CN105542597B - A kind of heat-reflecting heat-insulating high brightness base-material and preparation method thereof - Google Patents
A kind of heat-reflecting heat-insulating high brightness base-material and preparation method thereof Download PDFInfo
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- C09D5/004—Reflecting paints; Signal paints
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- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
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- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
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Abstract
The present invention relates to a kind of heat-reflecting heat-insulating high brightness base-material, is formulated by following components according to following ratio of weight and number：20 30 parts of water, 0.3 0.38 parts of thickener, 0.1 0.35 parts of multifunctional assistant, 0.4 0.7 parts of dispersant, 0.1 0.3 parts of sterilization antiseptic, 0.1 0.3 parts of mould inhibitor, 0.3 0.5 parts of wetting agent, 12 18 parts of micron order titanium white, 4 10 parts of functional stuffing, 18 23 parts of common fillers, 0.2 0.6 parts of defoamer, 23 parts of cosolvent, 1.8 2.4 parts of coalescents, 30 40 parts of pure-acrylic emulsion.Beneficial effects of the present invention：The invention has the advantages that：It is superior that the high brightness base-material combination property prepared is combined using component of the present invention and proportioning, there is excellent sun light reflective, adjustable polychrome, indoor temperature can be significantly reduced.
Description
Technical field
The present invention relates to technical field of coatings, more particularly to a kind of heat-reflecting heat-insulating high brightness base-material and preparation method thereof.
Background technology
Heat-reflecting insulating coating can make the effect of coated article generation temperature adjustment under sunshine irradiation, including solar energy screen
Cover coating, solar heat reflection paint, space insulating moulding coating, energy-saving and heat-insulating paint, temperature reduction IR camouflage paint etc..Wherein, the sun
Reflective coating is to reach the purpose of heat insulation and heat control, also known as reflectivity energy-saving coatings by the sunshine of reflecting part wavelength.
For the type coating using simply, energy-saving effect is obvious, is widely applied to the multiple fields such as building, oil, transport, is current
The focus of insulating moulding coating research.
Traditionally, high reflectance titanium dioxide is used for the reflection for optimizing visible ray, if adding color paste toning, sunshine reflection
Rate will decline to a great extent.In order that coloured surface can keep nice and cool under sunshine, to sightless near-infrared in solar spectrum
(IR) reflection of light becomes most important, because heat caused by this partial spectrum is most.
At present, heat-reflecting insulating coating on the market is mostly white, is using cenosphere and high reflectance titanium white
Major function color stuffing, sun luminous reflectance is higher, but color is single, it is impossible to meets the exterior coating color of building field
Various requirement.Colored heat reflection coatings are because of the high-absorbable in visible light wave range, and it is used and popularization is restricted.
The content of the invention
The present invention provides a kind of heat-reflecting heat-insulating high brightness base-material and preparation method thereof, and heat-reflecting heat-insulating of the invention is brilliant
The reflecting effect of sightless near-infrared (IR) light is excellent during degree base-material is applied on colored heat reflection coatings to solar spectrum, energy
Enough significantly reduce indoor temperature so that heat reflection coatings color is no longer single, adjustable polychrome.
A kind of heat-reflecting heat-insulating high brightness base-material, it is formulated by following components according to following ratio of weight and number：
The thickener is hydroxyethyl cellulose.
The pH adjusting agent that it is alkalescence that the multifunctional assistant, which is,.
The dispersant is polycarboxylate sodium.
The sterilization antiseptic is isothiazolinone biocide agent.
The mould inhibitor is octylisothiazolinone class mould inhibitor.
The wetting agent is nonionic surfactant.
The micron order titanium white is rutile type titanium white material of the particle diameter distribution in 1000~1200nm, passes through change
A kind of high infrared reflection rate and the filler of high-weatherability that TiO2 crystal sizes obtain.
The functional filler is hollow nano microballoon and far-infared ceramic powder according to 1：What 0.8-1 was mixed.
