CN105536678A - 一种具有柔性密封膜的反应釜 - Google Patents

一种具有柔性密封膜的反应釜 Download PDF

Info

Publication number
CN105536678A
CN105536678A CN201610087963.9A CN201610087963A CN105536678A CN 105536678 A CN105536678 A CN 105536678A CN 201610087963 A CN201610087963 A CN 201610087963A CN 105536678 A CN105536678 A CN 105536678A
Authority
CN
China
Prior art keywords
support
fixed
sealing
circular hole
spherical bearing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
CN201610087963.9A
Other languages
English (en)
Inventor
不公告发明人
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Publication of CN105536678A publication Critical patent/CN105536678A/zh
Withdrawn legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006Controlling or regulating processes
    • B01J19/0013Controlling the temperature of the process
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/21Mixers with rotary stirring devices in fixed receptacles; Kneaders characterised by their rotating shafts
    • B01F27/213Mixers with rotary stirring devices in fixed receptacles; Kneaders characterised by their rotating shafts characterised by the connection with the drive
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/90Heating or cooling systems
    • B01F35/91Heating or cooling systems using gas or liquid injected into the material, e.g. using liquefied carbon dioxide or steam
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/90Heating or cooling systems
    • B01F35/93Heating or cooling systems arranged inside the receptacle
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0066Stirrers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0073Sealings
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/26Nozzle-type reactors, i.e. the distribution of the initial reactants within the reactor is effected by their introduction or injection through nozzles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F35/00Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
    • B01F35/30Driving arrangements; Transmissions; Couplings; Brakes
    • B01F2035/35Use of other general mechanical engineering elements in mixing devices
    • B01F2035/351Sealings
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002Chemical plants
    • B01J2219/00004Scale aspects
    • B01J2219/00006Large-scale industrial plants
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00054Controlling or regulating the heat exchange system
    • B01J2219/00056Controlling or regulating the heat exchange system involving measured parameters
    • B01J2219/00058Temperature measurement
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00121Controlling the temperature by direct heating or cooling
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00121Controlling the temperature by direct heating or cooling
    • B01J2219/00123Controlling the temperature by direct heating or cooling adding a temperature modifying medium to the reactants
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00132Controlling the temperature using electric heating or cooling elements
    • B01J2219/00135Electric resistance heaters
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761Details of the reactor

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Accessories For Mixers (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Mixers Of The Rotary Stirring Type (AREA)

Abstract

本发明涉及一种具有柔性密封膜的反应釜,组成包括罐身、罐盖,罐盖中央开设圆孔,圆孔上方固定有支架,支架内设置有密封球面轴承,密封球面轴承的球体连接搅拌轴,密封球面轴承的轴承箱与支架固定,圆孔与球体之间固定有柔性密封膜,柔性密封膜与支架之间形成密封腔,该密封腔内注满纯水。本发明反应釜使用球轴承实现搅拌桨全方位的搅动,不留死角;选用柔性密封膜密封,使得内部罐内气体不泄露,有效保护操作人员且不会对环境造成污染;由于密封膜上方的密封腔内注有水,因此当罐内压力变化时,密封腔能够对密封膜起到良好的支撑作用,因此密封膜不会鼓起或塌陷,也就不会受到额外的张力,因此不易破损,使用寿命更长。

