CN103483963A - Multifunctional scrapping type single-component thermal insulation coating, multifunctional scrapping type bi-component thermal insulation coating and preparing methods of multifunctional scrapping type single-component thermal insulation coating and multifunctional scrapping type bi-component thermal insulation coating - Google Patents
Multifunctional scrapping type single-component thermal insulation coating, multifunctional scrapping type bi-component thermal insulation coating and preparing methods of multifunctional scrapping type single-component thermal insulation coating and multifunctional scrapping type bi-component thermal insulation coating Download PDFInfo
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Abstract
The invention relates to a multifunctional scrapping type single-component thermal insulation coating, a multifunctional scrapping type bi-component thermal insulation coating and preparing methods of the multifunctional scrapping type single-component thermal insulation coating and the multifunctional scrapping type bi-component thermal insulation coating. The multifunctional scrapping type single-component thermal insulation coating is formed by main paint. The main paint is prepared from, by weight, 2-3% of anti-freezing agent, 1-1.5% of dispersing agent, 1-2% of wetting agent, 0.15-0.2% of pH regulator, 0.3-0.6% of defoaming agent, 30-35% of emulsion, 25-35% of thermal insulation material, 0.4-0.8% of lignocellulose, 0.2-0.5% of mildew preventive, 0.3-0.6% of antibacterial agent, 0.15-0.3% of preservative and 1-3% of film-forming additive, the balance being water. The multifunctional scrapping type bi-component thermal insulation coating is formed by mixing main paint and white cement according to the weight ratio of 8-12:1. The multifunctional scrapping type single-component thermal insulation coating and the multifunctional scrapping type bi-component thermal insulation coating which are prepared with the methods are extremely low in heat conductivity coefficient, high in solar emissivity, good in thermal insulation function, free of cracking in impasto and capable of bringing a strong sense of decoration.
Description
Technical field
The present invention relates to a kind of building coating field, particularly scrape the type heat insulating coatings for a kind of multi-functional batch.
Background technology
Building heat insulation coating is one of focus of current building coating research, has obtained in recent years larger progress, and relevant paper and patent are also more.At present the research of building heat insulation coating mainly is divided into to both direction: one is building thermal-insulating coating, mostly be thick coating, thermal conductivity and the thicker coat-thickness lower by coating guarantee that the larger thermal resistance of coating is to reach the purpose of insulation, the lagging material of corresponding employing mostly is sepiolite that thermal conductivity is lower, pearlstone, expanded vermiculite etc., because the lagging material adopted mostly is colored materials, color is gloomy, cause thermal insulation coatings color complexity, decorate sense poor, therefore lessly be coated with for face; Two is insulating mold coating for construction, be generally thin coating, by improving coating reflectivity or thermal-radiating mode to reach heat insulation purpose, this class lagging material mostly is hollow microsphere, far-infrared radiation ceramic powder etc., but this kind of thick painting of coating is easy to crack, so such thermal insulating coating is multiplex, in building exterior wall face, be coated with, particularly reflective heat-insulation paint could play a role preferably under solar light irradiation.
Summary of the invention
The object of the present invention is to provide a kind of multi-functional batch to scrape single, double component heat insulating coatings of type and preparation method thereof, scrape the single, double component heat insulating coatings of type and not only possess extremely low thermal conductivity and higher sun emittance simultaneously for prepared by the present invention multi-functional batch, there is good heat insulation and heat insulation function, and thick painting do not ftracture, decorate sense strong.
The present invention is achieved in that a kind of multi-functional batch is scraped type single component heat insulating coatings, main paint, consists of, and described main paint is formulated according to following weight percent by following component:
In said components, a kind of or any mixing that described heat-insulating heat-preserving material is hollow glass micropearl, hollow ceramic microspheres and expended microsphere; Described emulsion is the acrylic ester copolymer elastic emulsion.
Further prioritization scheme is: the macrofiber that described lignocellulose is length 400-500 μ m.
Further prioritization scheme is: described dispersion agent is the better poly carboxylic acid ammonium salt of hydrophobicity dispersion agent.Described dispersion agent adopts the CA2500 dispersion agent of DOW Chemical or the SN-5027 dispersion agent of Sheng Nuopuke.
