CN105647683A - Fructus gleditsiae soap and preparing method thereof - Google Patents

Fructus gleditsiae soap and preparing method thereof Download PDF

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Publication number
CN105647683A
CN105647683A CN201610051730.3A CN201610051730A CN105647683A CN 105647683 A CN105647683 A CN 105647683A CN 201610051730 A CN201610051730 A CN 201610051730A CN 105647683 A CN105647683 A CN 105647683A
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China
Prior art keywords
fructus gleditsia
gelatin
benzalkonium bromide
methylisothiazolinone
stevioside
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覃永红
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Guangxi Nan Bazai Science And Technology Ltd
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Guangxi Nan Bazai Science And Technology Ltd
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    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C11D1/83—Mixtures of non-ionic with anionic compounds
    • C11D1/831—Mixtures of non-ionic with anionic compounds of sulfonates with ethers of polyoxyalkylenes without phosphates
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02—Inorganic compounds ; Elemental compounds
    • C11D3/04—Water-soluble compounds
    • C11D3/042—Acids
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/2003—Alcohols; Phenols
    • C11D3/2006—Monohydric alcohols
    • C11D3/2027—Monohydric alcohols unsaturated
    • C11D3/2031—Monohydric alcohols unsaturated fatty or with at least 8 carbon atoms in the alkenyl chain
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/2003—Alcohols; Phenols
    • C11D3/2065—Polyhydric alcohols
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/2075—Carboxylic acids-salts thereof
    • C11D3/2079—Monocarboxylic acids-salts thereof
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/22—Carbohydrates or derivatives thereof
    • C11D3/222—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
    • C11D3/225—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin etherified, e.g. CMC
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/26—Organic compounds containing nitrogen
    • C11D3/30—Amines; Substituted amines ; Quaternized amines
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/34—Organic compounds containing sulfur
    • C11D3/349—Organic compounds containing sulfur additionally containing nitrogen atoms, e.g. nitro, nitroso, amino, imino, nitrilo, nitrile groups containing compounds or their derivatives or thio urea
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/36—Organic compounds containing phosphorus
    • C11D3/362—Phosphates or phosphites
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/38—Products with no well-defined composition, e.g. natural products
    • C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/38—Products with no well-defined composition, e.g. natural products
    • C11D3/384—Animal products
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02—Anionic compounds
    • C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/14—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aliphatic hydrocarbons or mono-alcohols
    • C11D1/143—Sulfonic acid esters
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C11D1/72—Ethers of polyoxyalkylene glycols
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C11D1/72—Ethers of polyoxyalkylene glycols
    • C11D1/721—End blocked ethers

Abstract

The invention relates to fructus gleditsiae soap and a preparing method thereof. The soap is prepared from, by weight, 15-20% of fructus gleditsiae, 2-7% of sodium dodecyl sulfate, 5-10 parts of glycerin, 2-7% of stearic acid, 0.5-1% of vitamin A, 0.3-0.8% of gelatin, 2-4 % of phospholipid, 0.5-1% of mannitol, 1-5% of polyethylene glycol, 0.3-0.8% of hydroxymethyl cellulose, 0.1-0.5% of stevioside, 1-5% of cetostearyl alcohol, 0.1-0.5% of boric acid, 0.1-0.5% of benzalkonium bromide, 0.1-0.5% of methylisothiazolinone, 1-4% of polyoxyethylenated castor oil, 0.1-0.6% of poloxamer and the balance deionized water. The fructus gleditsiae is a natural raw material and has the weak-base and weak-acid characteristics; irritation to skin is small, and glycerin, gelatin and phospholipid can nourish the skin; boric acid has sterilization and disinfection functions. The soap does not irritate the skin, and can sterilize and disinfect the skin and nourish the skin.

