CN105639557A - Propolis honey paste containing oregano essential oil obtained by subcritical CO2 extraction, and preparation method of propolis honey paste - Google Patents
Propolis honey paste containing oregano essential oil obtained by subcritical CO2 extraction, and preparation method of propolis honey paste Download PDFInfo
- Publication number
- CN105639557A CN105639557A CN201511035254.8A CN201511035254A CN105639557A CN 105639557 A CN105639557 A CN 105639557A CN 201511035254 A CN201511035254 A CN 201511035254A CN 105639557 A CN105639557 A CN 105639557A
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- Prior art keywords
- extraction
- subcritical
- quintessence oil
- herba origani
- vulgaris quintessence
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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- 238000000605 extraction Methods 0.000 title claims abstract description 72
- 240000007673 Origanum vulgare Species 0.000 title claims abstract description 31
- 241000241413 Propolis Species 0.000 title claims abstract description 27
- 235000012907 honey Nutrition 0.000 title claims abstract description 27
- 229940069949 propolis Drugs 0.000 title claims abstract description 27
- 238000002360 preparation method Methods 0.000 title claims abstract description 10
- 235000013628 Lantana involucrata Nutrition 0.000 title abstract 7
- 235000006677 Monarda citriodora ssp. austromontana Nutrition 0.000 title abstract 7
- 239000000341 volatile oil Substances 0.000 title abstract 6
- 238000000034 method Methods 0.000 claims abstract description 12
- 239000003292 glue Substances 0.000 claims description 26
- 235000004383 Origanum vulgare subsp. vulgare Nutrition 0.000 claims description 24
- 239000000284 extract Substances 0.000 claims description 15
- 238000000926 separation method Methods 0.000 claims description 12
- 239000000843 powder Substances 0.000 claims description 10
- 238000010298 pulverizing process Methods 0.000 claims description 10
- 230000001954 sterilising effect Effects 0.000 claims description 8
- 238000004659 sterilization and disinfection Methods 0.000 claims description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 6
- 238000011049 filling Methods 0.000 claims description 5
- 238000002156 mixing Methods 0.000 claims description 5
- 238000001291 vacuum drying Methods 0.000 claims description 5
- 238000007865 diluting Methods 0.000 claims description 3
- 239000004744 fabric Substances 0.000 claims description 2
- 230000000694 effects Effects 0.000 abstract description 6
- 208000003251 Pruritus Diseases 0.000 abstract description 4
- 208000028990 Skin injury Diseases 0.000 abstract description 4
- 239000003814 drug Substances 0.000 abstract description 3
- 206010061218 Inflammation Diseases 0.000 abstract description 2
- 230000003260 anti-sepsis Effects 0.000 abstract description 2
- 229940079593 drug Drugs 0.000 abstract description 2
- 210000001835 viscera Anatomy 0.000 abstract description 2
- 239000004480 active ingredient Substances 0.000 abstract 2
- 244000273928 Zingiber officinale Species 0.000 abstract 1
- 235000006886 Zingiber officinale Nutrition 0.000 abstract 1
- 235000008397 ginger Nutrition 0.000 abstract 1
- 239000003053 toxin Substances 0.000 abstract 1
- 231100000765 toxin Toxicity 0.000 abstract 1
- 108700012359 toxins Proteins 0.000 abstract 1
- 238000002372 labelling Methods 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 206010000087 Abdominal pain upper Diseases 0.000 description 1
- 239000004382 Amylase Substances 0.000 description 1
- 102000013142 Amylases Human genes 0.000 description 1
- 108010065511 Amylases Proteins 0.000 description 1
- 206010048768 Dermatosis Diseases 0.000 description 1
- 206010019345 Heat stroke Diseases 0.000 description 1
- 108060003951 Immunoglobulin Proteins 0.000 description 1
- 206010044565 Tremor Diseases 0.000 description 1
- 206010047700 Vomiting Diseases 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 235000019418 amylase Nutrition 0.000 description 1
- 150000001720 carbohydrates Chemical class 0.000 description 1
- -1 chromocor compound Chemical class 0.000 description 1
- 230000035622 drinking Effects 0.000 description 1
- 150000004676 glycans Chemical class 0.000 description 1
- 235000008216 herbs Nutrition 0.000 description 1
- 102000018358 immunoglobulin Human genes 0.000 description 1
- 230000010354 integration Effects 0.000 description 1
- 235000008935 nutritious Nutrition 0.000 description 1
- 239000002574 poison Substances 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 229920001282 polysaccharide Polymers 0.000 description 1
- 239000005017 polysaccharide Substances 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 208000017520 skin disease Diseases 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 230000008673 vomiting Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
The invention provides propolis honey paste containing oregano essential oil obtained by subcritical CO2 extraction, belonging to the technical field of bee products. The propolis honey paste is prepared from the following components in parts by weight: 5-20 parts of oregano essential oil obtained by subcritical CO2 extraction, 70-90 parts of honey and 5-20 parts of propolis. The invention also provides a preparation method and an edible method of the propolis honey paste containing the oregano essential oil obtained by subcritical CO2 extraction. After the honey which has the functions of soothing the five internal organs, resolving the hundred toxins and complementing the hundred medicines is blended with the oregano essential oil obtained by subcritical CO2 extraction, the product edibility is improved, and the effective active ingredients in the honey, the propolis and oregano can be maintained; the propolis honey paste has the functions of antisepsis and anti-inflammation, and also has an external use effect for skin injury, pruritus and the like; the oregano essential oil is extracted by a subcritical CO2 extraction method, so that the effective active ingredients in fresh ginger can be maintained, the operation is simple, and the extraction rate is high.
