CN105660746A - Herbicide used in early period of field rice planting and preparation method of herbicide - Google Patents

Herbicide used in early period of field rice planting and preparation method of herbicide Download PDF

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Publication number
CN105660746A
CN105660746A CN201610148282.9A CN201610148282A CN105660746A CN 105660746 A CN105660746 A CN 105660746A CN 201610148282 A CN201610148282 A CN 201610148282A CN 105660746 A CN105660746 A CN 105660746A
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parts
herbicide
heating
semen
rice
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CN201610148282.9A
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Chinese (zh)
Inventor
刘兴武
徐飞
傅昌群
林友军
王玉贵
李霞
蔡昌武
吴春喜
李信
戴仕明
江磊
赵忠
张妙松
邵二凯
徐文斐
李平
赵龙凯
尤墩亚
娄功君
高建华
肖尚华
臧启军
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Anhui Huaxing Chemical Co Ltd
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Anhui Huaxing Chemical Co Ltd
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Priority to CN201610148282.9A priority Critical patent/CN105660746A/en
Publication of CN105660746A publication Critical patent/CN105660746A/en
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/02Saturated carboxylic acids or thio analogues thereof; Derivatives thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N37/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
    • A01N37/18Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group —CO—N<, e.g. carboxylic acid amides or imides; Thio analogues thereof
    • A01N37/26Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids containing the group —CO—N<, e.g. carboxylic acid amides or imides; Thio analogues thereof containing the group; Thio analogues thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/02Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
    • A01N43/04Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
    • A01N43/14Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
    • A01N43/16Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/48Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
    • A01N43/581,2-Diazines; Hydrogenated 1,2-diazines
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/64Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with three nitrogen atoms as the only ring hetero atoms
    • A01N43/661,3,5-Triazines, not hydrogenated and not substituted at the ring nitrogen atoms
    • A01N43/681,3,5-Triazines, not hydrogenated and not substituted at the ring nitrogen atoms with two or three nitrogen atoms directly attached to ring carbon atoms
    • A01N43/70Diamino—1,3,5—triazines with only one oxygen, sulfur or halogen atom or only one cyano, thiocyano (—SCN), cyanato (—OCN) or azido (—N3) group directly attached to a ring carbon atom
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N47/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
    • A01N47/08Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
    • A01N47/10Carbamic acid derivatives, i.e. containing the group —O—CO—N<; Thio analogues thereof
    • A01N47/24Carbamic acid derivatives, i.e. containing the group —O—CO—N<; Thio analogues thereof containing the groups, or; Thio analogues thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N47/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
    • A01N47/08Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
    • A01N47/28Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N<
    • A01N47/30Derivatives containing the group >N—CO—N aryl or >N—CS—N—aryl
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N61/00Biocides, pest repellants or attractants, or plant growth regulators containing substances of unknown or undetermined composition, e.g. substances characterised only by the mode of action
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N63/00Biocides, pest repellants or attractants, or plant growth regulators containing microorganisms, viruses, microbial fungi, animals or substances produced by, or obtained from, microorganisms, viruses, microbial fungi or animals, e.g. enzymes or fermentates
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/40Liliopsida [monocotyledons]
    • A01N65/44Poaceae or Gramineae [Grass family], e.g. bamboo, lemon grass or citronella grass
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Zoology (AREA)
  • Agronomy & Crop Science (AREA)
  • Environmental Sciences (AREA)
  • Plant Pathology (AREA)
  • Dentistry (AREA)
  • Wood Science & Technology (AREA)
  • Pest Control & Pesticides (AREA)
  • Microbiology (AREA)
  • Biotechnology (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Mycology (AREA)
  • Virology (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

The invention provides herbicide used in the early period of field rice planting. The herbicide is prepared from, by weight, 35-45 parts of acetochlor, 35-45 parts of atrazine, 15-19 parts of rhizoma atractylodis, 6-9 parts of burnt cortex phellodendri, 15-18 parts of rhizoma pinelliae, 12-14 parts of semen coicis, 5-7 parts of radix achyranthis bidentatae, 9-14 parts of waxgourd seeds, 30-50 parts of fructus momordicae, 50-60 parts of vinegar, 50-60 parts of peanuts, 50-60 parts of malt sugar, 1000-1200 parts of green tea, 70-80 parts of orange juice, 50-70 parts of tomato juice, 5-10 parts of rhizoma polygonati odorati, 200-220 parts of soybeans, 50-56 parts of straw, 10-15 parts of plant ash, 10-20 parts of filter mud from a sugar refinery, 1-2 parts of probiotics, 10-15 parts of diafenthiuron, 10-15 parts of methomyl, 10-15 parts of pyridaben and 10-15 parts of MaiBaoSu. The herbicide used in the early period of field rice planting and a preparation method of the herbicide have the advantages that the prepared herbicide is professionally used for removing weeds in the early period of field rice, the upward trend of the rice is not influenced, meanwhile the herbicide is permeated into the ground after being dissolved in water, and nutrient supply to the rice in the early period can be further achieved; by means of the method, plant diseases and insect pests are reduced, high quality and high yield are achieved, the yield of the rice is greatly raised, and the rice produced through the method is plumpy in particle, rich in nutrient and applicable to popularization.

Description

A kind of field Rice Cropping early stage herbicide and preparation method thereof
Technical field:
The present invention designs a kind of field weedicide, is specifically related to a kind of field Rice Cropping early stage herbicide and preparation method thereof.
Background technology:
Chemical weed control is the development trend of modern agriculture, the current major part in China farmland is widely used chemical herbicide, create very big economic benefit, but, by the investigation to farmland chemical weed controls such as Henan, Hebei, Shandong, find there is shortcoming on preventive effect and herbicide kind, use through herbicide for many years, all have there is resistance in various degree in major part weeds, existing herbicide is not by for the initial stage simultaneously, in mid-term, late period, Grain Growth Situation carried out corresponding weeding, and herbicidal effect is general.
Summary of the invention:
The technical problem to be solved is in that to overcome the defect of prior art, it is provided that a kind of field Rice Cropping early stage herbicide and preparation method thereof.
The technical problem to be solved realizes by the following technical solutions.
A kind of field Rice Cropping early stage herbicide, it is characterized in that: its each constituent content weight portion is: Acetochlor 35-45 part, atrazine 35-45 part, Rhizoma Atractylodis 15-19 part, charred Cortex Phellodendri 6-9 part, Rhizoma Pinelliae 15-18 part, Semen Coicis 12-14 part, Radix Achyranthis Bidentatae 5-7 part, Semen Benincasae 9-14 part, Fructus Momordicae 30-50 part, vinegar 50-60 part, Semen arachidis hypogaeae 50-60 part, maltose 50-60 part, green tea 1000-1200 part, orange juice 70-80 part, Fructus Lycopersici esculenti juice 50-70 part, Rhizoma Polygonati Odorati 5-10 part, Semen Glycines 200-220 part, straw 50-56 part, plant ash 10-15 part, filter mud of sugar refinery 10-20 part, 1 part of-2 parts of probiotic bacteria, diafenthiuron 10-15 part, Methomyl 10-15 part, pyridaben 10-15 part, Maibaosu 10-15 part.
