CN105581950A - Method for utilizing seaweed extract for preparing whitening and freckle removing seaweed paste - Google Patents
Method for utilizing seaweed extract for preparing whitening and freckle removing seaweed paste Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/676—Ascorbic acid, i.e. vitamin C
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
- A61K8/988—Honey; Royal jelly, Propolis
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/591—Mixtures of compounds not provided for by any of the codes A61K2800/592 - A61K2800/596
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Abstract
The invention relates to a method for utilizing seaweed extract for preparing whitening and freckle removing seaweed paste. According to the method, seaweed is cleaned and added into a reaction kettle containing a mixture of water and organic solvent, after high-speed stirring and pulping are carried out, a wetting penetrating agent is added, soaking extraction is carried out, some organic solvent is recovered by means of low-temperature and low-pressure distillation, seaweed residues and seaweed extract are obtained in a filter-pressing mode, the seaweed extract, a surfactant, a moisture preserving agent, a pearling agent and a whitening and freckle removing nutrient substance are mixed according to a certain mass ratio, and stirred uniformly to obtain the whitening and freckle removing seaweed paste. The seaweed rich in abundant protein, seaweed polysaccharides, seaweed acid, microelements and vitamins can supplement nutrition of skin, promote blood circulation, remove cutin, accelerate metabolism of the skin and make the skin smooth and elastic.
Description
Technical field
The present invention relates to a kind of method of utilizing seaweed extracted liquor to prepare water soluble algae skin-whitening speckle-removing cream.
Background technology
The method that current marine alga cosmetics are prepared seaweed extracted liquor is mainly the simple pulverizing of marine alga warp or poach and other nutritional labeling and mixes, and such extraction is very incomplete, causes a large amount of active components wastes of marine alga, and cosmetics do not reach gratifying effect yet.
Summary of the invention
Technical problem to be solved by this invention is that a kind of method of utilizing seaweed extracted liquor to prepare marine alga skin-whitening speckle-removing cream is provided. The method, by seaweed extracted liquor, surfactant, NMF, pearling agent and the perfect adaptation of whitening spot-removing nutriment, maximizes the effect of performance seaweed paste whitening spot-removing.
In order to solve the problems of the technologies described above, the present invention by the following technical solutions:
1), by fresh marine alga clean for subsequent use, or dry seaweed be dipped to and fresh marine alga moisture consistent state and clean for subsequent use, the alternate products that this step obtains is called A product;
2), deionized water, organic solvent and product A are joined respectively in reactor, pull an oar in the lump;
3), add wetting and penetrating agent after having broken slurry, at 20～45 DEG C, soak 12～72 hours;
4), low-temp low-pressure Distillation recovery part organic solvent: vapo(u)rizing temperature is 45～65 DEG C, and distillation pressure is-0.5～-1.2Mpa;
5), press filtration obtains marine alga slag and filtrate, described filtrate is seaweed extracted liquor;
6), by described seaweed extracted liquor, surfactant, NMF, pearling agent and whitening spot-removing nutriment according to certain mass than mix, after stirring, be marine alga skin-whitening speckle-removing cream;
Wherein the mass ratio of A product, deionized water, organic solvent and wetting and penetrating agent is 5～30:10～85:10～85:0.1～5; The mass ratio of seaweed extracted liquor, surfactant, NMF, pearling agent and whitening spot-removing nutriment is 5～85:1～50:1～50:1～50:5～85.
Described organic solvent is the two or more of a kind of or arbitrary proportion in pharmaceutical grade ethanol, pharmaceutical grade propane diols and pharmaceutical grade glycerine.
Described wetting and penetrating agent is neopelex, lauryl sodium sulfate, APES, sorbitan fatty acid ester-20, sorbitan fatty acid ester-30, sorbitan fatty acid ester-80, polyoxyethylene 20 sorbitan monolaurate-20, polyoxyethylene 20 sorbitan monolaurate-40, polyoxyethylene 20 sorbitan monolaurate-60, polyoxyethylene 20 sorbitan monolaurate-80, AEO-3, AEO-4, AEO-5, AEO-7, AEO-9, AEO-15, AEO-20, a kind of or arbitrary proportion in AEO-23 and dimethicone two or more,
Described surfactant is neopelex, sorbitan fatty acid ester-20, sorbitan fatty acid ester-30, sorbitan fatty acid ester-80, polyoxyethylene 20 sorbitan monolaurate-20, polyoxyethylene 20 sorbitan monolaurate-40, polyoxyethylene 20 sorbitan monolaurate-60, polyoxyethylene 20 sorbitan monolaurate-80, AEO-3, AEO-4, AEO-5, AEO-7, AEO-9, AEO-15, AEO-20, a kind of or arbitrary proportion in AEO-23 and dimethicone two or more,
Described NMF is the two or more of a kind of or arbitrary proportion in propane diols, glycerine and sorbierite; Described pearling agent is the two or more of a kind of or arbitrary proportion in stearic acid diethylene glycol dilaurate, EGDS, mica powder and pearl powder; Described whitening spot-removing nutriment is the two or more of a kind of or arbitrary proportion in honey, vitamin C, rose ethereal oil, root of Dahurain angelica extract, bighead atractylodes rhizome extract, burdock extract and rhizoma typhonii extract;
Described marine alga refers to: a kind of or arbitrary proportion in sea-tangle, laver, kelp, opotism and Enteromorpha two or more;
Described in step 5), it is 1200～4500 orders that filter press is selected filter cloth aperture.