Description
Technical field
The present invention relates to bee product technical field, specifically a kind of containing subcritical CO2The bee glue honeyed paste of the Herba Origani Vulgaris quintessence oil of extraction and its preparation method.
Background technology
Being rich in carbohydrate, protein, amino acid, vitamins and other nutritious components in existing technology in honey, honey is also rich in immunoglobulin (Ig), amylase, chromocor compound, the active polysaccharide isoreactivity factor. Wild marjoram has loose trembling with fear and delivers, flu-prevention, the effects such as treatment heatstroke, stomachache, vomiting. China's traditional medicine thinks that wild marjoram is a kind of integration of drinking and medicinal herbs drink simultaneously, it is possible to clearing heat and detoxicating, intelligence development of refreshing oneself.
Summary of the invention
In view of this, it is desirable to provide a kind of subcritical CO2The Herba Origani Vulgaris quintessence oil of extraction.
For achieving the above object, the technical scheme of the present invention is achieved in that a kind of subcritical CO2The Herba Origani Vulgaris quintessence oil of extraction, subcritical CO2Extraction comprises the steps:
A wild marjoram is cleaned by () after, vacuum-drying, adopts pulverizer that wild marjoram is carried out pulverization process and obtains wild marjoram powder;
B wild marjoram powder 30-50 object screen cloth after pulverizing is sieved by ();
(c) subcritical CO2Extraction: extracting pressure 5-15MPa, extraction temperature 15-30 DEG C, CO2Flow 160-190L/h, extraction time 1-4h, obtains Herba Origani Vulgaris quintessence oil primary products;
D () carries out secondary separation through rectifying tower again, separating pressure is 10-20MPa, separation temperature 40-60 DEG C, obtains Herba Origani Vulgaris quintessence oil product through processed.
Further, described step (b) is sieved with 40 object screen clothes.
Further, described step (c) extracting pressure 8.6MPa, extraction temperature 20 DEG C, CO2Flow 180L/h, extraction time 2h.
Further, described step (d) separating pressure is 14MPa, separation temperature 50 DEG C.
Another technical problem that the present invention to be solved is: provide above-mentioned containing subcritical CO2The bee glue honeyed paste of the Herba Origani Vulgaris quintessence oil of extraction.
Above-mentioned containing subcritical CO2The bee glue honeyed paste of the Herba Origani Vulgaris quintessence oil of extraction, comprises each component of following weight part number: subcritical CO2Extract obtain Herba Origani Vulgaris quintessence oil 5-20 part, honey 70-90 part, propolis 5-20 part.
Further, each component of following weight part number is comprised: subcritical CO2Extract obtain Herba Origani Vulgaris quintessence oil 8-15 part, honey 70-80 part, propolis 8-15 part.
Further, each component of following weight part number is comprised: subcritical CO2Extract obtain Herba Origani Vulgaris quintessence oil 10 parts, honey 80 parts, propolis 10 parts.
Another technical problem that the present invention to be solved is: provide above-mentioned containing subcritical CO2The preparation method of the bee glue honeyed paste of the Herba Origani Vulgaris quintessence oil of extraction.
Above-mentioned containing subcritical CO2The preparation method of the bee glue honeyed paste of the Herba Origani Vulgaris quintessence oil of extraction, comprises the steps:
(1) subcritical CO2Extraction obtains Herba Origani Vulgaris quintessence oil;
(2) subcritical CO is taken by above-mentioned weight part number2Extract the Herba Origani Vulgaris quintessence oil, honey and the propolis that obtain, after mixing, carry out homogeneous;
(3) filling, pasteurize is carried out after homogeneous.
