realizes by the following technical solutions.
A kind of non-toxic epoxy-soybean protein plant fuel oil, it is characterised in that: include following weight The raw material composition of part:
Including Semen Maydis oil 36-44 part, potassium permanganate 4-6 part, methanol 9-11 part, ethylene glycol 9-11 part, season Penta tetrol 4-6 part, sulfolane 9-11 part, zinc naphthenate 19-21 part, property-modifying additive 5-15 part, rudimentary Ether 6-10 part；
Also include soybean protein 100-120 part, Herba Lysimachiae 10-15 part, Spora Lygodii 10-15 part, Endothelium Corneum Gigeriae Galli 10-15 part, Radix Bupleuri 10-12 part, Fructus Aurantii Immaturus 8-10 part, Rhizoma Pinelliae 10-12 part, Radix Et Rhizoma Rhei 10-12 part, Radix Paeoniae Alba 10-12 Part, Radix Glycyrrhizae 5-8 part, scented tea 4-5 part, carbon tetrachloride 1-2 part, pentachlorophenol 2-5 part, floral water 10-20 Part, Fructus Forsythiae 0.5-1 part, Radix Isatidis 1-2 part, Folium Isatidis 1-2 part.
Described property-modifying additive is combustion adjuvant, propellant and anticorrosive.
The preparation method of described plant blended fuel, comprises the following steps:
(1), select one with the reactor of agitator, in reactor, then add in formula all points The Semen Maydis oil of amount and property-modifying additive open stirring, until being thoroughly mixed；
(2) potassium permanganate, sulfolane, zinc naphthenate and the rudimentary ether, by raw material, all adds anti- Answer in still, after being stirred and heated to 60-80 DEG C, isothermal reaction 2-4h；
(3), after the reaction of above-mentioned steps b terminates, reactor is cooled to 20-25 DEG C, by the first in raw material Alcohol and ethylene glycol are added thereto, and stand 5-10h after stirring；
(4), after step 3 standing terminates, taking out the supernatant, after being stirred, half obtained becomes Product；
(5), first soybean protein is under agitation added in chrysanthemum water simultaneously；
(6), stir into serum after, add Herba Lysimachiae, Spora Lygodii, Endothelium Corneum Gigeriae Galli, Radix Bupleuri, stir rapidly；
(7), be sequentially added into Fructus Aurantii Immaturus, the Rhizoma Pinelliae, Radix Et Rhizoma Rhei, the Radix Paeoniae Alba, Radix Glycyrrhizae, scented tea, carbon tetrachloride, five Chlorophenol, heated and stirred, heating-up temperature is 190 DEG C, duration 10 minutes；
(8), it is cooled to 70 DEG C, instills floral water, distill 1 hour, take out foreign material, obtain auxiliary material liquid；
(9), take Fructus Forsythiae, Radix Isatidis, Folium Isatidis, wrap up with earth, dry, remove earth, clean, Put into steam box to toast 1 minute, add in alembic, distill 10 minutes, take out Fructus Forsythiae, Radix Isatidis, greatly Folium Isatidis；
(10) auxiliary material liquid of semi-finished product and 1% is mixed with the moisture in 3% alembic, stirring, planted Thing blended fuel.
The invention has the beneficial effects as follows: the fuel oil of preparation in the present invention, it has preparation technology the most square Just, the quality of fuel oil is high, good energy saving property, and free from admixture after combustion does not has black smoke in combustion process simultaneously, It is not pungent, environment friendly and pollution-free, the most in the application, relative to common vegetable oil length burning time 20%, Adhesive force is strong, and using effect is obvious.
Detailed description of the invention:
For the technological means making the present invention realize, creation characteristic, reach purpose and effect and be readily apparent from Solve, below in conjunction with specific embodiment, the present invention is expanded on further.
Specific embodiment 1: a kind of non-toxic epoxy-soybean protein plant fuel oil, including following heavy The raw material composition of amount part:
Including Semen Maydis oil 36 parts, 4 parts of potassium permanganate, methanol 9 parts, ethylene glycol 9 parts, tetramethylolmethane 4 parts, Sulfolane 9 parts, zinc naphthenate 19 parts, property-modifying additive 5 parts, 6 parts of rudimentary ether；
Also include soybean protein 100 parts, Herba Lysimachiae 10 parts, Spora Lygodii 10 parts, Endothelium Corneum Gigeriae Galli 10 parts, Radix Bupleuri 10 parts, Fructus Aurantii Immaturus 8 parts, the Rhizoma Pinelliae 10 parts, Radix Et Rhizoma Rhei 10 parts, the Radix Paeoniae Alba 10 parts, 5 parts of Radix Glycyrrhizae, scented tea 4 parts, tetrachloro Change 1 part of carbon, pentachlorophenol 2 parts, floral water 10 parts, Fructus Forsythiae 0.5 part, Radix Isatidis 1 part, Folium Isatidis 1 part.
Property-modifying additive is combustion adjuvant, propellant and anticorrosive.
Specific embodiment 2: a kind of non-toxic epoxy-soybean protein plant fuel oil, including following heavy The raw material composition of amount part:
Including Semen Maydis oil 44 parts, 6 parts of potassium permanganate, methanol 11 parts, ethylene glycol 11 parts, tetramethylolmethane 6 parts, Sulfolane 11 parts, zinc naphthenate 21 parts, property-modifying additive 15 parts, 10 parts of rudimentary ether；
Also include soybean protein 120 parts, Herba Lysimachiae 15 parts, Spora Lygodii 15 parts, Endothelium Corneum Gigeriae Galli 15 parts, Radix Bupleuri 12 parts, Fructus Aurantii Immaturus 10 parts, the Rhizoma Pinelliae 12 parts, Radix Et Rhizoma Rhei 12 parts, the Radix Paeoniae Alba 12 parts, 8 parts of Radix Glycyrrhizae, scented tea 5 parts, four 2 parts of chlorination carbon, pentachlorophenol 5 parts, floral water 20 parts, Fructus Forsythiae 1 part, Radix Isatidis 2 parts, Folium Isatidis 2 parts.
Property-modifying additive is combustion adjuvant, propellant and anticorrosive.
The preparation method of a kind of non-toxic epoxy-soybean protein plant fuel oil, comprises the following steps:
(1), select one with the reactor of agitator, in reactor, then add in formula all points The Semen Maydis oil of amount and property-modifying additive open stirring, until being thoroughly mixed；
(2) potassium permanganate, sulfolane, zinc naphthenate and the rudimentary ether, by raw material, all adds anti- Answer in still, after being stirred and heated to 60-80 DEG C, isothermal reaction 2-4h；
(3), after the reaction of above-mentioned steps b terminates, reactor is cooled to 20-25 DEG C, by the first in raw material Alcohol and ethylene glycol are added thereto, and stand 5-10h after stirring；
(4), after step 3 standing terminates, the supernatant, after being stirred, the semi-finished product obtained are taken out；
(5), first soybean protein is under agitation added in chrysanthemum water simultaneously；
(6), stir into serum after, add Herba Lysimachiae, Spora Lygodii, Endothelium Corneum Gigeriae Galli, Radix Bupleuri, stir rapidly；
(7), be sequentially added into Fructus Aurantii Immaturus, the Rhizoma Pinelliae, Radix Et Rhizoma Rhei, the Radix Paeoniae Alba, Radix Glycyrrhizae, scented tea, carbon tetrachloride, five Chlorophenol, heated and stirred, heating-up temperature is 190 DEG C, duration 10 minutes；
(8), it is cooled to 70 DEG C, instills floral water, distill 1 hour, take out foreign material, obtain auxiliary material liquid；
(9), take Fructus Forsythiae, Radix Isatidis, Folium Isatidis, wrap up with earth, dry, remove earth, clean, Put into steam box to toast 1 minute, add in alembic, distill 10 minutes, taking-up Fructus Forsythiae, Radix Isatidis, Folium Isatidis；
(10) auxiliary material liquid of semi-finished product and 1% is mixed with the moisture in 3% alembic, stirring, obtain plant Blended fuel.
The ultimate principle of the present invention, principal character and advantages of the present invention have more than been shown and described.One's own profession Skilled person will appreciate that of industry, the present invention is not restricted to the described embodiments, above-described embodiment and explanation The principle that the present invention is simply described described in book, without departing from the spirit and scope of the present invention, The present invention also has various changes and modifications, and these changes and improvements both fall within claimed invention model In enclosing.Claimed scope is defined by appending claims and equivalent thereof.