The hollow nano microballoon be a kind of hollow closed spheroid, powdered Ultralight packing material, can effectively every
Thermal insulation amount；The far-infared ceramic powder is made one to synthesize calcining by inorganic mineral, nonmetal oxide and metal oxide
Kind of white powder, it is radiation-curable go out far ir rays more more than normal object.
The common fillers are titanium dioxide, calcined kaolin and coarse whiting according to 1：0.8-1：What 3.5-4 was mixed.
The defoamer is mineral oil defoaming agent.
The cosolvent is propane diols.
The coalescents are alcohol ester 12.
The pure-acrylic emulsion is acrylate and methacrylate copolymer.
A kind of preparation method of heat-reflecting heat-insulating high brightness base-material, including the step of sequentially carry out as follows：
(1) water of 20-30 parts is added in dispersion cylinder, the increasing of 0.3-0.38 parts is added under 300-600r/ minute speed
Thick dose, 15-20 minutes are stirred, are completely dissolved thickener；
(2) and then above-mentioned rotating speed is kept, adds 0.1-0.35 parts multifunctional assistant, 0.4-0.7 parts dispersant, 0.1-0.3
Part sterilization antiseptic, 0.1-0.3 parts mould inhibitor, 0.3-0.5 parts wetting agent and the defoamer of 0.1-0.3 parts, 10-15 points of stirring
Clock；
(3) above-mentioned rotating speed is then kept to add 12-18 part micron orders titanium white, 4-10 parts functional filler and 18-23 parts general
Logical filler, rotating speed is improved afterwards to 1300-1800r/ minutes, stirs 10-15 minutes；
(4) finally reduce rotating speed to 300-600r/ minutes, sequentially add 0.1-0.3 parts defoamer, 2-3 parts cosolvent,
1.8-2.4 parts coalescents and 30-40 part pure-acrylic emulsions, 10-15 minutes are stirred, produce product of the present invention.
The principle of the present invention：Led in the present invention using the graceful titanium whites of Altiris 550 of Hensel as heat reflection function of tonic chord pigment
The crystal size for changing rutile titanium dioxide is crossed, near infrared light can be effectively reflected, realize the possibility of colored heat reflection coatings
Property.In addition, adding cenosphere and far-infared ceramic powder in formula, the former can reduce the thermal conductivity factor of film, and the latter can carry
The hemispherical reflectance of high film.Three is used cooperatively, and can significantly reduce indoor temperature so that heat reflection coatings color is no longer single
One, adjustable polychrome.
Beneficial effects of the present invention：A kind of heat-reflecting heat-insulating high brightness base-material prepared by the present invention has the following advantages that：Adopt
It is superior that the high brightness base-material combination property prepared is combined with component of the present invention and proportioning, there is excellent sunshine to reflect
Property, adjustable polychrome, can significantly reduce indoor temperature.Base-material of the present invention also has excellent weatherability, water-alkali resistance.
Embodiment
In following product, the thickener is preferably the NATROSOL of Ashland companies of U.S. production (Asia is across dragon)
250HBR hydroxyethyl celluloses；
The multifunctional assistant is preferably the AMP-95 of LG-DOW company production；
The dispersant is preferably the OROTAN CA2500 of LG-DOW production；
The sterilization antiseptic is preferably that Sol company of Britain producesRS；
The mould inhibitor is preferably that Sol company of Britain producesEPW；
The wetting agent is preferably the SN-WET 996 of Japanese Nuo Puke productions；
The defoamer is preferably the Dispelair CF 246 of England Blackburn production；
The micron order titanium white is preferably the Altiris 550 of Hensel Man production；
The cenosphere is preferably the novel ultra-light cenosphere of Shanghai Ge Run Asias company production；
The far-infared ceramic powder is preferably the nano-scale far infrared ceramic powder of Hebei Zhen Chuan companies production；
The ordinary titanium powder is preferably the R668 titanium dioxides of Guangdong Hui Yuntai industry company production；
The calcined kaolin is preferably that the ultra-fine high white calcinings of the MXK201 of Inner Mongol Meng Xi kaolinite powders company production are high
Ridge soil；
The coarse whiting is preferably the SN-1083800 mesh powdered whitings of Fujian agriculture-countryside-farmer's calcium carbonate company production；
The cosolvent is preferably the propane diols of Shandong Depew chemical science and technology company production；
The coalescents are preferably the TEXANOL of Yi Si Man of U.S. production；
The pure-acrylic emulsion is preferably what BASF Aktiengesellschaft produced DS6266。
Case 1 is embodied
A kind of heat-reflecting heat-insulating high brightness base-material is prepared, is formulated by following components and ratio of weight and number：
The functional filler is hollow nano microballoon and far-infared ceramic powder according to 1：0.9 mixes.
The common fillers are titanium dioxide, calcined kaolin and coarse whiting according to 1：1：4 mix.
A kind of preparation method of heat-reflecting insulating coating, it includes following the step of sequentially carrying out：
(1) 19.24 parts of water is added in dispersion cylinder, 0.36 part of thickener is added under 300r/ minute speed and is stirred
Mix 15 minutes, be completely dissolved thickener.
(2) add 0.2 part of multifunctional assistant, 0.6 part of dispersant, 0.2 part of sterilization antiseptic, 0.2 part of mould inhibitor, 0.3 part
Wetting agent, 0.2 part of defoamer, stir 15 minutes.
(3) 16 parts of modified titanium whites, 6 parts of functional fillers and 20 parts of common fillers are added, with 1300r/ minute high-speed stirreds
10 minutes.
(4) rotating speed is reduced, sequentially adds 0.2 part of defoamer, 2.5 parts of cosolvents, 2 parts of coalescents, 32 parts of pure-acrylic emulsions,
Stirring produces product of the present invention in 10 minutes.
Case 2 is embodied
A kind of heat-reflecting heat-insulating high brightness base-material is prepared, is formulated by following components and ratio of weight and number：
The functional filler is hollow nano microballoon and far-infared ceramic powder according to 1：1 mixes.
The common fillers are titanium dioxide, calcined kaolin and coarse whiting according to 1：1：4 mix.
A kind of preparation method of heat-reflecting insulating coating, it includes following the step of sequentially carrying out：
(1) 16.23 parts of water is added in dispersion cylinder, 0.32 part of thickener is added under 300r/ minute speed and is stirred
Mix 15 minutes, be completely dissolved thickener.
(2) add 0.15 part of multifunctional assistant, 0.7 part of dispersant, 0.2 part of sterilization antiseptic, 0.2 part of mould inhibitor, 0.4 part
Wetting agent, 0.3 part of defoamer, stir 10 minutes.
(3) 14 parts of modified titanium whites, 4 parts of functional fillers and 24 parts of common fillers are added, with 1300r/ minute high-speed stirreds
10 minutes.
(4) rotating speed is reduced, sequentially adds 0.2 part of defoamer, 2.5 parts of cosolvents, 2 parts of coalescents, 34 parts of pure-acrylic emulsions,
Stirring produces product of the present invention in 10 minutes.
Specific embodiment 3
The functional filler is hollow nano microballoon and far-infared ceramic powder according to 1：0.9 mixes.
The common fillers are titanium dioxide, calcined kaolin and coarse whiting according to 1：0.9：3.7 mix.
(1) 20 parts of water is added in dispersion cylinder, 0.3 part of thickener is added under 300r/ minute speed, stirs 15 points
Clock, it is completely dissolved thickener；
(2) and then keep above-mentioned rotating speed, add 0.1 part of multifunctional assistant, 0.4 part of dispersant, 0.1 part of sterilization antiseptic,
0.1 part of mould inhibitor, 0.3 part of wetting agent and 0.1 part of defoamer, stir 10 minutes；
(3) above-mentioned rotating speed is then kept to add 12 parts of micron order titanium whites, 4 parts of functional fillers and 18 parts of fillers, Zhi Houti
High rotating speed stirs 10 minutes to 1300r/ minutes；
(4) rotating speed is finally reduced to 300r/ minutes, is sequentially added 0.1 part of defoamer, 2 parts of cosolvents, 1.8 parts of film forming and is helped
Agent and 30 parts of pure-acrylic emulsions, stir 10 minutes, produce product of the present invention.