Further prioritization scheme is: described wetting agent is the HLB(hydrophile-lipophile balance value) for the class of 10-16 without the APEO wetting agent, it adopts this FN211 wetting agent of the BD-109 wetting agent of DOW Chemical or hamming.
Further prioritization scheme is: described defoamer is mineral oils or silicone based defoamer.It adopts peaceful FoamasterNXZ defoamer or the FOAMSTARA10 defoamer of CF246 defoamer, section of Blackburn.
Further prioritization scheme is: the solid content of described acrylic ester copolymer elastic emulsion is 45%-50%, and second-order transition temperature is-20--25 ℃.Described frostproofer is propylene glycol or ethylene glycol.
Scrape type two-pack heat insulating coatings for a kind of multi-functional batch, the ratio of weight and number by main paint and white cement by 8-12:1 mixes: described main paint is formulated according to following weight percent by following component:
In said components, a kind of or any mixing that described heat-insulating heat-preserving material is hollow glass micropearl, hollow ceramic microspheres and expended microsphere; Described emulsion is the acrylic ester copolymer elastic emulsion.
Further prioritization scheme is: the macrofiber that described lignocellulose is length 400-500 μ m; Described dispersion agent is poly carboxylic acid ammonium salt dispersion agent; Described wetting agent is the wetting agent that HLB is 10-16; Described defoamer is mineral oils or silicone based defoamer; Described frostproofer is propylene glycol or ethylene glycol; The solid content of described acrylic ester copolymer elastic emulsion is 45%-50%, and second-order transition temperature is-20--25 ℃.
A kind ofly prepare the multi-functional crowd of preparation method who scrapes type single component heat insulating coatings, at first by frostproofer, dispersion agent, wetting agent, defoamer, after pH adjusting agent and water mix, disperse 5-10 minute under 200-400 rev/min of speed, then add emulsion redispersion 5-10 minute, then add heat-insulating heat-preserving material, lignocellulose, mould inhibitor and antiseptic-germicide, improve rotating speed to 800-1000 rev/min of dispersion 10-20 minute, then reduce rotating speed to 500-700 rev/min, add successively again sanitas, film coalescence aid and defoamer, disperse 8-12 minute to mixing, obtain main paint.
A kind ofly prepare the multi-functional crowd of preparation method who scrapes the two-component-type heat insulating coatings,
(1) prepare main paint according to following preparation method: after at first frostproofer, dispersion agent, wetting agent, defoamer, pH adjusting agent and water being mixed, disperse 5-10 minute under 200-400 rev/min of speed, then add emulsion redispersion 5-10 minute, then add heat-insulating heat-preserving material, lignocellulose, mould inhibitor and antiseptic-germicide, improve rotating speed to 800-1000 rev/min of dispersion 10-20 minute, then reduce rotating speed to 500-700 rev/min, add successively again sanitas, film coalescence aid and defoamer, disperse 8-12 minute to mixing, obtain main paint;
(2) the main paint prepared by step (1) and white cement are by the ratio of weight and number mixing and stirring of 8-12:1.
Multi-functional crowd of the present invention scrapes the type heat insulating coatings and has the following advantages:
1, the present invention had both overcome the poor shortcoming that should not be coated with for face of thick vacuum coatings decoration sense, had also overcome the thick painting of thin coating shortcoming easy to crack.The present invention uses hollow microsphere class material as heat-insulating heat-preserving material, hollow microsphere class material is that a class has the class heat-insulating heat-preserving material than low thermal conductivity and high reflectance concurrently, possess whiteness and feel preferably simultaneously, can not affect the decorative aesthetics of paint film during a large amount of the interpolation, but the anti-cracking performance of filming is had a certain impact, the present invention, by using elastic emulsion and long lignocellulose collocation to carry out balance, has overcome the thick painting of coating shortcoming easy to crack;
2, the snappiness acrylate copolymer emulsion that the present invention uses, can give snappiness that coating is outstanding lasting and good weathering resistance, wear resistance and sticking power;
3, coating of the present invention has possessed lower thermal conductivity and high sun reflectivity simultaneously, thick vacuum coating or heat-insulation and heat-preservation putty had both been can be used as, also can be used for thin matter sun reflective heat-insulation paint, this coating possesses the sliding feel of silk as flannelette simultaneously, can be used for the inner wall of building finish paint, also possess certain insulation effect when possessing special feel;
4, the form of construction work of this coating adopts to criticize and scrapes formula, both can meet the construction of thick coating and putty, also can meet the construction of thin matter exterior wall;
When 5, the present invention is as thick coating or the use of heat-insulation and heat-preservation putty, both can adopt the single component that main paint is only arranged, and also can adopt the two components that mixed by main paint and white cement, when adopting two component, anti-cracking performance and intensity increase significantly.During as thin coating, adopt and only have the single component of main paint to meet the demands.
