CN105613626A - Field rice planting middle-stage herbicide and preparation method thereof - Google Patents

Field rice planting middle-stage herbicide and preparation method thereof Download PDF

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Publication number
CN105613626A
CN105613626A CN201610148279.7A CN201610148279A CN105613626A CN 105613626 A CN105613626 A CN 105613626A CN 201610148279 A CN201610148279 A CN 201610148279A CN 105613626 A CN105613626 A CN 105613626A
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parts
water
bean curd
liquid
add
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Inventor
刘兴武
徐飞
傅昌群
林友军
王玉贵
李霞
蔡昌武
吴春喜
李信
戴仕明
江磊
赵忠
张妙松
邵二凯
徐文斐
李平
赵龙凯
尤墩亚
娄功君
高建华
肖尚华
臧启军
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Anhui Huaxing Chemical Co Ltd
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Anhui Huaxing Chemical Co Ltd
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Priority to CN201610148279.7A priority Critical patent/CN105613626A/en
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/18Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group —CO—N<, e.g. carboxylic acid amides or imides; Thio analogues thereof
    • A01N37/26Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group —CO—N<, e.g. carboxylic acid amides or imides; Thio analogues thereof containing the group; Thio analogues thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/48Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
    • A01N43/581,2-Diazines; Hydrogenated 1,2-diazines
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/64Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with three nitrogen atoms as the only ring hetero atoms
    • A01N43/661,3,5-Triazines, not hydrogenated and not substituted at the ring nitrogen atoms
    • A01N43/681,3,5-Triazines, not hydrogenated and not substituted at the ring nitrogen atoms with two or three nitrogen atoms directly attached to ring carbon atoms
    • A01N43/70Diamino—1,3,5—triazines with only one oxygen, sulfur or halogen atom or only one cyano, thiocyano (—SCN), cyanato (—OCN) or azido (—N3) group directly attached to a ring carbon atom
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N47/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
    • A01N47/08Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
    • A01N47/10Carbamic acid derivatives, i.e. containing the group —O—CO—N<; Thio analogues thereof
    • A01N47/24Carbamic acid derivatives, i.e. containing the group —O—CO—N<; Thio analogues thereof containing the groups, or; Thio analogues thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N47/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
    • A01N47/08Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
    • A01N47/28Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N<
    • A01N47/30Derivatives containing the group >N—CO—N aryl or >N—CS—N—aryl
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N61/00Biocides, pest repellants or attractants, or plant growth regulators containing substances of unknown or undetermined composition, e.g. substances characterised only by the mode of action
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N63/00Biocides, pest repellants or attractants, or plant growth regulators containing microorganisms, viruses, microbial fungi, animals or substances produced by, or obtained from, microorganisms, viruses, microbial fungi or animals, e.g. enzymes or fermentates
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N63/00Biocides, pest repellants or attractants, or plant growth regulators containing microorganisms, viruses, microbial fungi, animals or substances produced by, or obtained from, microorganisms, viruses, microbial fungi or animals, e.g. enzymes or fermentates
    • A01N63/10Animals; Substances produced thereby or obtained therefrom
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/40Liliopsida [monocotyledons]
    • A01N65/42Aloeaceae [Aloe family] or Liliaceae [Lily family], e.g. aloe, veratrum, onion, garlic or chives

