CN105521189A - Pus drawing-out and tissue regeneration promoting plaster and preparation method thereof - Google Patents

Abstract

The invention provides a pus drawing-out and tissue regeneration promoting plaster and a preparation method thereof. The pus drawing-out and tissue regeneration promoting plaster is prepared from elephant leather, Flos Carthami, Radix notoginseng, Herba Speranskiae Tuberculatae, Radix Cyathulae, Rhizoma Homalomenae, Schizophragma integrifolium, Crinis carbonisatus, Radix Saposhnikoviae, Scolopendra, Ossa Draconis, Semen strychni, zaocys, cortex eucommiae, eupolyphaga seu steleophaga, Typhonium giganteum, polyporus, ootheca mantidis, Trollius chinensis bunge, Cortex Phellodendri, Radix Scutellariae, tiger bone, radix ampelopsis, radix platycodonis, Boswellia carteri, myrrh, Radix Pleomele angustifolia, rosin, minium, calomel, talcum powder, lead powder, beeswax and soybean oil. The plaster has the advantages of low cost, simple preparation and no side effect, is capable of promoting local blood circulation obviously and improving nutrition of surrounding tissue to achieve effects of detumescence, inflammation reduction, analgesia, pus drawing-out, damp clearing, tissue regeneration promoting and bone spur eliminating, and specially has good effect in treating the kidney disease.

Description

A kind of removing toxic substances and promoting tissue regeneration black powder pastes and preparation method thereof

Technical field

The present invention relates to a kind of plaster, be specifically related to a kind of removing toxic substances and promoting tissue regeneration black powder and paste and preparation method thereof.

Background technology

At present, there is the patient of a large amount of bones, joint and muscle discomfort in China, such as, the diseases such as scapulohumeral periarthritis, arthralgia, bony spur, neck shoulder vertebra disease, sebaceous cyst, lipoma, uremia and nephritis, above-mentioned disease brings long-standing problem for patient, time serious, minimal invasive treatment is even caused to process.

Plaster of the prior art, when treating rheumatalgia, arthritis, lumbago and skelalgia and osteopatia sprain, generally has the problems such as the efficacy of a drug is little, drug effect is short, curative effect is not obvious.

Therefore, need a kind of external used medicine effectively can treating above-mentioned all kinds of disease badly, thus the associated conditions for the treatment of patient.

Summary of the invention

For the defect that prior art exists, the invention provides a kind of removing toxic substances and promoting tissue regeneration black powder to paste and preparation method thereof, there is the advantages such as cost is low, preparation technology simple, have no side effect, and, significantly can promote local blood circulation, improve surrounding tissue nutrition, reach promoting blood circulation and stopping pain, detumescence, antiinflammatory and analgesic effect.

The technical solution used in the present invention is as follows:

The invention provides a kind of removing toxic substances and promoting tissue regeneration black powder paste, comprise following crude drug: Corium elephatis, Flos Carthami, Radix Notoginseng, Herba speranskiae tuberculatae, Radix Achyranthis Bidentatae, Rhizoma Homalomenae, Cortex schizophragmatis integrifolii radicis, Crinis Carbonisatus, Radix Saposhnikoviae, Scolopendra, Os Draconis, Semen Strychni, Zaocys, the Cortex Eucommiae, eupolyphage sece steleophaga, Herba Typhonii gigantei, Polyporus, Ootheca Mantidis, Flos Trollii, Cortex Phellodendri, Radix Scutellariae, Os Draconis, Os Tigris, hold back in vain, Radix Platycodonis, Olibanum, Myrrha, Sanguis Draxonis, Colophonium, Plumbum preparatium, Calomelas, Pulvis Talci, Hydrocerussitum (Ceruse), Cera Flava and Oleum Glycines.

Preferably, the weight portion of each crude drug is:

Corium elephatis 50 ~ 70 weight portion; Flos Carthami 50 ~ 70 weight portion; Radix Notoginseng 50 ~ 70 weight portion; Herba speranskiae tuberculatae 50 ~ 70 weight portion; Radix Achyranthis Bidentatae 50 ~ 70 weight portion; Rhizoma Homalomenae 50 ~ 70 weight portion; Cortex schizophragmatis integrifolii radicis 50 ~ 70 weight portion; Crinis Carbonisatus 50 ~ 70 weight portion; Radix Saposhnikoviae 50 ~ 70 weight portion; Scolopendra 50 ~ 70 weight portion; Os Draconis 50 ~ 70 weight portion; Semen Strychni 50 ~ 70 weight portion; Zaocys 50 ~ 70 weight portion; The Cortex Eucommiae 50 ~ 70 weight portion; Eupolyphage sece steleophaga 50 ~ 70 weight portion; Herba Typhonii gigantei 50 ~ 70 weight portion; Polyporus 50 ~ 70 weight portion; Ootheca Mantidis 50 ~ 70 weight portion; Flos Trollii 50 ~ 70 weight portion; Cortex Phellodendri 50 ~ 70 weight portion; Radix Scutellariae 50 ~ 70 weight portion; Os Draconis 50 ~ 70 weight portion; Os Tigris 50 ~ 70 weight portion; Hold back 50 ~ 70 weight portions in vain; Radix Platycodonis 50 ~ 70 weight portion; Olibanum 50 ~ 70 weight portion; Myrrha 50 ~ 70 weight portion; Sanguis Draxonis 50 ~ 70 weight portion; Colophonium 50 ~ 70 weight portion; Plumbum preparatium 1500 ~ 2500 weight portion; Calomelas 0.1 ~ 1.0 weight portion; Pulvis Talci 500 ~ 900 weight portion; Hydrocerussitum (Ceruse) 100 ~ 300 weight portion; Cera Flava 50 ~ 80 weight portion; Oleum Glycines 4000 ~ 6000 weight portion.

Preferably, the weight portion of each crude drug is:

Corium elephatis 60 weight portion; Flos Carthami 60 weight portion; Radix Notoginseng 60 weight portion; Herba speranskiae tuberculatae 60 weight portion; Radix Achyranthis Bidentatae 60 weight portion; Rhizoma Homalomenae 60 weight portion; Cortex schizophragmatis integrifolii radicis 60 weight portion; Crinis Carbonisatus 60 weight portion; Radix Saposhnikoviae 60 weight portion; Scolopendra 60 weight portion; Os Draconis 60 weight portion; Semen Strychni 60 weight portion; Zaocys 60 weight portion; The Cortex Eucommiae 60 weight portion; Eupolyphage sece steleophaga 60 weight portion; Herba Typhonii gigantei 60 weight portion; Polyporus 60 weight portion; Ootheca Mantidis 60 weight portion; Flos Trollii 60 weight portion; Cortex Phellodendri 60 weight portion; Radix Scutellariae 60 weight portion; Os Draconis 60 weight portion; Os Tigris 60 weight portion; Hold back 60 weight portions in vain; Radix Platycodonis 60 weight portion; Olibanum 60 weight portion; Myrrha 60 weight portion; Sanguis Draxonis 60 weight portion; Colophonium 60 weight portion; Plumbum preparatium 2000 weight portion; Calomelas 0.5 weight portion; Pulvis Talci 700 weight portion; Hydrocerussitum (Ceruse) 200 weight portion; Cera Flava 65 weight portion; Oleum Glycines 5000 weight portion.

The preparation method that the present invention second object is pasted for providing a kind of removing toxic substances and promoting tissue regeneration black powder, comprises the following steps:

S1, by the Corium elephatis of formula ratio, Flos Carthami, Radix Notoginseng, Herba speranskiae tuberculatae, Radix Achyranthis Bidentatae, Rhizoma Homalomenae, Cortex schizophragmatis integrifolii radicis, Crinis Carbonisatus, Radix Saposhnikoviae, Scolopendra, Os Draconis, Semen Strychni, Zaocys, the Cortex Eucommiae, eupolyphage sece steleophaga, Herba Typhonii gigantei, Polyporus, Ootheca Mantidis, Flos Trollii, Cortex Phellodendri, Radix Scutellariae, Os Draconis, Os Tigris, hold back in vain, Radix Platycodonis is placed in a container, concoct with the Oleum Glycines of formula ratio; Wherein, concocting temperature is 30 ~ 50 DEG C, and concocted time is 60 ~ 80 hours;

S2, intermittent-heating is above-mentioned is equipped with the container concocting medicine, forms medicinal residues medicine liquid mixture;

S3, filter described medicinal residues medicine liquid mixture, filtering medicinal residues, obtain medicinal liquid;

S4, adopt medicinal liquid to 140 ~ 160 DEG C that moderate heat heating S3 obtains, then, the crude drug of following formula ratio is added: Olibanum, Myrrha, Sanguis Draxonis and Colophonium in the medicinal liquid after heating, and continue at 140 ~ 160 DEG C and temper, temper while stir, start cooling after making the viscosity of medicinal liquid reach paste, obtain the first paste;

S5, adopts the first paste to 140 ~ 160 DEG C that moderate heat heating S4 obtains, and then, adds the crude drug of following formula ratio: Plumbum preparatium, Calomelas, Pulvis Talci and Hydrocerussitum (Ceruse), obtain the second paste in the first paste after heating;

S6, adopts the second paste to 140 ~ 160 DEG C that moderate heat heating S5 obtains, and then, adds the Cera Flava of formula ratio, constantly stir in the second paste after heating, and the circular decorating film of through formation brownish black, preparation completes.

Preferably, in S1, concocting temperature is 40 DEG C, and concocted time is 72 hours.

Preferably, in S2, the number of times of intermittent-heating is 3 times, and S2 is specially:

First time heating: process of preparing Chinese medicine medicine to 180 ~ 195 DEG C obtained with big fire heating S1; Be down to room temperature and continue immersion 22 ~ 26 hours, obtaining the first medicinal residues medicine liquid mixture;

Second time heating, with described first medicinal residues medicine liquid mixture to 140 ~ 160 DEG C of moderate heat heating; Be down to room temperature and continue immersion 10 ~ 14 hours, obtaining the second medicinal residues medicine liquid mixture;

Third time heating, with described second medicinal residues medicine liquid mixture to 80 ~ 100 DEG C of slow fire heating; Be down to room temperature and continue immersion 5 ~ 7 hours, obtaining final described medicinal residues medicine liquid mixture, for the process of S3 step.

Preferably, in S2, the number of times of intermittent-heating is 3 times, and S2 is specially:

First time heating: the process of preparing Chinese medicine medicine to 190 DEG C obtained with big fire heating S1; Be down to room temperature and continue immersion 24 hours, obtaining the first medicinal residues medicine liquid mixture;

Second time heating, with the described first medicinal residues medicine liquid mixture to 150 DEG C of moderate heat heating; Be down to room temperature and continue immersion 12 hours, obtaining the second medicinal residues medicine liquid mixture;

Third time heating, with the described second medicinal residues medicine liquid mixture to 90 DEG C of slow fire heating; Be down to room temperature and continue immersion 6 hours, obtaining final described medicinal residues medicine liquid mixture, for the process of S3 step.

Preferably, in S4, described Olibanum, Myrrha, Sanguis Draxonis and Colophonium are pretreated crude drug;

Preprocess method is:

Sieve after crude drug Olibanum is pulverized, obtain the Olibanum of powdered form;

Sieve after crude drug Myrrha is pulverized, obtain the Myrrha of powdered form;

Sieve after crude drug Sanguis Draxonis is pulverized, obtain the Sanguis Draxonis of powdered form;

Sieve after crude drug Colophonium is pulverized, obtain the Colophonium of powdered form;

The Olibanum of described powdered form, the Myrrha of powdered form, the Sanguis Draxonis of powdered form and the Colophonium of powdered form are the crude drug that S4 uses.

Preferably, describedly crude drug Olibanum is pulverized rear mistake 200 mesh sieve; Describedly crude drug Myrrha is pulverized rear mistake 200 mesh sieve; Describedly crude drug Sanguis Draxonis is pulverized rear mistake 200 mesh sieve; Describedly crude drug Colophonium is pulverized rear mistake 200 mesh sieve.

Preferably, the time of tempering described in is 90 ~ 150 minutes;

In S6, after adding Cera Flava, the heated and stirred time is 150 ~ 200 minutes;

After S6, also comprise:

S7, the circular decorating film of the brownish black obtained by S6 is coated on non-woven fibre cloth, obtains removing toxic substances and promoting tissue regeneration black powder and pastes.

The present inventor is devoted for years to the research in Related Drug note, and in single test, unexpected discovery, in S2, adopts intermittent-heating to concoct the method for medicine, can significantly improve the effect of the plaster finally obtained, especially have the function for the treatment of gastropathy.Further, when the intermittent heating adopts first big fire to heat, then moderate heat heating, during the mode that last little fire heats, the plaster effect finally obtained obviously strengthens especially.

Wherein, Corium elephatis, is the skin of Elephantidae animal elephant, has effect of hemostasis.

Flos Carthami, another name: red indigo plant flower, thorn Flos Carthami, Compositae, Flos Carthami platymiscium, dry tubular flower, orange red, floral tube is carefully narrow, and tip 5 splits, and sliver is narrow linear, and flower pesticide is yellow, and be unified into pipe, exceed outside sliver, its central authorities have stigma to expose.The special fragrance of tool, mildly bitter flavor.To spend, length of a film, color are scarlet, the soft person of matter is good.Have stimulate the menstrual flow, effect of invigorating blood circulation;

Radix Notoginseng is Umbellales Araliaceae Radix Ginseng, and belong to herbaceos perennial, root stock is short, and fleshy tap root is cylindrical, palmately compound leaf, and umbel top is raw, brightly yellowish green; Calyx cup-shaped.There is hemostasis, dissipating blood stasis, detumescence, analgesic therapy effect;

Herba speranskiae tuberculatae, has another name called distiller’s yeast grass, Staggergrass etc.Part of being used as medicine is plant herb.So that herb color is green, dry, matter is tender, free from admixture person is good.Be distributed in all parts of the country.Mostly be artificial plantation.Reddish brown with stem color, be not with leaf, drying, free from admixture person for good.Annual herb flowers, produce the nations of China and India.Property happiness sunlight, be afraid of wet, heat-resistingly do not resist cold, be suitablely born in loose fertile micro-sour soil earth, but also barren-resistant.Adaptability is comparatively strong, transplants and easily survives, and growth rapidly.Seed is name Semen Impatientis also, and stem is name Herba speranskiae tuberculatae also, all can be used as medicine, and has blood circulation promoting and blood stasis dispelling, diuresis removing toxic substances, deep effect of stimulating the menstrual flow.

Radix Achyranthis Bidentatae, knee joint nature and flavor sweetness and bitterness is sour, flat, has dissipating blood stasis blood, detumescence effect.

Rhizoma Homalomenae, perennial herb.Rhizome is crawled, and thick 1.5 centimetres, fleshy tap root is cylindrical, slightly about 3 ~ 4 millimeters, close by filbert down.There is wind-damp dispelling, strengthening bone and muscle, pain relieving, effect of detumescence.

Cortex schizophragmatis integrifolii radicis is the plant of Rosaceae rubus.Shrub, high 1-3 meters; Overgrow after upright at the beginning of branch, close raw bronzing seta, glandular hair and sparse prickle.3 pieces, lobule, rare 5 pieces, avette, width egg shape or rhombus, rare ellipse, flowering fruit bearing stage is all uprightly carried out; Petal is upright, the shape of falling ovum cochlear or subcircular, aubergine, fruit hemispherical, diameter about 1 centimetre, and red, without hair, core has obvious wrinkle and hollow cave.The florescence 5-6 month, the fruit phase-7-8 moon.Be grown on the area of height above sea level 400 meters to 3,300 meters, many raw by the road, sylvan life and gully paddy low, be distributed in Japan; Korea; Europe; North America and China.There is effect of expelling wind and removing dampness.

Crinis Carbonisatus is Crinis Carbonisatus, has effect of repercussive, hemostasis.

Radix Saposhnikoviae, another name copper rue, Hui Yun, return grass, Rhizoma Cibotii, hundred kinds; The name of a kind of medicinal herbs, herbaceos perennial, main product in Hebei, Heilungkiang, Sichuan, the ground such as Inner Mongol.Have deliver dispel the wind, effect of removing dampness to relieve pain.

Scolopendra, be Lu Sheng arthropod, health is made up of many body segments, and on each joint, all length has step, therefore is that polypody is biological.There is effect of calmness and dizziness relieving, removing obstruction in the collateral to relieve pain, detoxicating and resolving stagnation of pathogens.

Os Draconis, another name Lu Hu loses life, that gal bone, Os Draconis, Os Draconis (calcined), five OS DRACONISs, green grass or young cropsization Os Draconis, OS DRACONIS, Os Draconis.Tranquillization with heavy prescription tranquillizing the mind by relieving convulsion, arresting sweating controlling nocturnal emission with astringent drugs, hemostasis astringing intestine to stop diarrhea, promoting tissue regeneration and ulcer healing.Control infantile convulsion demented, palpitation with a distress feeling is forgetful, insomnia and dreamful sleep, spontaneous sweating, and seminal emission stranguria with turbid discharge, tell nosebleed and have blood in stool, bleeding not during menses, dysentery proctoptosis, ulcer does not close up for a long time.

Semen Strychni is Loganiaceae Strychnos.Arbor, by microtriche during branch children, old branch is come off by hair.Blade papery, subcircular, wide ellipse are to avette, and nature and flavor are bitter.There is activating collaterals and eliminating stagnation, effect of reducing swelling and alleviating pain.

Zaocys, be the nonpoisonous snake that the bodily form is larger, body total length can reach more than 2.5m, and meridian distribution of property and flavor is sweet, flat, nontoxic.Return Liver Channel.Dispel the wind, active, effect of arresting convulsion.

The Cortex Eucommiae is Chinese famous and precious tonic herb.Sweet in the mouth, warm in nature.Return liver, kidney, stomach warp.There is liver and kidney tonifying, bone and muscle strengthening, Chong and Ren Meridians regulating, consolidate through antiabortive effect.

Eupolyphage sece steleophaga, refers to Eupolyphaga Seu Steleophaga, has another name called Eupolyphaga Seu Steleophaga, comprise eupolyphoge sinensis, ground beetle, cross street, dustpan worm, Ke Bo worm, Ticks worm, DIWUGUI, Cimex bedbug mother, lid worm, eupolyphage sece steleophaga, joint joint worm, Formica fusca brave.There is effect of invigorating blood circulation.

Herba Typhonii gigantei, Araeceae Typhonium Schott herbaceos perennial, tuber diameter 2-4 centimetre differs in size, and cervical region fibrous root is many.Leaf and inflorescence are extracted out simultaneously.The close raw purple dot of petiole, middle part following tool film quality sheath; Spathe purple, pipe portion cylindrical shape or oval shape avette, spadix several without stalk, appendages purple, male flower stockless, the flowering fruit bearing stage 6-9 month.There is drying dampness to eliminate phlegm, expelling wind and relieving convulsion, effect of detoxicating and resolving stagnation of pathogens.

Polyporus, in bar shaped, similar round or flat bulk, what have has branch, long 5-25 centimetre, diameter 2-6 centimetre.Body is light, and matter is hard, slightly in graininess.Surface black, grey black or brownish black, shrinkage or have strumae, section off-white color or yellow-white.Feeble QI, lightly seasoned.Promoting diuresis to eliminate damp pathogen.For dysuria, edema, has loose bowels, stranguria with turbid discharge, leukorrhagia.

Ootheca Mantidis is the ootheca of Mantidae insecticide Chinese mantid, southern mantis, wide abdomen Mantidis.Late autumn to time spring gathers, removing impurity, steam to worm's ovum after death, dry.Ootheca Mantidis sweet in the mouth, salty, property is put down, and not only tonification but also astringent therapy are the good medicine of reinforcing the kidney and supporting YANG, controlling nocturnal emission with astringent drugs reducing urination.The solid caused emission and spermatorrhea of all kidney yang deficiencies, vital essence mistake, the enuresis, frequent micturition, sexual impotence are sterile, all can select, especially should the enuresis, frequent micturition.

Flos Trollii, another name: non-irrigated lotus, Herba Tropaeoli tremble with fear lotus, land lotus, nonirrigated farmland lotus, globe-flower, golden pimple; Formal name used at school: TrolliuschinensisBunge is the plant of Ranunculaceae Trollius.Annual or perennial herb.Plant height 30-100 centimetre.Stem softness is sought connections with.Leaf is circular like Folium Nelumbinis, and flower shape is similar to loudspeaker, and calyx tube is elongated, common Huang, orange, redness.Have the short lily feet of mutation, strain shape is closely short, the close life of branch and leaf, and plant height only reaches 30 centimetres, is extremely suitable for potted plant viewing and admiring, the florescence 2-5 month.Be good decorative flower grass, also can form window scape.Tool medicinal function, can heat-clearing and toxic substances removing, cures mainly tonsillitis, otitis media.For acute and chronic tonsillitis, acute otitis media, acute myringitis, acute conjunctivitis, acute lymphangitis.

Cortex Phellodendri is the dry bark of rutaceae wampee (PhellodendronchinenseSchneid.) or Cortex Phellodendri (PhellodendronamurenseRupr.).After stripping bark, removing rough bark, dries through concocting as medicinal.There is antibacterial, antiinflammatory and antiulcer effect.

Radix Scutellariae, (Classification system: ScutellariabaicalensisGeorgi), another name Radix Scutellariae, tsuchikane tea root are Labiatae Scutellaria herbaceos perennials; Meat rhizome is plump, the hard papery of leaf, and lanceolar is to wire lanceolar, and raceme is pushed up raw on stem and branch, and corolla is purple, purplish red to blue, and filigree is flat, and style is elongated, floral disc ring-type, ovary brown, pyrene ovoid, flowering fruit bearing stage 7 ~ JIUYUE.Bitter in the mouth, cold in nature, there are heat clearing and damp drying, eliminating fire and detoxication, hemostasis, the effect such as antiabortive.Cure mainly the diseases such as epidemic febrile disease, upper respiratory tract infection, cough due to lung-heat, damp and hot jaundice, pneumonia, dysentery, hemoptysis, conjunctival congestion, frequent fetal movement, hypertension, carbuncle furuncle.The clinical antibiotic property of Radix Scutellariae is better than Rhizoma Coptidis, and does not develop immunity to drugs.

Os Draconis, have another name called Lu Hu and lose life, that gal bone, Os Draconis, Os Draconis (calcined), five OS DRACONISs, green grass or young cropsization Os Draconis, OS DRACONIS, Os Draconis.There is effect of tranquillizing the mind by relieving convulsion, arresting sweating controlling nocturnal emission with astringent drugs.

Os Tigris, be the skeleton of felid tiger, Os Tigris is classified as one of rare medicinal herbs by Chinese medicine, thinks the effects such as Os Tigris has benefit essence of reinforcing the kidney, strengthening the tendons and bones, Fructus Alpiniae Oxyphyllae are prolonged life, relaxing muscles and tendons to promote blood circulation, promoting blood circulation, strengthening the tendons and bones.

Holding back in vain, is the dried root of vitaceae Radix Ampelopsis Ampelopsisjaponica (Thunb.) Makino.Spring, Qiu Erji excavate, and removing silt and radicula, be cut into vertical lobe or inclined tab, dry.Hardship, is slightly cold, GUIXIN, liver, spleen channel, main carbuncle cellulitis wound, eliminating stagnation gas, pain relieving heat extraction.

Radix Platycodonis, another name burden flower, Radix Platycodonis, mitral flower, Latin literary fame: Platycodongrandiflorus (Jacq.) A.DC. English: BalloonFlower, campanulaceae, Platycodon grandiflouorum plant, perennial herb, stem height 20-120 centimetre, usual without hair, even close by undercoat, not branch, few top branch.Leaf is all verticillate, and part is verticillate to whole alternate, stockless or have extremely short handle, and blade is avette, and ovum shape is oval to lanceolar, the avette or ovum shape lanceolar of leaf, and flower skipper or dark violet white, can do ornamental flower; The Koreans are used as wild herbs and eat; Its root can be used as medicine, and has the effect such as eliminating phlegm and stopping cough, lung qi dispersing, evacuation of pus.

Olibanum is the gum resin of olive subject plant Boswellia carterii Birdw.There is regulating qi and activating blood, analgesic therapy, chase after effect of poison.

Myrrha, has another name called myrrh, is olive subject plant Herba Violae tree or the dry resin of Ha Didingshu.There is the effect promoting wound healing.

Sanguis Draxonis, another name: black horse Lin exhausts, sea wax, dragon's blood, wooden Sanguis Draxonis.There is promoting blood circulation to remove blood stasis, analgesic therapy, effect of hemostasia and promoting granulation.

Colophonium, has another name called Colophonium, loose cream, is the oleoresin obtained in pinaceae plant Pinus massoniana Lamb or its congener trunk, the legacy after distillation removing volatile oil.There is dispeiling pathogenic wind and removing dampness, effect of granulation promoting pain relieving.

Plumbum preparatium, has another name called Plumbum preparatium, red powder, Zhu Fen, lead powder used in cosmetics.Acrid in the mouth, be slightly cold, poisonous.Have antipyretic, draw out pus by applying a plaster to the affected part, put on flesh, effect of blood stasis removing.

Calomelas, main chloride containing mercurous, natural product person, name hornquicksilver (Hornquic-ksilver), though usually all use artificial preparation. chemically have another name called calomel. and this product toxicity is little, but boils altogether with water, then decompose and generate mercuric chloride and mercury metal, the latter two all have severe toxicity; When exposing, calomel color deepens gradually, also plays same change and tool is hypertoxic, produces the ground such as Hubei, Hebei, Hunan, Yunnan.Pulvis Talci.Calomelas external has bactericidal action.

Pulvis Talci, English by name PULVISTALCI, for white or off-white color, fine, without the powder of grittiness, hands touches with greasy feeling.Odorless, tasteless.This product is not all dissolved in water, the acid of rare ore deposit or rare alkali hydroxide solution.Can do medicinal.Inducing diuresis for treating stranguria syndrome, clearing away summer-heat, damp eliminating sore.For pyretic stranguria, stranguria caused by urinary stone, urinates hot puckery pain, heat-damp in summer excessive thirst, damp and hot watery diarrhea; External treatment eczema, eczema, miliaria.

Hydrocerussitum (Ceruse) is the C.I. 77597 be processed into lead.There is effect of removing toxic substances, granulation promoting and dampness removing to stop itchin.

Cera Flava, has another name called Cera Flava stone, alabaster.Gain the name because stone surface and inside have wax-like texture color sensation.Belong to silicon andesite or sandstone, Main Ingredients and Appearance is quartz, and the top layer of oily waxiness is low temperature fusant, and toughness is strong, and mohs hardness is 6.5 ~ 7.5.There is effect of astringent therapy, sore, granulation promoting, pain relieving.

Oleum Glycines, takes from soybean seed, and Oleum Glycines is the oils and fats that output is maximum in the world.Bean main body of oil is the ester that higher fatty acids and glycerol generate.Warm in nature, sweet in the mouth is pungent, tonify deficiency, intestine moistening.

Beneficial effect of the present invention is as follows:

Removing toxic substances and promoting tissue regeneration black powder provided by the invention pastes and preparation method thereof, has the advantage that cost is low, preparation technology simple and have no side effect, and, significantly can promote local blood circulation, improve surrounding tissue nutrition, reach detumescence, antiinflammatory and analgesia, draw out pus by applying a plaster to the affected part, dehumidifying, granulation promoting, changes the effect of bony spur; Especially good especially for nephropathy effects such as treatment uremias.Such as, can effectively treat in Nervous toxicity, herpes zoster, anus capsule, hemorrhoid, parotitis, lymphadenitis, mastitis, cyclomastopathy, lump in breast, osteomyelitis, nephritis, traumatic injury, stretch and dampen, lumbar muscle strain, muscle bag muscle is job-hoped, muscle foreign body, rheumatic ostalgia, scapulohumeral periarthritis, arthralgia, bony spur, neck shoulder vertebra is sick, sebaceous cyst, lipoma, postoperative incision festers the diseases such as disunion open-ended for a long time, has been confirmed by test example, total effective rate is 98.44%, visible, and therapeutic effect is very good.

Detailed description of the invention

Preparation method embodiment 1:

Formula: Corium elephatis 50 weight portion; Flos Carthami 50 weight portion; Radix Notoginseng 50 weight portion; Herba speranskiae tuberculatae 50 weight portion; Radix Achyranthis Bidentatae 50 weight portion; Rhizoma Homalomenae 50 weight portion; Cortex schizophragmatis integrifolii radicis 50 weight portion; Crinis Carbonisatus 50 weight portion; Radix Saposhnikoviae 50 weight portion; Scolopendra 50 weight portion; Os Draconis 50 weight portion; Semen Strychni 50 weight portion; Zaocys 50 weight portion; The Cortex Eucommiae 50 weight portion; Eupolyphage sece steleophaga 50 weight portion; Herba Typhonii gigantei 50 weight portion; Polyporus 50 weight portion; Ootheca Mantidis 50 weight portion; Flos Trollii 50 weight portion; Cortex Phellodendri 50 weight portion; Radix Scutellariae 50 weight portion; Os Draconis 50 weight portion; Os Tigris 50 weight portion; Hold back 50 weight portions in vain; Radix Platycodonis 50 weight portion; Olibanum 50 weight portion; Myrrha 50 weight portion; Sanguis Draxonis 50 weight portion; Colophonium 50 weight portion; Plumbum preparatium 1500 weight portion; Calomelas 0.1 weight portion; Pulvis Talci 500 weight portion; Hydrocerussitum (Ceruse) 100 weight portion; Cera Flava 50 weight portion; Oleum Glycines 4000 weight portion.

Preparation technology:

S1, by the Corium elephatis of formula ratio, Flos Carthami, Radix Notoginseng, Herba speranskiae tuberculatae, Radix Achyranthis Bidentatae, Rhizoma Homalomenae, Cortex schizophragmatis integrifolii radicis, Crinis Carbonisatus, Radix Saposhnikoviae, Scolopendra, Os Draconis, Semen Strychni, Zaocys, the Cortex Eucommiae, eupolyphage sece steleophaga, Herba Typhonii gigantei, Polyporus, Ootheca Mantidis, Flos Trollii, Cortex Phellodendri, Radix Scutellariae, Os Draconis, Os Tigris, hold back in vain, Radix Platycodonis is placed in a container, concoct with the Oleum Glycines of formula ratio; Wherein, concocting temperature is 30 DEG C, and concocted time is 80 hours;

S2, intermittent-heating is above-mentioned is equipped with the container concocting medicine, forms medicinal residues medicine liquid mixture;

First time heating: the process of preparing Chinese medicine medicine to 180 DEG C obtained with big fire heating S1; Be down to room temperature and continue immersion 22 hours, obtaining the first medicinal residues medicine liquid mixture;

Second time heating, with the described first medicinal residues medicine liquid mixture to 160 DEG C of moderate heat heating; Be down to room temperature and continue immersion 10 hours, obtaining the second medicinal residues medicine liquid mixture;

Third time heating, with the described second medicinal residues medicine liquid mixture to 80 DEG C of slow fire heating; Be down to room temperature and continue immersion 5 hours, obtaining final described medicinal residues medicine liquid mixture, for the process of S3 step.

S3, filter described medicinal residues medicine liquid mixture, filtering medicinal residues, obtain medicinal liquid;

S4, adopt the medicinal liquid to 140 DEG C that moderate heat heating S3 obtains, then, the crude drug of following formula ratio is added: Olibanum, Myrrha, Sanguis Draxonis and Colophonium in the medicinal liquid after heating, and continue at 140 DEG C and temper, temper while stir, the time of tempering is 90 minutes, start cooling after making the viscosity of medicinal liquid reach paste, obtain the first paste;

Wherein, Olibanum, Myrrha, Sanguis Draxonis and Colophonium are pretreated crude drug, and preprocess method is: sieve after being pulverized by crude drug Olibanum, obtain the Olibanum of powdered form;

Crude drug Myrrha is pulverized rear mistake 200 mesh sieve, obtain the Myrrha of powdered form;

Crude drug Sanguis Draxonis is pulverized rear mistake 200 mesh sieve, obtain the Sanguis Draxonis of powdered form;

Crude drug Colophonium is pulverized rear mistake 200 mesh sieve, obtain the Colophonium of powdered form;

S5, adopts the first paste to 140 DEG C that moderate heat heating S4 obtains, and then, adds the crude drug of following formula ratio: Plumbum preparatium, Calomelas, Pulvis Talci and Hydrocerussitum (Ceruse), obtain the second paste in the first paste after heating;

S6, adopts the second paste to 140 DEG C that moderate heat heating S5 obtains, and then, in the second paste after heating, add the Cera Flava of formula ratio, constantly stir, the heated and stirred time is 150 minutes, and the circular decorating film of through formation brownish black, preparation completes.

Preparation method embodiment 2:

Formula: Corium elephatis 70 weight portion; Flos Carthami 70 weight portion; Radix Notoginseng 70 weight portion; Herba speranskiae tuberculatae 70 weight portion; Radix Achyranthis Bidentatae 70 weight portion; Rhizoma Homalomenae 70 weight portion; Cortex schizophragmatis integrifolii radicis 70 weight portion; Crinis Carbonisatus 70 weight portion; Radix Saposhnikoviae 70 weight portion; Scolopendra 70 weight portion; Os Draconis 70 weight portion; Semen Strychni 70 weight portion; Zaocys 70 weight portion; The Cortex Eucommiae 70 weight portion; Eupolyphage sece steleophaga 70 weight portion; Herba Typhonii gigantei 70 weight portion; Polyporus 70 weight portion; Ootheca Mantidis 70 weight portion; Flos Trollii 70 weight portion; Cortex Phellodendri 70 weight portion; Radix Scutellariae 70 weight portion; Os Draconis 70 weight portion; Os Tigris 70 weight portion; Hold back 70 weight portions in vain; Radix Platycodonis 70 weight portion; Olibanum 70 weight portion; Myrrha 70 weight portion; Sanguis Draxonis 70 weight portion; Colophonium 70 weight portion; Plumbum preparatium 2500 weight portion; Calomelas 0.5 weight portion; Pulvis Talci 750 weight portion; Hydrocerussitum (Ceruse) 200 weight portion; Cera Flava 75 weight portion; Oleum Glycines 4000 ~ 6000 weight portion.

Preparation technology:

S1, by the Corium elephatis of formula ratio, Flos Carthami, Radix Notoginseng, Herba speranskiae tuberculatae, Radix Achyranthis Bidentatae, Rhizoma Homalomenae, Cortex schizophragmatis integrifolii radicis, Crinis Carbonisatus, Radix Saposhnikoviae, Scolopendra, Os Draconis, Semen Strychni, Zaocys, the Cortex Eucommiae, eupolyphage sece steleophaga, Herba Typhonii gigantei, Polyporus, Ootheca Mantidis, Flos Trollii, Cortex Phellodendri, Radix Scutellariae, Os Draconis, Os Tigris, hold back in vain, Radix Platycodonis is placed in a container, concoct with the Oleum Glycines of formula ratio; Wherein, concocting temperature is 40 DEG C, and concocted time is 60 hours;

S2, intermittent-heating is above-mentioned is equipped with the container concocting medicine, forms medicinal residues medicine liquid mixture;

First time heating: the process of preparing Chinese medicine medicine to 195 DEG C obtained with big fire heating S1; Be down to room temperature and continue immersion 26 hours, obtaining the first medicinal residues medicine liquid mixture;

Second time heating, with the described first medicinal residues medicine liquid mixture to 140 DEG C of moderate heat heating; Be down to room temperature and continue immersion 14 hours, obtaining the second medicinal residues medicine liquid mixture;

Third time heating, with the described second medicinal residues medicine liquid mixture to 90 DEG C of slow fire heating; Be down to room temperature and continue immersion 7 hours, obtaining final described medicinal residues medicine liquid mixture, for the process of S3 step.

S3, filter described medicinal residues medicine liquid mixture, filtering medicinal residues, obtain medicinal liquid;

S4, adopt the medicinal liquid to 160 DEG C that moderate heat heating S3 obtains, then, the crude drug of following formula ratio is added: Olibanum, Myrrha, Sanguis Draxonis and Colophonium in the medicinal liquid after heating, and continue at 160 DEG C and temper, temper while stir, the time of tempering is 150 minutes, start cooling after making the viscosity of medicinal liquid reach paste, obtain the first paste;

Wherein, Olibanum, Myrrha, Sanguis Draxonis and Colophonium are pretreated crude drug, and preprocess method is: sieve after being pulverized by crude drug Olibanum, obtain the Olibanum of powdered form;

Crude drug Myrrha is pulverized rear mistake 200 mesh sieve, obtain the Myrrha of powdered form;

Crude drug Sanguis Draxonis is pulverized rear mistake 200 mesh sieve, obtain the Sanguis Draxonis of powdered form;

Crude drug Colophonium is pulverized rear mistake 200 mesh sieve, obtain the Colophonium of powdered form;

S5, adopts the first paste to 160 DEG C that moderate heat heating S4 obtains, and then, adds the crude drug of following formula ratio: Plumbum preparatium, Calomelas, Pulvis Talci and Hydrocerussitum (Ceruse), obtain the second paste in the first paste after heating;

S6, adopts the second paste to 160 DEG C that moderate heat heating S5 obtains, and then, in the second paste after heating, add the Cera Flava of formula ratio, constantly stir, the heated and stirred time is 200 minutes, and the circular decorating film of through formation brownish black, preparation completes.

Preparation method embodiment 3:

Formula: Corium elephatis 60 weight portion; Flos Carthami 70 weight portion; Radix Notoginseng 55 weight portion; Herba speranskiae tuberculatae 60 weight portion; Radix Achyranthis Bidentatae 70 weight portion; Rhizoma Homalomenae 55 weight portion; Cortex schizophragmatis integrifolii radicis 65 weight portion; Crinis Carbonisatus 55 weight portion; Radix Saposhnikoviae 65 weight portion; Scolopendra 55 weight portion; Os Draconis 55 weight portion; Semen Strychni 65 weight portion; Zaocys 70 weight portion; The Cortex Eucommiae 55 weight portion; Eupolyphage sece steleophaga 50 weight portion; Herba Typhonii gigantei 65 weight portion; Polyporus 55 weight portion; Ootheca Mantidis 50 weight portion; Flos Trollii 50 weight portion; Cortex Phellodendri 70 weight portion; Radix Scutellariae 65 weight portion; Os Draconis 70 weight portion; Os Tigris 55 weight portion; Hold back 70 weight portions in vain; Radix Platycodonis 55 weight portion; Olibanum 65 weight portion; Myrrha 60 weight portion; Sanguis Draxonis 65 weight portion; Colophonium 55 weight portion; Plumbum preparatium 2000 weight portion; Calomelas 0.6 weight portion; Pulvis Talci 800 weight portion; Hydrocerussitum (Ceruse) 300 weight portion; Cera Flava 60 weight portion; Oleum Glycines 5500 weight portion.

Preparation technology:

S1, by the Corium elephatis of formula ratio, Flos Carthami, Radix Notoginseng, Herba speranskiae tuberculatae, Radix Achyranthis Bidentatae, Rhizoma Homalomenae, Cortex schizophragmatis integrifolii radicis, Crinis Carbonisatus, Radix Saposhnikoviae, Scolopendra, Os Draconis, Semen Strychni, Zaocys, the Cortex Eucommiae, eupolyphage sece steleophaga, Herba Typhonii gigantei, Polyporus, Ootheca Mantidis, Flos Trollii, Cortex Phellodendri, Radix Scutellariae, Os Draconis, Os Tigris, hold back in vain, Radix Platycodonis is placed in a container, concoct with the Oleum Glycines of formula ratio; Wherein, concocting temperature is 50 DEG C, and concocted time is 65 hours;

S2, intermittent-heating is above-mentioned is equipped with the container concocting medicine, forms medicinal residues medicine liquid mixture;

First time heating: the process of preparing Chinese medicine medicine to 185 DEG C obtained with big fire heating S1; Be down to room temperature and continue immersion 22 hours, obtaining the first medicinal residues medicine liquid mixture;

Second time heating, with the described first medicinal residues medicine liquid mixture to 145 DEG C of moderate heat heating; Be down to room temperature and continue immersion 11 hours, obtaining the second medicinal residues medicine liquid mixture;

Third time heating, with the described second medicinal residues medicine liquid mixture to 100 DEG C of slow fire heating; Be down to room temperature and continue immersion 7 hours, obtaining final described medicinal residues medicine liquid mixture, for the process of S3 step.

S3, filter described medicinal residues medicine liquid mixture, filtering medicinal residues, obtain medicinal liquid;

S4, adopt the medicinal liquid to 150 DEG C that moderate heat heating S3 obtains, then, the crude drug of following formula ratio is added: Olibanum, Myrrha, Sanguis Draxonis and Colophonium in the medicinal liquid after heating, and continue at 150 DEG C and temper, temper while stir, the time of tempering is 80 minutes, start cooling after making the viscosity of medicinal liquid reach paste, obtain the first paste;

Wherein, Olibanum, Myrrha, Sanguis Draxonis and Colophonium are pretreated crude drug, and preprocess method is: sieve after being pulverized by crude drug Olibanum, obtain the Olibanum of powdered form;

Crude drug Myrrha is pulverized rear mistake 200 mesh sieve, obtain the Myrrha of powdered form;

Crude drug Sanguis Draxonis is pulverized rear mistake 200 mesh sieve, obtain the Sanguis Draxonis of powdered form;

Crude drug Colophonium is pulverized rear mistake 200 mesh sieve, obtain the Colophonium of powdered form;

S5, adopts the first paste to 150 DEG C that moderate heat heating S4 obtains, and then, adds the crude drug of following formula ratio: Plumbum preparatium, Calomelas, Pulvis Talci and Hydrocerussitum (Ceruse), obtain the second paste in the first paste after heating;

S6, adopts the second paste to 150 DEG C that moderate heat heating S5 obtains, and then, in the second paste after heating, add the Cera Flava of formula ratio, constantly stir, the heated and stirred time is 170 minutes, and the circular decorating film of through formation brownish black, preparation completes.

Preparation method embodiment 4:

Formula: Corium elephatis 70 weight portion; Flos Carthami 70 weight portion; Radix Notoginseng 60 weight portion; Herba speranskiae tuberculatae 70 weight portion; Radix Achyranthis Bidentatae 60 weight portion; Rhizoma Homalomenae 65 weight portion; Cortex schizophragmatis integrifolii radicis 55 weight portion; Crinis Carbonisatus 60 weight portion; Radix Saposhnikoviae 55 weight portion; Scolopendra 70 weight portion; Os Draconis 60 weight portion; Semen Strychni 55 weight portion; Zaocys 65 weight portion; The Cortex Eucommiae 65 weight portion; Eupolyphage sece steleophaga 55 weight portion; Herba Typhonii gigantei 50 weight portion; Polyporus 55 weight portion; Ootheca Mantidis 55 weight portion; Flos Trollii 55 weight portion; Cortex Phellodendri 55 weight portion; Radix Scutellariae 55 weight portion; Os Draconis 60 weight portion; Os Tigris 65 weight portion; Hold back 65 weight portions in vain; Radix Platycodonis 70 weight portion; Olibanum 70 weight portion; Myrrha 60 weight portion; Sanguis Draxonis 55 weight portion; Colophonium 60 weight portion; Plumbum preparatium 2500 weight portion; Calomelas 0.3 weight portion; Pulvis Talci 700 weight portion; Hydrocerussitum (Ceruse) 200 weight portion; Cera Flava 80 weight portion; Oleum Glycines 5000 weight portion.

Preparation technology:

S1, by the Corium elephatis of formula ratio, Flos Carthami, Radix Notoginseng, Herba speranskiae tuberculatae, Radix Achyranthis Bidentatae, Rhizoma Homalomenae, Cortex schizophragmatis integrifolii radicis, Crinis Carbonisatus, Radix Saposhnikoviae, Scolopendra, Os Draconis, Semen Strychni, