CN105560118A - Dendrobium officinale mouth wash - Google Patents
Dendrobium officinale mouth wash Download PDFInfo
- Publication number
- CN105560118A CN105560118A CN201610039662.9A CN201610039662A CN105560118A CN 105560118 A CN105560118 A CN 105560118A CN 201610039662 A CN201610039662 A CN 201610039662A CN 105560118 A CN105560118 A CN 105560118A
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- herba dendrobii
- dendrobium officinale
- extract
- extraction
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
Abstract
The invention discloses dendrobium officinale mouth wash which comprises 0.1-15% of dendrobium officinale extractive. A preparation method of the dendrobium officinale extractive comprises the steps that dried dendrobium officinale stems are smashed and sieved by a sieve with 60 meshes, water is added into the dendrobium officinale powder based on the solid-liquid ratio of 1:20, the water and the dendrobium officinale powder are stirred, mixed and placed into a stainless steel cylinder, the sealed state is kept, then a container containing material liquid is added into an ultrasonic wave extractor for ultrasonic wave water-bath heating and extraction, the ultrasonic power is 500 W, the ultrasonic wave frequency is 45-50 Hz, the extraction temperature is 40-45 DEG C, the heat preservation extraction time is 30-40 min, a vacuum suction filtration pump is adopted for suction filtration after extraction is finished, the suction filtration fixed liquid is centrifugally separated for 10-15 min at the rotating speed of 5000-6000 r/min, and the obtained liquid supernatant is the dendrobium officinale extractive. The mouth wash is mainly made of dendrobium officinale and has the effects of resisting bacteria, diminishing inflammation, stopping bleeding, preventing oral malodor, promoting oral cavity wound healing and improving immunity.
Description
Technical field
The present invention relates to one and day protect articles for use, be specifically related to a kind of Herba Dendrobii collutory
Background technology
Herba Dendrobii, grow nonparasitically upon another plant for the orchid family is perennial herbaceous plant.Herba Dendrobii can be divided into tens of kinds, Dendrobium denneanum Kerr., Dendrobium nobile Lindl, horsewhip etc., and Herba Dendrobii is the superfine product of Herba Dendrobii, and it is gained the name because epidermis is ferrum green.Herba Dendrobii has unique medical value, is used as medicine with its stem, Chinese medicine name: Herba Dendrobii, belongs to the YIN-tonifying drug in tonic, " Chinese Pharmacopoeia ": reinforcing stomach reg fluid, nourishing YIN and clearing away heat.The tender stem of the minority kinds such as Herba Dendrobii, be twisted into helical form or spring-like, dry, commodity are called earrings dendrobium, have another name called Herba Dendrobii extract.Herba Dendrobii is rich in polysaccharide, dendrobine, free amino acid, vitamin (vitamin A, vitamin C, vitamin E), chlorophyll and various enzyme, not only oral absorption can be passed through, Herba Dendrobii can also stop blooding, promote wound healing, can outward for repairing damaged oral
Dendrobium officinale polysaccharide has the function of antibacterial, antiinflammatory, enhancing Cell-mediated Immunity, can anti-bacteria breeding for oral cavity, effectively prevents halitosis; Dendrobium officinale polysaccharide external can be stopped blooding, and can promote fibrinous growth, thus promotes wound healing, repairs damaged oral tissue.Herba Dendrobii contains aminoacid and the various trace elements useful to human body, and the water soluble polysaccharide included is a para-immunity reinforcing agent, leukocyte can be improved, promote that lymphocyte produces lymphokine, thus enhancing body humoral immune function, cellular immune function, enhancing body autoimmune, promotes to recover.Theory of Chinese medical science is thought, Herba Dendrobii cold nature, be the holy product of YIN nourishing, and aphtha, ulcer, gingival swelling and pain etc. mostly are caused by hyperactivity of fire caused by deficiency of YIN, therefore Herba Dendrobii can be used for above-mentioned oral problem.
Collutory is that the novel product scientists of Technology Times matches the ingredient of multiple treatment oral cavity, laryngopharyngeal diseases, site of disease can be directly acted on, there is good permeability, while treatment oral disease, also can remove because of mouth disease, eat the halitosis that peculiar smell foodstuff (rareripe, Bulbus Allii, cigarette, wine etc.) dyssomnia, psychentonia, dyspepsia etc. cause.At present, existing patent CN103893030A discloses a kind of Chinese herbal medicine mouthwash, also has patent CN103977264A to disclose and a kind ofly has anti-inflammation hemostasia Dendrobium officinale fruit toothpaste, but be applied to mouthrinse product there are no by Herba Dendrobii.