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Zoology (AREA)
  • Wood Science & Technology (AREA)
  • Dentistry (AREA)
  • Plant Pathology (AREA)
  • Agronomy & Crop Science (AREA)
  • Environmental Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Biotechnology (AREA)
  • Microbiology (AREA)
  • Virology (AREA)
  • Mycology (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention relates to a field rice planting middle-stage herbicide. The field rice planting middle-stage herbicide is prepared from, by weight, 35-45 parts of acetochlor, 35-45 parts of atrazine, 15-19 parts of radix polygoni multiflori, 6-9 parts of fried platycodon roots, 15-18 parts of scorch-fried bombyx batryticatus, 12-14 parts of bulbus fritillariae cirrhosae, 5-7 parts of scorch-fried pericarpium papaveris, 9-14 parts of pear peels, 30-50 parts of fructus momordicae, 50-60 parts of vinegar, 50-56 parts of straw, 10-15 parts of plant ash, 10-20 parts of sugar refinery filter mud, 1-2 parts of probiotics, 10-15 parts of diafenthiuron, 10-15 parts of methomyl, 10-15 parts of pyridaben, 10-15 parts of maibaosu, 60-70 parts of coprinus comatus, 80-90 parts of bean curds, 5-10 parts of ganoderma lucidum, 5-10 parts of salt, 5-10 parts of chicken essence, 5-10 parts of sesame oil, 200-210 parts of Ceylon black tea, 1,000-1,100 parts of boiled water, 100-110 parts of evaporated milk, 55-60 parts of white sugar, 20-25 parts of peanut kernels, 10-15 parts of milkvetch roots and 10-15 parts of radix angelicae sinensis. The prepared herbicide is specially used for removing field rice planting middle-stage weeds, the growth vigor of rice is not affected, the herbicide is dissolved in water and penetrates underground, and nutrition supply to the early-stage rice can be achieved.

