CN100999700A - Perfumed soap composition and preparation method thereof - Google Patents

Perfumed soap composition and preparation method thereof Download PDF

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Publication number
CN100999700A
CN100999700A CN 200610144573 CN200610144573A CN100999700A CN 100999700 A CN100999700 A CN 100999700A CN 200610144573 CN200610144573 CN 200610144573 CN 200610144573 A CN200610144573 A CN 200610144573A CN 100999700 A CN100999700 A CN 100999700A
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Prior art keywords
perfumed soap
agent
weight percentage
soap composition
composition according
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CN 200610144573
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Chinese (zh)
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赖焕荣
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Individual
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Abstract

The invention relates to a soft body soap composition without fatty acid salt, which comprises 18 to 30 weight percent of at least one gel, 45 to 80 weight percent of at least one surfactant and the balance of water; the gelling agent is preferably gelatin, or other chemical, mixture or compound having similar properties to gelatin. The invention also relates to a method for preparing the soap containing the soap composition, and the prepared soap is soft and elastic, can be compressed, extended or expanded, can float on the water surface and is not easy to sink into the water bottom.

Description

Perfumed soap composition and preparation method thereof
Technical field
The present invention relates to a kind of article for washing, particularly a kind of perfumed soap composition.
Background technology
Perfumed soap is a kind of daily necessities of well-known and widespread use.People are in order to improve the quality of soap, as the foaming power of perfumed soap and to the easy property handled of foamy, have done continuous trial.Be soil removability that improves and improve perfumed soap and the aesthetics that promotes perfumed soap, people have also made unremitting effort.
U.S. Patent application bulletin US2005/0107273A1 discloses a kind of perfumed soap composition with low abradability.This patent application discloses a kind of opaque Dirt removing block, wherein includes negatively charged ion soap, at least a synthetic surfactant, specific main gelifying agent, contains the wetting agent of glycerine and water, and these compositions each have concrete weight percentage.This U. S. application has openly also been mentioned the various types of perfumed soap compositions in United States Patent (USP) formerly and the application openly.
Perfumed soap composition of the prior art is all harder, and this is because up to the present all contain hard acid ester salt composition usually in the perfumed soap, and the present invention develops a kind of software perfumed soap and replaces traditional hardware perfumed soap for overcoming this defective just.
Summary of the invention
An object of the present invention is to provide a kind of softness, flexible and compressible and the software perfumed soap and the manufacture method thereof that extend; In addition, another object of the present invention provides a kind of software perfumed soap of bubbling through the water column, and, when using the composition wiping health of this software perfumed soap, can produce foam with cleaning action.
For making perfumed soap composition of the present invention, need two kinds of main basal component, i.e. gelatin (or other chemicals, mixture or compound of having similar quality with gelatin) and tensio-active agent.Gelatin is not only given perfumed soap with certain shape, and makes perfumed soap have elasticity and being compressed or extending.Also can comprise the composition that other is fit in the perfumed soap composition of the present invention.
The invention provides a kind of perfumed soap composition that does not contain ester fat hydrochlorate, perfumed soap wherein is the form of opaque blocks of solid, and in use can produce foam, and this soap bars has elasticity usually, and can be compressed and extend, and said composition includes:
A) at least a gelifying agent, it is counted by weight percentage and accounts for 18%~30%, and this gelifying agent is a gelatin, or other chemicals, mixture or the compound that have similar quality with gelatin;
B) have a kind of tensio-active agent at least, it is counted by weight percentage and accounts for 45%~80%; And
C) water, surplus.
At least a tensio-active agent in this perfumed soap composition provided by the invention comprises the tensio-active agent of following each component:
Sodium Lauryl Sulphate BP/USP is counted by weight percentage and is accounted for 10%~20%;