Embodiment
Below in conjunction with specific embodiment, the present invention will be described in detail.
(1) embodiment is as follows: scrape type single component heat insulating coatings for a kind of multi-functional batch, consist of main paint, described main paint is formulated according to following weight percent by following component:
Scrape type two-pack heat insulating coatings for a kind of multi-functional batch, the ratio of weight and number by main paint and white cement by 8-12:1 mixes: described main paint is formulated according to following weight percent by following component:
Wherein, a kind of or any mixing that described heat-insulating heat-preserving material is hollow glass micropearl, hollow ceramic microspheres and expended microsphere; Described emulsion is the acrylic ester copolymer elastic emulsion, and the solid content of described acrylic ester copolymer elastic emulsion is 45%-50%, and second-order transition temperature is-20--25 ℃.The macrofiber that described lignocellulose is length 400-500 μ m.Described frostproofer is propylene glycol or ethylene glycol.Described dispersion agent is the better poly carboxylic acid ammonium salt of hydrophobicity dispersion agent; Described dispersion agent adopts the CA2500 dispersion agent of DOW Chemical or the SN-5027 dispersion agent of Sheng Nuopuke, also can adopt similar other type product.Described wetting agent is the HLB(hydrophile-lipophile balance value) for the class of 10-16 without the APEO wetting agent, it adopts this FN211 wetting agent of the BD-109 wetting agent of DOW Chemical or hamming, also can adopt similar other type product.PH adjusting agent is the alkaline pH conditioning agent.Described defoamer is mineral oils or silicone based defoamer.Peaceful FoamasterNXZ defoamer or the FOAMSTARA10 defoamer of CF246 defoamer, section that it adopts Blackburn, also can adopt similar other type product.
A kind ofly prepare the multi-functional crowd of preparation method who scrapes type single component heat insulating coatings, at first by frostproofer, dispersion agent, wetting agent, defoamer, after pH adjusting agent and water mix, disperse 5-10 minute under 200-400 rev/min of speed, then add emulsion redispersion 5-10 minute, then add heat-insulating heat-preserving material, lignocellulose, mould inhibitor and antiseptic-germicide, improve rotating speed to 800-1000 rev/min of dispersion 10-20 minute, then reduce rotating speed to 500-700 rev/min, add successively again sanitas, film coalescence aid and defoamer, disperse 8-12 minute to mixing, obtain main paint.
A kind ofly prepare the multi-functional crowd of preparation method who scrapes the two-component-type heat insulating coatings,
(1) prepare main paint according to following preparation method: after at first frostproofer, dispersion agent, wetting agent, defoamer, pH adjusting agent and water being mixed, disperse 5-10 minute under 200-400 rev/min of speed, then add emulsion redispersion 5-10 minute, then add heat-insulating heat-preserving material, lignocellulose, mould inhibitor and antiseptic-germicide, improve rotating speed to 800-1000 rev/min of dispersion 10-20 minute, then reduce rotating speed to 500-700 rev/min, add successively again sanitas, film coalescence aid and defoamer, disperse 8-12 minute to mixing, obtain main paint;
(2) the main paint prepared by step (1) and white cement are by the ratio of weight and number mixing and stirring of 8-12:1.
(2), embodiment is as follows: below by embodiment, further illustrate the present invention:
Embodiment 1: scrape type single component heat insulating coatings for a kind of multi-functional batch, consist of main paint, described main paint is formulated according to following weight percent by following component:
A kind ofly prepare the multi-functional crowd of preparation method who scrapes type single-component heat insulating coatings, wherein prepared according to following preparation method by main paint: at first by 27% water, 3% frostproofer, 1.2% dispersion agent, 1.5% wetting agent, after 0.2% defoamer 1 and 0.2% pH adjusting agent are mixed, under 300 rev/mins of speed, disperse 10 minutes, then add 33% emulsion redispersion 8 minutes, then add 22% hollow glass micropearl, 8% expended microsphere, 0.6% lignocellulose, 0.3% mould inhibitor and 0.5% antiseptic-germicide, improving rotating speed to 900 rev/min disperses 15 minutes, then reduce rotating speed to 600 rev/min, add successively again 0.2% sanitas, 1.2% film coalescence aid 1, 0.8% film coalescence aid 2 and 0.3% defoamer 2, disperse 10 minutes to mixing.
A kind ofly prepare the multi-functional crowd of preparation method who scrapes the two-component-type heat insulating coatings, by the main paint of above-mentioned preparation and white cement by ratio of weight and the number of copies 8:1 mix, can criticize and scrape by machine or artificial mixing and stirring.
In the present embodiment component, described frostproofer is propylene glycol; Dispersion agent is the CA500 dispersion agent that DOW Chemical is produced; The BD-109 wetting agent that the wetting agent DOW Chemical is produced; PH adjusting agent is the AMP-95pH conditioning agent that DOW Chemical is produced; The CF246 defoamer that defoamer 1 is produced for Blackburn; Emulsion is the Elastene2468 emulsion that DOW Chemical is produced; Hollow glass micropearl is the heat-insulating heat-preserving material that particle diameter is 40-60 μ m; Expended microsphere is the heat-insulating heat-preserving material that particle diameter is 20-30 μ m; Lignocellulose is the PWC500 lignocellulose that German JRS company produces; The EPW mould inhibitor that mould inhibitor is the Bristol chemical production; Antiseptic-germicide is the husky ZOE antiseptic-germicide of producing of dragon; The HF sanitas that sanitas is the Bristol chemical production; The Coasol film coalescence aid that film coalescence aid 1 is produced for Yi Shiman; The Texnol film coalescence aid that film coalescence aid 2 is produced for Yi Shiman; Defoamer 2 is the peaceful A10 defoamer of producing of section.Said components also can adopt similar other type product.
Through to the test of the present embodiment, multi-functional crowd of the present invention scrape the type every technical performance index of single, double component heat insulating coatings and experimental data as shown in the table:
Multi-functional batch of every technical performance index and experimental data of scraping type single-component heat insulating coatings is as follows:
Multi-functional batch of every technical performance index and experimental data of scraping the two-component-type heat insulating coatings is as follows:
Embodiment 2: scrape type single component heat insulating coatings for a kind of multi-functional batch, consist of main paint, described main paint is formulated according to following weight percent by following component:
A kind ofly prepare the multi-functional crowd of preparation method who scrapes the one-pack type heat insulating coatings, wherein prepared according to following preparation method by main paint: at first by 20% water, 2.5% frostproofer, 1.5% dispersion agent, 2% wetting agent, after 0.2% defoamer 1 and 0.2% pH adjusting agent are mixed, under 400 rev/mins of speed, disperse 6 minutes, then add 35% emulsion redispersion 10 minutes, then add 20% hollow ceramic microspheres, 6% hollow glass micropearl, 8% expended microsphere, 0.8% lignocellulose, 0.3% mould inhibitor and 0.5% antiseptic-germicide, improving rotating speed to 1000 rev/min disperses 12 minutes, then reduce rotating speed to 700 rev/min, add successively again 0.2% sanitas, 1.3% film coalescence aid 1, 1.2% film coalescence aid 2 and 0.3% defoamer 2, disperse 8 minutes to mixing.
A kind ofly prepare the multi-functional crowd of preparation method who scrapes the two-component-type heat insulating coatings, by the main paint of above-mentioned preparation and white cement by ratio of weight and the number of copies 12:1 mix, can criticize and scrape by machine or artificial mixing and stirring.
