CN105724152B - A kind of borneol camphor tree method for fast growing - Google Patents

A kind of borneol camphor tree method for fast growing Download PDF

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CN105724152B
CN105724152B CN201610059091.5A CN201610059091A CN105724152B CN 105724152 B CN105724152 B CN 105724152B CN 201610059091 A CN201610059091 A CN 201610059091A CN 105724152 B CN105724152 B CN 105724152B
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borneol
camphor tree
extracting solution
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CN105724152A (en
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文沁
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01GHORTICULTURE; CULTIVATION OF VEGETABLES, FLOWERS, RICE, FRUIT, VINES, HOPS OR SEAWEED; FORESTRY; WATERING
    • A01G17/00Cultivation of hops, vines, fruit trees, or like trees
    • A01G17/005Cultivation methods
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05BPHOSPHATIC FERTILISERS
    • C05B1/00Superphosphates, i.e. fertilisers produced by reacting rock or bone phosphates with sulfuric or phosphoric acid in such amounts and concentrations as to yield solid products directly
    • C05B1/02Superphosphates
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G5/00Fertilisers characterised by their form
    • C05G5/20Liquid fertilisers

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Pest Control & Pesticides (AREA)
  • Botany (AREA)
  • Environmental Sciences (AREA)
  • Fertilizers (AREA)
  • Cultivation Of Plants (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)

Abstract

The present invention relates to a kind of borneol camphor tree method for fast growing, including on the imperial camphor seedling survived, daily 8 points to 17 points were sprayed water 10 seconds every 1 hour, and temperature is maintained at 25-30 DEG C, and humidity is maintained at 60%-70%;17 points to second day 8 points were sprayed water 15 seconds every 3 hours, and temperature is maintained at 15-20 DEG C, and humidity is maintained at 30%-40%;Every 3-4 point spray nutritious liquor in 4 day afternoon, the amount of spraying:150-170kg/ mus;Continuous culture harvests after 12 months, can be used to extract natural borneol.This method further promotes the growth of borneol camphor tree seedling, improves the purity of natural borneol.