Specific embodiment 4
The functional filler is hollow nano microballoon and far-infared ceramic powder according to 1：0.8 mixes.
The common fillers are titanium dioxide, calcined kaolin and coarse whiting according to 1：0.8：3.5 mix.
(1) 30 parts of water is added in dispersion cylinder, 0.38 part of thickener, stirring 20 is added under 600r/ minute speed
Minute, it is completely dissolved thickener；
(2) and then keep above-mentioned rotating speed, add 0.35 part of multifunctional assistant, 0.7 part of dispersant, 0.3 part of sterilization antiseptic,
0.3 part of mould inhibitor, 0.5 part of wetting agent and 0.3 part of defoamer, stir 10 minutes；
(3) above-mentioned rotating speed is then kept to add 18 parts of micron order titanium whites, 10 parts of functional fillers and 23 parts of fillers, Zhi Houti
High rotating speed stirs 15 minutes to 1800r/ minutes；
(4) rotating speed is finally reduced to 600r/ minutes, is sequentially added 0.3 part of defoamer, 3 parts of cosolvents, 2.4 parts of film forming and is helped
Agent and 40 parts of pure-acrylic emulsions, stir 15 minutes, produce product of the present invention.
Compared with prior art, the mixing of high brightness base-material and 0.01-1.2 part mill bases that the present invention is prepared, can be obtained
To the high brightness colored paint of multiple color.By testing the high brightness colored paint of multiple color, the sun luminous reflectance of colored paint
About 0.7, near-infrared sun reflectivity is about 0.85, more than the standard regulation in JGT 235-2014, illustrates to obtain brilliant
Degree colored paint can keep higher sun light reflective.
Tested with further reference to GB/T 9755-2014, show that this base-material also has excellent weatherability, water-fast
Alkali resistance.
Claims (2)
- A kind of 1. heat-reflecting heat-insulating high brightness base-material, it is characterised in that：Prepared by following components according to following ratio of weight and number and Into：Described common fillers are titanium dioxide, calcined kaolin and coarse whiting according to 1：0.8-1：What 3.5-4 was mixed；The functional filler is hollow nano microballoon and far-infared ceramic powder according to 1：What 0.8-1 was mixed；The micron order titanium white is rutile type titanium white material of the particle diameter in 1000~1200nm；The multifunctional assistant is alkaline pH adjusting agent；The thickener is hydroxyethyl cellulose；The dispersant is polycarboxylate sodium；The mould inhibitor is octylisothiazolinone class mould inhibitor；The sterilization antiseptic is isothiazolinone biocide agent；The wetting agent is nonionic surfactant；The defoamer is mineral oil defoaming agent；The cosolvent is propane diols；The coalescents are alcohol ester 12；It is described Pure-acrylic emulsion is acrylate and methacrylate copolymer.
- A kind of 2. preparation method of heat-reflecting heat-insulating high brightness base-material according to claim 1, it is characterised in that：Including such as Under the step of sequentially carrying out：(1) water of 20-30 parts is added in dispersion cylinder, the thickener of 0.3-0.38 parts is added under 300-600r/ minute speed, 15-20 minutes are stirred, are completely dissolved thickener；(2) and then above-mentioned rotating speed is kept, addition 0.1-0.35 parts multifunctional assistant, 0.4-0.7 parts dispersant, 0.1-0.3 parts are killed Bacterium preservative, 0.1-0.3 parts mould inhibitor, 0.3-0.5 parts wetting agent and the defoamer of 0.1-0.3 parts, stir 10-15 minutes；(3) then keep above-mentioned rotating speed to add 12-18 part micron orders titanium white, 4-10 parts functional filler and 18-23 parts commonly to fill out Material, rotating speed is improved afterwards to 1300-1800r/ minutes, stirs 10-15 minutes；(4) rotating speed is finally reduced to 300-600r/ minutes, sequentially adds 0.1-0.3 parts defoamer, 2-3 parts cosolvent, 1.8- 2.4 parts of coalescents and 30-40 part pure-acrylic emulsions, 10-15 minutes are stirred, are produced.
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