CN105726411A - Method for preparing seaweed nourishing cleanser by utilizing seaweed extract - Google Patents
Method for preparing seaweed nourishing cleanser by utilizing seaweed extract Download PDFInfo
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- CN105726411A CN105726411A CN201610189960.6A CN201610189960A CN105726411A CN 105726411 A CN105726411 A CN 105726411A CN 201610189960 A CN201610189960 A CN 201610189960A CN 105726411 A CN105726411 A CN 105726411A
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- fatty alcohol
- seaweed
- polyoxyethylene
- polyoxyethylene ether
- sargassum
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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- Dermatology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Detergent Compositions (AREA)
- Cosmetics (AREA)
Abstract
The invention relates to a method for preparing a seaweed nourishing cleanser by utilizing a seaweed extract. The method comprises the following steps: washing seaweeds, adding the seaweeds to a reaction kettle with a mixture of water and organic solvents, adding wetting and penetrating agents after stirring the materials at high speed for pulping, recovering part of the organic solvents through low temperature and low pressure distillation after soaking and extraction, finally obtaining seaweed residues and the seaweed extract through filter pressing, uniformly mixing the seaweed extract, surfactants and nutrients and adding potassium hydroxide to regulate the pH value to be neutral, thus obtaining the product, namely the seaweed nourishing cleanser. Being rich in plenty of seaweed proteins, seaweed polysaccharides, seaweed acids, trace elements and vitamins, the seaweeds can achieve the effects of supplementing skin nutrients, promoting blood circulation, removing cutin, speeding up skin metabolism and keeping skin smooth and elastic.
Description
Technical field
The present invention relates to a kind of method utilizing seaweed extracted liquor to prepare water soluble algae face cleaning nourishing breast.
Background technology
The method that seaweed extracted liquor prepared by current Sargassum cosmetics is mainly Sargassum and mixes through simply pulverizing or decocting in water and other nutritional labeling, and such extraction is very incomplete, causes a large amount of active component waste of Sargassum, and cosmetics do not reach gratifying effect yet.
Summary of the invention
The technical problem to be solved is to provide a kind of method utilizing seaweed extracted liquor to prepare Sargassum face cleaning nourishing breast.The method, by seaweed extracted liquor, surfactant and nutrient substance perfect adaptation, maximizes the effect playing Sargassum face cleaning nourishing breast.
In order to solve above-mentioned technical problem, the present invention by the following technical solutions:
1), fresh Sargassum is cleaned standby, or dry seaweed be dipped to fresh Sargassum moisture consistent state and clean standby, the alternate products that this step obtains is called A product；
2), deionized water, organic solvent and product A are added separately in reactor, pull an oar in the lump；
3), beaten and added wetting and penetrating agent after slurry, soaked 12～72 hours at 20～45 DEG C；
4), low-temp low-pressure Distillation recovery part organic solvent: vapo(u)rizing temperature is 45～65 DEG C, and distillation pressure is-0.5～-1.2Mpa；
5), filter pressing obtain Sargassum slag and filtrate, described filtrate is seaweed extracted liquor；
6), by described seaweed extracted liquor, surfactant and nutrient substance according to certain mass ratio mixing, after stirring, being cooled to room temperature, products obtained therefrom is called B product；
7), with potassium hydroxide adjusting B product pH value to neutral, products obtained therefrom is Sargassum face cleaning nourishing breast；
Wherein the mass ratio of A product, deionized water, organic solvent and wetting and penetrating agent is 5～30:10～85:10～85:0.1～5;The mass ratio of seaweed extracted liquor, surfactant and nutrient substance is 5～80:1～65:1～65.
Described organic solvent is the two or more of a kind of or arbitrary proportion in pharmaceutical grade ethanol, pharmaceutical grade propylene glycol and pharmaceutical grade glycerol.