Claims (3)

1. non-toxic epoxy-soybean protein plant fuel oil, it is characterised in that: include following The raw material composition of weight portion:
Including Semen Maydis oil 36-44 part, potassium permanganate 4-6 part, methanol 9-11 part, ethylene glycol 9-11 part, season Penta tetrol 4-6 part, sulfolane 9-11 part, zinc naphthenate 19-21 part, property-modifying additive 5-15 part, rudimentary Ether 6-10 part；
Also include soybean protein 100-120 part, Herba Lysimachiae 10-15 part, Spora Lygodii 10-15 part, Endothelium Corneum Gigeriae Galli 10-15 part, Radix Bupleuri 10-12 part, Fructus Aurantii Immaturus 8-10 part, Rhizoma Pinelliae 10-12 part, Radix Et Rhizoma Rhei 10-12 part, Radix Paeoniae Alba 10-12 Part, Radix Glycyrrhizae 5-8 part, scented tea 4-5 part, carbon tetrachloride 1-2 part, pentachlorophenol 2-5 part, floral water 10-20 Part, Fructus Forsythiae 0.5-1 part, Radix Isatidis 1-2 part, Folium Isatidis 1-2 part.
Described a kind of non-toxic epoxy-soybean protein plant fuel the most according to claim 1 Oil, it is characterised in that: described property-modifying additive is combustion adjuvant, propellant and anticorrosive.
Described a kind of non-toxic epoxy the most according to claim 1-soybean protein plant combustion Material oil, it is characterised in that: the preparation method of described plant blended fuel, comprise the following steps:
(1), select one with the reactor of agitator, in reactor, then add in formula all points The Semen Maydis oil of amount and property-modifying additive open stirring, until being thoroughly mixed；
(2) potassium permanganate, sulfolane, zinc naphthenate and the rudimentary ether, by raw material, all adds anti- Answer in still, after being stirred and heated to 60-80 DEG C, isothermal reaction 2-4h；
(3), after the reaction of above-mentioned steps b terminates, reactor is cooled to 20-25 DEG C, by the first in raw material Alcohol and ethylene glycol are added thereto, and stand 5-10h after stirring；
(4), after step 3 standing terminates, taking out the supernatant, after being stirred, half obtained becomes Product；
(5), first soybean protein is under agitation added in chrysanthemum water simultaneously；
(6), stir into serum after, add Herba Lysimachiae, Spora Lygodii, Endothelium Corneum Gigeriae Galli, Radix Bupleuri, stir rapidly；
(7), be sequentially added into Fructus Aurantii Immaturus, the Rhizoma Pinelliae, Radix Et Rhizoma Rhei, the Radix Paeoniae Alba, Radix Glycyrrhizae, scented tea, carbon tetrachloride, five Chlorophenol, heated and stirred, heating-up temperature is 190 DEG C, duration 10 minutes；
(8), it is cooled to 70 DEG C, instills floral water, distill 1 hour, take out foreign material, obtain auxiliary material liquid；
(9), take Fructus Forsythiae, Radix Isatidis, Folium Isatidis, wrap up with earth, dry, remove earth, clean, Put into steam box to toast 1 minute, add in alembic, distill 10 minutes, take out Fructus Forsythiae, Radix Isatidis, greatly Folium Isatidis；
(10) auxiliary material liquid of semi-finished product and 1% is mixed with the moisture in 3% alembic, stirring, planted Thing blended fuel.
CN201610111579.8A 2016-02-27 2016-02-27 Non-toxic epoxy resin-soybean protein plant fuel oil and preparation method thereof Pending CN105733696A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610111579.8A CN105733696A (en) 2016-02-27 2016-02-27 Non-toxic epoxy resin-soybean protein plant fuel oil and preparation method thereof

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Application Number Priority Date Filing Date Title
CN201610111579.8A CN105733696A (en) 2016-02-27 2016-02-27 Non-toxic epoxy resin-soybean protein plant fuel oil and preparation method thereof

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1319647A (en) * 2001-03-20 2001-10-31 中油燃料油有限公司 High sulfur heavy fuel desulfurating agent and use thereof
CN101302450A (en) * 2008-07-15 2008-11-12 周凯亮 Biosynthetic diesel and preparation thereof
CN103396857A (en) * 2013-06-25 2013-11-20 雷学军 Device and method for planting and comprehensive utilization of fast-growing plants to replace fossil energy
CN104694178A (en) * 2015-01-30 2015-06-10 安徽海德石油化工有限公司 Method for preparing fuel oil
CN104711043A (en) * 2015-01-30 2015-06-17 安徽海德石油化工有限公司 Novel burner plant oil and preparation method thereof

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1319647A (en) * 2001-03-20 2001-10-31 中油燃料油有限公司 High sulfur heavy fuel desulfurating agent and use thereof
CN101302450A (en) * 2008-07-15 2008-11-12 周凯亮 Biosynthetic diesel and preparation thereof
CN103396857A (en) * 2013-06-25 2013-11-20 雷学军 Device and method for planting and comprehensive utilization of fast-growing plants to replace fossil energy
CN104694178A (en) * 2015-01-30 2015-06-10 安徽海德石油化工有限公司 Method for preparing fuel oil
CN104711043A (en) * 2015-01-30 2015-06-17 安徽海德石油化工有限公司 Novel burner plant oil and preparation method thereof

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