Summary of the invention
The object of the invention is to, for prior art, provide a kind of Herba Dendrobii collutory.
For achieving the above object, the present invention takes following technical scheme: a kind of Herba Dendrobii collutory contains the Herba Dendrobii extract of 0.1 ~ 15%.
The preparation method of described Herba Dendrobii extract is: pulverized by dried Herba Dendrobii stem, cross 60 mesh sieves, be that 1:20 adds water and is uniformly mixed rearmounted rustless steel cylinder by dendrobium officinale powder by solid-to-liquid ratio, keep air-tight state, again the container filling feed liquid is joined in ultrasonic extractor and carry out ultrasound bath heating extraction, ultrasonic power is 500W, ultrasonic frequency is 45 ~ 50Hz, Extracting temperature is 40 ~ 45 DEG C, insulation extraction time 30 ~ 40min, after extraction terminates, sucking filtration is carried out with vacuum filtration pump, by sucking filtration mixed liquor centrifugalize 10 ~ 15min under the condition of rotating speed 5000 ~ 6000r/min, gained supernatant is Herba Dendrobii extracting solution.
Further, the component of described Herba Dendrobii collutory can also comprise: 1 ~ 5 part, Bulbus Allii, Radix Notoginseng 5 ~ 8 parts, Folium Callicarpae Formosanae 1 ~ 3 part, Herba Artemisiae Annuae 3 ~ 5 parts, Galla Chinensis 3 ~ 7 parts, Radix Ophiopogonis 3 ~ 5 parts, Rhizoma Phragmitis 4 ~ 6 parts, Herba Asari 1 ~ 3 part, 5 ~ 7 parts, Radix Glycyrrhizae, sodium monofluorophosphate 0.05 part, hibitane 0.005 part, ethanol 10 parts, glycerol 5 parts, sodium lauryl sulphate 1 part, polyoxyethylene hydrogenated Oleum Ricini 1 part, sodium fluoride 0.05 part, spice 0.1 part, deionized water 100 parts.
Wherein, described spice is the one of Flos Lonicerae extract, Flos Rosae Rugosae extract, Folium Menthae extract, Flos Jasmini Sambac extract.
Further, Herba Dendrobii is rich in polysaccharide, dendrobine, multiple free amino acid and mineral.Dendrobium officinale polysaccharide has the function of antibacterial, antiinflammatory, enhancing Cell-mediated Immunity, can anti-bacteria breeding for oral cavity, effectively prevents halitosis, also can be used for oral cavity hemostasis, and can fibrinous growth be promoted, thus promote wound healing, repair damaged oral tissue.Herba Dendrobii contains aminoacid and the various trace elements useful to human body, and the water soluble polysaccharide included is a para-immunity reinforcing agent, leukocyte can be improved, promote that lymphocyte produces lymphokine, thus enhancing body humoral immune function, cellular immune function, enhancing body autoimmune, promotes to recover.
Further, in Bulbus Allii, sulfur-containing compound has strong antibacterial and anti-inflammation functions, all has suppression and killing action to multiple coccus, bacillus, fungus and virus etc.
Further, Radix Notoginseng has another name called Radix Notoginseng, and Chinese crude drug Radix Notoginseng is using its root as medicinal effects, has dissipating blood stasis hemostasis, effect of subduing swelling and relieving pain.Cure mainly spitting of blood, spit blood, epistaxis, has blood in stool, metrorrhagia, traumatic hemorrhage, and breast ventral spine pain, tumbling down swells and ache.
Further, Folium Callicarpae Formosanae has another name called Callicarpa dichotoma, cercis, Folium Callicarpae Formosanae, and Folium Callicarpae Formosanae has the effect promoting blood coagulation, and Folium Callicarpae Formosanae all has inhibitory action in various degree to escherichia coli, shigella flexneri, staphylococcus aureus, Hemolytic streptococcus etc.
Further, Herba Artemisiae Annuae has clearing away summer-heat, and except steaming, preventing the attack (or recurrence) of malaria, for pathogenic summer-heat heating, fever due to yin deficiency, night fever abating at dawn, hectic fever due to YIN-deficiency consumptive fever, malaria cold and heat, jaundice due to damp-heat, has the effects such as malaria, antibacterial, parasiticide.