Described wetting and penetrating agent is dodecylbenzene sodium sulfonate, sodium lauryl sulphate, alkylphenol polyoxyethylene, sorbitan fatty acid ester-20, sorbitan fatty acid ester-30, sorbitan fatty acid ester-80, polyoxyethylene 20 sorbitan monolaurate-20, polyoxyethylene 20 sorbitan monolaurate-40, polyoxyethylene 20 sorbitan monolaurate-60, polyoxyethylene 20 sorbitan monolaurate-80, fatty alcohol-polyoxyethylene ether-3, fatty alcohol-polyoxyethylene ether-4, fatty alcohol-polyoxyethylene ether-5, fatty alcohol-polyoxyethylene ether-7, fatty alcohol-polyoxyethylene ether-9, fatty alcohol-polyoxyethylene ether-15, fatty alcohol-polyoxyethylene ether-20, a kind of or arbitrary proportion in fatty alcohol-polyoxyethylene ether-23 and dimethicone two or more；
Described surfactant is dodecylbenzene sodium sulfonate, sorbitan fatty acid ester-20, sorbitan fatty acid ester-30, sorbitan fatty acid ester-80, polyoxyethylene 20 sorbitan monolaurate-20, polyoxyethylene 20 sorbitan monolaurate-40, polyoxyethylene 20 sorbitan monolaurate-60, polyoxyethylene 20 sorbitan monolaurate-80, fatty alcohol-polyoxyethylene ether-3, fatty alcohol-polyoxyethylene ether-4, fatty alcohol-polyoxyethylene ether-5, fatty alcohol-polyoxyethylene ether-7, fatty alcohol-polyoxyethylene ether-9, fatty alcohol-polyoxyethylene ether-15, fatty alcohol-polyoxyethylene ether-20, a kind of or arbitrary proportion in fatty alcohol-polyoxyethylene ether-23 and dimethicone two or more；
Described nutrient substance is the two or more of a kind of or arbitrary proportion in arginine, aspartic acid, glutamic acid, valine, leucine, isoleucine, serine, glycine, alanine, threonine, sodium lactate, citric acid, glycerol and 1,3 butanediols.
Described Sargassum refers to: a kind of or arbitrary proportion in Thallus Laminariae (Thallus Eckloniae), Thallus Porphyrae, Thallus Laminariae (Thallus Eckloniae), opotism and Entermorpha two or more.
Described in step 5), pressure filter selects filter cloth aperture to be 1200～4500 orders.
The present invention has following Advantageous Effects:
1, in the present invention, Sargassum liquid adopts low temperature, Low Voltage Pure physics to extract, it is ensured that Sargassum effective ingredient is not destroyed.
2, seaweeds appearance has the protecting film of one layer of thickness; prevent external substance from invading; so simple water or organic solvent extract at normal temperatures and pressures can be very slow; the present invention adds wetting and penetrating agent can increase the affinity of water, organic solvent and Sargassum; make water and organic solvent when protecting film is not damaged by room temperature, normal pressure; rapid osmotic Sargassum protecting film, thus reaching the purpose of rapid extraction, is therefore more convenient for the application of heavy industrialization；Wetting and penetrating agent can also promote in Sargassum in effective ingredient rapid osmotic skin, improves the utilization rate of active component.
3, the present invention adopts the extracting method that deionized water and organic solvent combine, and reduces cost than simple organic solvent extraction.
4, the present invention adopts the extracting method that water and organic solvent combine, and adds the compatibility of product.
5, seaweed extracted liquor, surfactant and nutrient substance are combined by the present invention, and cutin effect of dispelling is particularly evident, uses rear skin gloss flexible.
Detailed description of the invention
The present invention is further illustrated below in conjunction with instantiation.
Embodiment 1
nullFresh Laminaria Japonica after cleaning is joined and fills deionized water、Pharmaceutical grade ethanol、The reactor of pharmaceutical grade propylene glycol and pharmaceutical grade glycerol is pulled an oar，The dodecylbenzene sodium sulfonate as wetting and penetrating agent is added after making beating、Alkylphenol polyoxyethylene、Sorbitan fatty acid ester-60 and dimethicone，Fresh Laminaria Japonica、Deionized water、Pharmaceutical grade ethanol、Pharmaceutical grade propylene glycol、Pharmaceutical grade glycerol、Dodecylbenzene sodium sulfonate、Alkylphenol polyoxyethylene、Sorbitan fatty acid ester-60 and dimethicone are according to mass ratio 18:18:20:15:28:0.2:0.3:0.3:0.2，Soak 46 hours at 30 DEG C，In negative pressure 1.0Mpa，Distillation recovery part organic solvent at temperature 55 DEG C，Pressure filter adopts 2500 order filter clothes to carry out filter pressing，Gained filtrate、Sorbitan fatty acid ester-30、Polyoxyethylene 20 sorbitan monolaurate-20、Polyoxyethylene 20 sorbitan monolaurate-40、Fatty alcohol-polyoxyethylene ether-3、Arginine、Aspartic acid、Glutamic acid、Valine、Leucine、Isoleucine、Serine、Glycine、Alanine、Threonine、Sodium lactate、Citric acid、Glycerol and 1,3 butanediols mix according to mass ratio 20:5:5:5:2:3:4:2:6:2:8:4:5:6:8:5:5:3:2，After stirring，Adding potassium hydroxide adjusts pH value to be neutral，It is Sargassum face cleaning nourishing breast.
