CN105690586A - Silicon rod slicing process - Google Patents

Silicon rod slicing process Download PDF

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Publication number
CN105690586A
CN105690586A CN201610202149.7A CN201610202149A CN105690586A CN 105690586 A CN105690586 A CN 105690586A CN 201610202149 A CN201610202149 A CN 201610202149A CN 105690586 A CN105690586 A CN 105690586A
Authority
CN
China
Prior art keywords
silicon rod
cut
distance
mortar
line
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610202149.7A
Other languages
Chinese (zh)
Inventor
张力峰
田利中
白青松
邹文龙
梁会宁
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
SUZHOU JINGYING PHOTOELECTRIC TECHNOLOGY CO LTD
Original Assignee
SUZHOU JINGYING PHOTOELECTRIC TECHNOLOGY CO LTD
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by SUZHOU JINGYING PHOTOELECTRIC TECHNOLOGY CO LTD filed Critical SUZHOU JINGYING PHOTOELECTRIC TECHNOLOGY CO LTD
Priority to CN201610202149.7A priority Critical patent/CN105690586A/en
Publication of CN105690586A publication Critical patent/CN105690586A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B28WORKING CEMENT, CLAY, OR STONE
    • B28DWORKING STONE OR STONE-LIKE MATERIALS
    • B28D5/00Fine working of gems, jewels, crystals, e.g. of semiconductor material; apparatus or devices therefor
    • B28D5/04Fine working of gems, jewels, crystals, e.g. of semiconductor material; apparatus or devices therefor by tools other than rotary type, e.g. reciprocating tools
    • B28D5/045Fine working of gems, jewels, crystals, e.g. of semiconductor material; apparatus or devices therefor by tools other than rotary type, e.g. reciprocating tools by cutting with wires or closed-loop blades
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B28WORKING CEMENT, CLAY, OR STONE
    • B28DWORKING STONE OR STONE-LIKE MATERIALS
    • B28D5/00Fine working of gems, jewels, crystals, e.g. of semiconductor material; apparatus or devices therefor
    • B28D5/0058Accessories specially adapted for use with machines for fine working of gems, jewels, crystals, e.g. of semiconductor material
    • B28D5/0076Accessories specially adapted for use with machines for fine working of gems, jewels, crystals, e.g. of semiconductor material for removing dust, e.g. by spraying liquids; for lubricating, cooling or cleaning tool or work
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M173/00Lubricating compositions containing more than 10% water
    • C10M173/02Lubricating compositions containing more than 10% water not containing mineral or fatty oils
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/02Hydroxy compounds
    • C10M2207/021Hydroxy compounds having hydroxy groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2207/022Hydroxy compounds having hydroxy groups bound to acyclic or cycloaliphatic carbon atoms containing at least two hydroxy groups
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/10Carboxylix acids; Neutral salts thereof
    • C10M2207/12Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2207/125Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids
    • C10M2207/127Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids polycarboxylic
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2209/00Organic macromolecular compounds containing oxygen as ingredients in lubricant compositions
    • C10M2209/10Macromolecular compoundss obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C10M2209/103Polyethers, i.e. containing di- or higher polyoxyalkylene groups
    • C10M2209/107Polyethers, i.e. containing di- or higher polyoxyalkylene groups of two or more specified different alkylene oxides covered by groups C10M2209/104 - C10M2209/106
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2217/00Organic macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10MLUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2223/00Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
    • C10M2223/02Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
    • C10M2223/04Phosphate esters
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/06Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10NINDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/12Inhibition of corrosion, e.g. anti-rust agents or anti-corrosives

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Processing Of Stones Or Stones Resemblance Materials (AREA)

Abstract

The invention discloses a silicon rod slicing process with low usage amount of cutting wires. A slicing machine is adopted to slice a silicon rod; firstly, the cleaned silicon rod, a glass plate and a crystal support are bonded in sequence; then, the crystal support is fixed on the slicing machine; mortar is sprayed to the cutting wires by nozzles on two sides of the silicon rod, so that the cutting wires are fully coated with the mortar; a movement mode of the cutting wires is advancement by a distance A, retreating by a distance of B and advancement by the distance of A; and the mortar comprises the following components in percentage by weight: 5% of polyether alkanolamine comb polymer, 4.2% of ethylene oxide and propylene oxide reverse copolymerized polyether, 0.5% of fatty ethylene oxide and propylene oxide derivative low-foam surface active agent, 0.5% of sodium succinate salt, 80% of polyols and addition products thereof, 2.4% of water soluble low-foam phosphate and derivatives thereof, and the balance of water. The silicon rod slicing process has the following advantages: the cutting wires are used for cutting in a reciprocating manner; and meanwhile, the proper mortar is used for reducing the usage amount of the cutting wires, so that the production cost is reduced.