Description

A kind of field water seed rice plants weedicide and its preparation method in mid-term
Technical field:
A kind of field weedicide of inventive design, is specifically related to a kind of field water seed rice and plants weedicide and its preparation method in mid-term.
Background technology:
Chemical weed control is the development trend of modern agriculture, the current major part in China farmland has widely used chemical herbicide, create very big economic benefit, but, by the investigation to farmland chemical weed controls such as Henan, Hebei, Shandong, find to there is shortcoming on preventive effect and weedicide kind, through the use of weedicide for many years, all have there is resistance in various degree in major part weeds, existing weedicide is not by for the initial stage simultaneously, in mid-term, late period, Grain Growth Situation carried out corresponding weeding, and herbicidal effect is general.
Summary of the invention:
Technical problem to be solved by this invention is to overcome the defect of prior art, it is provided that a kind of field water seed rice plants weedicide and its preparation method in mid-term.
Technical problem to be solved by this invention realizes by the following technical solutions.
A kind of field water seed rice plants weedicide in mid-term, it is characterized in that: its each component concentration weight part is: acetochlor 35-45 part, atrazine 35-45 part, Tuber Fleeceflower Root 15-19 part, fry balloonflower root 6-9 part, process stiff silkworm 15-18 part, Unibract Fritillary Bulb 12-14 part, process Poppy capsule 5-7 part, pears skin 9-14 part, Grosvenor Momordica 30-50 part, vinegar 50-60 part, stalk 50-56 part, plant ash 10-15 part, filter mud of sugar refinery 10-20 part, 1 part of-2 parts of probiotic bacterium, butyl ether urea 10-15 part, methomyl 10-15 part, pyridaben 10-15 part, Maibaosu 10-15 part, coprinus comatus 60-70 part, bean curd 80-90 part, glossy ganoderma 5-10 part, salt 5-10 part, chickens' extract 5-10 part, sesame oil 5-10 part, Ceylon's black tea 200-210 part, boiling water 1000-1100 part, light milk 100-110 part, white sugar 55-60 part, Semen arachidis hypogaeae 20-25 part, Radix Astragali 10-15 part, Radix Angelicae Sinensis 10-15 part.
Its preparation method comprises:
1) section after coprinus comatus being cleaned, is immersed in light milk, treats that light milk is absorbed totally by coprinus comatus, get peanut, grinds, be sprinkled upon in coprinus comatus;
2) while coprinus comatus absorbs light milk, bean curd is cut into slices, dries, be down to 35%-40% to the moisture in bean curd slice;
3) get the Radix Astragali, Radix Angelicae Sinensis grinds add in matrass, add Ceylon's black tea, distillation, collect distilled water,
4) bean curd slice being placed in distilled water, bean curd absorbs distilled water, when moisture content rises to 70%-75% in band bean curd, takes out bean curd, together it is placed in pot with coprinus comatus sheet, adds water, boiling, add glossy ganoderma in boiling simultaneously, boil to boiling, salt adding, chickens' extract and sesame oil;
5) cooling, as, under sunlight, treating that moisture steams dry, in residue, moisture content is when 10%-15%, takes out left drug;
6) by crushed stalk, length 1-3 centimetre, translate into plant ash and probiotic bacterium liquid and mix, pile wide 2 meters, high 1 meter, the bar shaped cone that length is not limit, builds with plastic cloth, through 2-3 week thermophilic fermentation, become brown or chocolate to stalk, then smash to pieces and sieve, add filter mud of sugar refinery mix and blend, drying, sieves;
7) by Tuber Fleeceflower Root, fry balloonflower root, process stiff silkworm, Unibract Fritillary Bulb, process Poppy capsule, pears skin be placed in vinegar, heat and soak 30 minutes, vinegar temperature controls more than 80 DEG C;
8) pull the medicinal material after immersion out, dry, grinding;
9) put into distiller, add 500ml water and distill, collect water vapour, obtain liquid;
10) liquid being placed in heating tank, utilize ultrasonic wave heating tank body, heating, collects water vapour in heat-processed, concentration of liquid medicine is evaporated totally to the liquid in heating tank;
11) choose fresh Grosvenor Momordica, squeeze into juice, mix with the water vapour collected;
12) microwave heating obtains liquid in 10 minutes;
13) left drug got in step 5 is immersed in the liquid in step, distillation, collect distillation gas, with step 8) in stirring thing mix, mix static 1 day;
14) by step 13) static after compound as in squeezing machine, squeezing water outlet, water intaking mixes with butyl ether urea, methomyl, pyridaben, Maibaosu;
15) being heated to 75 DEG C, add acetochlor, atrazine, stir 10 minutes, cooling, namely obtains weedicide.
The invention has the beneficial effects as follows: weedicide specialty prepared by this method is for removing the weeds in field paddy rice mid-term, do not affect paddy rice rising trend, weedicide infiltrates underground after being dissolved in water simultaneously, also paddy rice in mid-term can being played nutrition supply, present method reduces disease and pest, good quality and high output, significantly improve the output of paddy rice, the paddy rice full grains that present method is produced, nutritious, be suitable for promoting.
