CN105541283A - Anti-cracking copper artware clay sculpture material and preparation method thereof - Google Patents
Anti-cracking copper artware clay sculpture material and preparation method thereof Download PDFInfo
- Publication number
- CN105541283A CN105541283A CN201510939777.9A CN201510939777A CN105541283A CN 105541283 A CN105541283 A CN 105541283A CN 201510939777 A CN201510939777 A CN 201510939777A CN 105541283 A CN105541283 A CN 105541283A
- Authority
- CN
- China
- Prior art keywords
- weight part
- consumption
- preparation
- clay sculpture
- sculpture material
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000004927 clay Substances 0.000 title claims abstract description 54
- 239000000463 material Substances 0.000 title claims abstract description 47
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 title claims abstract description 45
- 229910052802 copper Inorganic materials 0.000 title claims abstract description 45
- 239000010949 copper Substances 0.000 title claims abstract description 45
- 238000002360 preparation method Methods 0.000 title claims abstract description 20
- 238000005336 cracking Methods 0.000 title abstract description 5
- 239000000047 product Substances 0.000 claims abstract description 19
- 230000032683 aging Effects 0.000 claims abstract description 17
- 239000012065 filter cake Substances 0.000 claims abstract description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 14
- 241000219138 Luffa Species 0.000 claims abstract description 13
- 235000003956 Luffa Nutrition 0.000 claims abstract description 13
- 244000302544 Luffa aegyptiaca Species 0.000 claims abstract description 13
- 235000009814 Luffa aegyptiaca Nutrition 0.000 claims abstract description 13
- 239000004372 Polyvinyl alcohol Substances 0.000 claims abstract description 13
- 238000009835 boiling Methods 0.000 claims abstract description 13
- 229920002451 polyvinyl alcohol Polymers 0.000 claims abstract description 13
- 229920000742 Cotton Polymers 0.000 claims abstract description 11
- 235000007164 Oryza sativa Nutrition 0.000 claims abstract description 11
- 241000241413 Propolis Species 0.000 claims abstract description 11
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 11
- 235000013312 flour Nutrition 0.000 claims abstract description 11
- 229940069949 propolis Drugs 0.000 claims abstract description 11
- 235000009566 rice Nutrition 0.000 claims abstract description 11
- 239000002253 acid Substances 0.000 claims abstract description 10
- 229910021538 borax Inorganic materials 0.000 claims abstract description 10
- 235000010339 sodium tetraborate Nutrition 0.000 claims abstract description 10
- 239000004328 sodium tetraborate Substances 0.000 claims abstract description 10
- 238000002156 mixing Methods 0.000 claims abstract description 5
- 238000001816 cooling Methods 0.000 claims abstract description 4
- 240000007594 Oryza sativa Species 0.000 claims abstract 3
- 238000000034 method Methods 0.000 claims description 14
- 239000002245 particle Substances 0.000 claims description 12
- OWEGMIWEEQEYGQ-UHFFFAOYSA-N 100676-05-9 Natural products OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(OC2C(OC(O)C(O)C2O)CO)O1 OWEGMIWEEQEYGQ-UHFFFAOYSA-N 0.000 claims description 10
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 10
- GUBGYTABKSRVRQ-PICCSMPSSA-N Maltose Natural products O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@@H](CO)OC(O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-PICCSMPSSA-N 0.000 claims description 10
- 230000005070 ripening Effects 0.000 claims description 10
- 150000002632 lipids Chemical class 0.000 claims description 9
- 238000002791 soaking Methods 0.000 claims description 3
- 238000010411 cooking Methods 0.000 claims description 2
- 230000029087 digestion Effects 0.000 claims description 2
- 238000007654 immersion Methods 0.000 claims 1
- 238000001914 filtration Methods 0.000 abstract description 4
- 238000004519 manufacturing process Methods 0.000 abstract description 4
- QYLFHLNFIHBCPR-UHFFFAOYSA-N 1-ethynylcyclohexan-1-ol Chemical compound C#CC1(O)CCCCC1 QYLFHLNFIHBCPR-UHFFFAOYSA-N 0.000 abstract 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 abstract 1
- 125000001931 aliphatic group Chemical group 0.000 abstract 1
- 238000004140 cleaning Methods 0.000 abstract 1
- 235000009508 confectionery Nutrition 0.000 abstract 1
- 239000000845 maltitol Substances 0.000 abstract 1
- VQHSOMBJVWLPSR-WUJBLJFYSA-N maltitol Chemical compound OC[C@H](O)[C@@H](O)[C@@H]([C@H](O)CO)O[C@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O VQHSOMBJVWLPSR-WUJBLJFYSA-N 0.000 abstract 1
- 229940035436 maltitol Drugs 0.000 abstract 1
- 235000010449 maltitol Nutrition 0.000 abstract 1
- 229910017604 nitric acid Inorganic materials 0.000 abstract 1
- 241000209094 Oryza Species 0.000 description 8
- 230000000052 comparative effect Effects 0.000 description 8
- 239000000243 solution Substances 0.000 description 7
- 238000000465 moulding Methods 0.000 description 3
- 230000003020 moisturizing effect Effects 0.000 description 2
- 239000007921 spray Substances 0.000 description 2
- GUBGYTABKSRVRQ-QUYVBRFLSA-N beta-maltose Chemical compound OC[C@H]1O[C@H](O[C@H]2[C@H](O)[C@@H](O)[C@H](O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@@H]1O GUBGYTABKSRVRQ-QUYVBRFLSA-N 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000002347 injection Methods 0.000 description 1
- 239000007924 injection Substances 0.000 description 1
- 239000002985 plastic film Substances 0.000 description 1
- 229920006255 plastic film Polymers 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000012216 screening Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/36—Reinforced clay-wares
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
- C04B33/1305—Organic additives
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
- C04B35/63—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B using additives specially adapted for forming the products, e.g.. binder binders
- C04B35/632—Organic additives
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
- C04B35/63—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B using additives specially adapted for forming the products, e.g.. binder binders
- C04B35/632—Organic additives
- C04B35/634—Polymers
- C04B35/63404—Polymers obtained by reactions only involving carbon-to-carbon unsaturated bonds
- C04B35/63416—Polyvinylalcohols [PVA]; Polyvinylacetates
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/71—Ceramic products containing macroscopic reinforcing agents
- C04B35/78—Ceramic products containing macroscopic reinforcing agents containing non-metallic materials
- C04B35/80—Fibres, filaments, whiskers, platelets, or the like
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3418—Silicon oxide, silicic acids or oxide forming salts thereof, e.g. silica sol, fused silica, silica fume, cristobalite, quartz or flint
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/50—Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
- C04B2235/52—Constituents or additives characterised by their shapes
- C04B2235/5208—Fibers
- C04B2235/5212—Organic
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/50—Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
- C04B2235/54—Particle size related information
- C04B2235/5418—Particle size related information expressed by the size of the particles or aggregates thereof
- C04B2235/5436—Particle size related information expressed by the size of the particles or aggregates thereof micrometer sized, i.e. from 1 to 100 micron
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Dispersion Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
Abstract
The invention discloses an anti-cracking copper artware clay sculpture material and a preparation method thereof. The preparation method comprises 1, immersing vegetable sponge of luffa and cotton in a nitric acid solution, filtering the solution and carrying out cleaning to obtain filter cake, 2, mixing loess, white clay, diatomite, sweet rice flour, polyvinyl alcohol, propolis, aliphatic acid, 1-ethynyl-1-cyclohexanol and water and carrying out aging treatment to obtain an aged product, and 3, mixing the aged product, the filter cake, maltitol and borax, carrying out boiling and carrying out cooling to obtain the anti-cracking copper artware clay sculpture material. The clay sculpture material does not crack in use, greatly improves work efficiency and reduces a production cost.
Description
Technical field
The present invention relates to clay sculpture, particularly, relate to a kind of crack resistence copper skill clay sculpture material and preparation method thereof.
Background technology
Clay sculpture is a requisite process in copper artware making processes, the predecessor of every part copper artware needs a clay sculpture prototype, clay sculpture be all through sculptors repeatedly try to figure out on the basis of Original Architectural Design original text, weigh after carry out create again, the moulding quality of clay sculpture, the embodiment of romantic charm are whether, the expression of intention presents directly impact product quality from now on, and an outstanding copper is carved product and be unable to do without outstanding sculptors.Clay sculpture concrete operation step has, sculpture clay get the raw materials ready screening, water spray wake up mud, take and make skeleton, holder mud device, upper large mud, moulding.From then on the stage start clay sculpture constantly spray water keep do not ftracture, the halfway general holiday wants covered with plastic film to carry out moisturizing until sculpture mould completes.