Embodiment 2
nullFresh Laminaria Japonica after cleaning is joined and fills deionized water、Pharmaceutical grade ethanol、The reactor of pharmaceutical grade propylene glycol and pharmaceutical grade glycerol is pulled an oar，The dodecylbenzene sodium sulfonate as wetting and penetrating agent is added after making beating、Alkylphenol polyoxyethylene、Sorbitan fatty acid ester-60 and dimethicone，Fresh Laminaria Japonica、Deionized water、Pharmaceutical grade ethanol、Pharmaceutical grade propylene glycol、Pharmaceutical grade glycerol、Dodecylbenzene sodium sulfonate、Alkylphenol polyoxyethylene、Sorbitan fatty acid ester-60 and dimethicone are according to mass ratio 18:18:20:15:28:0.2:0.3:0.3:0.2，Soak 46 hours at 30 DEG C，In negative pressure 1.0Mpa，Distillation recovery part organic solvent at temperature 55 DEG C，Pressure filter adopts 2500 order filter clothes to carry out filter pressing，Gained filtrate、Sorbitan fatty acid ester-30、Fatty alcohol-polyoxyethylene ether-9、Arginine、Aspartic acid、Glutamic acid、Valine、Leucine、Isoleucine、Serine、Glycine、Alanine、Threonine、Sodium lactate、Citric acid、Glycerol and 1,3 butanediols mix according to mass ratio 30:2:4:10:3:10:2:6:2:8:5:6:4:2:2:2:2，After stirring，Adding potassium hydroxide adjusts pH value to be neutral，It is Sargassum face cleaning nourishing breast.
Embodiment 3
nullFresh Laminaria Japonica after cleaning is joined and fills deionized water、Pharmaceutical grade ethanol、The reactor of pharmaceutical grade propylene glycol and pharmaceutical grade glycerol is pulled an oar，The dodecylbenzene sodium sulfonate as wetting and penetrating agent is added after making beating、Alkylphenol polyoxyethylene、Sorbitan fatty acid ester-60 and dimethicone，Fresh Laminaria Japonica、Deionized water、Pharmaceutical grade ethanol、Pharmaceutical grade propylene glycol、Pharmaceutical grade glycerol、Dodecylbenzene sodium sulfonate、Alkylphenol polyoxyethylene、Sorbitan fatty acid ester-60 and dimethicone are according to mass ratio 18:18:20:15:28:0.2:0.3:0.3:0.2，Soak 46 hours at 30 DEG C，In negative pressure 1.0Mpa，Distillation recovery part organic solvent at temperature 55 DEG C，Pressure filter adopts 2500 order filter clothes to carry out filter pressing，Gained filtrate、Sorbitan fatty acid ester-30、Dimethicone、Arginine、Aspartic acid、Glutamic acid、Valine、Leucine、Isoleucine、Serine、Glycine、Alanine、Threonine、Sodium lactate、Citric acid、Glycerol and 1,3 butanediols mix according to mass ratio 35:25:20:2:2:1:2:2:1:1:1:2:2:1:1:1:1，After stirring，Adding potassium hydroxide adjusts pH value to be neutral，It is Sargassum face cleaning nourishing breast.
Embodiment 4
nullFresh Laminaria Japonica after cleaning is joined and fills deionized water、Pharmaceutical grade ethanol、The reactor of pharmaceutical grade propylene glycol and pharmaceutical grade glycerol is pulled an oar，The dodecylbenzene sodium sulfonate as wetting and penetrating agent is added after making beating、Alkylphenol polyoxyethylene、Sorbitan fatty acid ester-60 and dimethicone，Fresh Laminaria Japonica、Deionized water、Pharmaceutical grade ethanol、Pharmaceutical grade propylene glycol、Pharmaceutical grade glycerol、Dodecylbenzene sodium sulfonate、Alkylphenol polyoxyethylene、Sorbitan fatty acid ester-60 and dimethicone are according to mass ratio 18:18:20:15:28:0.2:0.3:0.3:0.2，Soak 46 hours at 30 DEG C，In negative pressure 1.0Mpa，Distillation recovery part organic solvent at temperature 55 DEG C，Pressure filter adopts 2500 order filter clothes to carry out filter pressing，Gained filtrate、Sorbitan fatty acid ester-30、Fatty alcohol-polyoxyethylene ether-7、Fatty alcohol-polyoxyethylene ether-9、Arginine、Aspartic acid、Glutamic acid、Valine、Leucine、Isoleucine、Serine、Glycine、Alanine、Threonine、Sodium lactate、Citric acid、Glycerol and 1,3 butanediols mix according to mass ratio 70:2:4:1:2:1:1:2:3:1:1:2:1:2:2:2:2:1，After stirring，Adding potassium hydroxide adjusts pH value to be neutral，It is Sargassum face cleaning nourishing breast.
