CN105568529B - High-count and high-density degree is singed resistance to alkali mercerized stretch knit fabric and its production method - Google Patents
High-count and high-density degree is singed resistance to alkali mercerized stretch knit fabric and its production method Download PDFInfo
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Abstract
The present invention provides resistance to alkali mercerized stretch knit fabrics and its production method that a kind of high-count and high-density degree yarn singeing containing MS (such as XLA) easypro elastic fibre, fabric are not required to high temperature preboarding, comprising: step 1, provides the second fiber yarn；Step 2, the second fiber yarn and the MS after yarn singeing, mercerising, washing are relaxed and passes through knitting together with elastic fibre knitting fabric is made；Step 3, knitting fabric is impregnated in mercerising liquid, is washed；Step 4, the knitting fabric after washing bleached, dyed, dried, shaped.MS can be relaxed elastic fibre by the method for the present invention and some non-refractories must perhaps carry out the various fiber combinations exploitation of superhigh temperature and more not need high temperature preboarding or super heat-resisting new textile product, be had broad application prospects.
Description
Technical field
The present invention relates to a kind of textile fabric and its production method more particularly to a kind of relax the high-count and high-density of elastic fibre containing MS
Degree yarn singeing, elastic fabric are not required to the resistance to alkali mercerized knitted side material and its production method of high temperature preboarding.
Background technique
In the modern life, fiber using ubiquitous, however generally there are following defects for traditional elastic fiber: 1)
Draw ratio is big and unstable: in order to guarantee that the dimensional stability of fabric must carry out 180 DEG C or more of high temperature preboarding, still
It is otherwise tendering or melt viscous no more than 195 DEG C.2) strong alkali-acid resistance is poor: part encounter strong acid can with cotton as thawing or
Person rots；It encounters highly basic or the alkali mercerized improper fiber that will lead to follows the string, broken hole occurs in fracture of wire when serious.3) not chlorine-resistant
Drift: being restricted to high-elastic swimsuit is made, because of the long soaking time in the indoor pool using hypochlorite disinfectant, elasticity
Fibre damage and follow the string.4) anti-uv-ray is poor: with the improvement of living standards, healthy living is increasingly by people
Favor, the market demand of comfortable personal, natural environmental-protective elastic fabric coat is increasing, and traditional elastic fiber is to ultraviolet
Line aging has hampered the development of novel elastic fabric.5) initial tensile internal stress is excessive, and dress has tight not relaxing with
Suitable sense.6) most of traditional elastic fiber is obtained by the spinning of polyester-type+polyether-type macromolecule, and polyether-type macromolecular increases bullet
Easy fracture aging while property, the shelf-life is short, inconvenient to use.
The elastic fibre as shown in Figure 1, MS (MicroStretch) relaxes, including XLA fiber, are by new network cross-linked polyolefin
The high-tech elastomer that material is constituted.Distinctive molecular structure makes MS elastomer have stable chemical property, shows
Heat resistance, resistance to ag(e)ing and strong alkali-acid resistance performance free from worldly cares.It is added to and more has for the special processing of textile fabric and dress ornament
The distinct elements of effect.Prominent feature is: comfortable tensile-elasticity, suitable elasticity recovery and lasting stability, to design
Teacher, which provides to follow one's inclinations, makes that comfortable fit, posture be dynamic, soft not tight, streamline moves with oneself, fashion, modish, high-grade high
Shelves are woven and are knitted fabric.
The MS prominent feature of elastic fibre of relaxing is supplement to traditional elastic fiber disadvantage, such as: 1) high temperature resistant reach 220 DEG C with
On.2) not needing high temperature preboarding can get excellent dimensional stability.3) there is fabulous strong alkali-acid resistance performance, highly concentrated
Can rot cotton in degree sulfuric acid solution, and the easypro elastic fibre of MS remains intact latticed.It will not be broken in the mercerising caustic soda of high concentration
Bad original elastic fiber fabric lines.4) fabulous chlorine-resistant floats performance, is very suitable to make high-grade swimsuit and permanency shape.
5) high temperature preboarding is not needed, being more suitable for matching with any fiber of non-refractory produces elastic fabric.6) heat-resisting quantity is excellent
In traditional elastic fiber, new research direction is provided to produce high-grade fire-fighting fire retardant elastic fabric.7) excellent uvioresistant
Performance provides new fabric for the high-grade elastic anorak of exploitation.8) high temperature preboarding and the high temperature setting of finished product are not needed, from
The angle of energy-saving and emission-reduction reduces the consumption of the energy, to realize energy-saving and emission-reduction, reduces production cost and contributes.
However, since MS fiber rebound performance is poor compared to traditional elastic fiber spandex, in weaving process, due to drawing
, often there is broken end and fracture of wire, even broken hole phenomenon in the reason of expansion force.But MS relaxes, elastic fibre exists in dyeing and finishing process
The characteristics of not restoring and reset in the original location after big microstructure crystalline region and the fusing of amorphous area crosslinking points, brings active bullet to fabric
While property, there is also a kind of unstability.Therefore, how to make the easypro elastic fibre of MS preferably be applied to textile fabric, be this
Field technical staff's urgent problem.
Summary of the invention
Aiming at the problem that current MS relaxes elastic fibre in the presence of field of textiles application process, the present invention provides one kind to contain
The high-count and high-density degree yarn singeing of the easypro elastic fibre of MS, fabric are not required to resistance to alkali mercerized stretch knit fabric and its life of high temperature preboarding
Production method.
First aspect of the present invention be to provide it is a kind of produce the yarn singeing of high-count and high-density degree, fabric is not required to high temperature preboarding
The method of resistance to alkali mercerized stretch knit fabric, wherein the knitting fabric includes the easypro elastic fibre of MS and the second fiber, side of the present invention
Method includes:
Step 1, the second fiber yarn is provided；
Step 2, it will singe, the second fiber yarn after mercerising and MS relax and pass through knitting together with elastic fibre knitted side is made
Material；
Step 3, will knitting fabric in mercerising liquid again immersions, mercerising, it is sour in and wash；
Step 4, acid is neutralized, the knitting fabric after washing is bleached, dyes, washes, dries setting.
Wherein, second fiber includes the fiber yarn of yarn with different fineness, as 32S, 40S, 45S, 50S, 60S,
The yarn or strand of one or more of yarn count fineness in 80S, 100S, 150S, 200S.In one preferred embodiment of the invention,
Second fiber is at least combineeed and is twisted by two or three in 32S, 80S, 100S yarn count fiber.
Wherein, second fiber can be in animal origin, plant fiber, synthetic fibers any one or it is several
Kind.
The animal origin can be protein fibre, as in animal hair, silk, milk proem fiber any one or
Several, concrete example is such as unable to the protein fibre (such as milk proem fiber) of high temperature preboarding, the protein fibre of non-refractory
(such as animal hair fiber, such as cashmere, wool, the rabbit hair).
The plant fiber can be cellulose fibre, such as cotton, fiber crops, wood pulp cellulose, Modal fibre, tencel fiber, glue
Glue fiber etc. is natural or regenerated celulose fibre in any one or a few.
The synthetic fibers can be aramid fiber, terylene, spandex, nylon (polyamide fibre), acrylic fibers, polypropylene fibre, polyvinyl, polylactic acid PLA
Any one or a few in fiber.
Wherein, the easypro elastic fibre of the MS and the second fibre weight ratio are preferably 5-65: 35-95, more preferably 5-50:
50-95, more preferably 5-40: 60-95, more preferably 6-30: 70-94, more preferably 6-20: 80-94, more preferably 8-15:
84-92, more preferably 10-13: 87-90.
Wherein, the fiber number of the easypro elastic fibre of the MS is preferably 20D-140D, more preferably 40-100D, more preferably 50-
80D, more preferably 60-70D, such as 105D, 75D, 55D, 42D, 33D.
