CN105568689A - 沙发布阻燃成品发泡胶及其制备方法 - Google Patents

沙发布阻燃成品发泡胶及其制备方法 Download PDF

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CN105568689A
CN105568689A CN201511015472.5A CN201511015472A CN105568689A CN 105568689 A CN105568689 A CN 105568689A CN 201511015472 A CN201511015472 A CN 201511015472A CN 105568689 A CN105568689 A CN 105568689A
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flame retardant
foamed glue
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sofa cloth
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王晓芳
卓婵
赵俊焕
翟忠杰
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Huzhou Ruigao New Material Co Ltd
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Abstract

<b>本发明</b><b>公开的是</b><b>沙发布阻燃成品发泡胶及其制备方法，它按质量份主要包括以下原料；水性成膜树脂</b><b>90-120</b><b>份；磷系阻燃剂</b><b>15-30</b><b>份；金属水合物</b><b>20-40</b><b>份；</b><b>溴系阻燃剂</b><b>20-50</b><b>份；阻燃协效剂5-10份；交联剂1-5份；稳泡剂10-20份；水50-120份。本发明不仅具有优越阻燃效果，适合不同纹路的沙发布种，而且使用本发明的沙发布柔软度也得到了大幅度地提高。</b>

Description

沙发布阻燃成品发泡胶及其制备方法
技术领域
本发明涉及沙发布阻燃成品发泡胶及其制备方法，属于沙发布用阻燃剂技术领域。
技术背景
随着时代的发展与进步，人们对纺织材料性能的要求不断提高。对于沙发布的阻燃性能，目前国内外产业界都较为日益关注。
申请号为CN201220482772.X实用新型公开了一种复合阻燃沙发布，主要是从纤维交织结构角度做设计，但是对于沙发布的阻燃尤其是成碳封孔缺乏技术方案，其对于保护沙发布下面的非阻燃海绵无能为力。
一般出口英国等地的沙发布都必须通过BS5852-2006阻燃测试标准，现有的沙发布的阻燃都是采用气相阻燃，测试容易产生破洞，引燃海绵，无法通过BS5852测试。另一种阻燃工艺是采用直刮工艺，工艺简单，但是很多沙发布往往布纹比较粗，容易使浆料渗透到布缝隙中，导致加工的成品手感非常硬，无法达到客户要求。发泡胶经过烘箱烘干后胶水在织物表面形成中空的发泡层，能够产生非常柔软的效果。因此如何研发一款具有阻燃效果的沙发布发泡胶，成为了业界亟待解决的课题。
发明内容
本发明目的在于，提供一种沙发布阻燃成品发泡胶及其制备方法。本发明不仅具有优越阻燃效果，适合不同纹路的沙发布种，而且使用本发明的沙发布柔软度也得到了大幅度地提高。
本发明的技术方案。沙发布阻燃成品发泡胶，按质量份主要包括以下原料；
上述的沙发布阻燃成品发泡胶中，按质量份主要包括以下原料；
前述的沙发布阻燃成品发泡胶中，所述的水性成膜树脂选自水性丙烯酸树脂和/或水性聚氨酯树脂。
前述的沙发布阻燃成品发泡胶中，所述的磷系阻燃剂为多聚磷酸铵。
前述的沙发布阻燃成品发泡胶中，所述的金属水合物选自氢氧化镁和/或氢氧化铝。
前述的沙发布阻燃成品发泡胶中，所述的溴系阻燃剂为十溴二苯乙烷。
前述的沙发布阻燃成品发泡胶中，所述的阻燃协效剂为三氧化二锑和/或氧化锌。
前述的沙发布阻燃成品发泡胶中，所述的交联剂为封端聚醚异氰酸酯和/或氮丙啶交联剂。
前述的沙发布阻燃成品发泡胶中，所述的稳泡剂为硬脂酸铵和/或硬脂酸钠。
前述的沙发布阻燃成品发泡胶的制备方法，该方法是先向搅拌釜中加入100份水性成膜树脂，将转速调至300-500转/每分钟，搅拌10分钟，然后依次加入溴系阻燃剂、磷系阻燃剂、阻燃协效剂、金属水合物，搅拌均匀后，缓慢加入稳泡剂、交联剂和水，调节固含量至50±1％，采用碱溶胀增稠剂和氨水调节粘度1000-5000CPS,pH值7-9,即得成品发泡胶。
与现有技术比较，本发明具有良好的阻燃效果，适合各种纹路的布种，阻燃可以明显优于BS5852阻燃测试标准；产用本发明的沙发布柔软度也得到了大幅度地提高。经阻燃试验，参考英国BS5852阻燃测试标准1号火焰，测试时间20秒；观察20秒后火焰的续燃情况；要求火焰离开之后布面火焰2分钟离开。试验结果显示，使用本发明的沙发布布面现象成膜成碳，火焰现象为离火即熄灭，说明阻燃效果非常优越，而且使用本发明的沙发布的柔软度也通过相关标准。
具体实施方式
实施例1:沙发布阻燃成品发泡胶，按质量份主要包括以下原料；水性丙烯酸树脂50份，水性聚氨酯树脂50份，多聚磷酸铵15份，氢氧化镁35份，十溴二苯乙烷40份，三氧化二锑10份，封端聚醚异氰酸酯4份，硬脂酸铵20份，水80份。在上述原料的基础上，本发明还包括调节粘度的碱溶胀丙烯酸增稠剂适量和氨水适量，碱溶胀丙烯酸增稠剂和氨水可以根据粘度的要求，按常规技术获取加入量的多少。
上述的沙发布阻燃成品发泡胶的制备方法，先向搅拌釜中加入水性丙烯酸树脂和水性聚氨酯树脂，将转速调至300-500转/每分钟，搅拌10分钟，然后依次加入溴系阻燃剂、磷系阻燃剂、阻燃协效剂、金属水合物，搅拌均匀后，缓慢加入稳泡剂、交联剂和水，调节固含量至50±1％，采用碱溶胀增稠剂和氨水调节粘度1000-5000CPS,pH值7-9,即得成品发泡胶。
实施例2:沙发布阻燃成品发泡胶，按质量份主要包括以下原料；水性丙烯酸树脂90份，多聚磷酸铵20份，金属水合氧化物40份，十溴二苯乙烷20份，三氧化二锑7份，封端聚醚异氰酸酯4份，硬脂酸铵10份，水70份。
上述的沙发布阻燃成品发泡胶的制备方法，先向搅拌釜中加入水性丙烯酸树脂和水性聚氨酯树脂，将转速调至300-500转/每分钟，搅拌10分钟，然后依次加入溴系阻燃剂、磷系阻燃剂、阻燃协效剂、金属水合物，搅拌均匀后，缓慢加入稳泡剂、交联剂和水，调节固含量至50±1％，采用碱溶胀增稠剂和氨水调节粘度1000-5000CPS,pH值7-9,即得成品发泡胶。
实施例3:沙发布阻燃成品发泡胶，按质量份主要包括以下原料；水性聚氨酯115份，多聚磷酸铵20份，氢氧化铝30份，十溴二苯乙烷20份，氧化锌7份，氮丙啶交联剂4份，硬脂酸钠10份，水60份。
上述的沙发布阻燃成品发泡胶的制备方法，先向搅拌釜中加入水性丙烯酸树脂和水性聚氨酯树脂，将转速调至300-500转/每分钟，搅拌10分钟，然后依次加入溴系阻燃剂、磷系阻燃剂、阻燃协效剂、金属水合物，搅拌均匀后，缓慢加入稳泡剂、交联剂和水，调节固含量至50±1％，采用碱溶胀增稠剂和氨水调节粘度1000-5000CPS,pH值7-9,即得成品发泡胶。
实施例4：申请人对使用了实施例1、2和3中的阻燃成品发泡胶的沙发布作了阻燃性和柔软度测试，测试结果如下：
测试结果显示，与常规沙发布发泡胶相比，本发明的产品在柔软度和阻燃性方面均效果显著。

Claims (10)

1.沙发布阻燃成品发泡胶，其特征在于：按质量份主要包括以下原料；
水性成膜树脂90-120份；
磷系阻燃剂15-30份；
金属水合物20-40份；
溴系阻燃剂20-50份；
阻燃协效剂5-10份；
交联剂1-5份；
稳泡剂10-20份；
水50-120份。
2.根据权利要求1所述的沙发布阻燃成品发泡胶，其特征在于：按质量份主要包括以下原料；
水性成膜树脂100份；
磷系阻燃剂15份；
金属水合物35份；
溴系阻燃剂40份；
阻燃协效剂10份；
交联剂4份；
稳泡剂20份；
水80份。
3.根据权利要求1所述的沙发布阻燃成品发泡胶，其特征在于：所述的水性成膜树脂为水性丙烯酸树脂和/或水性聚氨酯树脂。
4.根据权利要求1所述的沙发布阻燃成品发泡胶，其特征在于：所述的磷系阻燃剂为多聚磷酸铵。
5.根据权利要求1所述的沙发布阻燃成品发泡胶，其特征在于：所述的金属水合物为氢氧化镁和/或氢氧化铝。
6.根据权利要求1所述的沙发布阻燃成品发泡胶，其特征在于：所述的溴系阻燃剂为十溴二苯乙烷。
7.根据权利要求1所述的沙发布阻燃成品发泡胶，其特征在于：所述的阻燃协效剂为三氧化二锑和/或氧化锌。
8.根据权利要求1所述的沙发布阻燃成品发泡胶，其特征在于：所述的交联剂为封端聚醚异氰酸酯和/或氮丙啶交联剂。
9.根据权利要求1所述的沙发布阻燃成品发泡胶，其特征在于：所述的稳泡剂为硬脂酸铵和/或硬脂酸钠。
10.根据权利要求1至9任一项所述的沙发布阻燃成品发泡胶的制备方法，其特征在于：先向搅拌釜中加入水性成膜树脂，将转速调至300-500转/每分钟，搅拌10分钟，然后依次加入溴系阻燃剂、磷系阻燃剂、阻燃协效剂、金属水合物，搅拌均匀后，缓慢加入稳泡剂、交联剂和水，调节固含量至50±1%，采用碱溶胀增稠剂和氨水调节粘度1000-5000CPS,pH值7-9,即得成品发泡胶。
CN201511015472.5A 2015-12-31 2015-12-31 沙发布阻燃成品发泡胶及其制备方法 Pending CN105568689A (zh)

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CN1635211A (zh) * 2003-12-31 2005-07-06 上海中大科技发展有限公司 厚重织物的阻燃涂层工艺
CN101498105A (zh) * 2008-07-11 2009-08-05 浙江传化股份有限公司 纺织品用水性发泡阻燃涂层胶及其制备方法
CN103627330A (zh) * 2012-08-29 2014-03-12 卢清友 一种复合胶料

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CN1635211A (zh) * 2003-12-31 2005-07-06 上海中大科技发展有限公司 厚重织物的阻燃涂层工艺
CN101498105A (zh) * 2008-07-11 2009-08-05 浙江传化股份有限公司 纺织品用水性发泡阻燃涂层胶及其制备方法
CN103627330A (zh) * 2012-08-29 2014-03-12 卢清友 一种复合胶料

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Application publication date: 20160511