Description

A kind of Fructus Gleditsia fancy soap and preparation method thereof
[technical field]
The present invention relates to a kind of hair conditioner.
[background technology]
Fancy soap, as the most common and most widely used personal cleansing articles for use of one, has the pluses and minuses of itself. The main component of some fancy soaps is sodium soap, and it is formed by oils and fats (vegetable oil or animal oil) saponification substantially. It is true that fatty acid and derivant thereof are most popular raw materials in cosmetics. But, owing to sodium soap has certain alkalescence (pH value is high), and skin surface is faintly acid, therefore, after using the fancy soap washing that Acid-Base strengths is high, the PH of skin surface has bigger rising, certain stimulation can be caused to cause the sensation of various discomfort the skin of hyperirritability, strong acid, highly basic also can wash away the lipid layer of skin surface simultaneously, make skin dry.
Fructus Gleditsia is the natural material of medicine food, health product, cosmetics and articles for washing, China's conventional washing articles for use. Li Shizhen (1518-1593 A.D.) Compendium of Material Medica have recorded the manufacture method of " soap group ": " in the raw high mountain of Fructus Gymnocladi Chinensis, the height of tree is big, and leaf such as wingceltis and Folium Gleditsiae are boiled and mash, and ball made by flour and all perfume (or spice), bath body face, de-sludging and greasy profit, is better than Fructus Gleditsia also ". Gleditsia sinensis Seeds contains abundant galactomannan gum and protein component, galactomannan gum is because of the rheological characteristic of its uniqueness, and it is used as thickening agent, stabilizer, binding agent, gellant, flotation agent, flocculant, dispersant etc., plant weak-alkaline and weak-acidic fancy soap, not affecting the recovery capability of skin itself, skin surface can recover original pH value after washing in 15-30 minute.
[summary of the invention]
For the deficiencies in the prior art, it is an object of the invention to provide a kind of Fructus Gleditsia fancy soap and preparation method thereof. described Fructus Gleditsia fancy soap is made up of the component of following weight parts: Fructus Gleditsia 15��20%, dodecyl sodium sulfate 2��7%, glycerol 5��10%, stearic acid 2��7%, vitamin A 0.5��1%, gelatin 0.3��0.8%, phosphatidase 2��4%, mannitol 0.5��1%, Polyethylene Glycol 1��5%, hydroxymethyl cellulose 0.3��0.8%, stevioside 0.1��0.5%, cetearyl alcohol 1��5%, boric acid 0.1��0.5%, benzalkonium bromide 0.1��0.5%, Methylisothiazolinone 0.1��0.5%, polyoxyethylene castor oil 1��4%, poloxamer 0.1��0.6%, deionized water surplus.
Further, described Fructus Gleditsia fancy soap is made up of the component of following weight parts: Fructus Gleditsia 16��18%, dodecyl sodium sulfate 3��6%, glycerol 6��8%, stearic acid 3��6%, vitamin A 0.6��0.9%, gelatin 0.5��0.7%, phosphatidase 2 .5��3.5%, mannitol 0.6��0.9%, Polyethylene Glycol 2��4%, hydroxymethyl cellulose 0.4��0.7%, stevioside 0.2��0.4%, cetearyl alcohol 2��4%, boric acid 0.2��0.4%, benzalkonium bromide 0.2��0.4%, Methylisothiazolinone 0.2��0.4%, polyoxyethylene castor oil 2��3%, poloxamer 0.2��0.4%, deionized water surplus.
Specifically, described Fructus Gleditsia fancy soap is made up of the component of following weight parts: Fructus Gleditsia 17%, dodecyl sodium sulfate 4%, glycerol 7%, stearic acid 5%, vitamin A 0.8%, gelatin 0.6%, phosphatidase 3 %, mannitol 0.8%, Polyethylene Glycol 3%, hydroxymethyl cellulose 0.6%, stevioside 0.3%, cetearyl alcohol 3%, boric acid 0.3%, benzalkonium bromide 0.3%, Methylisothiazolinone 0.3%, polyoxyethylene castor oil 2.5%, poloxamer 0.3%, deionized water surplus.
The preparation method of the Fructus Gleditsia fancy soap of the present invention comprises the following steps:
(1). weigh raw material by formula;
(2) being cut into slices by Fructus Gleditsia dry product, insert in impregnating autoclave by Fructus Gleditsia sheet, add water soaking 8��12 hours, obtain Fructus Gleditsia leachate, Fructus Gleditsia sheet is all submerged wherein by institute's amount of water;
(3). Fructus Gleditsia leachate, mannitol, hydroxymethyl cellulose, Polyethylene Glycol, dodecyl sodium sulfate, stevioside, poloxamer, benzalkonium bromide and deionized water heat to 60��80 DEG C in aqueous phase pot, stir, in suction vacuum emulsification pot;
(4). glycerol, stearic acid, gelatin, phospholipid, boric acid, benzalkonium bromide and polyoxyethylene castor oil are added in oil phase pot and heats to 60��80 DEG C, stir, in suction vacuum emulsification pot;
(5). start vacuum equipment, under vacuum conditions homogenizing 35��80min, stir borehole cooling;