Description

A kind of borneol camphor tree method for fast growing
Technical field
The present invention relates to field of plant cultivation, and in particular to a kind of borneol camphor tree method for fast growing.
Background technique
Borneol camphor tree Cirmamonun Camphora is both rare rare medicinal material and fine perfumery, is also important Industrial chemicals.There is the good reputation of plant gold, the natural borneol perfume (or spice) tree tree root that borneol camphor tree originates in Indonesia Sumatra island was once The main source of borneol, but since closely exhaustion has been felled in long-term transition.Borneol is recorded in the Northern and Southern Dynasties earliest, away from the present existing 2,000 Many years history, borneol is referred to as natural borneol in the classic of TCM, because of great transdermal function, is attributed to aromatic and inducing resuscitation medicinal material.
The existing technical report about borneol camphor tree fast-growth it is few, CN104663229A discloses a kind of borneol camphor tree The method for setting fast-growth although it accelerates the time from seedling to refinement borneol, while improving the purity of natural borneol, But the above-mentioned time is still too long in industrialization process, and purity cannot ensure, affect industrialization process.
Summary of the invention
The present invention is directed to current problem, provides a kind of improved borneol camphor tree method for fast growing.
In order to solve the above technical problems, one technical scheme adopted by the invention is that:A kind of borneol camphor tree fast-growth is provided Method includes the following steps:
1) on the imperial camphor seedling survived, daily 8 points to 17 points were sprayed water 10 seconds every 1 hour, and temperature is maintained at 25-30 DEG C, humidity is maintained at 60%-70%;17 points to second day 8 points were sprayed water 15 seconds every 3 hours, and temperature is maintained at 15-20 DEG C, humidity is maintained at 30%-40%;
2) every 3-4 point spray nutritious liquor in 4 day afternoon, the amount of spraying:150-170kg/ mus;
3) continuous culture harvests after 12 months, can be used to extract natural borneol;
Wherein nutrient solution prescription is:Calcium superphosphate 450-550mg/L, potassium nitrate 1100-1300mg/L, magnesium sulfate 550- 650mg/L, calcium nitrate 450-550mg/L, potassium dihydrogen phosphate 100-300mg/L, boric acid 0.3-0.7mg/L, manganese sulfate 2-3mg/ L, zinc sulfate 0.3-0.8mg/L, glycine 1-2mg/L, thiamine hydrochloride 1.0-1.5mg/L, pyridoxine hydrochloride 0.5-1.0mg/ L, niacin 0.5-1.0mg/L, ferrous sulfate 50-60mg/L, EDTA 20-30mg/L, cinnamomum camphora extracting solution 20-30g/L.
Preferably, the preparation method of the cinnamomum camphora extracting solution is:(1) yellow cinnamon leaf is dry, crush and obtain powder I, third Ketone mixes with powder I in mass ratio 3: 1~5: 1, refluxing extraction 30~50 minutes, filters extracting solution, and filtrate is concentrated to dryness, obtains Solid content II;
(2) the solid content II that step (1) obtains is mixed with water in mass ratio 1: 20~1: 50, is ultrasonically treated 10~20 points Clock obtains solid content II suspension i.e. cinnamomum camphora extracting solution.
Preferably, the nutrient solution prescription is:Calcium superphosphate 498mg/L, potassium nitrate 1205mg/L, magnesium sulfate 592mg/L, Calcium nitrate 483mg/L, potassium dihydrogen phosphate 200mg/L, boric acid 0.5mg/L, manganese sulfate 2.8mg/L, zinc sulfate 0.57mg/L, sweet ammonia Sour 1.4mg/L thiamine hydrochloride 1.2mg/L pyridoxine hydrochloride 0.7mg/L, niacin 0.9mg/L, ferrous sulfate 57.8mg/L, EDTA 25.7mg/L, cinnamomum camphora extracting solution 25g/L.
The beneficial effects of the invention are as follows:
1, according to the habit of borneol camphor tree, water spraying time is had adjusted, while correspondingly having adjusted the temperature and humidity of borneol camphor tree Environment, by above-mentioned adjustment, so that borneol camphor tree within the eugonic period, under suitable temperature and humidity environment, gives full play to Borneol camphor tree body-internal-circulation, generates a large amount of biomass, and in the lower environment of temperature and humidity, metabolism slows down, and reduces internal life The consumption of substance, and then be conducive to the accumulation of biomass;
2, nutrient solution is had adjusted, by largely testing, it is determined that the nutrient solution of the borneol camphor tree seedling that is more suitable growth is matched Side;
3, the extracting solution with the closer cinnamomum camphora of borneol camphor tree provenance relationship is creatively added in nutrient solution, since it contains There is special substance, in the case where changing extracting solution effect, further promotes the growth of borneol camphor tree seedling, improve the pure of natural borneol Degree.
Specific embodiment
The preferred embodiments of the present invention will be described in detail below so that advantages and features of the invention can be easier to by It will be appreciated by those skilled in the art that so as to make a clearer definition of the protection scope of the present invention.
The embodiment of the present invention includes:
Embodiment 1:
Round-the-clock water and fertilizer management implemented to the seedling on seedbed in greenhouse, the borneol camphor tree method for fast growing, including with Lower step:
1) on the imperial camphor seedling survived, daily 8 points to 17 points were sprayed water 10 seconds every 1 hour, and temperature is maintained at 25 DEG C, humidity is maintained at 60%;17 points to second day 8 points were sprayed water 15 seconds every 3 hours, and temperature is maintained at 15 DEG C, and humidity is kept 30%%;