Embodiment:
In order to the present invention is realized technique means, creation characteristic, reach object and effect is easy to understand, below in conjunction with specific embodiment, set forth the present invention further.
Specific embodiment 1: a kind of field water seed rice plants weedicide in mid-term, its each component concentration weight part is: acetochlor 35 parts, atrazine 35 parts, Tuber Fleeceflower Root 15 parts, fry balloonflower root 6 parts, process stiff silkworm 15 parts, Unibract Fritillary Bulb 12 parts, process Poppy capsule 5 parts, pears skin 9 parts, Grosvenor Momordica 30 parts, vinegar 50 parts, stalk 50 parts, plant ash 10 parts, filter mud of sugar refinery 10 parts, 1 part of probiotic bacterium, butyl ether urea 10 parts, methomyl 10 parts, pyridaben 10 parts, Maibaosu 10 parts, coprinus comatus 60 parts, bean curd 80 parts, glossy ganoderma 5 parts, salt 5 parts, chickens' extract 5 parts, sesame oil 5 parts, Ceylon's black tea 200 parts, 1000 parts, boiling water, light milk 100 parts, white sugar 55 parts, 20 parts, Semen arachidis hypogaeae, the Radix Astragali 10 parts, Radix Angelicae Sinensis 10 parts.
Specific embodiment 2: a kind of field water seed rice plants weedicide in mid-term, its each component concentration weight part is: acetochlor 45 parts, atrazine 45 parts, Tuber Fleeceflower Root 19 parts, fry balloonflower root 9 parts, process stiff silkworm 18 parts, Unibract Fritillary Bulb 14 parts, process Poppy capsule 7 parts, pears skin 14 parts, Grosvenor Momordica 50 parts, vinegar 60 parts, stalk 56 parts, plant ash 15 parts, filter mud of sugar refinery 20 parts, 2 parts of probiotic bacteriums, butyl ether urea 15 parts, methomyl 15 parts, pyridaben 15 parts, Maibaosu 15 parts, coprinus comatus 70 parts, bean curd 90 parts, glossy ganoderma 10 parts, salt 10 parts, chickens' extract 10 parts, sesame oil 10 parts, Ceylon's black tea 210 parts, 1100 parts, boiling water, light milk 110 parts, white sugar 60 parts, 25 parts, Semen arachidis hypogaeae, the Radix Astragali 15 parts, Radix Angelicae Sinensis 15 parts.
Its preparation method comprises:
1) section after coprinus comatus being cleaned, is immersed in light milk, treats that light milk is absorbed totally by coprinus comatus, get peanut, grinds, be sprinkled upon in coprinus comatus;
2) while coprinus comatus absorbs light milk, bean curd is cut into slices, dries, be down to 35%-40% to the moisture in bean curd slice;
3) get the Radix Astragali, Radix Angelicae Sinensis grinds add in matrass, add Ceylon's black tea, distillation, collect distilled water,
4) bean curd slice being placed in distilled water, bean curd absorbs distilled water, when moisture content rises to 70%-75% in band bean curd, takes out bean curd, together it is placed in pot with coprinus comatus sheet, adds water, boiling, add glossy ganoderma in boiling simultaneously, boil to boiling, salt adding, chickens' extract and sesame oil;
5) cooling, as, under sunlight, treating that moisture steams dry, in residue, moisture content is when 10%-15%, takes out left drug;
6) by crushed stalk, length 1-3 centimetre, translate into plant ash and probiotic bacterium liquid and mix, pile wide 2 meters, high 1 meter, the bar shaped cone that length is not limit, builds with plastic cloth, through 2-3 week thermophilic fermentation, become brown or chocolate to stalk, then smash to pieces and sieve, add filter mud of sugar refinery mix and blend, drying, sieves;
7) by Tuber Fleeceflower Root, fry balloonflower root, process stiff silkworm, Unibract Fritillary Bulb, process Poppy capsule, pears skin be placed in vinegar, heat and soak 30 minutes, vinegar temperature controls more than 80 DEG C;
8) pull the medicinal material after immersion out, dry, grinding;
9) put into distiller, add 500ml water and distill, collect water vapour, obtain liquid;
10) liquid being placed in heating tank, utilize ultrasonic wave heating tank body, heating, collects water vapour in heat-processed, concentration of liquid medicine is evaporated totally to the liquid in heating tank;
11) choose fresh Grosvenor Momordica, squeeze into juice, mix with the water vapour collected;
12) microwave heating obtains liquid in 10 minutes;
13) left drug got in step 5 is immersed in the liquid in step, distillation, collect distillation gas, with step 8) in stirring thing mix, mix static 1 day;
14) by step 13) static after compound as in squeezing machine, squeezing water outlet, water intaking mixes with butyl ether urea, methomyl, pyridaben, Maibaosu;
15) being heated to 75 DEG C, add acetochlor, atrazine, stir 10 minutes, cooling, namely obtains weedicide.
More than show and describe the ultimate principle of the present invention, the advantage of main characteristic sum the present invention. The technician of the industry should understand; the present invention is not restricted to the described embodiments; the principle that the present invention is just described described in above-described embodiment and specification sheets; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications, and these changes and improvements all fall in the claimed scope of the invention. The claimed scope of the present invention is defined by appending claims and equivalent thereof.