(6). vacuum emulsification pot adds vitamin A and Methylisothiazolinone when being cooled to 40��50 DEG C, stirs;
(7). continue cool to room temperature, discharging.
In sum, the invention have the advantage that Fructus Gleditsia is natural material, there is weak-alkaline and weak-acidic feature, the zest of skin is little; Olive oil, gelatin and phospholipid can nourishes rough skin, Methylisothiazolinone has a sterilizing effect, can life-time service, it is also possible to as the use of daily nursing. After using, skin lubrication, glossy, flexible.
[detailed description of the invention]
The following examples can help those skilled in the art more fully to understand the present invention, but cannot be intended to limit the present invention in any manner.
Embodiment 1
The weight portion of each raw material of Fructus Gleditsia fancy soap is: Fructus Gleditsia 20g, dodecyl sodium sulfate 7g, glycerol 10g, stearic acid 7g, retinol1 g, gelatin 0.8g, phosphatidase 4 g, mannitol 1g, Polyethylene Glycol 5g, hydroxymethyl cellulose 0.8g, stevioside 0.5g, cetearyl alcohol 5g, boric acid 0.5g, benzalkonium bromide 0.5g, Methylisothiazolinone 0.5g, polyoxyethylene castor oil 4g, poloxamer 0.6g. Deionized water 31.8g.
Preparation method: weigh raw material by formula, Fructus Gleditsia dry product is cut into slices, Fructus Gleditsia sheet is inserted in impregnating autoclave, add water soaking 9 hours, obtain Fructus Gleditsia leachate, Fructus Gleditsia sheet is all submerged wherein by institute's amount of water, then by Fructus Gleditsia leachate, mannitol, hydroxymethyl cellulose, Polyethylene Glycol, dodecyl sodium sulfate, stevioside, poloxamer, benzalkonium bromide and deionized water heat to 60 DEG C in aqueous phase pot, stir, in suction vacuum emulsification pot, by glycerol, stearic acid, gelatin, phospholipid, boric acid, benzalkonium bromide and polyoxyethylene castor oil and addition oil phase pot heat to 60 DEG C, stir, in suction vacuum emulsification pot,Start vacuum equipment, under vacuum conditions homogenizing 80min, stir borehole cooling; Vacuum emulsification pot adds vitamin A and Methylisothiazolinone when being cooled to 40 DEG C, stirs; Continue cool to room temperature, discharging.
Embodiment 2
The weight portion of each raw material of Fructus Gleditsia fancy soap is: Fructus Gleditsia 15g, dodecyl sodium sulfate 2g, glycerol 5g, stearic acid 2g, vitamin A 0.5g, gelatin 0.3g, phosphatidase 2 g, mannitol 0.5g, Polyethylene Glycol 1g, hydroxymethyl cellulose 0.3g, stevioside 0.1g, cetearyl alcohol 1g, boric acid 0.1g, benzalkonium bromide 0.1g, Methylisothiazolinone 0.1g, polyoxyethylene castor oil 1g, poloxamer 0.1g, deionized water 68.9.
Preparation method: weigh raw material by formula, Fructus Gleditsia dry product is cut into slices, Fructus Gleditsia sheet is inserted in impregnating autoclave, add water soaking 10 hours, obtain Fructus Gleditsia leachate, Fructus Gleditsia sheet is all submerged wherein by institute's amount of water, then by Fructus Gleditsia leachate, mannitol, hydroxymethyl cellulose, Polyethylene Glycol, dodecyl sodium sulfate, stevioside, poloxamer, benzalkonium bromide and deionized water heat to 80 DEG C in aqueous phase pot, stir, in suction vacuum emulsification pot, by glycerol, stearic acid, gelatin, phospholipid, boric acid, benzalkonium bromide and polyoxyethylene castor oil and addition oil phase pot heat to 80 DEG C, stir, in suction vacuum emulsification pot, start vacuum equipment, under vacuum conditions homogenizing 35min, stir borehole cooling, vacuum emulsification pot adds vitamin A and Methylisothiazolinone when being cooled to 50 DEG C, stirs, continue cool to room temperature, discharging.
Embodiment 3
The weight portion of each raw material of Fructus Gleditsia fancy soap is: Fructus Gleditsia 18g, dodecyl sodium sulfate 6g, glycerol 8g, stearic acid 6g, vitamin A 0.9g, gelatin 0.7g, phosphatidase 3 .5g, mannitol 0.9g, Polyethylene Glycol 4g, hydroxymethyl cellulose 0.7g, stevioside 0.4g, cetearyl alcohol 4g, boric acid 0.4g, benzalkonium bromide 0.4g, Methylisothiazolinone 0.4g, polyoxyethylene castor oil 3g, poloxamer 0.4g, deionized water 42.3g.
Preparation method: weigh raw material by formula, Fructus Gleditsia dry product is cut into slices, Fructus Gleditsia sheet is inserted in impregnating autoclave, add water soaking 11 hours, obtain Fructus Gleditsia leachate, Fructus Gleditsia sheet is all submerged wherein by institute's amount of water, then by Fructus Gleditsia leachate, mannitol, hydroxymethyl cellulose, Polyethylene Glycol, dodecyl sodium sulfate, stevioside, poloxamer, benzalkonium bromide and deionized water heat to 72 DEG C in aqueous phase pot, stir, in suction vacuum emulsification pot, by glycerol, stearic acid, gelatin, phospholipid, boric acid, benzalkonium bromide and polyoxyethylene castor oil and addition oil phase pot heat to 77 DEG C, stir, in suction vacuum emulsification pot, start vacuum equipment, under vacuum conditions homogenizing 55min, stir borehole cooling, vacuum emulsification pot adds vitamin A and Methylisothiazolinone when being cooled to 41 DEG C, stirs, continue cool to room temperature, discharging.
Embodiment 4
The weight portion of each raw material of Fructus Gleditsia fancy soap is: Fructus Gleditsia 16g, dodecyl sodium sulfate 3g, glycerol 6g, stearic acid 3g, vitamin A 0.6g, gelatin 0.5g, phosphatidase 2 .5g, mannitol 0.6g, Polyethylene Glycol 2g, hydroxymethyl cellulose 0.4g, stevioside 0.2g, cetearyl alcohol 2g, boric acid 0.2g, benzalkonium bromide 0.2g, Methylisothiazolinone 0.2g, polyoxyethylene castor oil 2g, poloxamer 0.2g, deionized water 60.4g.
Preparation method: weigh raw material by formula;Raw material is weighed by formula, Fructus Gleditsia dry product is cut into slices, Fructus Gleditsia sheet is inserted in impregnating autoclave, add water soaking 9 hours, obtain Fructus Gleditsia leachate, Fructus Gleditsia sheet is all submerged wherein by institute's amount of water, then by Fructus Gleditsia leachate, mannitol, hydroxymethyl cellulose, Polyethylene Glycol, dodecyl sodium sulfate, stevioside, poloxamer, benzalkonium bromide and deionized water heat to 71 DEG C in aqueous phase pot, stir, in suction vacuum emulsification pot, by glycerol, stearic acid, gelatin, phospholipid, boric acid, benzalkonium bromide and polyoxyethylene castor oil and addition oil phase pot heat to 76 DEG C, stir, in suction vacuum emulsification pot, start vacuum equipment, under vacuum conditions homogenizing 50min, stir borehole cooling, vacuum emulsification pot adds vitamin A and Methylisothiazolinone when being cooled to 44 DEG C, stirs, continue cool to room temperature, discharging.
Embodiment 5
The weight portion of each raw material of Fructus Gleditsia fancy soap is: Fructus Gleditsia 17g, dodecyl sodium sulfate 4g, glycerol 7g, stearic acid 5g, vitamin A 0.8g, gelatin 0.6g, phosphatidase 3 g, mannitol 0.8g, Polyethylene Glycol 3g, hydroxymethyl cellulose 0.6g, stevioside 0.3g, cetearyl alcohol 3g, boric acid 0.3g, benzalkonium bromide 0.3g, Methylisothiazolinone 0.3g, polyoxyethylene castor oil 2.5g, poloxamer 0.3g, deionization 51.2g.
Preparation method: weigh raw material by formula, raw material is weighed by formula, Fructus Gleditsia dry product is cut into slices, Fructus Gleditsia sheet is inserted in impregnating autoclave, add water soaking 11 hours, obtain Fructus Gleditsia leachate, Fructus Gleditsia sheet is all submerged wherein by institute's amount of water, then by Fructus Gleditsia leachate, mannitol, hydroxymethyl cellulose, Polyethylene Glycol, dodecyl sodium sulfate, stevioside, poloxamer, benzalkonium bromide and deionized water heat to 73 DEG C in aqueous phase pot, stir, in suction vacuum emulsification pot, by glycerol, stearic acid, gelatin, phospholipid, boric acid, benzalkonium bromide and polyoxyethylene castor oil and addition oil phase pot heat to 75 DEG C, stir, in suction vacuum emulsification pot, start vacuum equipment, under vacuum conditions homogenizing 53min, stir borehole cooling, vacuum emulsification pot adds vitamin A and Methylisothiazolinone when being cooled to 47 DEG C, stirs, continue cool to room temperature, discharging.
Soothing effect is tested
Compare with the product obtained by embodiment 1��5 and certain commercially available product. Experimenter is the women of routine use skin nursing products. 60 experimenters being randomly divided into 6 groups, indices is provided 0-10 and divides, 10 points of representatives are the most satisfied, and 0 point represents dissatisfied. Result is as shown in table 1. Can drawing, skin is had better maintenance effect by the Fructus Gleditsia fancy soap of the present invention.
Table 1:
Embodiment 1 Embodiment 2 Embodiment 3 Embodiment 4 Embodiment 5 Commercially available product
Cleannes 8.6 8.0 8.1 8.6 8.4 7.6
Use rear comfort level 8.9 8.3 8.6 8.8 8.6 7.6
Moisture retention 8.5 8.2 8.6 8.9 8.2 7.0
Although, above the present invention is described in detail with a general description of the specific embodiments, but on basis of the present invention, it is possible to it is made some modifications or improvements, and this will be apparent to those skilled in the art. Therefore, these modifications or improvements without departing from theon the basis of the spirit of the present invention, belong to the scope of protection of present invention.