Further illustrate below in conjunction with experimental data and the method have the benefit that
For the filtrate that Different Extraction Method on market is collected, carrying out the detection of Sargassum polysaccharides after oven drying at low temperature, testing result is table 1 such as.
Table 1
| Comminuting method | Water-boiling method | Pulverize water-boiling method | The inventive method | |
| Sargassum polysaccharides (%) | 10.2 | 18.2 | 26.4 | 42.1 |
Adopt Sargassum polysaccharides content in the seaweed extracted liquor of this method the highest as can be seen from Table 1.
1 physical data
Inventor collects 300 examples in May, 2014 altogether between in November, 2015, age women between 28 to 42 years old, does effectiveness comparison for common face cleaning nourishing breast (except not adding seaweed extracted liquor, other manufacture method is identical with embodiment 4), embodiment 4.
1.2 experimental techniques
First with warm water, face is drenched, then cleansing milk is squeezed in the centre of the palm, in the centre of the palm, cleansing milk is rubbed with the hands and bubble, after foaming, by facial milk cleanser uniform application in facial skin, massage facial skin 2 minutes gently back and forth with the form looped clockwise, rinse well with water, every day 1 time, within 4 months, be a cycle.
1.3 experimental designs
300 people are divided into 2 groups, often organize 150 people and test respectively.
2 experimental results
Common face cleaning nourishing breast (except not adding seaweed extracted liquor, other manufacture method is identical with embodiment 2) investigation satisfaction is 70.3%；It is 85.6% that embodiment 2 investigates satisfaction；Be satisfied with standard: to no skin irritation, substantially feel comfortably cool after using, soft, without greasy feeling, skin gloss is flexible.
3 discuss
Testing just for the product of the different manufacturers Different Extraction Method can collected on market, done Sargassum polysaccharides detection, being not necessarily that certain city field energy is collected is best, and notebook data can only illustrate most like products that product of the present invention is better than on market to collect.
Claims (5)
1. one kind utilizes the method that seaweed extracted liquor prepares Sargassum face cleaning nourishing breast, it is characterised in that carry out according to following steps:
1), fresh Sargassum is cleaned standby, or dry seaweed be dipped to fresh Sargassum moisture consistent state and clean standby, the alternate products that this step obtains is called A product；
2), deionized water, organic solvent and product A are added separately in reactor, pull an oar in the lump；
3), beaten and added wetting and penetrating agent after slurry, soaked 12～72 hours at 20～45 DEG C；
4), low-temp low-pressure Distillation recovery part organic solvent: vapo(u)rizing temperature is 45～65 DEG C, and distillation pressure is-0.5～-1.2Mpa；
5), filter pressing obtain Sargassum slag and filtrate, described filtrate is seaweed extracted liquor；
6), by described seaweed extracted liquor, surfactant and nutrient substance according to certain mass ratio mixing, after stirring, being cooled to room temperature, products obtained therefrom is called B product；
7), with potassium hydroxide adjusting B product pH value to neutral, products obtained therefrom is Sargassum face cleaning nourishing breast；
Wherein the mass ratio of A product, deionized water, organic solvent and wetting and penetrating agent is 5～30:10～85:10～85:0.1～5;The mass ratio of seaweed extracted liquor, surfactant and nutrient substance is 5～80:1～65:1～65.
2. utilize the method that seaweed extracted liquor prepares Sargassum face cleaning nourishing breast as claimed in claim 1, it is characterised in that: described organic solvent is the two or more of a kind of or arbitrary proportion in pharmaceutical grade ethanol, pharmaceutical grade propylene glycol and pharmaceutical grade glycerol.
null3. utilize the method that seaweed extracted liquor prepares Sargassum face cleaning nourishing breast as claimed in claim 1，It is characterized in that: described wetting and penetrating agent is dodecylbenzene sodium sulfonate、Sodium lauryl sulphate、Alkylphenol polyoxyethylene、Sorbitan fatty acid ester-20、Sorbitan fatty acid ester-30、Sorbitan fatty acid ester-80、Polyoxyethylene 20 sorbitan monolaurate-20、Polyoxyethylene 20 sorbitan monolaurate-40、Polyoxyethylene 20 sorbitan monolaurate-60、Polyoxyethylene 20 sorbitan monolaurate-80、Fatty alcohol-polyoxyethylene ether-3、Fatty alcohol-polyoxyethylene ether-4、Fatty alcohol-polyoxyethylene ether-5、Fatty alcohol-polyoxyethylene ether-7、Fatty alcohol-polyoxyethylene ether-9、Fatty alcohol-polyoxyethylene ether-15、Fatty alcohol-polyoxyethylene ether-20、A kind of or arbitrary proportion in fatty alcohol-polyoxyethylene ether-23 and dimethicone two or more；Described surfactant is dodecylbenzene sodium sulfonate, sorbitan fatty acid ester-20, sorbitan fatty acid ester-30, sorbitan fatty acid ester-80, polyoxyethylene 20 sorbitan monolaurate-20, polyoxyethylene 20 sorbitan monolaurate-40, polyoxyethylene 20 sorbitan monolaurate-60, polyoxyethylene 20 sorbitan monolaurate-80, fatty alcohol-polyoxyethylene ether-3, fatty alcohol-polyoxyethylene ether-4, fatty alcohol-polyoxyethylene ether-5, fatty alcohol-polyoxyethylene ether-7, fatty alcohol-polyoxyethylene ether-9, fatty alcohol-polyoxyethylene ether-15, fatty alcohol-polyoxyethylene ether-20, a kind of or arbitrary proportion in fatty alcohol-polyoxyethylene ether-23 and dimethicone two or more；Described nutrient substance is the two or more of a kind of or arbitrary proportion in arginine, aspartic acid, glutamic acid, valine, leucine, isoleucine, serine, glycine, alanine, threonine, sodium lactate, citric acid, glycerol and 1,3 butanediols.
4. utilize the method that seaweed extracted liquor prepares Sargassum face cleaning nourishing breast as claimed in claim 1, it is characterised in that: described Sargassum refers to: a kind of or arbitrary proportion in Thallus Laminariae (Thallus Eckloniae), Thallus Porphyrae, Thallus Laminariae (Thallus Eckloniae), opotism and Entermorpha two or more.
5. utilize the method that seaweed extracted liquor prepares Sargassum face cleaning nourishing breast as claimed in claim 1, it is characterised in that: described in step 5), pressure filter selects filter cloth aperture to be 1200～4500 orders.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610189960.6A CN105726411A (en) | 2016-03-30 | 2016-03-30 | Method for preparing seaweed nourishing cleanser by utilizing seaweed extract |
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| CN201610189960.6A CN105726411A (en) | 2016-03-30 | 2016-03-30 | Method for preparing seaweed nourishing cleanser by utilizing seaweed extract |
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| CN105726411A true CN105726411A (en) | 2016-07-06 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106509652A (en) * | 2016-11-08 | 2017-03-22 | 雅安职业技术学院 | Method for preparing diced pork in pot by use of microwave heating sterilization |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102641223A (en) * | 2011-02-18 | 2012-08-22 | 株式会社爱茉莉太平洋 | Cosmetic composition for improving skin tone or skin elasticity |
| CN103613674A (en) * | 2013-09-09 | 2014-03-05 | 华南农业大学 | Extraction method for astragalus polysacharin |
| CN104592409A (en) * | 2015-01-12 | 2015-05-06 | 陕西师范大学 | Method for extracting high-activity phellinus linteus polysaccharide at low pressure and low temperature |
| CN105395392A (en) * | 2015-11-19 | 2016-03-16 | 重庆维可健康咨询有限公司 | Anti-aging skin cream |
-
2016
- 2016-03-30 CN CN201610189960.6A patent/CN105726411A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102641223A (en) * | 2011-02-18 | 2012-08-22 | 株式会社爱茉莉太平洋 | Cosmetic composition for improving skin tone or skin elasticity |
| CN103613674A (en) * | 2013-09-09 | 2014-03-05 | 华南农业大学 | Extraction method for astragalus polysacharin |
| CN104592409A (en) * | 2015-01-12 | 2015-05-06 | 陕西师范大学 | Method for extracting high-activity phellinus linteus polysaccharide at low pressure and low temperature |
| CN105395392A (en) * | 2015-11-19 | 2016-03-16 | 重庆维可健康咨询有限公司 | Anti-aging skin cream |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106509652A (en) * | 2016-11-08 | 2017-03-22 | 雅安职业技术学院 | Method for preparing diced pork in pot by use of microwave heating sterilization |
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Application publication date: 20160706 |