The present invention has following useful technique effect:
1, in the present invention, marine alga liquid adopts low temperature, Low Voltage Pure physics to extract, and has ensured that marine alga active ingredient is not destroyed.
2, seaweeds appearance has the diaphragm of one deck thickness, prevent external substance intrusion, so simple water or organic solvent extract at normal temperatures and pressures can be very slow, the present invention adds wetting and penetrating agent can increase the compatibility of water, organic solvent and marine alga, make water and organic solvent in the situation that normal temperature, normal pressure do not damage diaphragm, rapid osmotic marine alga diaphragm, thus reach the object of rapid extraction, be therefore more convenient for the application of heavy industrialization; Wetting and penetrating agent can also impel in marine alga in active ingredient rapid osmotic skin, improves the utilization rate of active component.
3, the present invention adopts the extracting method that deionized water and organic solvent combine, than extracting and reduced cost with organic solvent merely.
4, the present invention adopts the extracting method that water and organic solvent combine, and has increased the compatibility of product.
5, the present invention is by seaweed extracted liquor, surfactant, NMF, pearling agent and the combination of whitening spot-removing nutriment, and whitening spot-removing is remarkably productive.
Detailed description of the invention
Further illustrate the present invention below in conjunction with instantiation.
Embodiment 1
Fresh Laminaria Japonica after cleaning is joined and fills deionized water, pharmaceutical grade ethanol, in the reactor of pharmaceutical grade propane diols and pharmaceutical grade glycerine, pull an oar, after making beating, add the neopelex as wetting and penetrating agent, APES, sorbitan fatty acid ester-60 and dimethicone, Fresh Laminaria Japonica, deionized water, pharmaceutical grade ethanol, pharmaceutical grade propane diols, pharmaceutical grade glycerine, neopelex, APES, sorbitan fatty acid ester-60 and dimethicone are according to mass ratio 18:18:20:15:28:0.2:0.3:0.3:0.2, soak 46 hours at 30 DEG C, in negative pressure 1.0Mpa, Distillation recovery part organic solvent at 55 DEG C of temperature, filter press adopts 2500 order filter clothes to carry out press filtration, gained filtrate, sorbitan fatty acid ester-30, polyoxyethylene 20 sorbitan monolaurate-20, polyoxyethylene 20 sorbitan monolaurate-40, AEO-3, glycerine, propane diols, sorbierite, stearic acid diethylene glycol dilaurate, EGDS, mica powder, honey, vitamin C, rose ethereal oil, root of Dahurain angelica extract, bighead atractylodes rhizome extract, burdock extract and rhizoma typhonii extract mix according to mass ratio 10:5:5:5:2:5:5:5:3:4:2:6:2:8:9:10:6:8, after stirring, are marine alga skin-whitening speckle-removing cream.
Embodiment 2
Fresh Laminaria Japonica after cleaning is joined and fills deionized water, pharmaceutical grade ethanol, in the reactor of pharmaceutical grade propane diols and pharmaceutical grade glycerine, pull an oar, after making beating, add the neopelex as wetting and penetrating agent, APES, sorbitan fatty acid ester-60 and dimethicone, Fresh Laminaria Japonica, deionized water, pharmaceutical grade ethanol, pharmaceutical grade propane diols, pharmaceutical grade glycerine, neopelex, APES, sorbitan fatty acid ester-60 and dimethicone are according to mass ratio 18:18:20:15:28:0.2:0.3:0.3:0.2, soak 46 hours at 30 DEG C, in negative pressure 1.0Mpa, Distillation recovery part organic solvent at 55 DEG C of temperature, filter press adopts 2500 order filter clothes to carry out press filtration, gained filtrate, sorbitan fatty acid ester-30, AEO-9, glycerine, sorbierite, stearic acid diethylene glycol dilaurate, EGDS, mica powder, honey, vitamin C, rose ethereal oil, root of Dahurain angelica extract, bighead atractylodes rhizome extract, burdock extract and rhizoma typhonii extract mix according to mass ratio 30:10:5:2:3:4:3:2:2:6:10:8:5:6:4, after stirring, are marine alga skin-whitening speckle-removing cream.
Embodiment 3
Fresh Laminaria Japonica after cleaning is joined and fills deionized water, pharmaceutical grade ethanol, in the reactor of pharmaceutical grade propane diols and pharmaceutical grade glycerine, pull an oar, after making beating, add the neopelex as wetting and penetrating agent, APES, sorbitan fatty acid ester-60 and dimethicone, Fresh Laminaria Japonica, deionized water, pharmaceutical grade ethanol, pharmaceutical grade propane diols, pharmaceutical grade glycerine, neopelex, APES, sorbitan fatty acid ester-60 and dimethicone are according to mass ratio 18:18:20:15:28:0.2:0.3:0.3:0.2, soak 46 hours at 30 DEG C, in negative pressure 1.0Mpa, Distillation recovery part organic solvent at 55 DEG C of temperature, filter press adopts 2500 order filter clothes to carry out press filtration, gained filtrate, sorbitan fatty acid ester-30, dimethicone, sorbierite, stearic acid diethylene glycol dilaurate, EGDS, mica powder, honey, vitamin C, rose ethereal oil, root of Dahurain angelica extract, bighead atractylodes rhizome extract, burdock extract and rhizoma typhonii extract mix according to mass ratio 35:5:10:8:2:4:2:4:7:5:4:2:5:7, after stirring, are marine alga skin-whitening speckle-removing cream.
Embodiment 4
Fresh Laminaria Japonica after cleaning is joined and fills deionized water, pharmaceutical grade ethanol, in the reactor of pharmaceutical grade propane diols and pharmaceutical grade glycerine, pull an oar, after making beating, add the neopelex as wetting and penetrating agent, APES, sorbitan fatty acid ester-60 and dimethicone, Fresh Laminaria Japonica, deionized water, pharmaceutical grade ethanol, pharmaceutical grade propane diols, pharmaceutical grade glycerine, neopelex, APES, sorbitan fatty acid ester-60 and dimethicone are according to mass ratio 18:18:20:15:28:0.2:0.3:0.3:0.2, soak 46 hours at 30 DEG C, in negative pressure 1.0Mpa, Distillation recovery part organic solvent at 55 DEG C of temperature, filter press adopts 2500 order filter clothes to carry out press filtration, gained filtrate, sorbitan fatty acid ester-30, AEO-7, AEO-9, glycerine, stearic acid diethylene glycol dilaurate, EGDS, mica powder, honey, vitamin C, rose ethereal oil, root of Dahurain angelica extract, bighead atractylodes rhizome extract, burdock extract and rhizoma typhonii extract mix according to mass ratio 35:3:3:4:3:3:7:4:6:4:10:4:5:6:3, after stirring, are marine alga skin-whitening speckle-removing cream.
Further illustrate beneficial effect of the present invention below in conjunction with experimental data:
The filtrate of collecting for Different Extraction Method on market, carries out the detection of algal polysaccharides after low temperature drying, testing result is as table 1.
Table 1
| Comminuting method | Water-boiling method | Pulverize water-boiling method | The inventive method | |
| Algal polysaccharides (%) | 10.2 | 18.2 | 26.4 | 42.1 |
Adopt as can be seen from Table 1 in the seaweed extracted liquor of this method algal polysaccharides content the highest.
1 physical data
Inventor collects altogether 400 examples between year November in May, 2014 to 2015, and the women of age between 28 to 42 years old does effect comparison for common skin-whitening speckle-removing cream (except not adding seaweed extracted liquor, other preparation method is identical with embodiment 2), embodiment 2.
1.2 experimental technique
Evenly being applied in facial skin, every day 1 time, 4 months is one-period.
1.3 experimental design
400 people are divided into 2 groups, and every group of 200 people test respectively.
2 experimental results
Common skin-whitening speckle-removing cream (except not adding seaweed extracted liquor, other preparation method is identical with embodiment 2) investigation satisfaction is 72.4%; It is 86.5% that embodiment 2 investigates satisfaction. Be satisfied with standard: to skin nonirritant, after use, obviously feel comfortably cool, soft, without greasy feeling, skin gloss is flexible, whitening effect is obvious, on the face spot obviously desalination even disappear.