Description

Silicon rod slicing technique
Technical field
The present invention relates to a kind of silicon rod slicing technique。
Background technology
Silicon rod cutting is an important step in silicon wafer production technique, special line of cut is needed when cutting, because to avoid broken string when cutting as far as possible, usually line of cut is once by also cutting silicon rod, frequent broken string can cause the phenomenons such as cutting deformation silicon wafer variable thickness, damage, therefore line of cut cannot re-use after having cut silicon rod and belong to expendable consumed product, line of cut make consumption still very big, cause the wasting of resources。
Summary of the invention
The technical problem to be solved is: provide the silicon rod slicing technique that a kind of line of cut makes consumption few。
For solving above-mentioned technical problem, the technical solution used in the present invention is: a kind of silicon rod slicing technique, adopt microtome that silicon rod is cut into slices, it is specially first by cleaned silicon rod, glass plate and crystal holder stick together successively, then crystal holder is fixed on microtome, first start motor driven roller to rotate together with line of cut, line of cut is carried out spray furnace by the nozzle of silicon rod both sides, make line of cut fills mortar, the motion mode of line of cut is advance A distance, retreat B distance, readvance A distance, retreat B distance, the like, crystal holder drives silicon rod to move down and make line of cut cutting silicon rod until silicon rod is completely cut-off, wherein A > B, the weight percent composition of mortar is polyether chain alkanolamine comb-shaped polymer 5%, oxirane and the reverse copolyether 4.2% of expoxy propane, aliphatic oxirane and propylene oxide derivatives low foaming surfactant 0.5%, succinic acid sodium salt 0.5%, polyhydric alcohol and addition product 80% thereof, the low bubble phosphate ester of water solublity and derivant 2.4% thereof, all the other are water。
The invention has the beneficial effects as follows: utilize line of cut to come and go cutting, use suitable mortar to reduce the consumption that makes of line of cut simultaneously, reduce production cost。
Detailed description of the invention
Silicon rod slicing technique of the present invention, adopt microtome that silicon rod is cut into slices, it is specially first by cleaned silicon rod, glass plate and crystal holder stick together successively, then crystal holder is fixed on microtome, first start motor driven roller to rotate together with line of cut, line of cut is carried out spray furnace by the nozzle of silicon rod both sides, make line of cut fills mortar, crystal holder drives silicon rod to move down and make line of cut cutting silicon rod until silicon rod is completely cut-off, the motion mode of line of cut is advance A distance, retreat B distance, readvance A distance, retreat B distance, the like, wherein A > B, the mode cutting silicon rod utilizing line of cut to come and go and to advance, the utilization rate of line of cut is made to reach under ensureing the continuous situation of line of cut maximum, the weight percent composition of mortar is polyether chain alkanolamine comb-shaped polymer 5%, oxirane and the reverse copolyether 4.2% of expoxy propane, aliphatic oxirane and propylene oxide derivatives low foaming surfactant 0.5%, succinic acid sodium salt 0.5%, polyhydric alcohol and addition product 80% thereof, the low bubble phosphate ester of water solublity and derivant 2.4% thereof, all the other are water。This mortar has the greasy property of excellence, dispersibility and appropriate wettability, it is possible to eliminates the stress phenomena between line of cut and silicon rod in cutting process, improves silicon wafer ratio defective product;Mortar also has and extremely strong carries performance, suspendability;Good heat dissipation effect;For aqueous, environmental protective product;Good rustless property, anti-rancid performance, product stability is good, long service life;Without ionic soil, effectively eliminate the pollution of metal ion especially iron ion;Efficiently solve the deposition problems again of cutting powder, it is to avoid the chemical bonding adsorption phenomena of silicon face, it is simple to the cleaning of silicon wafer and following process。After using above-mentioned mortar so that silicon rod is easier to cut, in conjunction with the cutting mode of reciprocation type, comparing with original, line of cut can save half, is substantially reduced production cost。

Claims (1)