Zetesol NL is counted by weight percentage and is accounted for 15%~25%;
Cocoamidopropyl betaine is counted by weight percentage and is accounted for 15%~25%;
Coconut oil diethanol amide is counted by weight percentage and is accounted for 5%~10%.
At least a gelifying agent in this perfumed soap composition provided by the invention preferably contains gelatin and the water of being made up of modified amino acid, at room temperature forming the yellow crystal solid, and can be dissolved in and forms yellow solution in the hot water.The efflorescence value of gelatin (bloom number) 100 to 250 or more than, the efflorescence value characterizes the gel strength of gelatin, efflorescence value high viscosity more is big more.Gelatin belongs to viscose glue, hydrophilic colloid and derivative thereof and protein-based in chemical classification.Gelatin can be used as tackiness agent, bacteriolysant and thickening material in aqueous solution.So gelatin is used so that formed product.When gelatin is dissolved in the hot water, it will discharge fragrance and have viscosity, and when cooling, product will keep shape and hardening.When product contacts with water at low temperatures, just can dissolve.Other can be in order to replace gelatin to use or to use simultaneously with gelatin with the same or analogous raw material of gelatin on function, these raw materials comprise viscose glue, hydrophilic colloid and derivative thereof and protein, as agar-agar, Natvosol, protein, xanthan gum, pectin, guar gum, cellulose gum, Collagen Hydrolysate, carrageenin, Lalgine, dextran and chitin.
For making perfumed soap have different foaming powers, elasticity and/or intensity of compression or extensibility, gelatin and surfactant concentrations are just different.So, increase the consumption of gelatin and keep other composition constant, will reduce elasticity and the intensity of compression and the extensibility of product.Increase the consumption of any tensio-active agent and keep other composition constant, increase the foam that makes product simultaneously that its elasticity and intensity of compression and extensibility also increase, thereby make product soft more and compress than being easier to.
Tensio-active agent at room temperature is solid or liquid preferably, and has foaming power and foam characteristics, and the effect of cleaning skin and hair is arranged, and has the surface tension of removing the smeary performance and lowering water as emulsifying agent.This tensio-active agent can be one or both in amphoterics, cats product, anion surfactant and the nonionogenic tenside.Except that above said tensio-active agent, other has the raw material with the same or similar function of above-mentioned tensio-active agent, also can be as replacing this tensio-active agent.
Can also comprise one or more following an amount of compositions in this perfumed soap composition provided by the invention:
Have a kind of skin-care agent or wetting agent of making at least;
Has a kind of sanitas at least;
Has a kind of cakingagent at least;
Have a kind of pH control or conditioning agent at least;
Has a kind of oxidative bleaching agent at least;
Has a kind of essence at least;
And has a kind of tinting material at least.
Described skin-care agent or wetting agent preferably glycerine, it at room temperature is a colourless liquid, can be used as wetting agent.Except that glycerine, other on function with the same or analogous raw material of glycerine, also can replace glycerine to use.
Preferred Tegosept M of described sanitas or propylben, this sanitas at room temperature is solid or liquid, and is widely used as microbiological antiseptic.Except that foregoing preservatives, other on function with the same or analogous raw material of this sanitas, also can replace using.
Described cakingagent preferably polyethylene alcohol, it is often used as membrane-forming agent, tackiness agent and/or thickening material.Polyvinyl alcohol is the colourless crystallization solid in room temperature, can be dissolved in hot water.Except that polyvinyl alcohol, other raw material such as Polyvinylpyrolidone (PVP), Polyvinylpyrolidone (PVP)/vinyl acetate copolymer or other on function with the same or analogous raw material of polyvinyl alcohol, can be as replacing polyvinyl alcohol.
Described pH control or conditioning agent can adopt trolamine, because of it has weakly alkaline.Except that trolamine, other raw material such as sodium hydroxide, potassium hydroxide or other weak base or strong alkali compound, or other on function with the same or analogous raw material of trolamine, can be as replacing trolamine.
Described oxidative bleaching agent can adopt chlorinated lime, and as making the product bleaching, this SYNTHETIC OPTICAL WHITNER can be solid or liquid.Except that chlorinated lime, other on function with the same or analogous raw material of chlorinated lime, can be as replacing chlorinated lime.
