CN105687058A - Method for preparing water-soluble scar repairing seaweed cream by utilizing seaweed extract - Google Patents
Method for preparing water-soluble scar repairing seaweed cream by utilizing seaweed extract Download PDFInfo
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- CN105687058A CN105687058A CN201610189636.4A CN201610189636A CN105687058A CN 105687058 A CN105687058 A CN 105687058A CN 201610189636 A CN201610189636 A CN 201610189636A CN 105687058 A CN105687058 A CN 105687058A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/02—Algae
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K47/00—Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
- A61K47/30—Macromolecular organic or inorganic compounds, e.g. inorganic polyphosphates
- A61K47/32—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds, e.g. carbomers, poly(meth)acrylates, or polyvinyl pyrrolidone
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/0012—Galenical forms characterised by the site of application
- A61K9/0014—Skin, i.e. galenical aspects of topical compositions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/06—Ointments; Bases therefor; Other semi-solid forms, e.g. creams, sticks, gels
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/333—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using mixed solvents, e.g. 70% EtOH
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/50—Methods involving additional extraction steps
- A61K2236/53—Liquid-solid separation, e.g. centrifugation, sedimentation or crystallization
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Abstract
The invention relates to a method for preparing water-soluble scar repairing seaweed cream by utilizing seaweed extract. The method comprises the following steps: adding seaweed into a reaction kettle which is filled with water and an organic solvent; sizing, adding a wetting agent, soaking and extracting; reclaiming partial organic solvent by low-temperature low-pressure distillation; and finally, preparing seaweed residues and seaweed extract by a filter-press mode, mixing the seaweed extract, medical-grade polyvinyl alcohol solution and a nutritional repairing substance according to a certain mass ratio, and uniformly stirring to obtain the water-soluble scar repairing seaweed cream. Seaweed rich in seaweed protein, seaweed polysaccharide, alginic acid, trace elements and vitamins can be used for supplying skin nutrition, promoting blood circulation, removing cutin and accelerating skin metabolism, so that skin can be smooth and elastic.
Description
Technical field
The present invention relates to a kind of method utilizing seaweed extracted liquor to prepare water solublity cicatrix reparation seaweed paste。
Background technology
Preparing the method for seaweed mask at present to be mainly Sargassum and pulverize or decocting in water mixes with other nutritional labeling through simple, such extraction is very incomplete, causes a large amount of active component of Sargassum to waste;The film forming matter film-formation result of Sargassum itself is poor, water resistance is weak, it is impossible to effectively lock moisture, the seaweed mask that therefore direct algae component is made ageing short, and nutrient substance can not be fully absorbed by skin, thus causing that facial film does not reach ideal effect。
Summary of the invention
The technical problem to be solved is to provide a kind of method utilizing seaweed extracted liquor to prepare water solublity cicatrix reparation seaweed paste。The Sargassum active component extracted, pharmaceutical grade Polyethylene alcoholic solution and nutrition are repaired material perfect adaptation by the method, maximize the effect playing cicatrix reparation seaweed paste。
In order to solve above-mentioned technical problem, the present invention by the following technical solutions:
Fresh Sargassum is cleaned standby, or dry seaweed be dipped to fresh Sargassum moisture consistent state and clean standby, the alternate products that this step obtains is called A product, by deionized water, organic solvent and product A are added separately in reactor, pull an oar in the lump, wetting and penetrating agent is added after having broken slurry, soak 12~72 hours at 20~45 DEG C, low-temp low-pressure Distillation recovery part organic solvent: vapo(u)rizing temperature is 45~65 DEG C, distillation pressure is-0.5~-1.2Mpa, filter pressing obtains Sargassum slag and filtrate, described filtrate is seaweed extracted liquor, by described seaweed extracted liquor, pharmaceutical grade Polyethylene alcoholic solution and nutrition repair material according to certain mass than mixing, after stirring, it is and utilizes seaweed extracted liquor coproduction water solublity cicatrix to repair seaweed paste。
Wherein the mass ratio of A product, deionized water, organic solvent and wetting and penetrating agent is 5~30:10~85:10~85:0.1~5;It is 30~85:5~54:1~64 that the mass ratio of material is repaired in seaweed extracted liquor, pharmaceutical grade Polyethylene alcoholic solution and nutrition;Pharmaceutical grade Polyethylene alcoholic solution concentration is 1~7%。
Described organic solvent is the two or more of a kind of or arbitrary proportion in pharmaceutical grade ethanol, pharmaceutical grade propylene glycol and pharmaceutical grade glycerol。
Wetting and penetrating agent is dodecylbenzene sodium sulfonate, sodium lauryl sulphate, alkylphenol polyoxyethylene, sorbitan fatty acid ester-20, sorbitan fatty acid ester-30, sorbitan fatty acid ester-80, polyoxyethylene 20 sorbitan monolaurate-20, polyoxyethylene 20 sorbitan monolaurate-40, polyoxyethylene 20 sorbitan monolaurate-60, polyoxyethylene 20 sorbitan monolaurate-80, fatty alcohol-polyoxyethylene ether-3, fatty alcohol-polyoxyethylene ether-4, fatty alcohol-polyoxyethylene ether-5, fatty alcohol-polyoxyethylene ether-7, fatty alcohol-polyoxyethylene ether-9, fatty alcohol-polyoxyethylene ether-15, fatty alcohol-polyoxyethylene ether-20, a kind of or arbitrary proportion in fatty alcohol-polyoxyethylene ether-23 and dimethicone two or more;Described nutrition reparation material is the two or more of a kind of or arbitrary proportion in Mel, vitamin C, vitamin A, vitamin B2, vitamin B6, vitamin E, rose ethereal oil and Ovum Gallus domesticus album。
Described Sargassum refers to: a kind of or arbitrary proportion in Thallus Laminariae (Thallus Eckloniae), Thallus Porphyrae, Thallus Laminariae (Thallus Eckloniae), opotism and Entermorpha two or more。
Described in step 5), pressure filter selects filter cloth aperture to be 1200~4500 orders。
The present invention has following Advantageous Effects:
1, in the present invention, Sargassum liquid adopts low temperature, Low Voltage Pure physics to extract, it is ensured that Sargassum effective ingredient is not destroyed。
2, seaweeds appearance has the protecting film of one layer of thickness; prevent external substance from invading; so simple water or organic solvent extract at normal temperatures and pressures can be very slow; the present invention adds wetting and penetrating agent can increase the affinity of water, organic solvent and Sargassum; make water and organic solvent when protecting film is not damaged by room temperature, normal pressure; rapid osmotic Sargassum protecting film, thus reaching the purpose of rapid extraction, is therefore more convenient for the application of heavy industrialization;Wetting and penetrating agent can also promote in Sargassum in effective ingredient rapid osmotic skin, improves the utilization rate of active component。
3, the present invention adopts the extracting method that deionized water and organic solvent combine, and reduces cost than simple organic solvent extraction。
4, the present invention adopts the extracting method that water and organic solvent combine, and adds the compatibility of product。
5, the present invention adopts pharmaceutical grade Polyethylene alcohol as film forming matter relative to the film forming matter of Sargassum own, has good film-forming property, the excellent feature of water proofing property, it is possible to delay the evaporation of moisture in facial film, improves the ageing of seaweed paste, is conducive to the skin absorption to nutrient substance。
