CN105594837A - Processing method of freeze-dried Chinese wolfberries with pedicles - Google Patents

Processing method of freeze-dried Chinese wolfberries with pedicles Download PDF

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Publication number
CN105594837A
CN105594837A CN201510985253.3A CN201510985253A CN105594837A CN 105594837 A CN105594837 A CN 105594837A CN 201510985253 A CN201510985253 A CN 201510985253A CN 105594837 A CN105594837 A CN 105594837A
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CN
China
Prior art keywords
fruit
freeze
drying
base
matrimony vine
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201510985253.3A
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Chinese (zh)
Inventor
帅放文
王向峰
章家伟
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Ningxia county is in the south of the Yangtze River wolfberry products Co. Ltd.
Original Assignee
Hunan Er Kang Pharmaceutical Co Ltd
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Publication date
Application filed by Hunan Er Kang Pharmaceutical Co Ltd filed Critical Hunan Er Kang Pharmaceutical Co Ltd
Priority to CN201510985253.3A priority Critical patent/CN105594837A/en
Publication of CN105594837A publication Critical patent/CN105594837A/en
Pending legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23BPRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
    • A23B7/00Preservation or chemical ripening of fruit or vegetables
    • A23B7/02Dehydrating; Subsequent reconstitution
    • A23B7/024Freeze-drying, i.e. cryodessication or lyophilisation

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Preparation Of Fruits And Vegetables (AREA)
  • Storage Of Fruits Or Vegetables (AREA)

Abstract

The invention discloses a processing method of freeze-dried Chinese wolfberries with pedicles. The processing method is characterized by comprising technological procedures of raw material screening, cleaning, sterilization, vacuum freeze-drying, damp-proof packaging and the like. The freeze-dried Chinese wolfberries prepared with the method have the green pedicels, are almost consistent with fresh Chinese wolfberries in appearance, have the bright color and full grains and are fragrant, crisp and delicious, the storage time is long, and nutritional ingredients in the fresh Chinese wolfberries can be reserved to the maximum extent.

