CN105601126B - 一种海洋蓝色双银低辐射镀膜玻璃 - Google Patents

一种海洋蓝色双银低辐射镀膜玻璃 Download PDF

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CN105601126B
CN105601126B CN201610080935.4A CN201610080935A CN105601126B CN 105601126 B CN105601126 B CN 105601126B CN 201610080935 A CN201610080935 A CN 201610080935A CN 105601126 B CN105601126 B CN 105601126B
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thickness
silver
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glass
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余华骏
黄颖
梁瑞记
艾发智
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DONGGUAN SG ENGINEERING GLASS CO LTD
CSG Holding Co Ltd
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    • C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
    • C03C17/34—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions
    • C03C17/36—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
    • C03C17/34—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions
    • C03C17/36—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal
    • C03C17/3602—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal the metal being present as a layer
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
    • C03C17/34—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions
    • C03C17/36—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal
    • C03C17/3602—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal the metal being present as a layer
    • C03C17/3626—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal the metal being present as a layer one layer at least containing a nitride, oxynitride, boronitride or carbonitride
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
    • C03C17/34—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions
    • C03C17/36—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal
    • C03C17/3602—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal the metal being present as a layer
    • C03C17/3639—Multilayers containing at least two functional metal layers
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
    • C03C17/34—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions
    • C03C17/36—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal
    • C03C17/3602—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal the metal being present as a layer
    • C03C17/3644—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal the metal being present as a layer the metal being silver
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
    • C03C17/34—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions
    • C03C17/36—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal
    • C03C17/3602—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal the metal being present as a layer
    • C03C17/3657—Surface treatment of glass, not in the form of fibres or filaments, by coating with at least two coatings having different compositions at least one coating being a metal the metal being present as a layer the multilayer coating having optical properties
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C2217/00—Coatings on glass
    • C03C2217/70—Properties of coatings
    • C—CHEMISTRY; METALLURGY
    • C03—GLASS; MINERAL OR SLAG WOOL
    • C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C2218/00—Methods for coating glass
    • C03C2218/10—Deposition methods
    • C03C2218/15—Deposition methods from the vapour phase
    • C03C2218/154—Deposition methods from the vapour phase by sputtering
    • C03C2218/156—Deposition methods from the vapour phase by sputtering by magnetron sputtering

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Abstract

本发明属于玻璃技术领域，具体涉及一种海洋蓝色双银低辐射镀膜玻璃，其结构为：玻璃基片/第一复合介质层/第一银层/第一保护层/第二复合介质层/第二银层/第二保护层/第三复合介质层；本发明反射色呈现海洋蓝色，能够完美替代海洋蓝原片，从不同角度观察，颜色皆稳定；不会出现不同批次颜色不一样的情况，同时可以提高生产效率。