6, material combination is repaired in seaweed extracted liquor, pharmaceutical grade Polyethylene alcoholic solution and nutrition by the present invention, and scar of dispelling effect is obvious。
Detailed description of the invention
The present invention is further illustrated below in conjunction with instantiation。
Embodiment 1
Fresh Laminaria Japonica after cleaning is joined and fills deionized water, pharmaceutical grade ethanol, the reactor of pharmaceutical grade propylene glycol and pharmaceutical grade glycerol is pulled an oar, after making beating, adds the dodecylbenzene sodium sulfonate as wetting and penetrating agent, alkylphenol polyoxyethylene, sorbitan fatty acid ester-60 and dimethicone, Fresh Laminaria Japonica, deionized water, pharmaceutical grade ethanol, pharmaceutical grade propylene glycol, pharmaceutical grade glycerol, dodecylbenzene sodium sulfonate, alkylphenol polyoxyethylene, sorbitan fatty acid ester-60 and dimethicone are according to mass ratio 18:18:20:15:28:0.2:0.3:0.3:0.2, soak 46 hours at 30 DEG C, Distillation recovery part organic solvent at negative pressure 1.0Mpa, temperature 55 DEG C, pressure filter adopts 2500 order filter clothes to carry out filter pressing, gained filtrate, pharmaceutical grade Polyethylene alcoholic solution, Mel, vitamin C, vitamin A, vitamin B2, vitamin B6, vitamin E, rose ethereal oil and Ovum Gallus domesticus album mix according to mass ratio 35:15:6:4:5:6:6:10:8:5, after stirring, are water solublity cicatrix and repair seaweed paste。
Embodiment 2
Fresh Laminaria Japonica after cleaning is joined and fills deionized water, pharmaceutical grade ethanol, the reactor of pharmaceutical grade propylene glycol and pharmaceutical grade glycerol is pulled an oar, after making beating, adds the dodecylbenzene sodium sulfonate as wetting and penetrating agent, alkylphenol polyoxyethylene, sorbitan fatty acid ester-60 and dimethicone, Fresh Laminaria Japonica, deionized water, pharmaceutical grade ethanol, pharmaceutical grade propylene glycol, pharmaceutical grade glycerol, dodecylbenzene sodium sulfonate, alkylphenol polyoxyethylene, sorbitan fatty acid ester-60 and dimethicone are according to mass ratio 18:18:20:15:28:0.2:0.3:0.3:0.2, soak 46 hours at 30 DEG C, Distillation recovery part organic solvent at negative pressure 1.0Mpa, temperature 55 DEG C, pressure filter adopts 2500 order filter clothes to carry out filter pressing, gained filtrate, pharmaceutical grade Polyethylene alcoholic solution, Mel, vitamin C, vitamin A, vitamin B2, vitamin B6, vitamin E, rose ethereal oil and Ovum Gallus domesticus album mix according to mass ratio 30:20:6:6:4:5:6:10:8:5, after stirring, are water solublity cicatrix and repair seaweed paste。
Embodiment 3
Fresh Laminaria Japonica after cleaning is joined and fills deionized water, pharmaceutical grade ethanol, the reactor of pharmaceutical grade propylene glycol and pharmaceutical grade glycerol is pulled an oar, after making beating, adds the dodecylbenzene sodium sulfonate as wetting and penetrating agent, alkylphenol polyoxyethylene, sorbitan fatty acid ester-60 and dimethicone, Fresh Laminaria Japonica, deionized water, pharmaceutical grade ethanol, pharmaceutical grade propylene glycol, pharmaceutical grade glycerol, dodecylbenzene sodium sulfonate, alkylphenol polyoxyethylene, sorbitan fatty acid ester-60 and dimethicone are according to mass ratio 18:18:20:15:28:0.2:0.3:0.3:0.2, soak 46 hours at 30 DEG C, Distillation recovery part organic solvent at negative pressure 1.0Mpa, temperature 55 DEG C, pressure filter adopts 2500 order filter clothes to carry out filter pressing, gained filtrate, pharmaceutical grade Polyethylene alcoholic solution, Mel, vitamin C, vitamin A, vitamin B2, vitamin B6, vitamin E, rose ethereal oil and Ovum Gallus domesticus album mix according to mass ratio 40:10:5:10:6:5:7:6:4:7, after stirring, are water solublity cicatrix and repair seaweed paste。