Can also comprise one or more essence and flavoring agents in the prescription of this software perfumed soap, use so that perfumed soap has the effect of " perfume ", and can also comprise one or more tinting materials so that perfumed soap has required color.
Described skin-care agent or the wetting agent weight percentage in composition is 3~8%; The weight percentage of described sanitas in composition is 0.3~0.5%; The weight percentage of described cakingagent in composition is 2~3%; Described pH control or the weight percentage of conditioning agent in composition are 1~2%; The weight percentage of described oxygenant in composition is 1~2%; The weight percentage of described spices in composition is 0.5~2%; The weight percentage of described tinting material in composition is 0.1~0.2%; And the weight percentage of water in composition is 25~40%.
Preferably, the prescription of perfumed soap composition of the present invention is as follows:
Composition Weight percent
Gelatin 18-30
Glycerine 3-8
Zetesol NL 15-25
Cocoamidopropyl betaine 15-25
Coconut oil diethanol amide 5-10
Sodium Lauryl Sulphate BP/USP 10-20
Tegosept M 0.2-0.3
Propylben 0.1-0.2
Essence 0.5-2
Polyvinyl alcohol 2-3
Trolamine 1-2
Chlorinated lime 1-2
Tinting material 0.1-0.2
Water is added into 100%
Above-mentioned per-cent umber is to count (w/w%) frequently with the weight percent of the whole composition of single ingredients constitute to characterize.
The manufacture method of software perfumed soap provided by the invention is: at first, polyvinyl alcohol is dissolved in the hot water until obtaining limpid solution.Other prepares a phase solution, and this solution contains 85 ℃ water, and glycerine and sanitas are added in the solution successively, dissolves fully until all raw materials, gelatin is added this solution and dissolving formation yellow solution again.Subsequently this yellow solution is joined in the limpid polyvinyl alcohol solution, add trolamine and chlorinated lime again, until dissolving fully.At last, add all tensio-active agents until dissolving fully and solution at room temperature being placed one hour until obtaining limpid yellow solution.When solution is cooled to about 50 ℃, pours into this yellow solution in the mould and place about five hours so that its curing.From mould, take out this and contain the gelinite of soap composition, at room temperature air-dry 2~3 days.Last moulding promptly gets perfumed soap of the present invention.
In the above-mentioned manufacturing perfumed soap composition process of the present invention, when yellow solution being cooled to about 50 ℃, stir solution so that the product that inclusion of air wherein, obtains at last also can be bubbled through the water column because of having air to be coated wherein to have more elasticity.
Not fatty hydrochlorate in the perfumed soap composition provided by the invention, prepared is a kind of software perfumed soap, can adhere in the plane, even vertically adhere to, this is because its surface has viscosity to a certain degree; This perfumed soap is soft flexible and can be compressed, extend or expand, and can bubble through the water column through the perfumed soap product that method of the present invention makes, and is difficult for sinking under water.
Embodiment
Take by weighing following compositions in following ratio:
Composition Weight percent
Gelatin 20
Glycerine 5
Zetesol NL 15
Cocoamidopropyl betaine 20
Coconut oil diethanol amide 5
Sodium Lauryl Sulphate BP/USP 15
Tegosept M 0.2
Propylben 0.1
Essence 1.0
Polyvinyl alcohol 2.5
Trolamine 1.5
Chlorinated lime 1.5
Tinting material 0.1
Water is added into 100%
Above-mentioned polyvinyl alcohol is dissolved in the hot water until obtaining limpid solution;
Other prepares a phase solution, and this solution contains 85 ℃ water, and glycerine and sanitas are added in the solution successively, dissolves fully until all raw materials, gelatin is added this solution and dissolving formation yellow solution again;
Subsequently this yellow solution is joined in the limpid polyvinyl alcohol solution, add trolamine and chlorinated lime again, until dissolving fully;
At last, add all tensio-active agents until dissolving fully and solution at room temperature being placed one hour until obtaining limpid yellow solution, when solution is cooled to about 50 ℃, stir solution so that inclusion of air wherein, is poured into this yellow solution in the mould then and placed about five hours so that its curing.From mould, take out this and contain the gelinite of soap composition, at room temperature air-dry 2~3 days.Last moulding promptly gets perfumed soap of the present invention.