Further, the condition of pasteurize is 57 DEG C of sterilization 30min.
Another technical problem that the present invention to be solved is: provide above-mentioned containing subcritical CO2The eating method of the bee glue honeyed paste of the Herba Origani Vulgaris quintessence oil of extraction.
Above-mentioned containing subcritical CO2The eating method of the bee glue honeyed paste of the Herba Origani Vulgaris quintessence oil of extraction: once a day, each 10-20g, takes after diluting with water, and the mass ratio of bee glue honeyed paste and water is 1:5-10, continuous 7 days.
Relative to prior art, the present invention has following advantage:
(1) the present invention has advantage and positively effect be: honey five viscera settling, separates hundred poison, and hundred medicines, and propolis and subcritical CO2The Herba Origani Vulgaris quintessence oil of extraction is formulated together, improves product edibility, and the effective active composition in honey, propolis, wild marjoram is retained simultaneously; Owing to adopting technique scheme, product of the present invention has antisepsis and anti-inflammation, can outward for effects such as skin injury, itch.
(2) the present invention adopts subcritical CO2The method of extraction extracts Herba Origani Vulgaris quintessence oil, not only makes the effective active composition in wild marjoram be protected, and simple to operate, extraction yield height.
Embodiment
It should be noted that, when not conflicting, the embodiment in the present invention and the feature in embodiment can combine mutually.
Below in conjunction with embodiment, the present invention is described in detail.
Embodiment one
A kind of containing subcritical CO2The bee glue honeyed paste of the Herba Origani Vulgaris quintessence oil of extraction, comprises each component of following weight: subcritical CO2Extract obtain Herba Origani Vulgaris quintessence oil 10g, honey 80g, propolis 10g.
Above-mentioned containing subcritical CO2The preparation method of the bee glue honeyed paste of the Herba Origani Vulgaris quintessence oil of extraction, comprises the steps:
(1) subcritical CO2Extraction obtains Herba Origani Vulgaris quintessence oil, subcritical CO2Extraction step is as follows:
A 200g wild marjoram is cleaned by () after, vacuum-drying, adopts pulverizer that wild marjoram is carried out pulverization process and obtains wild marjoram powder;
B wild marjoram powder after pulverizing is sieved by () with 40 object screen clothes;
(c) subcritical CO2Extraction: extracting pressure 8.6MPa, extraction temperature 20 DEG C, CO2Flow 180L/h, extraction time 2h, obtains Herba Origani Vulgaris quintessence oil primary products, and extraction yield is 25.5%;
D () carries out secondary separation through rectifying tower again, separating pressure is 14MPa, separation temperature 50 DEG C, obtains Herba Origani Vulgaris quintessence oil product through processed, and extraction yield is 10%;
(2) subcritical CO is taken by above-mentioned weight2Extract the Herba Origani Vulgaris quintessence oil, honey and the propolis that obtain, after mixing, carry out homogeneous;
(3) filling, pasteurize 57 DEG C of sterilization 30min are carried out after homogeneous, after sterilization, warehouse-in of labelling.
Every part of product is containing the Herba Origani Vulgaris quintessence oil of 10%, the propolis containing 10%.
Embodiment two
A kind of containing subcritical CO2The bee glue honeyed paste of the Herba Origani Vulgaris quintessence oil of extraction, comprises each component of following weight: subcritical CO2Extract obtain Herba Origani Vulgaris quintessence oil 15g, honey 75g, propolis 10g.
Above-mentioned containing subcritical CO2The preparation method of the bee glue honeyed paste of the Herba Origani Vulgaris quintessence oil of extraction, comprises the steps:
(1) subcritical CO2Extraction obtains Herba Origani Vulgaris quintessence oil, subcritical CO2Extraction step is as follows:
A 200g wild marjoram is cleaned by () after, vacuum-drying, adopts pulverizer that wild marjoram is carried out pulverization process and obtains wild marjoram powder;
B wild marjoram powder after pulverizing is sieved by () with 30 object screen clothes;
(c) subcritical CO2Extraction: extracting pressure 10MPa, extraction temperature 28 DEG C, CO2Flow 165L/h, extraction time 3h, obtains Herba Origani Vulgaris quintessence oil primary products, and extraction yield is 24.8%;
D () carries out secondary separation through rectifying tower again, separating pressure is 15MPa, separation temperature 45 DEG C, obtains Herba Origani Vulgaris quintessence oil product through processed, and extraction yield is 5.1%;
(2) subcritical CO is taken by above-mentioned weight2Extract the Herba Origani Vulgaris quintessence oil, honey and the propolis that obtain, after mixing, carry out homogeneous;
(3) filling, pasteurize 57 DEG C of sterilization 30min are carried out after homogeneous, after sterilization, warehouse-in of labelling.