Description

一种海洋蓝色双银低辐射镀膜玻璃
技术领域
本发明属于玻璃技术领域，具体涉及一种海洋蓝色双银低辐射镀膜玻璃。
背景技术
海洋蓝原片属于特殊颜色的浮法玻璃基片，与普通白玻基片工艺不同，所以海洋蓝原片采购价格较高、采购周期长，且存在不同浮法厂家的原片颜色有色差的情况，色玻又不宜大批量长期储存，因此使用海洋蓝原片成本高，不利于产品及时交货。
发明内容
为了解决上述问题，本发明的目的在于提供一种通过磁控溅射镀膜制得的海洋蓝色双银低辐射镀膜玻璃，该玻璃不仅颜色稳定，不会出现不同批次颜色不一样的情况，而且反射色呈现海洋蓝色，能够完美替代海洋蓝原片。
本发明是通过以下技术方案来实现的：
一种海洋蓝色双银低辐射镀膜玻璃，所述海洋蓝色双银低辐射镀膜玻璃的结构为：玻璃基片/第一复合介质层/第一银层/第一保护层/第二复合介质层/第二银层/第二保护层/第三复合介质层。
较佳地，所述第一复合介质层的厚度为28～40nm、第一银层的厚度为5～10nm、第一保护层的厚度为3～8nm、第二复合介质层的厚度为80～100nm、第二银层的厚度为10～15nm、第二保护层的厚度为3～5nm、第三复合介质层的厚度为30～40nm。
较佳地，所述第一复合介质层为氮化硅和氧化锌复合介质层；所述氮化硅的厚度为20～25nm，所述氧化锌的厚度为8～15nm。
较佳地，所述第一保护层和第二保护层为镍铬层。
较佳地，所述第二复合介质层为氮化硅/氧化锌锡/氧化锌/AZO(陶瓷掺铝氧化锌)。所述氮化硅的厚度为35～45nm、氧化锌锡的厚度为30～40nm、氧化锌的厚度为8～15nm、AZO(陶瓷掺铝氧化锌)的厚度为3～8nm。
较佳地，所述第三复合介质层为AZO(陶瓷掺铝氧化锌)层和化硅层；所述AZO(陶瓷掺铝氧化锌)的厚度为3～8nm、氮化硅的厚度为25～35nm。
较佳地，所述第一银层和第一保护层之间还设有厚度为5～10nm的金属铜层。
较佳地，所述海洋蓝色双银低辐射镀膜玻璃l*g为30～70，a*g为-10～5，b*g为-10～-40。
较佳地，所述海洋蓝色双银低辐射镀膜玻璃，玻面正面颜色：l*g为40～50，a*g为-3～-4，b*g为-18～-19；玻面45度侧面颜色：l*g为40～50，a*g为-4～-5，b*g为-16～-17。
其中，Lab色彩空间是由国际照明委员会(CIE)于1976年制定的。它是用L*、a*、b*三个互相垂直的坐标轴来表示一个色彩空间，L*轴表示明度，黑在底端，白在顶端。+a*表示红色，-a*表示绿色，+b*表示黄色，-b*表示蓝色，a*轴是红-绿色轴，b*轴是黄-蓝色轴。任何颜色的色相和特征都可以用a*、b*数值来表示，用L*、a*、b*三个数值可以描述自然界中的任何色彩。L*值的范围为100(白)至0(黑)，这样的最大范围在印刷品上并不能体现出来，对于优质铜版纸，L*值的范围不超过95(白)和5(黑)。a*和b*的变化范围从-100到100。任一颜色可以用空间中对应点的L*、a*、b*确定。
本发明采用普通白玻原片，通过磁控溅射镀膜，镀制了一种海洋蓝颜色的双银低辐射镀膜玻璃产品。本发明不需要额外颜料，其呈现的海洋蓝颜色是通过在优质浮法玻璃表面镀上多层金属、金属化合物薄膜后而获得的，镀膜玻璃的颜色为干涉色，当薄膜的光学厚度与某波长的可见光波长成一定倍数时主要反射该种可见光的颜色，光学上称为干涉光的颜色，即干涉色。干涉色因薄膜的厚度不同而变化。最终呈现的颜色与膜层结构、每层膜的厚度都有关系。该产品颜色稳定，不会出现不同批次颜色不一样的情况，反射色呈现海洋蓝色，能够完美替代海洋蓝原片，从而减少海洋蓝原片采购的问题，减少公司采购成本，同时可以提高生产效率，及时完成产品交货。
附图说明
图1为本发明的结构示意图；
图2为本发明的另一结构示意图
具体的实施方式
下面结合具体实施方式对本发明作进一步的详细说明，以助于本领域技术人员理解本发明。
实施例1
见图1，一种海洋蓝色双银低辐射镀膜玻璃，结构为：玻璃基片1/第一复合介质层21[氮化硅层(22nm)/氧化锌层(10nm)]/银层31(6nm)/金属铜层5(8nm)/镍铬层41(5nm)/第二复合介质层22[氮化硅层(40nm)/氧化锌锡层(35nm)/氧化锌层(10nm)/AZO层(5nm)]/银层32(13nm)/镍铬层42(4nm)/第三复合介质层23[AZO层(5nm)/氮化硅层(30nm)]。
实施例2
一种海洋蓝色双银低辐射镀膜玻璃，结构为：玻璃基片/氮化硅层(20nm)/氧化锌层(8nm)/银层(5nm)/金属铜层(5nm)/镍铬层(3nm)/氮化硅层(35nm)/氧化锌锡层(30nm)/氧化锌层(8nm)/AZO层(3nm)/银层(10nm)/镍铬层(3nm)/AZO层(3nm)/氮化硅层(25nm)。
实施例3
一种海洋蓝色双银低辐射镀膜玻璃，结构为：玻璃基片/氮化硅层(25nm)/氧化锌层(15nm)/银层(10nm)/金属铜层(10nm)/镍铬层(8nm)/氮化硅层(45nm)/氧化锌锡层(40nm)/氧化锌层(15nm)/AZO层(8nm)/银层(15nm)/镍铬层(5nm)/AZO层(8nm)/氮化硅层(35nm)。
实施例4
一种海洋蓝色双银低辐射镀膜玻璃，结构为：玻璃基片/氮化硅层(21nm)/氧化锌层(14nm)/银层(7nm)/金属铜层(6nm)/镍铬层(4nm)/氮化硅层(38nm)/氧化锌锡层(32nm)/氧化锌层(9nm)/AZO层(4nm)/银层(13nm)/镍铬层(4nm)/AZO层(7nm)/氮化硅层(31nm)。
实施例5
一种海洋蓝色双银低辐射镀膜玻璃，结构为：玻璃基片/氮化硅层(23nm)/氧化锌层(9nm)/银层(8nm)/金属铜层(7nm)/镍铬层(6nm)/氮化硅层(41nm)/氧化锌锡层(37nm)/氧化锌层(11nm)/AZO层(6nm)/银层(12nm)/镍铬层(4nm)/AZO层(4nm)/氮化硅层(26nm)。
实施例6
一种海洋蓝色双银低辐射镀膜玻璃，结构为：玻璃基片/氮化硅层(24nm)/氧化锌层(12nm)/银层(9nm)/金属铜层(9nm)/镍铬层(5nm)/氮化硅层(43nm)/氧化锌锡层(33nm)/氧化锌层(13nm)/AZO层(7nm)/银层(14nm)/镍铬层(5nm)/AZO层(6nm)/氮化硅层(27nm)。
实施例7
见图2，一种海洋蓝色双银低辐射镀膜玻璃，结构为：玻璃基片1/第一复合介质层21[氮化硅层(22nm)/氧化锌层(10nm)]/银层31(6nm)/镍铬层41(5nm)/第二复合介质层22[氮化硅层(40nm)/氧化锌锡层(35nm)/氧化锌层(10nm)/AZO层(5nm)]/银层32(13nm)/镍铬层42(4nm)/第三复合介质层23[AZO层(5nm)/氮化硅层(30nm)]。
实施例8
一种海洋蓝色双银低辐射镀膜玻璃，结构为：玻璃基片/氮化硅层(23nm)/氧化锌层(12nm)/银层(5nm)/镍铬层(8nm)/氮化硅层(45nm)/氧化锌锡层(30nm)/氧化锌层(8nm)/AZO层(4nm)/银层(10nm)/镍铬层(5nm)/AZO层(8nm)/氮化硅层(25nm)。
上述实施例，只是本发明的较佳实施例，并非用来限制本发明实施范围，故凡以本发明权利要求所述的特征及原理所做的等效变化或修饰，均应包括在本发明权利要求范围之内。
洋蓝色的双银产品光学参数：
玻面正面颜色(室外面的正面)：l*g为48.3，a*g为-3.28，b*g为-18.8；
玻面45度侧面颜色(室外面的侧面)：l*g为48.7，a*g为-4.36，b*g为-16.09，正面和侧面颜色基本不变，外观反射色均反纯正的海洋蓝色，能够完完美替代海洋蓝原片。