2) every 4 day afternoon, 3 spray nutritious liquors, the amount of spraying:150kg/ mus;
3) continuous culture harvests after 12 months, can be used to extract natural borneol;
Wherein nutrient solution prescription is:Calcium superphosphate 450mg/L, potassium nitrate 1100mg/L, magnesium sulfate 550mg/L, calcium nitrate 450mg/L, potassium dihydrogen phosphate 100mg/L, boric acid 0.3mg/L, manganese sulfate 2mg/L, zinc sulfate 0.3mg/L, glycine 1mg/L, Thiamine hydrochloride 1.0mg/L, pyridoxine hydrochloride 0.5mg/L, niacin 0.5mg/L, ferrous sulfate 50mg/L, EDTA 20mg/L are fragrant Camphor tree extracting solution 20g/L.
The preparation method of the cinnamomum camphora extracting solution is:(1) yellow cinnamon leaf is dry, crushing obtains powder I, acetone and powder The mixing of I in mass ratio 3: 1, refluxing extraction 30 minutes, filter extracting solution, and filtrate is concentrated to dryness, and obtain solid content II;
(2) the solid content II that step (1) obtains is mixed with water in mass ratio 1: 20, is ultrasonically treated 10 minutes, consolidate Shape object II suspension, that is, cinnamomum camphora extracting solution.
Embodiment 2:
Round-the-clock water and fertilizer management implemented to the seedling on seedbed in greenhouse, the borneol camphor tree method for fast growing, including with Lower step:
1) on the imperial camphor seedling survived, daily 8 points to 17 points were sprayed water 10 seconds every 1 hour, and temperature is maintained at 30 DEG C, humidity is maintained at 70%;17 points to second day 8 points were sprayed water 15 seconds every 3 hours, and temperature is maintained at 20 DEG C, and humidity is kept 40%;
2) every 4 day afternoon, 4 spray nutritious liquors, the amount of spraying:170kg/ mus;
3) continuous culture harvests after 12 months, can be used to extract natural borneol;
Wherein nutrient solution prescription is:Calcium superphosphate 550mg/L, potassium nitrate 1300mg/L, magnesium sulfate 650mg/L, calcium nitrate 550mg/L, potassium dihydrogen phosphate 300mg/L, boric acid 0.7mg/L, manganese sulfate 3mg/L, zinc sulfate 0.8mg/L, glycine 2mg/L, Thiamine hydrochloride 1.5mg/L, pyridoxine hydrochloride 1.0mg/L, niacin 1.0mg/L, ferrous sulfate 60mg/L, EDTA 30mg/L are fragrant Camphor tree extracting solution 30g/L.
Preferably, the preparation method of the cinnamomum camphora extracting solution is:(1) yellow cinnamon leaf is dry, crush and obtain powder I, third Ketone mixes with powder I in mass ratio 5: 1, refluxing extraction 50 minutes, filters extracting solution, and filtrate is concentrated to dryness, and obtains solid content II;
(2) the solid content II that step (1) obtains is mixed with water in mass ratio I: 50, is ultrasonically treated 20 minutes, consolidate Shape object II suspension, that is, cinnamomum camphora extracting solution.
Embodiment 3:
Round-the-clock water and fertilizer management implemented to the seedling on seedbed in greenhouse, the borneol camphor tree method for fast growing, including with Lower step:
1) on the imperial camphor seedling survived, daily 8 points to 17 points were sprayed water 10 seconds every 1 hour, and temperature is maintained at 28 DEG C, humidity is maintained at 65%;17 points to second day 8 points were sprayed water 15 seconds every 3 hours, and temperature is maintained at 18 DEG C, and humidity is kept 35%;
2) every 4 day afternoon, 3 spray nutritious liquors, the amount of spraying:160kg/ mus;
3) continuous culture harvests after 12 months, can be used to extract natural borneol;
Wherein nutrient solution prescription is:Calcium superphosphate 498mg/L, potassium nitrate 1205mg/L, magnesium sulfate 592mg/L, calcium nitrate 483mg/L, potassium dihydrogen phosphate 200mg/L, boric acid 0.5mg/L, manganese sulfate 2.8mg/L, zinc sulfate 0.57mg/L, glycine 1.4mg/L, thiamine hydrochloride 1.2mg/L, pyridoxine hydrochloride 0.7mg/L, niacin 0.9mg/L, ferrous sulfate 57.8mg/L, EDTA 25.7mg/L, cinnamomum camphora extracting solution 25g/L.
The preparation method of the cinnamomum camphora extracting solution is:(1) yellow cinnamon leaf is dry, crushing obtains powder I, acetone and powder The mixing of I in mass ratio 4: 1, refluxing extraction 40 minutes, filter extracting solution, and filtrate is concentrated to dryness, and obtain solid content II;
(2) the solid content II that step (1) obtains is mixed with water in mass ratio 1: 35, is ultrasonically treated 15 minutes, consolidate Shape object II suspension, that is, cinnamomum camphora extracting solution.
Comparative example
It is several with the seedling of the same batch taken root on the 10th of September in 2014, it is tested using 3 method of embodiment, and point Not not spray water with the seedling of nutrient solution field grown (control 1) and according to the seedling of CN104663229A (control 2) growth As control, the one year seedling test on the 10th of September in 2015 is grown into, comparative test result is as shown in table 1, it is seen then that borneol camphor tree seedling Using that after the present processes annual growth, can extract natural borneol in greenhouse, purity, content and extracted amount are super Cross two controls.
1 comparative test data of table
The above description is only an embodiment of the present invention, is not intended to limit the scope of the invention, all to utilize this hair Equivalent structure or equivalent flow shift made by bright description is applied directly or indirectly in other relevant technology necks Domain is included within the scope of the present invention.