Claims (4)

1. a Fructus Gleditsia fancy soap, it is characterized in that, it is made up of the component of following weight parts: Fructus Gleditsia 15��20%, dodecyl sodium sulfate 2��7%, glycerol 5��10%, stearic acid 2��7%, vitamin A 0.5��1%, gelatin 0.3��0.8%, phosphatidase 2��4%, mannitol 0.5��1%, Polyethylene Glycol 1��5%, hydroxymethyl cellulose 0.3��0.8%, stevioside 0.1��0.5%, cetearyl alcohol 1��5%, boric acid 0.1��0.5%, benzalkonium bromide 0.1��0.5%, Methylisothiazolinone 0.1��0.5%, polyoxyethylene castor oil 1��4%, poloxamer 0.1��0.6%, deionized water surplus.
2. Fructus Gleditsia fancy soap according to claim 1, it is characterized in that, it is made up of the component of following weight parts: Fructus Gleditsia 16��18%, dodecyl sodium sulfate 3��6%, glycerol 6��8%, stearic acid 3��6%, vitamin A 0.6��0.9%, gelatin 0.5��0.7%, phosphatidase 2 .5��3.5%, mannitol 0.6��0.9%, Polyethylene Glycol 2��4%, hydroxymethyl cellulose 0.4��0.7%, stevioside 0.2��0.4%, cetearyl alcohol 2��4%, boric acid 0.2��0.4%, benzalkonium bromide 0.2��0.4%, Methylisothiazolinone 0.2��0.4%, polyoxyethylene castor oil 2��3%, poloxamer 0.2��0.4%, deionized water surplus.
3. Fructus Gleditsia fancy soap according to claim 2, it is characterized in that, be made up of the component of following weight parts: Fructus Gleditsia 17%, dodecyl sodium sulfate 4%, glycerol 7%, stearic acid 5%, vitamin A 0.8%, gelatin 0.6%, phosphatidase 3 %, mannitol 0.8%, Polyethylene Glycol 3%, hydroxymethyl cellulose 0.6%, stevioside 0.3%, cetearyl alcohol 3%, boric acid 0.3%, benzalkonium bromide 0.3%, Methylisothiazolinone 0.3%, polyoxyethylene castor oil 2.5%, poloxamer 0.3%, deionized water surplus.
4. the preparation method of the Fructus Gleditsia fancy soap according to claims 1 to 3 any one, it is characterised in that comprise the following steps:
(1). weigh raw material by formula;
(2) being cut into slices by Fructus Gleditsia dry product, insert in impregnating autoclave by Fructus Gleditsia sheet, add water soaking 8��12 hours, obtain Fructus Gleditsia leachate, Fructus Gleditsia sheet is all submerged wherein by institute's amount of water;
(3). Fructus Gleditsia leachate, mannitol, hydroxymethyl cellulose, Polyethylene Glycol, dodecyl sodium sulfate, stevioside, poloxamer, benzalkonium bromide and deionized water heat to 60��80 DEG C in aqueous phase pot, stir, in suction vacuum emulsification pot;
(4). glycerol, stearic acid, gelatin, phospholipid, boric acid, benzalkonium bromide and polyoxyethylene castor oil are added in oil phase pot and heats to 60��80 DEG C, stir, in suction vacuum emulsification pot;
(5). start vacuum equipment, under vacuum conditions homogenizing 35��80min, stir borehole cooling;
(6). vacuum emulsification pot adds vitamin A and Methylisothiazolinone when being cooled to 40��50 DEG C, stirs;
(7). continue cool to room temperature, discharging.
CN201610051730.3A 2016-01-26 2016-01-26 Fructus gleditsiae soap and preparing method thereof Pending CN105647683A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109528623A (en) * 2018-12-29 2019-03-29 珠海横琴亘德生物科技有限公司 It is a kind of to wash shield soap for clean skin care