Embodiment 4
Fresh Laminaria Japonica after cleaning is joined and fills deionized water, pharmaceutical grade ethanol, the reactor of pharmaceutical grade propylene glycol and pharmaceutical grade glycerol is pulled an oar, after making beating, adds the dodecylbenzene sodium sulfonate as wetting and penetrating agent, alkylphenol polyoxyethylene, sorbitan fatty acid ester-60 and dimethicone, Fresh Laminaria Japonica, deionized water, pharmaceutical grade ethanol, pharmaceutical grade propylene glycol, pharmaceutical grade glycerol, dodecylbenzene sodium sulfonate, alkylphenol polyoxyethylene, sorbitan fatty acid ester-60 and dimethicone are according to mass ratio 18:18:20:15:28:0.2:0.3:0.3:0.2, soak 46 hours at 30 DEG C, Distillation recovery part organic solvent at negative pressure 1.0Mpa, temperature 55 DEG C, pressure filter adopts 2500 order filter clothes to carry out filter pressing, gained filtrate, pharmaceutical grade Polyethylene alcoholic solution, Mel, vitamin C, vitamin A, vitamin B2, vitamin B6, vitamin E, rose ethereal oil and Ovum Gallus domesticus album mix according to mass ratio 35:10:4:12:5:5:10:10:4:5, after stirring, are water solublity cicatrix and repair seaweed paste。
Further illustrate below in conjunction with experimental data and the method have the benefit that
For the filtrate that Different Extraction Method on market is collected, carrying out the detection of Sargassum polysaccharides after oven drying at low temperature, testing result is table 1 such as。
Table 1
Comminuting method | Water-boiling method | Pulverize water-boiling method | The inventive method | |
Sargassum polysaccharides (%) | 10.2 | 18.2 | 26.4 | 42.1 |
Adopt Sargassum polysaccharides content in the seaweed extracted liquor of this method the highest as can be seen from Table 1。
1 physical data
Inventor collects 400 examples in May, 2014 altogether between in November, 2015, age is between 28 to 42 years old, effectiveness comparison is done for common scar cream of dispelling (except not adding seaweed extracted liquor, other manufacture method is identical with embodiment 3), embodiment 1, embodiment 2, embodiment 3, embodiment 4。
1.2 experimental techniques
By laboratory sample uniform application in cicatrix place, 3 times weekly, 6 months be a cycle。
1.3 experimental designs
400 people are divided into 5 groups, often organize 80 people and test respectively。
2 experimental results
Common cicatrix repairing paste (except not adding seaweed extracted liquor, other manufacture method is identical with embodiment 2) investigation satisfaction is 65.2%;It is 72.4% that embodiment 1 investigates satisfaction;It is 75.1% that embodiment 2 investigates satisfaction;It is 87.6% that embodiment 3 investigates satisfaction;It is 73.5% that embodiment 4 investigates satisfaction。It is satisfied with standard: to no skin irritation, uses rear cicatrix substantially to desalinate and even disappear。
3 discuss
Testing just for the product of the different manufacturers Different Extraction Method can collected on market, done Sargassum polysaccharides detection, being not necessarily that certain city field energy is collected is best, and notebook data can only illustrate most like products that product of the present invention is better than on market to collect;The repairing effect of cicatrix is relevant with the time of cicatrization, and the time is more short more easily repairs, and time cicatrix reparation more of a specified duration is got up can be very slow。
Claims (5)
1. one kind utilizes seaweed extracted liquor to prepare the method that water solublity cicatrix repairs seaweed paste, it is characterised in that carry out according to following steps:
1), fresh Sargassum is cleaned standby, or dry seaweed be dipped to fresh Sargassum moisture consistent state and clean standby, the alternate products that this step obtains is called product A;
2), deionized water, organic solvent and product A are added separately in reactor, pull an oar in the lump;
3), beaten and added wetting and penetrating agent after slurry, soaked 12~72 hours at 20~45 DEG C;
4), low-temp low-pressure Distillation recovery part organic solvent: vapo(u)rizing temperature is 45~65 DEG C, and distillation pressure is-0.5~-1.2Mpa;
5), filter pressing obtain Sargassum slag and filtrate, described filtrate is seaweed extracted liquor;
6), by described seaweed extracted liquor, pharmaceutical grade Polyethylene alcoholic solution and nutrition repair material according to certain mass than mixing, after stirring, be water solublity cicatrix and repair seaweed paste;
Wherein the mass ratio of A product, deionized water, organic solvent and wetting and penetrating agent is 5~30:10~85:10~85:0.1~5;It is 30~85:5~54:1~64 that the mass ratio of material is repaired in seaweed extracted liquor, pharmaceutical grade Polyethylene alcoholic solution and nutrition;Pharmaceutical grade Polyethylene alcoholic solution concentration is 1~7%。
2. utilize seaweed extracted liquor to prepare the method that water solublity cicatrix repairs seaweed paste as claimed in claim 1, it is characterised in that: described organic solvent is the two or more of a kind of or arbitrary proportion in pharmaceutical grade ethanol, pharmaceutical grade propylene glycol and pharmaceutical grade glycerol。
3. utilize seaweed extracted liquor to prepare the method that water solublity cicatrix repairs seaweed paste as claimed in claim 1, it is characterized in that: described wetting and penetrating agent is dodecylbenzene sodium sulfonate, sodium lauryl sulphate, alkylphenol polyoxyethylene, sorbitan fatty acid ester-20, sorbitan fatty acid ester-30, sorbitan fatty acid ester-80, polyoxyethylene 20 sorbitan monolaurate-20, polyoxyethylene 20 sorbitan monolaurate-40, polyoxyethylene 20 sorbitan monolaurate-60, polyoxyethylene 20 sorbitan monolaurate-80, fatty alcohol-polyoxyethylene ether-3, fatty alcohol-polyoxyethylene ether-4, fatty alcohol-polyoxyethylene ether-5, fatty alcohol-polyoxyethylene ether-7, fatty alcohol-polyoxyethylene ether-9, fatty alcohol-polyoxyethylene ether-15, fatty alcohol-polyoxyethylene ether-20, a kind of or arbitrary proportion in fatty alcohol-polyoxyethylene ether-23 and dimethyl-silicon wet goods two or more;Described nutrition reparation material is the two or more of a kind of or arbitrary proportion in Mel, vitamin C, vitamin A, vitamin B2, vitamin B6, vitamin E, rose ethereal oil and Ovum Gallus domesticus album。
4. utilize seaweed extracted liquor to prepare the method that water solublity cicatrix repairs seaweed paste as claimed in claim 1, it is characterised in that: described Sargassum refers to: a kind of or arbitrary proportion in Thallus Laminariae (Thallus Eckloniae), Thallus Porphyrae, Thallus Laminariae (Thallus Eckloniae), opotism and Entermorpha two or more。
5. utilize seaweed extracted liquor to prepare the method that water solublity cicatrix repairs seaweed paste as claimed in claim 1, it is characterised in that: described in step 5), pressure filter selects filter cloth aperture to be 1200~4500 orders。
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107550769A (en) * | 2017-09-14 | 2018-01-09 | 王雷 | A kind of preparation method of marine alga ferment facial mask |
CN107693421A (en) * | 2017-10-20 | 2018-02-16 | 烟台宇诚企业管理咨询有限公司 | A kind of scar eliminating composition containing marine organism extract and preparation method thereof |
CN113081914A (en) * | 2021-03-31 | 2021-07-09 | 上海花宫生物技术研发有限公司 | Extraction process of pure dew of algae of Zostera marina |
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2016
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107550769A (en) * | 2017-09-14 | 2018-01-09 | 王雷 | A kind of preparation method of marine alga ferment facial mask |
CN107693421A (en) * | 2017-10-20 | 2018-02-16 | 烟台宇诚企业管理咨询有限公司 | A kind of scar eliminating composition containing marine organism extract and preparation method thereof |
CN113081914A (en) * | 2021-03-31 | 2021-07-09 | 上海花宫生物技术研发有限公司 | Extraction process of pure dew of algae of Zostera marina |
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