Claims (3)

1. a kind of borneol camphor tree method for fast growing, which is characterized in that include the following steps:
1) on the imperial camphor seedling survived, daily 8 points to 17 points were sprayed water 10 seconds every 1 hour, and temperature is maintained at 25-30 DEG C, humidity is maintained at 60%-70%;17 points to second day 8 points were sprayed water 15 seconds every 3 hours, and temperature is maintained at 15-20 DEG C, wet Degree is maintained at 30%-40%;
2) every 3-4 point spray nutritious liquor in 4 day afternoon, the amount of spraying:150-170kg/ mus;
3) continuous culture harvests after 12 months, can be used to extract natural borneol;
Wherein nutrient solution prescription is:Calcium superphosphate 450-550mg/L, potassium nitrate 1100-1300mg/L, magnesium sulfate 550-650mg/ L, calcium nitrate 450-550mg/L, potassium dihydrogen phosphate 100-300mg/L, boric acid 0.3-0.7mg/L, manganese sulfate 2-3mg/L, sulfuric acid Zinc 0.3-0.8mg/L, glycine 1-2mg/L, thiamine hydrochloride 1.0-1.5mg/L, pyridoxine hydrochloride 0.5-1.0mg/L, niacin 0.5-1.0mg/L, ferrous sulfate 50-60mg/L, EDTA 20-30mg/L, cinnamomum camphora extracting solution 20-30g/L.
2. borneol camphor tree method for fast growing according to claim 1, which is characterized in that the preparation of the cinnamomum camphora extracting solution Method is:(1) yellow cinnamon leaf is dry, crush and obtain powder I, acetone mixes with powder I in mass ratio 3: 1~5: 1, refluxing extraction 30~50 minutes, extracting solution is filtered, filtrate is concentrated to dryness, and obtains solid content II;
(2) the solid content II that step (1) obtains is mixed with water in mass ratio 1: 20~1: 50, is ultrasonically treated 10~20 minutes, Obtain solid content II suspension i.e. cinnamomum camphora extracting solution.
3. such as the described in any item borneol camphor tree method for fast growing of claim 1-2, which is characterized in that the nutrient solution prescription For:Calcium superphosphate 498mg/L, potassium nitrate 1205mg/L, magnesium sulfate 592mg/L, calcium nitrate 483mg/L, potassium dihydrogen phosphate 200mg/L, boric acid 0.5mg/L, manganese sulfate 2.8mg/L, zinc sulfate 0.57mg/L, glycine 1.4mg/L, thiamine hydrochloride 1.2mg/L, pyridoxine hydrochloride 0.7mg/L, niacin 0.9mg/L, ferrous sulfate 57.8mg/L, EDTA 25.7mg/L, cinnamomum camphora are extracted Liquid 25g/L.
CN201610059091.5A 2016-01-29 2016-01-29 A kind of borneol camphor tree method for fast growing Expired - Fee Related CN105724152B (en)

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CN104663229A (en) * 2015-03-16 2015-06-03 江苏金叶子生物科技有限公司 Quick growth method for cinnamomum camphora tree
CN104756678A (en) * 2015-03-16 2015-07-08 江苏金叶子生物科技有限公司 Cinnamomum camphora shearing picking method
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CN104663405A (en) * 2015-03-16 2015-06-03 江苏金叶子生物科技有限公司 Quick propagation method for cinnamomum camphora tree
CN104663229A (en) * 2015-03-16 2015-06-03 江苏金叶子生物科技有限公司 Quick growth method for cinnamomum camphora tree
CN104756678A (en) * 2015-03-16 2015-07-08 江苏金叶子生物科技有限公司 Cinnamomum camphora shearing picking method
CN104871901A (en) * 2015-05-29 2015-09-02 江西北辰德天然生物科技有限公司 Cinnamomum camphora seedling cultivation method

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