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0186148A2 (en) * 1984-12-24 1986-07-02 The B.F. GOODRICH Company Toilet soap containing polymeric thickener
CN100999700A (en) * 2006-01-13 2007-07-18 赖焕荣 Perfumed soap composition and preparation method thereof
CN102899198A (en) * 2012-09-13 2013-01-30 青岛文创科技有限公司 Moisture-retaining whitening handmade soap
CN104293546A (en) * 2014-09-26 2015-01-21 蒋坤锷 Deep cleaning soap
CN104293545A (en) * 2014-09-26 2015-01-21 蒋坤锷 Natural Gleditsia sinensis toilet soap

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0186148A2 (en) * 1984-12-24 1986-07-02 The B.F. GOODRICH Company Toilet soap containing polymeric thickener
CN100999700A (en) * 2006-01-13 2007-07-18 赖焕荣 Perfumed soap composition and preparation method thereof
CN102899198A (en) * 2012-09-13 2013-01-30 青岛文创科技有限公司 Moisture-retaining whitening handmade soap
CN104293546A (en) * 2014-09-26 2015-01-21 蒋坤锷 Deep cleaning soap
CN104293545A (en) * 2014-09-26 2015-01-21 蒋坤锷 Natural Gleditsia sinensis toilet soap

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109528623A (en) * 2018-12-29 2019-03-29 珠海横琴亘德生物科技有限公司 It is a kind of to wash shield soap for clean skin care
CN109528623B (en) * 2018-12-29 2021-09-24 珠海横琴亘德生物科技有限公司 Washing and caring soap for cleaning and caring skin

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Application publication date: 20160608