Its preparation method includes:
1) good quality soybeans is chosen, decortication;
2) taking the soybean soaking of decortication in orange juice, soak duration 1-2 hour, wherein immersion process is divided into three sections, leading portion soaking temperature 50 DEG C, stage casing soaking temperature is 30 DEG C, and back segment soaking temperature is 50 DEG C, and is separately added into 1/5,3/5,1/5 Fructus Lycopersici esculenti juice in three step immersion processes;
3) Semen Glycines after soaking is gone to wear into slurry with Semen arachidis hypogaeae;
4) through 100 mesh screen, bean milk is obtained;
5) by heating soybean milk to 100 DEG C, keep 20 minutes, then bean milk is put in the skin rising pot filling with green tea, keep temperature 80-90 DEG C, add Rhizoma Polygonati Odorati, maltose, every one, 2-5 minute device Glycine max (L.) Merr., till bean milk takes;
6) take step 1) in Testa Glycines grinds,
7) by step 5) in the Glycine max (L.) Merr. be placed on ice cube, cool down 1-2 minute, be cooled to 60 DEG C, by 6 while cooling) in powder be sprinkled upon on the Glycine max (L.) Merr.;
8) by crushed stalk, length 1-3 centimetre, translate into mix with plant ash and prebiotic bacterium solution, pile wide 2 meters, high 1 meter, that length is not limit bar shaped cone, builds with Polypropylence Sheet, through 2-3 week hot fermentation, to straw overstrike or pitchy, then smash to pieces and sieve, add filter mud of sugar refinery mix and blend, dry, sieve;
9) Rhizoma Atractylodis, charred Cortex Phellodendri, the Rhizoma Pinelliae, Semen Coicis, Radix Achyranthis Bidentatae, Semen Benincasae are placed in vinegar, immersion 30 minutes of heating, vinegar temperature controls more than 80 DEG C;
10) pull the medical material after immersion out, dry, grind;
11) put in distillator, add 500ml water and distill, collect steam, obtain medicinal liquid;
12) medicinal liquid is placed in heating tank, utilizes ultrasound wave heating tank body, heating, heating process is collected steam, the medicinal liquid in concentration of liquid medicine to heating tank is evaporated totally;
13) choose fresh Fructus Momordicae, squeeze into juice, mix with the steam collected;
14) microwave heating obtains liquid in 10 minutes;
15) take the Glycine max (L.) Merr. in step 7 to be immersed in the liquid in step, distillation, collect distillation gas, with step 8) in stirring thing mix, mix static 1 day;
16) by step 15) static after compound as in squeezer, squeeze water outlet, water intaking mixes with diafenthiuron, Methomyl, pyridaben, Maibaosu;
17) heating is to 75 DEG C, adds Acetochlor, atrazine, stirs 10 minutes, and namely cooling obtains herbicide.
The invention has the beneficial effects as follows: herbicide specialty prepared by this law is for removing the weeds of field Oryza sativa L. early stage, do not affect Oryza sativa L. rising trend, herbicide permeates the ground after being dissolved in water simultaneously, early stage Oryza sativa L. also can play nutrition supply, and this method reduces pest and disease damage, good quality and high output, the yield of Oryza sativa L. is greatly improved, the rice grain that this method is produced is full, nutritious, is suitable to promote.
Detailed description of the invention:
For the technological means making the present invention realize, creation characteristic, reach purpose and effect and be easy to understand, below in conjunction with specific embodiment, the present invention is expanded on further.
Specific embodiment 1: a kind of field Rice Cropping early stage herbicide, its each constituent content weight portion is: Acetochlor 35 parts, atrazine 35 parts, Rhizoma Atractylodis 15 parts, charred Cortex Phellodendri 6 parts, the Rhizoma Pinelliae 15 parts, Semen Coicis 12 parts, Radix Achyranthis Bidentatae 5 parts, Semen Benincasae 9 parts, Fructus Momordicae 30 parts, vinegar 50 parts, Semen arachidis hypogaeae 50 parts, maltose 50 parts, green tea 1000 parts, orange juice 70 parts, Fructus Lycopersici esculenti juice 50 parts, Rhizoma Polygonati Odorati 5 parts, Semen Glycines 200 parts, straw 50 parts, plant ash 10 parts, 10 parts, 1 part probiotic bacteria of filter mud of sugar refinery, diafenthiuron 10 parts, Methomyl 10 parts, pyridaben 10 parts, Maibaosu 10 parts.