In one preferred embodiment of the invention, in the knitting process described in step 2, the easypro elastic fibre withdrawal speed of MS is
40-50m/min, more preferably 45-50m/min, such as 46m/min, 48m/min；Second fiber withdrawal speed is 120-180m/
Min, more preferably 120-150m/min, more preferably 120-140m/min, such as 130m/min, 135m/min.
In one preferred embodiment of the invention, in the knitting process described in step 2, MS relaxes elastic fibre total draft multiple
Preferably 2-3.5, more preferably 2.5-3.5, such as 3 ± 0.2.
In one preferred embodiment of the invention, in the knitting process described in step 2, the easypro elastic fibre tension of MS is preferably
Control is in 7-8CN.
In one preferred embodiment of the invention, in step 3, described in mercerising liquid in soaking process, condition is excellent
Be selected as: concentration of caustic soda 110-270g/L, more preferably 165-190g/L, rolling alkali temperature is room temperature -- 55 DEG C, more preferably room
Temperature -- 35 DEG C, speed 15-30m/min.
In one preferred embodiment of the invention, in step 3, described in mercerising liquid in soaking process, when immersion
Between preferably 8-100s, more preferably 10-60s, such as 15s, 20s, 30s.
In one preferred embodiment of the invention, enter mercerising reaction zone 10-20s after immersion described in step 3；Again into
Enter breadth, the grammes per square metre stable region of mercerising tentering, residence time 10-20s.
In one preferred embodiment of the invention, in the water-washing process described in step 3, washing temperature is preferably 30-90
℃。
In one preferred embodiment of the invention, in the water-washing process described in step 3, sequence and condition are as follows: 60 DEG C of heat
10s-70 DEG C of 10s-80 DEG C of hot water wash 10s-60 DEG C of hot water wash acid of washing neutralizes 10-20s-80 DEG C of hot water wash 10-20s- and rolls
Water cloth outputting.
In one preferred embodiment of the invention, in dyeing course described in step 4, comprising:
A) pre-treatment, sequence and condition are as follows: hydrogen peroxide is added, is warming up to 45-55 DEG C with the speed of 2-3 DEG C/min, keeps
It after 5-15min, is heated up 5-10 DEG C with the speed of 0.5-2 DEG C/min, after keeping 5-15min, is heated up with the speed of 0.5-2 DEG C/min
It is bleached to 85-110 DEG C, is then cooled to 70 DEG C or less with the speed of 2 DEG C/min；
B it) dyes: dyestuff is added, is warming up to 40-85 DEG C with the speed of 1-2 DEG C/min, and keep 50-80min, fixation, soap
It washes, is then cooled to environment temperature, is washed later.Wherein, the washing process is preferably 80-90 DEG C of hot water wash
10min -50-60 DEG C of hot water wash 10min-cold water is washed till colourless.
In one preferred embodiment of the invention, in shaping process described in step 4, temperature is preferably controlled in 130-
It 185 DEG C, can be determined according to the performance of the second fiber.
In one preferred embodiment of the invention, in shaping process described in step 4, speed is preferably controlled in 20-
35m/min, more preferably 25-30m/min；Overfeeding 20-35%, more preferably 25-30%.
In one preferred embodiment of the invention, second silvalin carries out step of singing before knitting, with
To satisfactory finish.
In one preferred embodiment of the invention, second silvalin impregnates in mercerising liquid before knitting, so
After wash.Wherein, the mercerising liquid for impregnating the second silvalin can be identical or different with the mercerising liquid for impregnating knitting fabric.
Wherein, in the second silvalin soaking process, condition is preferred are as follows: alkali concentration 180-270g/L, more preferably
200-270g/L, mercerising liquid temperature are 10-30 DEG C, soaking time 60-120s；Water-washing process after the second silvalin immersion
It include: the washing of first time high temperature and second of low temperature washing, wherein the temperature of the high temperature washing is preferably 70-100 DEG C, institute
Stating low temperature washing temperature is preferably 40-60 DEG C.
The second aspect of the present invention be to provide a kind of high-count and high-density degree yarn singeing produced of any one of the above method,
Fabric is not required to the resistance to alkali mercerized knitted side material of high temperature preboarding.