Claims (19)

1. a perfumed soap composition that does not contain ester fat hydrochlorate is characterized in that, comprises:
(a) at least a gelifying agent of weight percentage 18%~30%;
(b) at least a tensio-active agent of weight percentage 45%~80%; And
(c) water of surplus.
2. perfumed soap composition according to claim 1 is characterized in that, described gelifying agent is to be selected from least a in gelatin, viscose glue, hydrophilic colloid and derivative thereof, the protein.
3. perfumed soap composition according to claim 1, it is characterized in that described gelifying agent is to be selected from least a in agar-agar, Natvosol, protein, xanthan gum, pectin, guar gum, cellulose gum, Collagen Hydrolysate, carrageenin, Lalgine, dextran, the chitin.
4. perfumed soap composition according to claim 1, it is characterized in that described at least a tensio-active agent is amphoterics, cats product, anion surfactant or the nonionogenic tenside that is solid or liquid state in the room temperature situation.
5. according to claim 1 or 4 described perfumed soap compositions, it is characterized in that described at least a tensio-active agent comprises:
Sodium Lauryl Sulphate BP/USP, weight percentage 10%~20%;
Zetesol NL, weight percentage 15%~25%;
Cocoamidopropyl betaine, weight percentage 15%~25%;
Coconut oil diethanol amide, weight percentage 5%~10%.
6. perfumed soap composition according to claim 1 is characterized in that, also comprises at least a following ingredients in the described perfumed soap composition:
At least a skin-care agent or the wetting agent of making;
At least a sanitas;
At least a cakingagent;
At least a pH control or conditioning agent;
At least a oxidative bleaching agent;
At least a essence; And
At least a tinting material.
7. perfumed soap composition according to claim 6 is characterized in that, described at least a nursing agent or wetting agent are glycerine.
8. perfumed soap composition according to claim 7 is characterized in that, the weight percentage of described at least a nursing agent or wetting agent is 3~8%.
9. perfumed soap composition according to claim 6 is characterized in that, described at least a sanitas is Tegosept M or propylben.
10. according to claim 6 or 8 described perfumed soap compositions, it is characterized in that the weight percentage of described at least a sanitas is 0.3~0.5%.
11. perfumed soap composition according to claim 6 is characterized in that, described at least a cakingagent is to be selected from least a in polyvinyl alcohol, Polyvinylpyrolidone (PVP), the Polyvinylpyrolidone (PVP)/vinyl acetate copolymer.
12., it is characterized in that the weight percentage of described at least a cakingagent is 2~3% according to claim 6 or 11 described perfumed soap compositions.
13. perfumed soap composition according to claim 6 is characterized in that, described at least a pH control or conditioning agent are trolamines.
14., it is characterized in that the weight percentage of described at least a pH control or conditioning agent is 1~2% according to claim 6 or 12 described perfumed soap compositions.
15. perfumed soap composition according to claim 6 is characterized in that, described at least a oxidative bleaching agent is a chlorinated lime.
16., it is characterized in that the weight percentage of described at least a oxidative bleaching agent is 1~2% according to claim 6 or 15 described perfumed soap compositions.
17. perfumed soap composition according to claim 6 is characterized in that, the weight percentage of described at least a essence is 0.5~2%.
18. a method for preparing the perfumed soap that contains the described perfumed soap composition of claim 1 is characterized in that, comprises following steps:
Take by weighing each component in the ratio that pre-determines;
Polyvinyl alcohol is dissolved in the hot water until obtaining limpid polyvinyl alcohol solution;
Other prepares a phase solution, and just glycerine and sanitas add in this solution of 85 ℃ of water temperatures successively until dissolving fully;
Gelatin is added this another phase solution to be dissolved fully until it;
This another phase solution is joined in the aforementioned polyvinyl alcohol solution;
Trolamine and chlorinated lime are joined in the above-mentioned mixing solutions;
Add tensio-active agent and arrive above-mentioned mixing solutions, the solution that obtains is at room temperature placed one hour until obtaining limpid yellow solution until dissolving fully;
Above-mentioned yellow solution is cooled to 50 ℃, is injected in the mould and placed five hours, until solidifying;
The gel that contains perfumed soap composition after from mould, taking out this and solidifying, and at room temperature placed 2 to 3 days, moulding makes perfumed soap.
19. according to the described method for preparing perfumed soap of claim 18, it is characterized in that, described yellow solution be cooled to 50 ℃ and inject mould before, stir this solution with to entrained air wherein.
CN 200610144573 2006-01-13 2006-11-02 Perfumed soap composition and preparation method thereof Pending CN100999700A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
HK06100625A HK1081060A2 (en) 2006-01-13 2006-01-13 Soap bar composition
HK06100625.7 2006-01-13

Publications (1)

Publication Number Publication Date
CN100999700A true CN100999700A (en) 2007-07-18

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103194330A (en) * 2013-03-30 2013-07-10 杭州师范大学 Environment-friendly potent hand soap
CN105647683A (en) * 2016-01-26 2016-06-08 广西南岜仔科技有限公司 Fructus gleditsiae soap and preparing method thereof
CN106420370A (en) * 2016-08-12 2017-02-22 古巧渝 Jelly soap and preparing method thereof
CN109234085A (en) * 2018-08-16 2019-01-18 惠州兆婷化妆品有限公司 A kind of floating soap and preparation method thereof
CN110791394A (en) * 2019-11-08 2020-02-14 张彩芳 Efficient decontamination soap and preparation method thereof

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103194330A (en) * 2013-03-30 2013-07-10 杭州师范大学 Environment-friendly potent hand soap
CN105647683A (en) * 2016-01-26 2016-06-08 广西南岜仔科技有限公司 Fructus gleditsiae soap and preparing method thereof
CN106420370A (en) * 2016-08-12 2017-02-22 古巧渝 Jelly soap and preparing method thereof
CN109234085A (en) * 2018-08-16 2019-01-18 惠州兆婷化妆品有限公司 A kind of floating soap and preparation method thereof
CN109234085B (en) * 2018-08-16 2020-08-25 惠州兆婷化妆品有限公司 Floating soap and preparation method thereof
CN110791394A (en) * 2019-11-08 2020-02-14 张彩芳 Efficient decontamination soap and preparation method thereof
CN110791394B (en) * 2019-11-08 2021-08-17 山东正基药业有限公司 Decontamination soap

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