3 discuss
An experiment product for the different manufacturers Different Extraction Method that can collect on market, do algal polysaccharides detection, what city's field energy was collected certainly is not necessarily best, and notebook data can only illustrate that product of the present invention is better than the most like products that can collect on market; Being formed with much because endocrine goes wrong and causes of spot, wanting thoroughly to dispel needs health conditioning and cosmetics to coordinate, and just can reach most desired effect.
Claims (5)
1. utilize seaweed extracted liquor to prepare a method for marine alga skin-whitening speckle-removing cream, it is characterized in that carrying out according to following steps:
1), by fresh marine alga clean for subsequent use, or dry seaweed be dipped to and fresh marine alga moisture consistent state and clean for subsequent use, the alternate products that this step obtains is called A product;
2), deionized water, organic solvent and product A are joined respectively in reactor, pull an oar in the lump;
3), add wetting and penetrating agent after having broken slurry, at 20～45 DEG C, soak 12～72 hours;
4), low-temp low-pressure Distillation recovery part organic solvent: vapo(u)rizing temperature is 45～65 DEG C, and distillation pressure is-0.5～-1.2Mpa;
5), press filtration obtains marine alga slag and filtrate, described filtrate is seaweed extracted liquor;
6), by described seaweed extracted liquor, surfactant, NMF, pearling agent and whitening spot-removing nutriment according to certain mass than mix, after stirring, be marine alga skin-whitening speckle-removing cream;
Wherein the mass ratio of A product, deionized water, organic solvent and wetting and penetrating agent is 5～30:10～85:10～85:0.1～5; The mass ratio of seaweed extracted liquor, surfactant, NMF, pearling agent and whitening spot-removing nutriment is 5～85:1～50:1～50:1～50:5～85.
2. the method for utilizing seaweed extracted liquor to prepare marine alga skin-whitening speckle-removing cream as claimed in claim 1, is characterized in that: described organic solvent is the two or more of a kind of or arbitrary proportion in pharmaceutical grade ethanol, pharmaceutical grade propane diols and pharmaceutical grade glycerine.
3. the method for utilizing seaweed extracted liquor to prepare marine alga skin-whitening speckle-removing cream as claimed in claim 1, it is characterized in that: described wetting and penetrating agent is neopelex, lauryl sodium sulfate, APES, sorbitan fatty acid ester-20, sorbitan fatty acid ester-30, sorbitan fatty acid ester-80, polyoxyethylene 20 sorbitan monolaurate-20, polyoxyethylene 20 sorbitan monolaurate-40, polyoxyethylene 20 sorbitan monolaurate-60, polyoxyethylene 20 sorbitan monolaurate-80, AEO-3, AEO-4, AEO-5, AEO-7, AEO-9, AEO-15, AEO-20, a kind of or arbitrary proportion in AEO-23 and dimethicone two or more, described surfactant is neopelex, sorbitan fatty acid ester-20, sorbitan fatty acid ester-30, sorbitan fatty acid ester-80, polyoxyethylene 20 sorbitan monolaurate-20, polyoxyethylene 20 sorbitan monolaurate-40, polyoxyethylene 20 sorbitan monolaurate-60, polyoxyethylene 20 sorbitan monolaurate-80, AEO-3, AEO-4, AEO-5, AEO-7, AEO-9, AEO-15, AEO-20, a kind of or arbitrary proportion in AEO-23 and dimethicone two or more, described NMF is the two or more of a kind of or arbitrary proportion in propane diols, glycerine and sorbierite, described pearling agent is the two or more of a kind of or arbitrary proportion in stearic acid diethylene glycol dilaurate, EGDS, mica powder and pearl powder, described whitening spot-removing nutriment is the two or more of a kind of or arbitrary proportion in honey, vitamin C, rose ethereal oil, root of Dahurain angelica extract, bighead atractylodes rhizome extract, burdock extract and rhizoma typhonii extract.
4. the method for utilizing seaweed extracted liquor to prepare marine alga skin-whitening speckle-removing cream as claimed in claim 1, is characterized in that: described marine alga refers to: a kind of or arbitrary proportion in sea-tangle, laver, kelp, opotism and Enteromorpha two or more.
5. the method for utilizing seaweed extracted liquor to prepare marine alga skin-whitening speckle-removing cream as claimed in claim 1, is characterized in that: described in step 5), it is 1200～4500 orders that filter press is selected filter cloth aperture.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106902031A (en) * | 2017-03-24 | 2017-06-30 | 福建师范大学 | A kind of preparation method of the moisturizing cream containing seaweed extracted liquor |
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