1. silicon rod slicing technique, it is characterized in that: adopt microtome that silicon rod is cut into slices, it is specially first by cleaned silicon rod, glass plate and crystal holder stick together successively, then crystal holder is fixed on microtome, first start motor driven roller to rotate together with line of cut, line of cut is carried out spray furnace by the nozzle of silicon rod both sides, make line of cut fills mortar, the motion mode of line of cut is advance A distance, retreat B distance, readvance A distance, retreat B distance, the like, crystal holder drives silicon rod to move down and make line of cut cutting silicon rod until silicon rod is completely cut-off, wherein A > B, the weight percent composition of mortar is polyether chain alkanolamine comb-shaped polymer 5%, oxirane and the reverse copolyether 4.2% of expoxy propane, aliphatic oxirane and propylene oxide derivatives low foaming surfactant 0.5%, succinic acid sodium salt 0.5%, polyhydric alcohol and addition product 80% thereof, the low bubble phosphate ester of water solublity and derivant 2.4% thereof, all the other are water。
CN201610202149.7A 2016-03-31 2016-03-31 Silicon rod slicing process Pending CN105690586A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610202149.7A CN105690586A (en) 2016-03-31 2016-03-31 Silicon rod slicing process

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610202149.7A CN105690586A (en) 2016-03-31 2016-03-31 Silicon rod slicing process

Publications (1)

Publication Number Publication Date
CN105690586A true CN105690586A (en) 2016-06-22

Family

ID=56218196

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610202149.7A Pending CN105690586A (en) 2016-03-31 2016-03-31 Silicon rod slicing process

Country Status (1)

Country Link
CN (1) CN105690586A (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107379294A (en) * 2017-07-20 2017-11-24 阜宁协鑫光伏科技有限公司 The method of diamond wire recycling cutting silicon chip
CN108357003A (en) * 2018-05-11 2018-08-03 青岛高测科技股份有限公司 A kind of cutting head and the two line excavation machines comprising the head
CN108568914A (en) * 2018-05-03 2018-09-25 浙江海顺新能源有限公司 A kind of solar silicon wafers processing cutting method
CN112428463A (en) * 2020-11-19 2021-03-02 上海中欣晶圆半导体科技有限公司 Method for line breakage and line restoration in crystal bar line cutting machining process

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2002060777A (en) * 2000-08-22 2002-02-26 Ishii Hyoki Corp Aqueous slurry for wire saw
JP2006096951A (en) * 2004-09-30 2006-04-13 Kyodo Yushi Co Ltd Water-soluble machining oil, slurry, and machining method
CN101664970A (en) * 2009-09-03 2010-03-10 无锡尚品太阳能电力科技有限公司 Monocrystal silicon-rod butting technique
CN102344776A (en) * 2010-08-06 2012-02-08 安集微电子(上海)有限公司 Cutting fluid for cutting of scroll saw
CN103242944A (en) * 2013-04-23 2013-08-14 上海晔宗光伏科技有限公司 Multifunctional water-based environment-friendly recyclable crystal silicon precision cutting liquid
CN103991140A (en) * 2014-04-28 2014-08-20 阳光硅谷电子科技有限公司 Diamond wire-electrode cutting technology for silicon rod
CN104191533A (en) * 2014-09-04 2014-12-10 无锡尚品太阳能电力科技有限公司 Silicon wafer reciprocating cutting technology

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2002060777A (en) * 2000-08-22 2002-02-26 Ishii Hyoki Corp Aqueous slurry for wire saw
JP2006096951A (en) * 2004-09-30 2006-04-13 Kyodo Yushi Co Ltd Water-soluble machining oil, slurry, and machining method
CN101664970A (en) * 2009-09-03 2010-03-10 无锡尚品太阳能电力科技有限公司 Monocrystal silicon-rod butting technique
CN102344776A (en) * 2010-08-06 2012-02-08 安集微电子(上海)有限公司 Cutting fluid for cutting of scroll saw
CN103242944A (en) * 2013-04-23 2013-08-14 上海晔宗光伏科技有限公司 Multifunctional water-based environment-friendly recyclable crystal silicon precision cutting liquid
CN103991140A (en) * 2014-04-28 2014-08-20 阳光硅谷电子科技有限公司 Diamond wire-electrode cutting technology for silicon rod
CN104191533A (en) * 2014-09-04 2014-12-10 无锡尚品太阳能电力科技有限公司 Silicon wafer reciprocating cutting technology

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107379294A (en) * 2017-07-20 2017-11-24 阜宁协鑫光伏科技有限公司 The method of diamond wire recycling cutting silicon chip
CN108568914A (en) * 2018-05-03 2018-09-25 浙江海顺新能源有限公司 A kind of solar silicon wafers processing cutting method
CN108357003A (en) * 2018-05-11 2018-08-03 青岛高测科技股份有限公司 A kind of cutting head and the two line excavation machines comprising the head
CN112428463A (en) * 2020-11-19 2021-03-02 上海中欣晶圆半导体科技有限公司 Method for line breakage and line restoration in crystal bar line cutting machining process

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Application publication date: 20160622