In the present embodiment component, described frostproofer is ethylene glycol; Dispersion agent is the SN-5027 dispersion agent that Sheng Nuopuke produces; The FN211 wetting agent of this production of wetting agent hamming; PH adjusting agent is the AMP-95pH conditioning agent that DOW Chemical is produced; The FoamasterNXZ defoamer that defoamer 1 is produced for Blackburn; Emulsion is the Elastene2468 emulsion that DOW Chemical is produced; Hollow ceramic microspheres is the heat-insulating heat-preserving material that particle diameter is 40-60 μ m; Hollow glass micropearl is the heat-insulating heat-preserving material that particle diameter is 40-60 μ m; Expended microsphere is the heat-insulating heat-preserving material that particle diameter is 20-30 μ m; Lignocellulose is the PWC500 lignocellulose that German JRS company produces; Mould inhibitor is the husky ZOE-T mould inhibitor of producing of dragon; Antiseptic-germicide is the husky ZOE antiseptic-germicide of producing of dragon; The B20 sanitas that sanitas is the Bristol chemical production; The Coasol film coalescence aid that film coalescence aid 1 is produced for Yi Shiman; The Texnol film coalescence aid that film coalescence aid 2 is produced for Yi Shiman; Defoamer 2 is the peaceful A10 defoamer of producing of section.Said components also can adopt similar other type product.
Through to the test of the present embodiment, multi-functional crowd of the present invention scrape the type every technical performance index of single, double component heat insulating coatings and experimental data as shown in the table:
Multi-functional batch of every technical performance index and experimental data of scraping type single-component heat insulating coatings is as follows:
Multi-functional batch of every technical performance index and experimental data of scraping the two component heat insulating coatings of type is as follows:
Embodiment 3: scrape type single component heat insulating coatings for a kind of multi-functional batch, consist of main paint, described main paint is formulated according to following weight percent by following component:
A kind ofly prepare the multi-functional crowd of preparation method who scrapes type single component heat insulating coatings, wherein prepared according to following preparation method by main paint: at first by 31% water, 3% frostproofer, 1% dispersion agent, 2% wetting agent, after 0.15% defoamer 1 and 0.2% pH adjusting agent are mixed, under 250 rev/mins of speed, disperse 10 minutes, then add 30% emulsion redispersion 5 minutes, then add 20% hollow ceramic microspheres, 8% expended microsphere, 0.8% lignocellulose, 0.5% mould inhibitor and 0.3% antiseptic-germicide, improving rotating speed to 800 rev/min disperses 20 minutes, then reduce rotating speed to 500 rev/min, add successively again 0.3% sanitas, 1.3% film coalescence aid 1, 1.2% film coalescence aid 2 and 0.25% defoamer 2, disperse 12 minutes to mixing.
A kind ofly prepare the multi-functional crowd of preparation method who scrapes the two-component-type heat insulating coatings, by the main paint of above-mentioned preparation and white cement by ratio of weight and the number of copies 10:1 mix, can criticize and scrape by machine or artificial mixing and stirring.
In the present embodiment component, described frostproofer is propylene glycol; Dispersion agent is the CA500 dispersion agent that DOW Chemical is produced; The BD-109 wetting agent that the wetting agent DOW Chemical is produced; PH adjusting agent is the AMP-95pH conditioning agent that DOW Chemical is produced; The CF246 defoamer that defoamer 1 is produced for Blackburn; Emulsion is the Elastene2468 emulsion that DOW Chemical is produced; Hollow ceramic microspheres is the heat-insulating heat-preserving material that particle diameter is 40-60 μ m; Expended microsphere is the heat-insulating heat-preserving material that particle diameter is 20-30 μ m; Lignocellulose is the PWC500 lignocellulose that German JRS company produces; Mould inhibitor is the husky ZOE-T mould inhibitor of producing of dragon; Antiseptic-germicide is the nanometer silver that Korea S's Samsung is produced; The RS sanitas that sanitas is the Bristol chemical production; The Coasol film coalescence aid that film coalescence aid 1 is produced for Yi Shiman; The Texnol film coalescence aid that film coalescence aid 2 is produced for Yi Shiman; Defoamer 2 is the peaceful A10 defoamer of producing of section.Said components also can adopt similar other type product.
Through to the test of the present embodiment, multi-functional crowd of the present invention scrape the type every technical performance index of single, double component heat insulating coatings and experimental data as shown in the table:
Multi-functional batch of every technical performance index and experimental data of scraping type single-component heat insulating coatings is as follows:
Multi-functional batch of every technical performance index and experimental data of scraping the two component heat insulating coatings of type is as follows:
Test result from the above embodiments: the present invention possesses lower thermal conductivity and high sun reflectivity simultaneously, and can meet every detection index of external wall finish paint; It is strong that the paint film good hand touch is decorated sense.The two component heat insulating coatings that adopt main paint and white cement to be mixed with, can greatly improve anti-cracking performance, the thickness that multi-functional crowd of the present invention scrapes type single-component heat insulating coatings all can not ftracture within 1.5mm, and the multi-functional batch of thickness of scraping the two component heat insulating coatings of type all can not ftracture within 3mm.