Further, Galla Chinensis sour in the mouth is puckery, cold in nature.Return lung, large intestine, kidney channel, cure mainly chronic cough of deficiency lung; Spontaneous sweating; Chronic dysentery chronic diarrhea; Proctoptosis; Seminal emission; Nebulousurine; Various hemorrhage; Carbuncle furuncle.
Further, Radix Ophiopogonis YIN nourishing and the production of body fluid promoting, lung moistening clears away heart-fire.For dryness of the lung dry cough, chronic consumptive disease is coughed, and Tianjin wound is thirsty, vexed insomnia, and interior-heat is quenched one's thirst, dryness of the intestine constipation; Pharyngeal diphtheria, can control dryness of the lung dry cough, spits blood, spitting of blood, consumptive lung disease, lung abscess, and asthenia dysphoria with smothery sensation, quenches one's thirst, and calentura Tianjin is hindered, dry mouth and throat, constipation.
Further, Rhizoma Phragmitis, reduce phlegm and internal heat pathogenic fire reducing, for calentura excessive thirst, gastropyretic vomiting, cough due to lung-heat, lung abscess vomiting pus, the puckery pain of pyretic stranguria.
Further, Herba Asari has expelling wind and cold, understand things pain-stopping, effect that warming the lung to resolve fluid-retention, antiinflammatory, immunosuppressant and resistance state are anti-.
Further, Radix Glycyrrhizae sweet in the mouth is sweet, and property is gentle, enters the heart, spleen, lung, stomach four warp.Raw with cooler, can eliminating fire and detoxication, relieving spasm to stop pain; Process with partially warm, can fall apart exterior cold, invigorating the spleen and replenishing QI.In addition, Radix Glycyrrhizae is also good at being in harmonious proportion the property of medicine, separates the poison of hundred medicines.
The invention has the beneficial effects as follows:
1, collutory of the present invention take Herba Dendrobii as primary raw material, the effect having antibacterial, antiinflammatory, stop blooding, prevent halitosis, promote the healing of oral cavity wound, improve immunity.
2, in the present invention, the extraction of Herba Dendrobii adopts ultrasonic extraction, and have extraction time shortening, energy consumption is low, and extraction efficiency is high, and extraction temperature is low, can not destroy the advantage of the effective ingredient with thermally labile, facile hydrolysis or oxidation characteristic.
Detailed description of the invention
Below in conjunction with specific embodiment, to the bright further instruction of this law.
Embodiment 1
A kind of Herba Dendrobii collutory contains the Herba Dendrobii extract of 0.1%, also comprise the following component of mass parts: 3 parts, Bulbus Allii, Radix Notoginseng 6 parts, Folium Callicarpae Formosanae 2 parts, Herba Artemisiae Annuae 4 parts, Galla Chinensis 5 parts, Radix Ophiopogonis 4 parts, Rhizoma Phragmitis 5 parts, Herba Asari 2 parts, 6 parts, Radix Glycyrrhizae, sodium monofluorophosphate 0.05 part, hibitane 0.005 part, ethanol 10 parts, glycerol 5 parts, sodium lauryl sulphate 1 part, polyoxyethylene hydrogenated Oleum Ricini 1 part, sodium fluoride 0.05 part, spice 0.1 part, deionized water 100 parts, spice is Flos Lonicerae extract.
The preparation method of Herba Dendrobii extract is: pulverized by dried Herba Dendrobii stem, cross 60 mesh sieves, be that 1:20 adds water and is uniformly mixed rearmounted rustless steel cylinder by dendrobium officinale powder by solid-to-liquid ratio, keep air-tight state, again the container filling feed liquid is joined in ultrasonic extractor and carry out ultrasound bath heating extraction, ultrasonic power is 500W, ultrasonic frequency is 45Hz, Extracting temperature is 40 DEG C, insulation extraction time 30min, after extraction terminates, sucking filtration is carried out with vacuum filtration pump, by sucking filtration mixed liquor centrifugalize 10min under the condition of rotating speed 5000r/min, gained supernatant is Herba Dendrobii extracting solution.
Embodiment 2
A kind of Herba Dendrobii collutory contains the Herba Dendrobii extract of 15%, also comprise the following component of mass parts: 1 part, Bulbus Allii, Radix Notoginseng 5 parts, Folium Callicarpae Formosanae 1 part, Herba Artemisiae Annuae 3 parts, Galla Chinensis 3 parts, Radix Ophiopogonis 3 parts, Rhizoma Phragmitis 4 parts, Herba Asari 1 part, 5 parts, Radix Glycyrrhizae, sodium monofluorophosphate 0.05 part, hibitane 0.005 part, ethanol 10 parts, glycerol 5 parts, sodium lauryl sulphate 1 part, polyoxyethylene hydrogenated Oleum Ricini 1 part, sodium fluoride 0.05 part, spice 0.1 part, deionized water 100 parts, spice is Flos Rosae Rugosae extract.
The preparation method of Herba Dendrobii extract is: pulverized by dried Herba Dendrobii stem, cross 60 mesh sieves, be that 1:20 adds water and is uniformly mixed rearmounted rustless steel cylinder by dendrobium officinale powder by solid-to-liquid ratio, keep air-tight state, again the container filling feed liquid is joined in ultrasonic extractor and carry out ultrasound bath heating extraction, ultrasonic power is 500W, ultrasonic frequency is 50Hz, Extracting temperature is 45 DEG C, insulation extraction time 40min, after extraction terminates, sucking filtration is carried out with vacuum filtration pump, by sucking filtration mixed liquor centrifugalize 15min under the condition of rotating speed 6000r/min, gained supernatant is Herba Dendrobii extracting solution.
Embodiment 3
A kind of Herba Dendrobii collutory contains the Herba Dendrobii extract of 10%, also comprise the following component of mass parts: 5 parts, Bulbus Allii, Radix Notoginseng 8 parts, Folium Callicarpae Formosanae 3 parts, Herba Artemisiae Annuae 5 parts, Galla Chinensis 7 parts, Radix Ophiopogonis 5 parts, Rhizoma Phragmitis 6 parts, Herba Asari 3 parts, 7 parts, Radix Glycyrrhizae, sodium monofluorophosphate 0.05 part, hibitane 0.005 part, ethanol 10 parts, glycerol 5 parts, sodium lauryl sulphate 1 part, polyoxyethylene hydrogenated Oleum Ricini 1 part, sodium fluoride 0.05 part, spice 0.1 part, deionized water 100 parts, spice is Folium Menthae extract.
The preparation method of Herba Dendrobii extract is: pulverized by dried Herba Dendrobii stem, cross 60 mesh sieves, be that 1:20 adds water and is uniformly mixed rearmounted rustless steel cylinder by dendrobium officinale powder by solid-to-liquid ratio, keep air-tight state, again the container filling feed liquid is joined in ultrasonic extractor and carry out ultrasound bath heating extraction, ultrasonic power is 500W, ultrasonic frequency is 50Hz, Extracting temperature is 42 DEG C, insulation extraction time 35min, after extraction terminates, sucking filtration is carried out with vacuum filtration pump, by sucking filtration mixed liquor centrifugalize 13min under the condition of rotating speed 6000r/min, gained supernatant is Herba Dendrobii extracting solution.
Claims (4)
1. a Herba Dendrobii collutory, is characterized in that: containing the Herba Dendrobii extract of 0.1 ~ 15% in described collutory.
2. a kind of Herba Dendrobii collutory according to claim 1, it is characterized in that: the preparation method of described Herba Dendrobii extract is: dried Herba Dendrobii stem is pulverized, cross 60 mesh sieves, be that 1:20 adds water and is uniformly mixed rearmounted rustless steel cylinder by dendrobium officinale powder by solid-to-liquid ratio, keep air-tight state, again the container filling feed liquid is joined in ultrasonic extractor and carry out ultrasound bath heating extraction, ultrasonic power is 500W, ultrasonic frequency is 45 ~ 50Hz, Extracting temperature is 40 ~ 45 DEG C, insulation extraction time 30 ~ 40min, after extraction terminates, sucking filtration is carried out with vacuum filtration pump, by sucking filtration mixed liquor centrifugalize 10 ~ 15min under the condition of rotating speed 5000 ~ 6000r/min, gained supernatant is Herba Dendrobii extracting solution.
3. a kind of Herba Dendrobii collutory according to claim 1, is characterized in that: described Herba Dendrobii collutory also comprises: 1 ~ 5 part, Bulbus Allii, Radix Notoginseng 5 ~ 8 parts, Folium Callicarpae Formosanae 1 ~ 3 part, Herba Artemisiae Annuae 3 ~ 5 parts, Galla Chinensis 3 ~ 7 parts, Radix Ophiopogonis 3 ~ 5 parts, Rhizoma Phragmitis 4 ~ 6 parts, Herba Asari 1 ~ 3 part, 5 ~ 7 parts, Radix Glycyrrhizae, sodium monofluorophosphate 0.05 part, hibitane 0.005 part, ethanol 10 parts, glycerol 5 parts, sodium lauryl sulphate 1 part, polyoxyethylene hydrogenated Oleum Ricini 1 part, sodium fluoride 0.05 part, spice 0.1 part, deionized water 100 parts.
4. a kind of Herba Dendrobii collutory according to claim 1, is characterized in that: described spice is the one of Flos Lonicerae extract, Flos Rosae Rugosae extract, Folium Menthae extract, Flos Jasmini Sambac extract.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610039662.9A CN105560118A (en) | 2016-01-21 | 2016-01-21 | Dendrobium officinale mouth wash |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610039662.9A CN105560118A (en) | 2016-01-21 | 2016-01-21 | Dendrobium officinale mouth wash |
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| CN105560118A true CN105560118A (en) | 2016-05-11 |
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| CN201610039662.9A Pending CN105560118A (en) | 2016-01-21 | 2016-01-21 | Dendrobium officinale mouth wash |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106377474A (en) * | 2016-10-09 | 2017-02-08 | 倪飞鹏 | Dendrobium officinale mask and manufacturing method thereof |
| CN106729656A (en) * | 2016-12-07 | 2017-05-31 | 江山 | A kind of oral care composition for treating dry and its application in toothpaste |
| CN107149571A (en) * | 2017-04-17 | 2017-09-12 | 廖华勇 | Jasmin general type mouthwash |
| CN107320401A (en) * | 2017-08-18 | 2017-11-07 | 武汉华士特工业生物技术开发有限公司 | A kind of mouthwash of pre- anti-caries and preparation method thereof |
| CN110327262A (en) * | 2019-08-07 | 2019-10-15 | 广西中医药大学 | Sweet golden gargle of one kind and its preparation method and application |
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| CN1088429A (en) * | 1993-01-14 | 1994-06-29 | 吴霜 | A kind of medicine oral cavity fragrant liquid that is used for the treatment of the halitosis and the cause of disease |
| CN104367876A (en) * | 2014-11-21 | 2015-02-25 | 邱宝花 | Oral care solution and preparation method thereof |
| CN104926956A (en) * | 2015-06-26 | 2015-09-23 | 广西健宝石斛有限责任公司 | Method of extracting Dendrobium candidum polysaccharides via ultrasonic optimization |
-
2016
- 2016-01-21 CN CN201610039662.9A patent/CN105560118A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1088429A (en) * | 1993-01-14 | 1994-06-29 | 吴霜 | A kind of medicine oral cavity fragrant liquid that is used for the treatment of the halitosis and the cause of disease |
| CN104367876A (en) * | 2014-11-21 | 2015-02-25 | 邱宝花 | Oral care solution and preparation method thereof |
| CN104926956A (en) * | 2015-06-26 | 2015-09-23 | 广西健宝石斛有限责任公司 | Method of extracting Dendrobium candidum polysaccharides via ultrasonic optimization |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106377474A (en) * | 2016-10-09 | 2017-02-08 | 倪飞鹏 | Dendrobium officinale mask and manufacturing method thereof |
| CN106729656A (en) * | 2016-12-07 | 2017-05-31 | 江山 | A kind of oral care composition for treating dry and its application in toothpaste |
| CN106729656B (en) * | 2016-12-07 | 2020-11-10 | 江山 | Oral care composition for treating dry mouth and application of oral care composition in toothpaste |
| CN107149571A (en) * | 2017-04-17 | 2017-09-12 | 廖华勇 | Jasmin general type mouthwash |
| CN107320401A (en) * | 2017-08-18 | 2017-11-07 | 武汉华士特工业生物技术开发有限公司 | A kind of mouthwash of pre- anti-caries and preparation method thereof |
| CN110327262A (en) * | 2019-08-07 | 2019-10-15 | 广西中医药大学 | Sweet golden gargle of one kind and its preparation method and application |
| CN110327262B (en) * | 2019-08-07 | 2022-04-15 | 广西中医药大学 | Ganjin gargle and preparation method and application thereof |
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