Every part of product is containing the Herba Origani Vulgaris quintessence oil of 15%, the propolis containing 10%.
Embodiment three
A kind of containing subcritical CO2The bee glue honeyed paste of the Herba Origani Vulgaris quintessence oil of extraction, comprises each component of following weight: subcritical CO2Extract obtain Herba Origani Vulgaris quintessence oil 20g, honey 70g, propolis 10g.
Above-mentioned containing subcritical CO2The preparation method of the bee glue honeyed paste of the Herba Origani Vulgaris quintessence oil of extraction, comprises the steps:
(1) subcritical CO2Extraction obtains Herba Origani Vulgaris quintessence oil, subcritical CO2Extraction step is as follows:
A 200g wild marjoram is cleaned by () after, vacuum-drying, adopts pulverizer that wild marjoram is carried out pulverization process and obtains wild marjoram powder;
B wild marjoram powder after pulverizing is sieved by () with 50 object screen clothes;
(c) subcritical CO2Extraction: extracting pressure 15MPa, extraction temperature 20 DEG C, CO2Flow 190L/h, extraction time 1h, obtains Herba Origani Vulgaris quintessence oil primary products, and extraction yield is 25.0%;
D () carries out secondary separation through rectifying tower again, separating pressure is 10MPa, separation temperature 40 DEG C, obtains Herba Origani Vulgaris quintessence oil product through processed, and extraction yield is 5.6%;
(2) subcritical CO is taken by above-mentioned weight2Extract the Herba Origani Vulgaris quintessence oil, honey and the propolis that obtain, after mixing, carry out homogeneous;
(3) filling, pasteurize 57 DEG C of sterilization 30min are carried out after homogeneous, after sterilization, warehouse-in of labelling.
Every part of product is containing the Herba Origani Vulgaris quintessence oil of 20%, the propolis containing 10%.
Clinical trial
In order to confirm that this product is for skin injury, itch etc. have certain effect, have carried out clinical trial, and test-results is in table 1.
Now select 20 dermatosis patients, by embodiment 1-3 containing subcritical CO2The bee glue honeyed paste of the Herba Origani Vulgaris quintessence oil of extraction gives each edible for patients respectively, and eating method is: once a day, each 15g, takes after diluting with water, and the mass ratio of bee glue honeyed paste and water is 1:6, continuous 7 days. Its result for the treatment of is such as following table:
Table 1 clinical test results
Simultaneous test | Rehabilitation | Alleviate | Invalid |
Embodiment one | 19 | 1 | 0 |
Embodiment two | 18 | 1 | 1 |
Embodiment three | 18 | 1 | 1 |
Not containing the bee glue honeyed paste of Herba Origani Vulgaris quintessence oil | 3 | 4 | 13 |
Prove that the present invention is compared with the commercially available bee glue honeyed paste not containing Herba Origani Vulgaris quintessence oil, has and alleviates skin injury preferably, effect of itch according to clinical trial.
The foregoing is only the better embodiment of the present invention, not in order to limit the present invention, within the spirit and principles in the present invention all, any amendment of doing, equivalent replacement, improvement etc., all should be included within protection scope of the present invention.
Claims (10)
1. a subcritical CO2The Herba Origani Vulgaris quintessence oil of extraction, it is characterised in that: subcritical CO2Extraction comprises the steps:
A wild marjoram is cleaned by () after, vacuum-drying, adopts pulverizer that wild marjoram is carried out pulverization process and obtains wild marjoram powder;
B wild marjoram powder 30-50 object screen cloth after pulverizing is sieved by ();
(c) subcritical CO2Extraction: extracting pressure 5-15MPa, extraction temperature 15-30 DEG C, CO2Flow 160-190L/h, extraction time 1-4h, obtains Herba Origani Vulgaris quintessence oil primary products;
D () carries out secondary separation through rectifying tower again, separating pressure is 10-20MPa, separation temperature 40-60 DEG C, obtains Herba Origani Vulgaris quintessence oil product through processed.
2. subcritical CO according to claim 12The Herba Origani Vulgaris quintessence oil of extraction, it is characterised in that: described step (b) is sieved with 40 object screen clothes.
3. subcritical CO according to claim 12The Herba Origani Vulgaris quintessence oil of extraction, it is characterised in that: described step (c) extracting pressure 8.6MPa, extraction temperature 20 DEG C, CO2Flow 180L/h, extraction time 2h.