Above-mentioned embodiment just is explained in detail technical scheme of the present invention, and the present invention has more than and only is confined to above-described embodiment, and every any improvement or replacement according to the principle of the invention, all should be within protection scope of the present invention.
Claims (8)
1. scrape type single component heat insulating coatings for one kind multi-functional batch, it is characterized in that: main paint, consist of, described main paint is formulated according to following weight percent by following component:
In said components, one or more any mixing that described heat-insulating heat-preserving material is hollow glass micropearl, hollow ceramic microspheres and expended microsphere; Described emulsion is the acrylic ester copolymer elastic emulsion.
2. scrape type single-component heat insulating coatings for multi-functional batch according to claim 1, it is characterized in that: the macrofiber that described lignocellulose is length 400-500 μ m; Described dispersion agent is poly carboxylic acid ammonium salt dispersion agent; Described wetting agent is the wetting agent that HLB is 10-16; Described defoamer is mineral oils or silicone based defoamer; Described frostproofer is propylene glycol or ethylene glycol.
3. scrape type single-component heat insulating coatings for multi-functional batch according to claim 1, it is characterized in that: the solid content of described acrylic ester copolymer elastic emulsion is 45%-50%, and second-order transition temperature is-20--25 ℃.
4. scrape type two-pack heat insulating coatings for one kind multi-functional batch, it is characterized in that: the ratio of weight and number by main paint and white cement by 8-12:1 mixes: described main paint is formulated according to following weight percent by following component:
In said components, one or more any mixing that described heat-insulating heat-preserving material is hollow glass micropearl, hollow ceramic microspheres and expended microsphere; Described emulsion is the acrylic ester copolymer elastic emulsion.
5. scrape type two-pack heat insulating coatings for multi-functional batch according to claim 1, it is characterized in that: the macrofiber that described lignocellulose is length 400-500 μ m; Described dispersion agent is poly carboxylic acid ammonium salt dispersion agent; Described wetting agent is the wetting agent that HLB is 10-16; Described defoamer is mineral oils or silicone based defoamer; Described frostproofer is propylene glycol.
6. scrape type two-pack heat insulating coatings for multi-functional batch according to claim 1, it is characterized in that: the solid content of described acrylic ester copolymer elastic emulsion is 45%-50%, and second-order transition temperature is-20--25 ℃.
7. one kind for the preparation of the multi-functional crowd of preparation method who scrapes type single component heat insulating coatings claimed in claim 1, it is characterized in that: at first by frostproofer, dispersion agent, wetting agent, defoamer, after pH adjusting agent and water mix, disperse 5-10 minute under 200-400 rev/min of speed, then add emulsion redispersion 5-10 minute, then add heat-insulating heat-preserving material, lignocellulose, mould inhibitor and antiseptic-germicide, improve rotating speed to 800-1000 rev/min of dispersion 10-20 minute, then reduce rotating speed to 500-700 rev/min, add successively again sanitas, film coalescence aid and defoamer, disperse 8-12 minute to mixing, obtain main paint.
8. one kind for the preparation of the multi-functional crowd of preparation method who scrapes the two-component-type heat insulating coatings claimed in claim 4, it is characterized in that:
(1) prepare main paint according to following preparation method: after at first frostproofer, dispersion agent, wetting agent, defoamer, pH adjusting agent and water being mixed, disperse 5-10 minute under 200-400 rev/min of speed, then add emulsion redispersion 5-10 minute, then add heat-insulating heat-preserving material, lignocellulose, mould inhibitor and antiseptic-germicide, improve rotating speed to 800-1000 rev/min of dispersion 10-20 minute, then reduce rotating speed to 500-700 rev/min, add successively again sanitas, film coalescence aid and defoamer, disperse 8-12 minute to mixing, obtain main paint;
(2) the main paint prepared by step (1) and white cement are by the ratio of weight and number mixing and stirring of 8-12:1.
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