Specific embodiment 2: a kind of field Rice Cropping early stage herbicide, its each constituent content weight portion is: Acetochlor 45 parts, atrazine 45 parts, Rhizoma Atractylodis 19 parts, charred Cortex Phellodendri 9 parts, the Rhizoma Pinelliae 18 parts, Semen Coicis 14 parts, Radix Achyranthis Bidentatae 7 parts, Semen Benincasae 14 parts, Fructus Momordicae 50 parts, vinegar 60 parts, Semen arachidis hypogaeae 60 parts, maltose 60 parts, green tea 1200 parts, orange juice 80 parts, Fructus Lycopersici esculenti juice 70 parts, Rhizoma Polygonati Odorati 10 parts, Semen Glycines 220 parts, straw 56 parts, plant ash 15 parts, 20 parts, 2 parts probiotic bacterias of filter mud of sugar refinery, diafenthiuron 15 parts, Methomyl 15 parts, pyridaben 15 parts, Maibaosu 15 parts.
Its preparation method includes:
1) good quality soybeans is chosen, decortication;
2) taking the soybean soaking of decortication in orange juice, soak duration 1-2 hour, wherein immersion process is divided into three sections, leading portion soaking temperature 50 DEG C, stage casing soaking temperature is 30 DEG C, and back segment soaking temperature is 50 DEG C, and is separately added into 1/5,3/5,1/5 Fructus Lycopersici esculenti juice in three step immersion processes;
3) Semen Glycines after soaking is gone to wear into slurry with Semen arachidis hypogaeae;
4) through 100 mesh screen, bean milk is obtained;
5) by heating soybean milk to 100 DEG C, keep 20 minutes, then bean milk is put in the skin rising pot filling with green tea, keep temperature 80-90 DEG C, add Rhizoma Polygonati Odorati, maltose, every one, 2-5 minute device Glycine max (L.) Merr., till bean milk takes;
6) take step 1) in Testa Glycines grinds,
7) by step 5) in the Glycine max (L.) Merr. be placed on ice cube, cool down 1-2 minute, be cooled to 60 DEG C, by 6 while cooling) in powder be sprinkled upon on the Glycine max (L.) Merr.;
8) by crushed stalk, length 1-3 centimetre, translate into mix with plant ash and prebiotic bacterium solution, pile wide 2 meters, high 1 meter, that length is not limit bar shaped cone, builds with Polypropylence Sheet, through 2-3 week hot fermentation, to straw overstrike or pitchy, then smash to pieces and sieve, add filter mud of sugar refinery mix and blend, dry, sieve;
9) Rhizoma Atractylodis, charred Cortex Phellodendri, the Rhizoma Pinelliae, Semen Coicis, Radix Achyranthis Bidentatae, Semen Benincasae are placed in vinegar, immersion 30 minutes of heating, vinegar temperature controls more than 80 DEG C;
10) pull the medical material after immersion out, dry, grind;
11) put in distillator, add 500ml water and distill, collect steam, obtain medicinal liquid;
12) medicinal liquid is placed in heating tank, utilizes ultrasound wave heating tank body, heating, heating process is collected steam, the medicinal liquid in concentration of liquid medicine to heating tank is evaporated totally;
13) choose fresh Fructus Momordicae, squeeze into juice, mix with the steam collected;
14) microwave heating obtains liquid in 10 minutes;
15) take the Glycine max (L.) Merr. in step 7 to be immersed in the liquid in step, distillation, collect distillation gas, with step 8) in stirring thing mix, mix static 1 day;
16) by step 15) static after compound as in squeezer, squeeze water outlet, water intaking mixes with diafenthiuron, Methomyl, pyridaben, Maibaosu;
17) heating is to 75 DEG C, adds Acetochlor, atrazine, stirs 10 minutes, and namely cooling obtains herbicide.
The ultimate principle of the present invention, principal character and advantages of the present invention have more than been shown and described. Skilled person will appreciate that of the industry; the present invention is not restricted to the described embodiments; described in above-described embodiment and description is that principles of the invention is described; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications, and these changes and improvements both fall within the claimed scope of the invention. Claimed scope is defined by appending claims and equivalent thereof.