MS can be relaxed and elastic fibre and some non-refractories or must carry out the various fibers of superhigh temperature by the method for the present invention
Combination, exploitation do not need high temperature preboarding or super heat-resisting new textile product more；Prepared knitting fabric is suitble to make
Make the monofilament light of singing high-grade, moisture absorption is ventilative, mariages light of singing, monofilament light of not singing, mariages light of not singing, is not required to make a reservation for
Shape, it is necessary to the textile fabric of high temperature preboarding；Anorak, football shirt, the gym outfit of outdoor activity, soft skirt, shorts, elastic force
Brassiere, elastic force bawneen, corduroy, knitted stretch underwear, socks etc.；More suitable for the elasticity swimming of indoor swimming anti-chlorine ion
Dress, has broad application prospects.
Detailed description of the invention
Fig. 1 is the easypro elastic fibre dimensional network structure schematic diagram of MS；
Fig. 2 is pre-treatment bleaching process flow diagram and technical parameter in knitting fabric dyeing course；
Fig. 3 is medium temperature reactive dyeing process flow diagram and technical parameter in knitting fabric dyeing course.
Specific embodiment
Embodiment 1
Step 1,80-100S long wool cotton is provided,
1.1. yarn is combineeed
(1) equipment: Japanese Murata NO.28 doubling winder, II two-for-one twister of NO.363-.
(2) combine principle: according to product specification, selecting high Zhi Changrong cotton yarn, 80S, 100S are combineeed and twisted.Principle
It is: is less than the twist 30% or so of woven yarn for the yarn twist of knitting.
(3) reference value of the twist:
4.2 yarn singeing
(1) equipment: Italian RITE S.P.A company, model GRR.N gassing frame.
(2) technical parameter: 1050-1100 DEG C of burner central temperature, linear velocity 720m/min.
4.3 yarn mercerisings
(1) equipment: Italian JAEGGLI company, model HL2000 Mercerising machines for yarns.
(2) technical parameter:
A. mercerising concentration of lye 190g/L (22Be °) -225g/L (25Be °)
B. mercerising alkali liquid temperature 15-20 ± 2 DEG C or room temperature
C. caustic dip time 100 seconds
D. time 100-150 seconds ventilative (overall process 4 ' 20 ")
E. 80 DEG C of first time hot water wash --- second of 50 DEG C of hot water wash --- acid neutralizes --- third time hot water wash 60-70
DEG C --- cold water is washed.
Step 2, it is knitted
(1) equipment: Italian ORIZIO company, model JOHN/C circular knitting machine.
(2) technical parameter
A.75D the easypro elastic fibre withdrawal speed 48m/min cotton withdrawal speed 135m/min of MS
B.MS relaxes elastic fibre total draft multiple 3
C.MS relaxes elastic fibre tension 7-8CN, yarn ratio 91%, and MS relaxes elastic fibre ratio 9%
Step 3, mercerising
(1) equipment: Switzerland's Benniger (BENNINGER) company, AH300 needle plate type tentering mercerizing machine
(2) technical parameter:
A. 30 DEG C of mercerising alkali liquid temperature
B. mercerising concentration of lye 160-180g/L
C. caustic dip time 10-25s, reaction time 10-20s, tentering mercerising stable region residence time 10-20s
D. speed 20-25m/min
E. 60-70 DEG C of spray washing temperature, time 20-40s
F.70-50-60 DEG C of-90 DEG C of hot water wash of-80 DEG C of DEG C hot water wash hot water wash sour neutralization-washing-squezzing cloth outputtings
Step 4, it dyes, shape
It has been found that not only its elasticity of the elastic influence of fabric construction, the control of heating process more influence it and stretch bullet
Property and resilience.Control measure are as follows: be added under room temperature after dye material, cloth feeding, it is necessary to slowly heating.Referring to Fig. 2 and Fig. 3, it is
Activation MS relaxes the nexus of elastic fibre molecule soft chain segment, is heated up, is given when reaching 50 DEG C certain with the speed of 1.5 DEG C/min
Activation soaking time (such as 10min), then with the speed of 1 DEG C/min be warming up to 60 DEG C further activation macromoleculars, take multistage
Heat preservation, the method repeatedly to heat up, make it generate stable elasticity.The temperature of specific activation heat preservation can be according to the glass of fiber itself
Depending on change transition temperature Tg.Then, dye pre-treatment and dyeing are carried out further according to another component fibre performance, in dyeing course such as
Fruit repeats primary above-mentioned technique, and elasticity can be more stable.In order to repeatedly form netted point structure, increase its elasticity recovery, one
Fixed should be noted that after processing, dyeing, soap boiling, hot water wash, is cooled to 70-80 DEG C or less drain before each high temperature.Purpose makes greatly
Molecule segment is slowly cooling to stablize and then dries setting.In general, once being formed after stable elasticity, even if rising again
Temperature has been much smaller than for the first time elasticity effect.
Specific dyeing is as follows:
A) pre-treatment, sequence and condition are as follows: hydrogen peroxide is added, is warming up to 50 DEG C with the speed of 1-2 DEG C/min, keeps
After 10min, 60 DEG C are warming up to the speed of 1-2 DEG C/min, after keeping 10min, is warming up to 105 DEG C with the speed of 1-2 DEG C/min
It is bleached, is then cooled to 70 DEG C or less with the speed of 2 DEG C/min；
B it) dyes: dyestuff is added, is warming up to 55-65 DEG C with the speed of 1-2 DEG C/min, and keep 50-80min, then arranges
Liquid is cooled to environment temperature, carries out 80 DEG C of 15min that soap, 50 DEG C of pickling 10min later, finally washes 10min.
150-160 DEG C of tentering setting.
The performance of a variety of knitting fabrics of 1 the method for embodiment of the present invention production is as shown in table 1.
Embodiment 2
Second silvalin is combing JC Quality Pure Cotton Yarn Production.
Technological parameter in knitting process:
MS relaxes elastic fibre withdrawal speed 46m/min the second silvalin withdrawal speed 135m/min
MS relaxes elastic fibre total draft multiple 3
MS relaxes elastic fibre tension 7-8CN
Ratio: the second silvalin 87%, MS relax elastic fibre 13%
Mercerization parameter:
Pad soda bath: concentration 240g/L (26Be °), 4028A bleeding agent；Rolling alkali temperature is room temperature；It is anti-into room temperature
Answer expanding mercerising area；Hot water wash, acidity, washing, cloth outputting PH control are in 5-6.
Dyeing, setting process:
It is dyed according to 1 the method for embodiment.
150-160 DEG C of setting temperature, speed 25m/min；Overfeeding 25-30%.
The performance of a variety of knitting fabrics of 2 the method for embodiment of the present invention production is as shown in table 2.
Table 2
Specific implementation example of the invention is described in detail above, but it is merely an example, the present invention is not
It is limited to specific implementation example described above.To those skilled in the art, what any couple of present invention carried out, which be equal, repairs
Change and substitutes also all among scope of the invention.Therefore, made impartial change without departing from the spirit and scope of the invention
It changes and modifies, all should be contained within the scope of the invention.
Claims (7)
1. it is a kind of produce the yarn singeing of high-count and high-density degree, fabric be not required to high temperature preboarding resistance to alkali mercerized stretch knit fabric side
Method, which is characterized in that the knitting fabric includes the easypro elastic fibre of MS and the second fiber, which comprises
Step 1, the second fiber yarn is provided；
Step 2, it will singe, mercerising, the second fiber yarn after washing and MS relax and pass through knitting together with elastic fibre knitted side is made
Material；
Step 3, knitting fabric is impregnated in mercerising liquid, acid neutralizes, washing；
Step 4, the knitting fabric after washing dyed, dry setting；
Wherein, second fiber includes the fiber of yarn with different fineness；
Second fiber is at least combineeed and is twisted by two or three in 32S, 80S, 100S yarn count fiber；
The fiber number of the easypro elastic fibre of the MS is 60D-70D；
The easypro elastic fibre of the MS and the second fibre weight ratio are 5-15: 85-95；
In the knitting process described in step 2, MS relaxes elastic fibre withdrawal speed for 40-50m/min, and the second fiber withdrawal speed is
120-180m/min；
In the knitting process described in step 2, MS relaxes elastic fibre total draft multiple for 2-3.5；
In the knitting process described in step 2, MS relaxes elastic fibre tension to control in 7-8CN；
Described in step 3 in mercerising liquid in soaking process, condition are as follows: concentration of caustic soda 110-270g/L, it is normal for rolling alkali temperature
- 55 DEG C of temperature, speed 15-30m/min；
In step 3, in the water-washing process, sequence and condition are as follows: 60 DEG C of hot water wash 10s -70 DEG C hot water wash 10s -80 DEG C
Hot water wash 10s -60 DEG C acid neutralizes 80 DEG C of hot water wash 10-20s-squezzing-cloth outputtings of 10-20s -.
2. the method according to claim 1, wherein second fiber is selected from animal origin, plant fiber, conjunction
At any one or a few in fiber.
3. according to the method described in claim 2, it is characterized in that, second fiber is selected from the albumen for being unable to high temperature preboarding
Matter fiber.
4. according to the method described in claim 2, it is characterized in that, second fiber is selected from the protein fibre of non-refractory
Dimension.
5. according to the method described in claim 2, it is characterized in that, second fiber be selected from aramid fiber, terylene, spandex, nylon,
Acrylic fibers, polypropylene fibre, polyvinyl, polylactic acid PLA fiber any one or a few.
6. the method according to claim 1, wherein in dyeing course described in step 4, comprising:
A) pre-treatment, sequence and condition are as follows: hydrogen peroxide is added, is warming up to 45-55 DEG C with the speed of 2-3 DEG C/min, keeps 5-
It after 15min, is heated up 5-10 DEG C with the speed of 0.5-2 DEG C/min, after keeping 5-15min, is warming up to the speed of 0.5-2 DEG C/min
100-110 DEG C is bleached, and is then cooled to 70 DEG C or less with the speed of 2 DEG C/min；
B it) dyeing: dyestuff is added, is warming up to 40-85 DEG C with the speed of 1-2 DEG C/min, and keep 50-80min, fixation is soaped,
Then it is cooled to environment temperature, 10min -50-60 DEG C of hot water wash 10min-cold water of 80-90 DEG C of hot water wash is carried out later and is washed till nothing
Color.
7. the high-count and high-density degree yarn singeing that one kind produces method according to claim 1, fabric are not required to high temperature preboarding
Resistance to alkali mercerized knitted side material.
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| CN108552636A (en) * | 2018-05-17 | 2018-09-21 | 苏州凤霓绣叶文化艺术有限公司 | A kind of cheongsam with aesthetics |
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| US6941775B2 (en) * | 2002-04-05 | 2005-09-13 | Electronic Textile, Inc. | Tubular knit fabric and system |
| CN101392444B (en) * | 2007-09-18 | 2011-11-23 | 华纺股份有限公司 | Dyeing and finishing process of polyolefin elastic fiber fabric coated by polyester cotton filling yarn |
| CN101200852B (en) * | 2007-12-10 | 2010-08-25 | 宁波雅戈尔日中纺织印染有限公司 | Processing method for low-elastic non-ironing knitted face fabric |
| CN101381919A (en) * | 2008-10-17 | 2009-03-11 | 江苏联发纺织股份有限公司 | Cotton-real silk XLA intertexture and producing method thereof |
| CN102433653A (en) * | 2011-09-30 | 2012-05-02 | 常熟市梅李镇宾理服饰制衣厂 | Bamboo fiber woolen fabric |
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| CN102888688B (en) * | 2012-09-20 | 2015-07-29 | 浙江华欣新材料股份有限公司 | A kind of color polyester transition silk colorful carpet hand woven line and manufacture method thereof |
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