At present, the clay sculpture material of copper artware in use often occurs situation about ftractureing so not only significantly reducing the working efficiency of sculptors, also can cause the waste of time and resource simultaneously, and then also increase production cost.
Summary of the invention
The object of this invention is to provide a kind of crack resistence copper skill clay sculpture material and preparation method thereof, obtain clay sculpture material by the method and in use do not ftracture, drastically increase working efficiency and also reduce production cost simultaneously.
To achieve these goals, the invention provides a kind of preparation method of crack resistence copper skill clay sculpture material, comprising:
1) Vegetable Sponge of Luffa and cotton are soaked in salpeter solution, then filter, clean to obtain filter cake;
2) ripening is carried out with obtained ageing product by after loess, carclazyte, diatomite, sticky rice flour, polyvinyl alcohol, propolis, lipid acid, the mixing of 1-ethynyl-1-hexamethylene alcohol and water;
3) ageing product, filter cake, maltose alcohol are mixed with borax, and carry out boiling, then cool with obtained crack resistence copper skill clay sculpture material.
Present invention also offers a kind of crack resistence copper skill clay sculpture material, this crack resistence copper skill clay sculpture material is obtained by the preparation of above-mentioned method.
Pass through technique scheme, the present invention makes the crack resistence copper skill clay sculpture material obtained in use have indehiscent characteristic by the synergy of Vegetable Sponge of Luffa, cotton, loess, carclazyte, diatomite, sticky rice flour, polyvinyl alcohol, propolis, lipid acid, 1-ethynyl-1-hexalin, maltose alcohol and borax and water, ripening and boiling, drastically increase the working efficiency of operator, also play the effect reducing production cost simultaneously.
Other features and advantages of the present invention are described in detail in embodiment part subsequently.
Embodiment
Below the specific embodiment of the present invention is described in detail.Should be understood that, embodiment described herein, only for instruction and explanation of the present invention, is not limited to the present invention.
The invention provides a kind of preparation method of crack resistence copper skill clay sculpture material, comprising:
1) Vegetable Sponge of Luffa and cotton are soaked in salpeter solution, then filter, clean to obtain filter cake;
2) ripening is carried out with obtained ageing product by after loess, carclazyte, diatomite, sticky rice flour, polyvinyl alcohol, propolis, lipid acid, the mixing of 1-ethynyl-1-hexamethylene alcohol and water;
3) ageing product, filter cake, maltose alcohol are mixed with borax, and carry out boiling, then cool with obtained crack resistence copper skill clay sculpture material.
In step 1 of the present invention) in, the consumption of each material can be selected in wide scope, but in order to improve the character that do not ftracture of obtained copper skill clay sculpture material further, preferably, in step 1) in, relative to the Vegetable Sponge of Luffa of 1 weight part, the consumption of cotton is 1.5-2 weight part, and the pH of salpeter solution is 4.5-6.Further preferably, relative to the Vegetable Sponge of Luffa of 1 weight part, the consumption of salpeter solution is 20-30 weight part.
In step 1 of the present invention) in, the condition of soaking can be selected in wide scope, but in order to improve the character that do not ftracture of obtained copper skill clay sculpture material further, preferably, soak and at least meet the following conditions: soaking temperature is 15-35 DEG C, and soak time is 10-15h.
In step 2 of the present invention) in, the consumption of each material can be selected in wide scope, but in order to improve the character that do not ftracture of obtained copper skill clay sculpture material further, preferably, in step 2) in, relative to the loess of 100 weight parts, the consumption of carclazyte is 10-17 weight part, diatomaceous consumption is 7-12 weight part, the consumption of sticky rice flour is 3-4.5 weight part, the consumption of polyvinyl alcohol is 25-36 weight part, the consumption of propolis is 1.5-2.7 weight part, the consumption of lipid acid is 1.1-1.9 weight part, the consumption of 1-ethynyl-1-hexalin is 0.5-1.1 weight part, the consumption of water is 120-150 weight part.
In step 2 of the present invention) in, the weight-average molecular weight of loess, carclazyte and diatomaceous particle diameter and polyvinyl alcohol can be selected in wide scope, but in order to improve the character that do not ftracture of obtained copper skill clay sculpture material further, preferably, in loess, carclazyte and diatomite, the particle diameter of any one or many persons is 20-30 μm; The weight-average molecular weight of polyvinyl alcohol is 3000-4500.
In step 2 of the present invention) in, the condition of ripening can be selected in wide scope, but in order to improve the character that do not ftracture of obtained copper skill clay sculpture material further, preferably, ripening at least meets the following conditions: Aging Temperature is 35-45 DEG C, and digestion time is 2-3 days.
In step 3 of the present invention) in, the consumption of each material can be selected in wide scope, but in order to improve the character that do not ftracture of obtained copper skill clay sculpture material further, preferably, in step 3) in, relative to the ageing product of 100 weight parts, the consumption of filter cake is 22-30 weight part, the consumption of maltose alcohol is 5-9 weight part, and the consumption of borax is 3-8 weight part.
In step 3 of the present invention) in, the condition of boiling can be selected in wide scope, but in order to improve the character that do not ftracture of obtained copper skill clay sculpture material further, preferably, boiling at least meets the following conditions: boiling temperature is 150-200 DEG C, and cooking time is 5-6h.
In step 3 of the present invention) in, the temperature of cooling can be selected in wide scope, but in order to improve the character that do not ftracture of obtained copper skill clay sculpture material further, preferably, the temperature of cooling is 15-35 DEG C.
Present invention also offers a kind of crack resistence copper skill clay sculpture material, this crack resistence copper skill clay sculpture material is obtained by the preparation of above-mentioned method.
Below will be described the present invention by embodiment
Embodiment 1
1) at 25 DEG C, Vegetable Sponge of Luffa, cotton and salpeter solution (pH is 5) mixed according to the weight ratio of 1:1.8:25 and soak 13h, then filtering, clean to obtain filter cake;
2) loess (particle diameter is 25 μm), carclazyte (particle diameter is 25 μm), diatomite (particle diameter is 25 μm), sticky rice flour, polyvinyl alcohol, propolis, lipid acid, 1-ethynyl-1-hexamethylene alcohol and water are mixed according to the weight ratio of 100:14:10:4:30:2:1.5:0.8:130, then at 40 DEG C ripening 2.5 days with obtained ageing product;
3) described ageing product, filter cake, maltose alcohol are mixed with the weight ratio of borax according to 100:25:7:6, and carry out boiling 5.5h in 180 DEG C, then cool at 25 DEG C with obtained crack resistence copper skill clay sculpture materials A 1.
Embodiment 2
1) at 15 DEG C, Vegetable Sponge of Luffa, cotton and salpeter solution (pH is 4.5) mixed according to the weight ratio of 1:1.5:20 and soak 10h, then filtering, clean to obtain filter cake;
2) loess (particle diameter is 20 μm), carclazyte (particle diameter is 20 μm), diatomite (particle diameter is 20 μm), sticky rice flour, polyvinyl alcohol, propolis, lipid acid, 1-ethynyl-1-hexamethylene alcohol and water are mixed according to the weight ratio of 100:10:7:3:25:1.5:1.1:0.5:120, then at 35 DEG C ripening 2 days with obtained ageing product;
3) described ageing product, filter cake, maltose alcohol are mixed with the weight ratio of borax according to 100:22:5:3, and carry out boiling 5h in 150 DEG C, then cool at 15 DEG C with obtained crack resistence copper skill clay sculpture materials A 2.
Embodiment 3
1) at 35 DEG C, Vegetable Sponge of Luffa, cotton and salpeter solution (pH is 6) mixed according to the weight ratio of 1:2:30 and soak 15h, then filtering, clean to obtain filter cake;
2) loess (particle diameter is 30 μm), carclazyte (particle diameter is 30 μm), diatomite (particle diameter is 30 μm), sticky rice flour, polyvinyl alcohol, propolis, lipid acid, 1-ethynyl-1-hexamethylene alcohol and water are mixed according to the weight ratio of 100:17:12:4.5:36:2.7:1.9:1.1:150, then at 45 DEG C ripening 2-3 days with obtained ageing product;
3) described ageing product, filter cake, maltose alcohol are mixed with the weight ratio of borax according to 100:30:9:8, and carry out boiling 6h in 200 DEG C, then cool at 35 DEG C with obtained crack resistence copper skill clay sculpture materials A 3.
Comparative example 1
Carry out obtained copper skill clay sculpture material B 1 according to the method for embodiment 1, unlike, step 1) in do not use Vegetable Sponge of Luffa.
Comparative example 2
Carry out obtained copper skill clay sculpture material B 2 according to the method for embodiment 1, unlike, step 1) in do not use cotton.
Comparative example 3
Carry out obtained copper skill clay sculpture material B 3 according to the method for embodiment 1, unlike, step 1) in do not use carclazyte.
Comparative example 4
Carry out obtained copper skill clay sculpture material B 4 according to the method for embodiment 1, unlike, step 1) in do not use diatomite.
Comparative example 5
Carry out obtained copper skill clay sculpture material B 5 according to the method for embodiment 1, unlike, step 1) in do not use sticky rice flour.
Comparative example 6
Carry out obtained copper skill clay sculpture material B 6 according to the method for embodiment 1, unlike, step 1) in do not use propolis.
Comparative example 7
Carry out obtained copper skill clay sculpture material B 7 according to the method for embodiment 1, unlike, step 1) in do not use maltose alcohol.
Application examples 1
First copper skill clay sculpture material and water to be sprayed water the mud 24h that wakes up according to the weight ratio of 100:50 by above-mentioned copper skill clay sculpture material, then carry out moulding, then surface sprinkling moisturizing (4 times/day is carried out, continue 3 days, relative to the copper skill clay sculpture material of 100g, each injection flow rate is 5-10g), dry in the shade at being finally placed in 15 DEG C 20 days, finally add up the cracking rate on the surface of clay sculpture finished product
concrete outcome is in table 1.
Table 1
Known by above-described embodiment, comparative example and application examples, copper skill clay sculpture material provided by the invention has excellent not cracking property.
More than describe the preferred embodiment of the present invention in detail; but the present invention is not limited to the detail in above-mentioned embodiment, within the scope of technical conceive of the present invention; can carry out multiple simple variant to technical scheme of the present invention, these simple variant all belong to protection scope of the present invention.
It should be noted that in addition, each concrete technical characteristic described in above-mentioned embodiment, in reconcilable situation, can be combined by any suitable mode, in order to avoid unnecessary repetition, the present invention illustrates no longer separately to various possible array mode.
In addition, also can carry out arbitrary combination between various different embodiment of the present invention, as long as it is without prejudice to thought of the present invention, it should be considered as content disclosed in this invention equally.
Claims (10)
1. a preparation method for crack resistence copper skill clay sculpture material, is characterized in that, comprising:
1) Vegetable Sponge of Luffa and cotton are soaked in salpeter solution, then filter, clean to obtain filter cake;
2) ripening is carried out with obtained ageing product by after loess, carclazyte, diatomite, sticky rice flour, polyvinyl alcohol, propolis, lipid acid, the mixing of 1-ethynyl-1-hexamethylene alcohol and water;
3) described ageing product, filter cake, maltose alcohol are mixed with borax, and carry out boiling, then cool with obtained crack resistence copper skill clay sculpture material.
2. preparation method according to claim 1, wherein, in step 1) in, relative to the described Vegetable Sponge of Luffa of 1 weight part, the consumption of described cotton is 1.5-2 weight part, and the pH of described salpeter solution is 4.5-6.
3. preparation method according to claim 2, wherein, relative to the described Vegetable Sponge of Luffa of 1 weight part, the consumption of described salpeter solution is 20-30 weight part;
Preferably, described immersion at least meets the following conditions: soaking temperature is 15-35 DEG C, and soak time is 10-15h.
4. according to the preparation method in claim 1-3 described in any one, wherein, in step 2) in, relative to the described loess of 100 weight parts, the consumption of described carclazyte is 10-17 weight part, described diatomaceous consumption is 7-12 weight part, the consumption of described sticky rice flour is 3-4.5 weight part, the consumption of described polyvinyl alcohol is 25-36 weight part, the consumption of described propolis is 1.5-2.7 weight part, the consumption of described lipid acid is 1.1-1.9 weight part, the consumption of described 1-ethynyl-1-hexalin is 0.5-1.1 weight part, the consumption of described water is 120-150 weight part.
5. preparation method according to claim 4, wherein, in described loess, carclazyte and diatomite, the particle diameter of any one or many persons is 20-30 μm; The weight-average molecular weight of described polyvinyl alcohol is 3000-4500.
6. preparation method according to claim 5, wherein, described ripening at least meets the following conditions: Aging Temperature is 35-45 DEG C, and digestion time is 2-3 days.
7. according to the preparation method in claim 1-3,5 and 6 described in any one, wherein, in step 3) in, relative to the described ageing product of 100 weight parts, the consumption of described filter cake is 22-30 weight part, the consumption of described maltose alcohol is 5-9 weight part, and the consumption of described borax is 3-8 weight part.
8. preparation method according to claim 7, wherein, described boiling at least meets the following conditions: boiling temperature is 150-200 DEG C, and cooking time is 5-6h.
9. preparation method according to claim 7, wherein, the temperature of described cooling is 15-35 DEG C.
10. a crack resistence copper skill clay sculpture material, is characterized in that, described crack resistence copper skill clay sculpture material is obtained by the method preparation in claim 1-9 described in any one.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510939777.9A CN105541283A (en) | 2015-12-15 | 2015-12-15 | Anti-cracking copper artware clay sculpture material and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510939777.9A CN105541283A (en) | 2015-12-15 | 2015-12-15 | Anti-cracking copper artware clay sculpture material and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105541283A true CN105541283A (en) | 2016-05-04 |
Family
ID=55820909
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510939777.9A Pending CN105541283A (en) | 2015-12-15 | 2015-12-15 | Anti-cracking copper artware clay sculpture material and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105541283A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108609919A (en) * | 2018-04-26 | 2018-10-02 | 河南工学院 | A kind of handicraft clay sculpture material and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101524944A (en) * | 2008-03-07 | 2009-09-09 | 曹丽丽 | Method for fabricating clay sculpture craftwork |
| CN104261777A (en) * | 2014-09-16 | 2015-01-07 | 吴持跃 | Clay sculpture Buddha repair material and preparation method thereof |
| CN104261794A (en) * | 2014-09-16 | 2015-01-07 | 吴持跃 | Handicraft clay sculpture material and preparation method thereof |
-
2015
- 2015-12-15 CN CN201510939777.9A patent/CN105541283A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101524944A (en) * | 2008-03-07 | 2009-09-09 | 曹丽丽 | Method for fabricating clay sculpture craftwork |
| CN104261777A (en) * | 2014-09-16 | 2015-01-07 | 吴持跃 | Clay sculpture Buddha repair material and preparation method thereof |
| CN104261794A (en) * | 2014-09-16 | 2015-01-07 | 吴持跃 | Handicraft clay sculpture material and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108609919A (en) * | 2018-04-26 | 2018-10-02 | 河南工学院 | A kind of handicraft clay sculpture material and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104589438B (en) | A kind of antique-imitation method of jujube wood | |
| CN104009122B (en) | The do over again processing method of silicon chip of a kind of serigraphy | |
| PH12019502732A1 (en) | Hair conditioning composition having improved rinsing properties | |
| CN103923413A (en) | PVC (Polyvinyl Chloride) film and production process thereof | |
| CN105541283A (en) | Anti-cracking copper artware clay sculpture material and preparation method thereof | |
| CN103058626A (en) | Ecological healthy functional work of art and production method of same | |
| CN105541284A (en) | Loess-white clay copper artware clay sculpture model and preparation method thereof | |
| CN101041555A (en) | Ornamental glass having etching pattern and multicolor pattern and and method for manufacturing same | |
| CN108294965A (en) | A kind of mounting flower explosion salt | |
| CN105462126A (en) | Environment-friendly copper technology clay sculpture material and preparation method thereof | |
| CN105541196A (en) | High-strength copper artware clay sculpture material and preparation method thereof | |
| CN105541195A (en) | Concussion crack-resistant copper artware clay sculpture material and preparation method thereof | |
| CN105504614A (en) | Loess-chernozem copper craft clay model and preparing method thereof | |
| CN105541285A (en) | Loess-kaolin copper artware clay sculpture model and preparation method thereof | |
| CN103668398A (en) | Magnesium-lithium alloy surface treatment method and product | |
| CN105349291A (en) | Casing cleaning solution material composition, and preparation method and application thereof | |
| CN104479930A (en) | Fruit surface cleaning agent and preparation method thereof | |
| CN105461285A (en) | Loess-dark loessial soil copper technology clay model and preparation method thereof | |
| CN105859182B (en) | A kind of multi-functional inner wall surface material of mud negative ion powder and preparation method thereof | |
| CN104312800A (en) | PS plate/CTP plate cleaning liquid and preparation method thereof | |
| CN203781905U (en) | Aeration device | |
| KR20110072640A (en) | Processing method of nano-silver with porcelain | |
| JP2010538035A5 (en) | ||
| JP2018150540A5 (en) | ||
| CN104210307A (en) | Production method of root carving |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20160504 |