Claims (4)

1.一种海洋蓝色双银低辐射镀膜玻璃，其特征在于，所述海洋蓝色双银低辐射镀膜玻璃的结构为：玻璃基片/第一复合介质层/第一银层/第一保护层/第二复合介质层/第二银层/第二保护层/第三复合介质层；所述第一复合介质层的厚度为28～40nm、第一银层的厚度为5～10nm、第一保护层的厚度为3～8nm、第二复合介质层的厚度为80～100nm、第二银层的厚度为10～15nm、第二保护层的厚度为3～5nm、第三复合介质层的厚度为30～40nm；所述第一复合介质层为氮化硅和氧化锌复合介质层；所述氮化硅的厚度为20～25nm，所述氧化锌的厚度为8～15nm；所述第一保护层和第二保护层为镍铬层；所述第二复合介质层为氮化硅/氧化锌锡/氧化锌/AZO；所述氮化硅的厚度为35～45nm、氧化锌锡的厚度为30～40nm、氧化锌的厚度为8～15nm、AZO的厚度为3～8nm；所述第三复合介质层为AZO层和化硅层；所述AZO的厚度为3～8nm、氮化硅的厚度为25～35nm。
2.如权利要求1所述海洋蓝色双银低辐射镀膜玻璃，其特征在于，所述第一银层和第一保护层之间还设有厚度为5～10nm的金属铜层。
3.如权利要求1所述海洋蓝色双银低辐射镀膜玻璃，其特征在于，所述海洋蓝色双银低辐射镀膜玻璃l*g为30～70，a*g为-10～5，b*g为-10～-40。
4.如权利要求3所述海洋蓝色双银低辐射镀膜玻璃，其特征在于，所述海洋蓝色双银低辐射镀膜玻璃，玻面正面颜色：l*g为40～50，a*g为-3～-4，b*g为-18～-19；玻面45度侧面颜色：l*g为40～50，a*g为-4～-5，b*g为-16～-17。
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CN106746732A (zh) * 2017-01-19 2017-05-31 吴江南玻华东工程玻璃有限公司 一种无偏振光干扰色的纳米涂层玻璃
CN107586047B (zh) * 2017-09-04 2020-08-21 咸宁南玻节能玻璃有限公司 一种天空蓝双银低辐射镀膜玻璃及制备方法
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