4. subcritical CO according to claim 12The Herba Origani Vulgaris quintessence oil of extraction, it is characterised in that: described step (d) separating pressure is 14MPa, separation temperature 50 DEG C.
5. one kind contains the subcritical CO described in the arbitrary item of claim 1-42The bee glue honeyed paste of the Herba Origani Vulgaris quintessence oil of extraction, it is characterised in that: each component comprising following weight part number: subcritical CO2Extract obtain Herba Origani Vulgaris quintessence oil 5-20 part, honey 70-90 part, propolis 5-20 part.
6. one according to claim 5 is containing subcritical CO2The bee glue honeyed paste of the Herba Origani Vulgaris quintessence oil of extraction, it is characterised in that: each component comprising following weight part number: subcritical CO2Extract obtain Herba Origani Vulgaris quintessence oil 8-15 part, honey 70-80 part, propolis 8-15 part.
7. one according to claim 5 is containing subcritical CO2The bee glue honeyed paste of the Herba Origani Vulgaris quintessence oil of extraction, it is characterised in that: each component comprising following weight part number: subcritical CO2Extract obtain Herba Origani Vulgaris quintessence oil 10 parts, honey 80 parts, propolis 10 parts.
8. prepare as claimed in claim 5 containing subcritical CO for one kind2The method of the bee glue honeyed paste of the Herba Origani Vulgaris quintessence oil of extraction, it is characterised in that: comprise the steps:
(1) subcritical CO2Extraction obtains Herba Origani Vulgaris quintessence oil;
(2) subcritical CO is taken by above-mentioned weight part number2Extract the Herba Origani Vulgaris quintessence oil, honey and the propolis that obtain, after mixing, carry out homogeneous;
(3) filling, pasteurize is carried out after homogeneous.
9. according to claim 8 containing subcritical CO2The preparation method of the bee glue honeyed paste of the Herba Origani Vulgaris quintessence oil of extraction, it is characterised in that: the condition of pasteurize is 57 DEG C of sterilization 30min.
10. one kind contains subcritical CO as claimed in claim 52The eating method of the bee glue honeyed paste of the Herba Origani Vulgaris quintessence oil of extraction, it is characterised in that: once a day, each 10-20g, takes after diluting with water, and the mass ratio of bee glue honeyed paste and water is 1:5-10, continuous 7 days.
Priority Applications (1)
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CN201511035254.8A CN105639557A (en) | 2015-12-31 | 2015-12-31 | Propolis honey paste containing oregano essential oil obtained by subcritical CO2 extraction, and preparation method of propolis honey paste |
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CN201511035254.8A CN105639557A (en) | 2015-12-31 | 2015-12-31 | Propolis honey paste containing oregano essential oil obtained by subcritical CO2 extraction, and preparation method of propolis honey paste |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106035609A (en) * | 2016-08-06 | 2016-10-26 | 尹浩 | Biogenic composite pork preservative |
CN106212634A (en) * | 2016-08-06 | 2016-12-14 | 灏规旦 | A kind of cold fresh pork natural antiseptic agent and preparation method thereof |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1288370A (en) * | 1998-01-16 | 2001-03-21 | 安德烈·皮埃尔·莫里斯 | Mixture contg. honey, at least one essential oil and/or at least one essential oil derivative |
CN1943619A (en) * | 2006-11-03 | 2007-04-11 | 湖北福人药业股份有限公司 | Method for preparing Chinese medicine origanum volatile oil and its soft capsule |
CN103627515A (en) * | 2013-12-06 | 2014-03-12 | 杨传德 | Health-care sesame oil with effects of tonifying kidney and improving eyesight |
-
2015
- 2015-12-31 CN CN201511035254.8A patent/CN105639557A/en active Pending
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1288370A (en) * | 1998-01-16 | 2001-03-21 | 安德烈·皮埃尔·莫里斯 | Mixture contg. honey, at least one essential oil and/or at least one essential oil derivative |
CN1943619A (en) * | 2006-11-03 | 2007-04-11 | 湖北福人药业股份有限公司 | Method for preparing Chinese medicine origanum volatile oil and its soft capsule |
CN103627515A (en) * | 2013-12-06 | 2014-03-12 | 杨传德 | Health-care sesame oil with effects of tonifying kidney and improving eyesight |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106035609A (en) * | 2016-08-06 | 2016-10-26 | 尹浩 | Biogenic composite pork preservative |
CN106212634A (en) * | 2016-08-06 | 2016-12-14 | 灏规旦 | A kind of cold fresh pork natural antiseptic agent and preparation method thereof |
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