Description

A kind of processing method with base of a fruit freeze-drying matrimony vine
Technical field
The present invention relates to health food manufacture field, be specifically related to a kind of processing method with base of a fruit freeze-drying matrimony vine.
Background technology
Matrimony vine is traditional rare traditional Chinese medicine, is again a kind of tonic food. In the traditional Chinese medical science, think that the flat taste of matrimony vine property is sweet, there is effect of benefiting shrewd head, moistening lung. And matrimony vine contains the nutritional labelings such as abundant natural Beta-carotene, vitamin C, matrimony vine proteoglycan, betaine, linoleic acid and iron, phosphorus, calcium, there is qi-restoratives to calm the nerves, improving eyesight is dispeled the wind, nourshing kidney moistening lung and protect the effects such as liver is antitumor. But the shelf-life of medlar fresh fruit is extremely of short duration, in preparation process, easily there is again the loss of secondary pollution and nutritional labeling taking the dry dried fruit of lycium barbarum as master of traditional airing system, have a strong impact on the development of matrimony vine industry.
The fast development of freeze drying technology, has solved the problem occurring in airing technical process effectively. Existing freeze-drying matrimony vine technology generally need to be passed through raw material selection, sorting and impurity elimination, once cleaning, dewaxing treatment, secondary cleaning, vacuum freeze drying and packaging and other steps (patent publication No.: CN104543843). Medlar fresh fruit epidermis and base of fruit are destroyed serious but carried out twice common cleaning and dewaxing treatment in this technology implementation process, cause that final products base of fruit comes off, craping deform, had a strong impact on mouthfeel and outward appearance; In addition, in vacuum freeze drying process, utilize the mode freeze-drying medlar fresh fruit that shelf gradient-heated heats up to cause the moisture of final products too high, have a strong impact on its mouthfeel.
Summary of the invention
The present invention relates to a kind of processing method with base of a fruit freeze-drying matrimony vine, its unique distinction is, comprises following methods program:
(1) raw material screening: select scarlet full band base of a fruit medlar fresh fruit, remove impurity and bad fruit;
(2) clean: the impurity on medlar fresh fruit surface and silt are cleaned up by purified water, drain surface moisture;
(3) sterilization: the band base of a fruit medlar fresh fruit ethanolic solution obtaining is carried out to sterilization processing;
(4) vacuum freeze drying: the band base of a fruit medlar fresh fruit obtaining is put into freeze drier, treat that temperature reaches below 40 DEG C, vacuum freeze drying, moisture≤5% of control final products;
(5) damp-prrof packing;
(6) finished product carries out sterilizing with ultraviolet irradiation method.
2. in program (2), use purified water to clean in the mode of atomizing spray by conveyer belt the medlar fresh fruit obtaining. Regulating the scavenging period of the rotating speed control medlar fresh fruit of conveyer belt is 5 ~ 8min. Atomizing spray can reduce the damage of medlar fresh fruit epidermis in cleaning process and coming off of base of fruit to greatest extent, ensures that final products full grains come off without distortion, the complete nothing of base of fruit.
3. in program (3), use ethanolic solution to carry out sterilization in the mode of atomizing spray the medlar fresh fruit obtaining by conveyer belt, wherein the volume fraction of ethanolic solution is 70% ~ 75%. Regulating the sterilizing time of the rotating speed control medlar fresh fruit of conveyer belt is 5 ~ 8min.
In program (4) by the band base of a fruit medlar fresh fruit obtaining evenly, be layered in stainless steel freeze-drying pallet individual layer, put in the drying box of freeze drier, in the time that temperature of charge reaches below-40 DEG C, open vavuum pump, maintaining after 60 ~ 90min, in 30min, be warming up to-20 DEG C, after reaching-20 DEG C, in 30min, be cooled to-40 DEG C, keep, after 90 ~ 120min, dividing plate being carried out to temperature programming
Temperature programming method is:
Do not keep 30 ~ 120min higher than-40 DEG C in temperature;
In 90 ~ 120min, be warming up to-25 DEG C ~-20 DEG C, keep 200 ~ 360min;
In 50 ~ 90min, be warming up to-10 DEG C ~ 0 DEG C, keep 250 ~ 450min
In 60 ~ 160min, be warming up to 15 ~-20 DEG C,
In 60 ~ 160min, be warming up to 25 ~-30 DEG C,
In 30 ~ 80min, be warming up to 40 ~ 45 DEG C, keep 360 ~ 480min.
5. the band base of a fruit freeze-drying matrimony vine obtaining in program (5), at 20 ± 5 DEG C, is packed in the environment of relative humidity≤30%, adds food desiccant in packaging bag.
In program (6) by the packed band base of a fruit freeze-drying matrimony vine obtaining with 2500 ~ 5000 kilorad irradiation 60 ~ 120min to the finished product sterilization that carries out disinfection.
Beneficial effect of the present invention is, has fundamentally solved the problems such as the particle shrinkage, the color and luster that occur in airing technique are gloomy, secondary pollution, nutrient loss, has realized process innovation from many-sides such as taste, health, nutrition. The band base of a fruit freeze-drying matrimony vine lovely luster, the base of fruit that utilize the present invention to process be complete not to come off, full grains without distortion, nutritional labeling without loss.
Detailed description of the invention
Embodiment 1:
Hand picking lovely luster, full grains, the band base of a fruit medlar fresh fruit that fruit is complete, and remove the impurity such as blade, branch, gravel and bad fruit. Then band base of a fruit medlar fresh fruit is placed on conveyer belt, cleans surperficial impurity and silt by purified water by the mode of atomizing spray, it is 5min that the rotating speed of adjusting conveyer belt makes its scavenging period. Then band base of a fruit fresh fruit is placed on conveyer belt, the ethanolic solution that is 75% by volume fraction carries out sterilization by the mode of atomizing spray, and it is 5min that the rotating speed of adjusting conveyer belt makes its sterilizing time.
By the band base of a fruit medlar fresh fruit after sterilization evenly, be layered in stainless steel freeze-drying pallet, put in the drying box of freeze drier individual layer. In the time that temperature of charge reaches below-40 DEG C, open vavuum pump, maintaining after 60 ~ 90min, in 30min, be warming up to-20 DEG C, in 30min, be cooled to-40 DEG C after reaching-20 DEG C, keep, after 90 ~ 120min, dividing plate being carried out to temperature programming,
Temperature programming method is:
Do not keep 90min higher than-40 DEG C in temperature;
In 90min, be warming up to-25 DEG C, keep 200min;
In 50min, be warmed up to-10 DEG C, keep 250min
In 60min, be warmed up to-10 DEG C,
In 160min, be warmed up to 25 DEG C,
In 80min, heat up 45 DEG C, keep 480min.
Qualified freeze-drying matrimony vine, at 25 DEG C, is packed with sealed bag in the environment of relative air humidity 25%, and add food desiccant.
Sampling, the method specifying by GB/T18672-2014 standard, the moisture of measuring final products is 3%.
Embodiment 2:
Hand picking lovely luster, full grains, the band base of a fruit medlar fresh fruit that fruit is complete, and remove the impurity such as blade, branch, gravel and bad fruit. Then band base of a fruit medlar fresh fruit is placed on conveyer belt, cleans surperficial impurity and silt by purified water by the mode of atomizing spray, it is 8min that the rotating speed of adjusting conveyer belt makes its scavenging period, artificial removal's carpopodium after draining away the water. Then fresh fruit is placed on conveyer belt, the ethanolic solution that is 70% by volume fraction carries out sterilization by the mode of atomizing spray, and it is 8min that the rotating speed of adjusting conveyer belt makes its sterilizing time.
By the band base of a fruit medlar fresh fruit after sterilization evenly, be layered in stainless steel freeze-drying pallet, put in the drying box of freeze drier individual layer. In the time that temperature of charge reaches below-40 DEG C, open vavuum pump, maintaining after 60 ~ 90min, in 30min, be warming up to-20 DEG C, in 30min, be cooled to-40 DEG C after reaching-20 DEG C, keep, after 90 ~ 120min, dividing plate being carried out to temperature programming,
Temperature programming method is:
Do not keep 120min higher than-40 DEG C in temperature;
In 120min, be warming up to-20 DEG C, keep 360min;
In 60min, be warmed up to 0 DEG C, keep 450min
In 120min, be warmed up to 0 DEG C,
In 120min, be warmed up to 20 DEG C,
In 60min, heat up 45 DEG C, keep 420min.
Qualified freeze-drying matrimony vine, at 25 DEG C, is packed with sealed bag in the environment of relative air humidity 22%, and add food desiccant.
Sampling, the method specifying by GB/T18672-2014 standard, the moisture of measuring final products is 2%.
Embodiment 3:
Hand picking lovely luster, full grains, the band base of a fruit medlar fresh fruit that fruit is complete, and remove the impurity such as blade, branch, gravel and bad fruit. Then band base of a fruit medlar fresh fruit is placed on conveyer belt, cleans surperficial impurity and silt by purified water by the mode of atomizing spray, it is 6min that the rotating speed of adjusting conveyer belt makes its scavenging period, artificial removal's carpopodium after draining away the water. Then fresh fruit is placed on conveyer belt, the ethanolic solution that is 72% by volume fraction carries out sterilization by the mode of atomizing spray, and it is 6min that the rotating speed of adjusting conveyer belt makes its sterilizing time.
By the band base of a fruit medlar fresh fruit after sterilization evenly, be layered in stainless steel freeze-drying pallet, put in the drying box of freeze drier individual layer. In the time that temperature of charge reaches below-40 DEG C, open vavuum pump, maintaining after 60 ~ 90min, in 30min, be warming up to-20 DEG C, in 30min, be cooled to-40 DEG C after reaching-20 DEG C, keep, after 90 ~ 120min, dividing plate being carried out to temperature programming,
Temperature programming method is:
Do not keep 60min higher than-40 DEG C in temperature;
In 100min, be warming up to-22 DEG C, keep 280min;
In 80min, be warmed up to-5 DEG C, keep 300min
In 100min, be warmed up to 10 DEG C,
In 100min, be warmed up to 25 DEG C,
In 40min, heat up 40 DEG C, keep 400min.
Qualified freeze-drying matrimony vine, at 25 DEG C, is packed with sealed bag in the environment of relative air humidity 22%, and add food desiccant.
Sampling, the method specifying by GB/T18672-2014 standard, the moisture of measuring final products is 4%.
Before and after freeze-drying, all the band base of a fruit FRUCTUS LYCII grain of above each embodiment is sampled, every embodiment gets 5 increments, observes mode of appearance, measures average grain diameter, tastes taste. Testing result is as shown in the table.
Result shows, after the freeze-drying that this method obtains, is with base of a fruit matrimony vine size almost not dwindle. Color and luster is ruddy, and it is green that carpopodium keeps, and slightly firmly can extract. Fruit feel is harder, the one-tenth powder of pinching, and taste is extremely sweet, and aftertaste and fresh fructus lycii are basically identical, and mouthfeel slightly sticks to one's teeth.
Separately get matrimony vine after each embodiment freeze-drying, use proper amount of clear water to bubble open, observe its water suction recovery situation, and with fresh fructus lycii contrast, after finding that it fully absorbs water, outward appearance and fresh fructus lycii are basically identical, mouthfeel is slightly soft, taste is basically identical.

Claims (6)

1. the processing method with base of a fruit freeze-drying matrimony vine, is characterized in that, comprises following process:
(1) raw material screening: select scarlet full band base of a fruit medlar fresh fruit, remove impurity and bad fruit;
(2) clean: the impurity on medlar fresh fruit surface and silt are cleaned up by purified water, drain surface moisture;
(3) sterilization: the band base of a fruit medlar fresh fruit ethanolic solution obtaining is carried out to sterilization processing;
(4) vacuum freeze drying: the band base of a fruit medlar fresh fruit obtaining is put into freeze drier, treat that temperature reaches below 40 DEG C, vacuum freeze drying, moisture≤5% of control final products;
(5) damp-prrof packing;
(6) finished product carries out sterilizing with ultraviolet irradiation method.
2. the processing method with base of a fruit freeze-drying matrimony vine according to claim 1, is characterized in that: in program (2), use purified water to clean in the mode of atomizing spray the medlar fresh fruit obtaining by conveyer belt.
3. the processing method with base of a fruit freeze-drying matrimony vine according to claim 1, is characterized in that: in program (3), use ethanolic solution to carry out sterilization in the mode of atomizing spray the medlar fresh fruit obtaining by conveyer belt, wherein the volume fraction of ethanolic solution is 70% ~ 75%.
4. the processing method with base of a fruit freeze-drying matrimony vine according to claim 1, it is characterized in that: in program (4) by the band base of a fruit medlar fresh fruit obtaining evenly, be layered in stainless steel freeze-drying pallet individual layer, put in the drying box of freeze drier, in the time that temperature of charge reaches below-40 DEG C, open vavuum pump, maintaining after 60 ~ 90min, in 30min, be warming up to-20 DEG C, in 30min, be cooled to-40 DEG C after reaching-20 DEG C, keep after 90 ~ 120min, dividing plate is carried out to temperature programming
Temperature programming method is:
Do not keep 30 ~ 120min higher than-40 DEG C in temperature;
In 90 ~ 120min, be warming up to-25 DEG C ~-20 DEG C, keep 200 ~ 360min;
In 50 ~ 90min, be warming up to-10 DEG C ~ 0 DEG C, keep 250 ~ 450min
In 60 ~ 160min, be warming up to 15 ~-20 DEG C,
In 60 ~ 160min, be warming up to 25 ~-30 DEG C,
In 30 ~ 80min, be warming up to 40 ~ 45 DEG C, keep 360 ~ 480min.
5. the processing method with base of a fruit freeze-drying matrimony vine according to claim 1, is characterized in that: the band base of a fruit freeze-drying matrimony vine obtaining in program (5), at 20 ± 5 DEG C, is packed in the environment of relative humidity≤30%, adds food desiccant in packaging bag.
6. the processing method with base of a fruit freeze-drying matrimony vine according to claim 1, is characterized in that: in program (6) by the packed band base of a fruit freeze-drying matrimony vine obtaining with 2500 ~ 5000 kilorad irradiation 60 ~ 120min to the finished product sterilization that carries out disinfection.
CN201510985253.3A 2015-12-25 2015-12-25 Processing method of freeze-dried Chinese wolfberries with pedicles Pending CN105594837A (en)

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Application Number Priority Date Filing Date Title
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107242424A (en) * 2017-06-07 2017-10-13 大连海升果业有限责任公司 A kind of preparation method of serviceberry freeze-dried powder
CN109588655A (en) * 2018-10-16 2019-04-09 湖南奇异生物科技有限公司 A kind of preparation method of antifatigue gumbo piece

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104543843A (en) * 2015-01-14 2015-04-29 宁夏森淼种业生物工程有限公司 Method for processing freeze-dried Chinese wolfberry

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104543843A (en) * 2015-01-14 2015-04-29 宁夏森淼种业生物工程有限公司 Method for processing freeze-dried Chinese wolfberry

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
柴京福: "枸杞子的干制机理和干燥方法", 《农区牧区机械化》 *

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107242424A (en) * 2017-06-07 2017-10-13 大连海升果业有限责任公司 A kind of preparation method of serviceberry freeze-dried powder
CN107242424B (en) * 2017-06-07 2020-12-08 大连海升果业有限责任公司 Preparation method of mountain ash fruit freeze-dried powder
CN109588655A (en) * 2018-10-16 2019-04-09 湖南奇异生物科技有限公司 A kind of preparation method of antifatigue gumbo piece

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C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C41 Transfer of patent application or patent right or utility model
CB03 Change of inventor or designer information

Inventor after: Chen Hong

Inventor before: Shuai Fangwen

Inventor before: Wang Xiangfeng

Inventor before: Zhang Jiawei

COR Change of bibliographic data
TA01 Transfer of patent application right

Effective date of registration: 20161229

Address after: 751200 the Ningxia Hui Autonomous Region city centre in the County International Trading Center Building No. 36 West wolfberry

Applicant after: Ningxia county is in the south of the Yangtze River wolfberry products Co. Ltd.

Address before: 410331 Hunan province Changsha city Changsha national biological industry base No. 167 Kangping Road, Hunan Kang pharmaceutical Limited by Share Ltd

Applicant before: Hunan Er-Kang Pharmaceutical Co., Ltd.

RJ01 Rejection of invention patent application after publication
RJ01 Rejection of invention patent application after publication

Application publication date: 20160525