Claims (2)

1. a field water seed rice plants weedicide in mid-term, it is characterized in that: its each component concentration weight part is: acetochlor 35-45 part, atrazine 35-45 part, Tuber Fleeceflower Root 15-19 part, fry balloonflower root 6-9 part, process stiff silkworm 15-18 part, Unibract Fritillary Bulb 12-14 part, process Poppy capsule 5-7 part, pears skin 9-14 part, Grosvenor Momordica 30-50 part, vinegar 50-60 part, stalk 50-56 part, plant ash 10-15 part, filter mud of sugar refinery 10-20 part, 1 part of-2 parts of probiotic bacterium, butyl ether urea 10-15 part, methomyl 10-15 part, pyridaben 10-15 part, Maibaosu 10-15 part, coprinus comatus 60-70 part, bean curd 80-90 part, glossy ganoderma 5-10 part, salt 5-10 part, chickens' extract 5-10 part, sesame oil 5-10 part, Ceylon's black tea 200-210 part, boiling water 1000-1100 part, light milk 100-110 part, white sugar 55-60 part, Semen arachidis hypogaeae 20-25 part, Radix Astragali 10-15 part, Radix Angelicae Sinensis 10-15 part.
2. plant weedicide in mid-term according to a kind of field water seed rice described in claim 1, it is characterised in that: its preparation method comprises:
1) section after coprinus comatus being cleaned, is immersed in light milk, treats that light milk is absorbed totally by coprinus comatus, get peanut, grinds, be sprinkled upon in coprinus comatus;
2) while coprinus comatus absorbs light milk, bean curd is cut into slices, dries, be down to 35%-40% to the moisture in bean curd slice;
3) get the Radix Astragali, Radix Angelicae Sinensis grinds add in matrass, add Ceylon's black tea, distillation, collect distilled water,
4) bean curd slice being placed in distilled water, bean curd absorbs distilled water, when moisture content rises to 70%-75% in band bean curd, takes out bean curd, together it is placed in pot with coprinus comatus sheet, adds water, boiling, add glossy ganoderma in boiling simultaneously, boil to boiling, salt adding, chickens' extract and sesame oil;
5) cooling, as, under sunlight, treating that moisture steams dry, in residue, moisture content is when 10%-15%, takes out left drug;
6) by crushed stalk, length 1-3 centimetre, translate into plant ash and probiotic bacterium liquid and mix, pile wide 2 meters, high 1 meter, the bar shaped cone that length is not limit, builds with plastic cloth, through 2-3 week thermophilic fermentation, become brown or chocolate to stalk, then smash to pieces and sieve, add filter mud of sugar refinery mix and blend, drying, sieves;
7) by Tuber Fleeceflower Root, fry balloonflower root, process stiff silkworm, Unibract Fritillary Bulb, process Poppy capsule, pears skin be placed in vinegar, heat and soak 30 minutes, vinegar temperature controls more than 80 DEG C;
8) pull the medicinal material after immersion out, dry, grinding;
9) put into distiller, add 500ml water and distill, collect water vapour, obtain liquid;
10) liquid being placed in heating tank, utilize ultrasonic wave heating tank body, heating, collects water vapour in heat-processed, concentration of liquid medicine is evaporated totally to the liquid in heating tank;
11) choose fresh Grosvenor Momordica, squeeze into juice, mix with the water vapour collected;
12) microwave heating obtains liquid in 10 minutes;
13) left drug got in step 5 is immersed in the liquid in step, distillation, collect distillation gas, with step 8) in stirring thing mix, mix static 1 day;
14) by step 13) static after compound as in squeezing machine, squeezing water outlet, water intaking mixes with butyl ether urea, methomyl, pyridaben, Maibaosu;
15) being heated to 75 DEG C, add acetochlor, atrazine, stir 10 minutes, cooling, namely obtains weedicide.
CN201610148279.7A 2016-03-15 2016-03-15 Field rice planting middle-stage herbicide and preparation method thereof Pending CN105613626A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109430298A (en) * 2018-12-29 2019-03-08 南京高正农用化工有限公司 A kind of big granula of paddy field weed-killer and preparation method thereof
CN110367291A (en) * 2019-07-31 2019-10-25 乐东广陵南繁服务有限公司 A kind of careless agent of hybrid rice suppression

Citations (5)

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CN101103673A (en) * 2007-07-16 2008-01-16 内蒙古自治区农牧业机械技术推广站 Weeds control method for protective cultivating corn field in agriculture and animal husbandry alternative area
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Application publication date: 20160601