Claims (2)

1. a field Rice Cropping early stage herbicide, it is characterized in that: its each constituent content weight portion is: Acetochlor 35-45 part, atrazine 35-45 part, Rhizoma Atractylodis 15-19 part, charred Cortex Phellodendri 6-9 part, Rhizoma Pinelliae 15-18 part, Semen Coicis 12-14 part, Radix Achyranthis Bidentatae 5-7 part, Semen Benincasae 9-14 part, Fructus Momordicae 30-50 part, vinegar 50-60 part, Semen arachidis hypogaeae 50-60 part, maltose 50-60 part, green tea 1000-1200 part, orange juice 70-80 part, Fructus Lycopersici esculenti juice 50-70 part, Rhizoma Polygonati Odorati 5-10 part, Semen Glycines 200-220 part, straw 50-56 part, plant ash 10-15 part, filter mud of sugar refinery 10-20 part, 1 part of-2 parts of probiotic bacteria, diafenthiuron 10-15 part, Methomyl 10-15 part, pyridaben 10-15 part, Maibaosu 10-15 part.
2. a kind of field according to claim 1 Rice Cropping early stage herbicide, it is characterised in that: its preparation method includes:
1) good quality soybeans is chosen, decortication;
2) taking the soybean soaking of decortication in orange juice, soak duration 1-2 hour, wherein immersion process is divided into three sections, leading portion soaking temperature 50 DEG C, stage casing soaking temperature is 30 DEG C, and back segment soaking temperature is 50 DEG C, and is separately added into 1/5,3/5,1/5 Fructus Lycopersici esculenti juice in three step immersion processes;
3) Semen Glycines after soaking is gone to wear into slurry with Semen arachidis hypogaeae;
4) through 100 mesh screen, bean milk is obtained;
5) by heating soybean milk to 100 DEG C, keep 20 minutes, then bean milk is put in the skin rising pot filling with green tea, keep temperature 80-90 DEG C, add Rhizoma Polygonati Odorati, maltose, every one, 2-5 minute device Glycine max (L.) Merr., till bean milk takes;
6) take step 1) in Testa Glycines grinds,
7) by step 5) in the Glycine max (L.) Merr. be placed on ice cube, cool down 1-2 minute, be cooled to 60 DEG C, by 6 while cooling) in powder be sprinkled upon on the Glycine max (L.) Merr.;
8) by crushed stalk, length 1-3 centimetre, translate into mix with plant ash and prebiotic bacterium solution, pile wide 2 meters, high 1 meter, that length is not limit bar shaped cone, builds with Polypropylence Sheet, through 2-3 week hot fermentation, to straw overstrike or pitchy, then smash to pieces and sieve, add filter mud of sugar refinery mix and blend, dry, sieve;
9) Rhizoma Atractylodis, charred Cortex Phellodendri, the Rhizoma Pinelliae, Semen Coicis, Radix Achyranthis Bidentatae, Semen Benincasae are placed in vinegar, immersion 30 minutes of heating, vinegar temperature controls more than 80 DEG C;
10) pull the medical material after immersion out, dry, grind;
11) put in distillator, add 500ml water and distill, collect steam, obtain medicinal liquid;
12) medicinal liquid is placed in heating tank, utilizes ultrasound wave heating tank body, heating, heating process is collected steam, the medicinal liquid in concentration of liquid medicine to heating tank is evaporated totally;
13) choose fresh Fructus Momordicae, squeeze into juice, mix with the steam collected;
14) microwave heating obtains liquid in 10 minutes;
15) take the Glycine max (L.) Merr. in step 7 to be immersed in the liquid in step, distillation, collect distillation gas, with step 8) in stirring thing mix, mix static 1 day;
16) by step 15) static after compound as in squeezer, squeeze water outlet, water intaking mixes with diafenthiuron, Methomyl, pyridaben, Maibaosu;
17) heating is to 75 DEG C, adds Acetochlor, atrazine, stirs 10 minutes, and namely cooling obtains herbicide.
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