Description

一种具有柔性密封膜的反应釜
技术领域
本发明涉及一种化工反应釜。
背景技术
现在市面上大多数用于制备印染助剂的反应釜没有设置搅拌装置,使得反应的物料搅拌不充分和不均匀,这就直接导致反应速度慢,且反应不完全,浪费了资源,提高了生产成本,且反应后罐内残留下的一些反应介质容易腐蚀,影响了反应设备,不能提高经济效益。
为了解决上述问题,中国实用新型专利CN203123964U,公开了一种用于制备印染助剂的反应装置,其在罐盖上安装有伸入于罐身内的搅拌轴,搅拌轴底端安装有锚形桨叶,实现对物料的搅拌,加快反应速度。
然而某些印染助剂在制备过程中有有害物质挥发出,因此需要在密闭环境中进行搅拌。传统带搅拌反应釜大多采用填料密封或机械密封,填料密封的密封性能差且阻力大、易损耗;而机械密封则价格高,使用一段时间后密封性能下降,维护更换成本高昂。
此外,有时反应需要一定的加热环境,传统只能通过对罐体加热来实现对物料的加热,加热速度缓慢且罐内物料温度不均匀,不利于反应的顺利进行。
发明内容
本发明的目的在于:克服上述现有技术的缺陷,提出一种化工反应釜。
为了达到上述目的,本发明提出的化工反应釜,组成包括罐身、罐盖、搅拌电机、搅拌轴、搅拌桨,所述罐身上设有投料口、出料口,其特征在于:所述罐盖中央开设圆孔,圆孔上方固定有支架,所述支架内设置有密封球面轴承,所述密封球面轴承的球体连接搅拌轴,密封球面轴承的轴承箱与支架固定,所述圆孔与球体之间固定有柔性密封膜,所述柔性密封膜与支架之间形成密封腔,该密封腔内注满纯水;所述罐身底部安装有电加热管,所述电加热管上方的罐身内壁固定有朝斜下方向喷射的喷嘴,所述电加热管下方的罐身底部固定有抽水口,所述罐身外设置有将抽水口与喷嘴连接的管路,管路上安装有水泵。
本发明化工反应釜,进一步的改进在于:
1、所述罐盖上安装有观察口。
2、所述罐盖上安装有插入罐身内的温度计。
3、所述柔性密封膜呈环形,内外侧分别通过法兰与球体、罐盖圆孔密封连接。
4、所述罐盖与罐身的接口处卡装接合。
5、所述罐盖上安装有排气管,所述排气管上装有泄压阀。
6、所述喷嘴的喷射方向与搅拌轴转动方向相反。
本发明反应釜使用球轴承实现搅拌桨全方位的搅动,不留死角;选用柔性密封膜密封,使得内部罐内气体不泄露,有效保护操作人员且不会对环境造成污染;由于密封膜上方的密封腔内注有水,因此当罐内压力变化时,特别是压力大幅增加时或压力急剧降低时,密封腔能够对密封膜起到良好的支撑作用,这是因为当外界压力变化时液体的体积随几乎不发生变化,因此密封膜不会鼓起或塌陷,也就不会受到额外的张力,因此不易破损,使用寿命更长。
故,本发明所用的密封结构成本低廉,且能够承受罐内不同的压力变化,具有更强的适应性。
此外,罐身内设置有电加热管,能够对物料进行加热,并且采用水循环喷射的方式提高加热的均匀度,能够迅速将热量传递给罐身内的物料,实现对物料加热的目的,比传统不带加热或者对罐身加热的设备,本发明反应釜能够使物料更均匀的被加热,提高物料的反应速度和平稳性,进一步提高生产效率。
附图说明
下面结合附图对本发明作进一步的说明。
图1是本发明反应釜结构示意图。
图2是本发明的喷嘴喷射水流示意图。
图3是电加热管示意图。
图中标号示意如下:
1-罐身,1'-罐盖,2-电机,3-搅拌轴,4-搅拌桨,5-投料口,6-出料口,7-观察口,8-支架,9-轴承箱,10-球体,11-柔性密封膜,12-密封腔,13-喷嘴,14-电加热管,15-温度计,16-水泵,17-管路,18-排气管,19-泄压阀,20-抽水口。
具体实施方式
下面结合附图和具体实施例对本发明做进一步说明。
如图1所示,为本发明化工反应釜,组成包括罐身1和设置于罐身1上方的罐盖1',罐盖1'与罐身1的接口处卡装接合,罐盖1'上安装有排气管18,排气管18上装有泄压阀19,罐盖1'上还安装有观察口7、插入罐身1内的温度计15,罐身1上设有投料口5、出料口6,所述罐盖1'安装有伸入于罐身1内由电机2驱动的搅拌轴3,搅拌轴3底部固定有搅拌桨4,罐盖1'中央开设圆孔,圆孔上方固定有支架8,支架8内设置有密封球面轴承(由轴承箱9和球体10),密封球面轴承的球体10连接搅拌轴3,密封球面轴承的轴承箱9与支架8固定,圆孔与球体10之间固定有环形柔性密封膜11,环形柔性密封膜11内外侧分别通过法兰与球体10、罐盖圆孔密封连接;柔性密封膜11与支架8之间形成密封腔12,该密封腔12内注满纯水;罐身1底部安装有螺旋形电加热管14(见图3),电加热管14上方的罐身1内壁固定有朝斜下方向喷射的喷嘴13,电加热管13下方的罐身底部固定有抽水口20,罐身外设置有将抽水口20与喷嘴13连接的管路17,管路17上安装有水泵16。可利用水泵将物料从罐身底部抽出,并从喷嘴喷出,一方面提高搅拌效果,另一方便可提高加热均匀性。如图2所示,本例中,喷嘴13的喷射方向C与搅拌轴转动方向A相反。本例中,搅拌桨除了进行公转外,还进行自传,图中,B为搅拌桨自转转动方向。图中,1为罐身。
除上述实施例外,本发明还可以有其他实施方式。凡采用等同替换或等效变换形成的技术方案,均落在本发明要求的保护范围。

Claims (1)

1.一种化工反应釜,组成包括罐身、罐盖、搅拌电机、搅拌轴、搅拌桨,所述罐身上设有投料口、出料口,其特征在于:所述罐盖中央开设圆孔,圆孔上方固定有支架,所述支架内设置有密封球面轴承,所述密封球面轴承的球体连接搅拌轴,密封球面轴承的轴承箱与支架固定,所述圆孔与球体之间固定有柔性密封膜,所述柔性密封膜与支架之间形成密封腔,该密封腔内注满纯水;所述罐身底部安装有电加热管,所述电加热管上方的罐身内壁固定有朝斜下方向喷射的喷嘴,所述电加热管下方的罐身底部固定有抽水口,所述罐身外设置有将抽水口与喷嘴连接的管路,管路上安装有水泵;
所述罐盖上安装有插入罐身内的温度计;
所述柔性密封膜呈环形,内外侧分别通过法兰与球体、罐盖圆孔密封连接。
CN201610087963.9A 2014-03-31 2014-03-31 一种具有柔性密封膜的反应釜 Withdrawn CN105536678A (zh)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201410125574.1A CN103861547B (zh) 2014-03-31 2014-03-31 一种化工反应釜

Related Parent Applications (1)

Application Number Title Priority Date Filing Date
CN201410125574.1A Division CN103861547B (zh) 2014-03-31 2014-03-31 一种化工反应釜

Publications (1)

Publication Number Publication Date
CN105536678A true CN105536678A (zh) 2016-05-04

Family

ID=50900916

Family Applications (5)

Application Number Title Priority Date Filing Date
CN201410125574.1A Expired - Fee Related CN103861547B (zh) 2014-03-31 2014-03-31 一种化工反应釜
CN201610087963.9A Withdrawn CN105536678A (zh) 2014-03-31 2014-03-31 一种具有柔性密封膜的反应釜
CN201610087566.1A Withdrawn CN105582874A (zh) 2014-03-31 2014-03-31 具有柔性密封膜的化工反应釜
CN201610088101.8A Withdrawn CN105521755A (zh) 2014-03-31 2014-03-31 化工反应釜
CN201610086847.5A Withdrawn CN105597649A (zh) 2014-03-31 2014-03-31 具有柔性密封膜的反应釜

Family Applications Before (1)

Application Number Title Priority Date Filing Date
CN201410125574.1A Expired - Fee Related CN103861547B (zh) 2014-03-31 2014-03-31 一种化工反应釜

Family Applications After (3)

Application Number Title Priority Date Filing Date
CN201610087566.1A Withdrawn CN105582874A (zh) 2014-03-31 2014-03-31 具有柔性密封膜的化工反应釜
CN201610088101.8A Withdrawn CN105521755A (zh) 2014-03-31 2014-03-31 化工反应釜
CN201610086847.5A Withdrawn CN105597649A (zh) 2014-03-31 2014-03-31 具有柔性密封膜的反应釜

Country Status (1)

Country Link
CN (5) CN103861547B (zh)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107029617A (zh) * 2017-05-25 2017-08-11 李悦菡 一种磁力搅拌器
CN110586016A (zh) * 2019-09-29 2019-12-20 杨苗珍 一种工业化合物反应用搅拌装置
CN114524547A (zh) * 2022-03-03 2022-05-24 济南市环境研究院(济南市黄河流域生态保护促进中心) 一种高效除磷的一体化城镇生活污水处理系统及方法
CN115672230B (zh) * 2022-09-29 2023-08-18 云南云天化股份有限公司 一种烷基磷酸酯低聚物制备系统及其制备方法

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101844048B (zh) * 2010-03-08 2013-06-12 曾沂水 静密封搅拌器
CN202570171U (zh) * 2012-06-10 2012-12-05 刘方旭 一种双层加温加气搅拌反应釜

Also Published As

Publication number Publication date
CN103861547B (zh) 2016-02-10
CN105582874A (zh) 2016-05-18
CN105597649A (zh) 2016-05-25
CN105521755A (zh) 2016-04-27
CN103861547A (zh) 2014-06-18

Similar Documents

Publication Publication Date Title
CN203778069U (zh) 一种化工反应釜
CN103933918B (zh) 一种反应釜
CN103933917B (zh) 一种反应装置
CN103861547B (zh) 一种化工反应釜
CN203790941U (zh) 一种反应釜
CN203778073U (zh) 一种精炼剂反应装置
CN105688734B (zh) 一种密封搅拌装置
CN203790942U (zh) 一种反应装置
CN103846074B (zh) 一种精炼剂反应装置
CN105709677B (zh) 反应装置
CN104001466B (zh) 可温控的精练剂反应釜
CN103861543B (zh) 一种用于生产印染助剂的反应釜
CN208032570U (zh) 一种用于生产单组分环保粘合剂的反应釜
CN206229268U (zh) 一种醇基燃料的制备设备
CN105664831A (zh) 一种化工反应釜
CN205517397U (zh) 环氧树脂复合物用三轴搅拌釜
CN212215491U (zh) 一种防泄漏的高速型化工反应釜
CN105664821B (zh) 一种密封反应装置
CN205207686U (zh) 搅拌器用机械密封装置
CN209816107U (zh) 一种生物工程用发酵罐
CN201776142U (zh) 搪玻璃反应罐
CN206045861U (zh) 一种泄露密封剂制备装置
CN204503012U (zh) 一种双层搅拌反应釜

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
WW01 Invention patent application withdrawn after publication
WW01 Invention patent application withdrawn after publication

Application publication date: 20160504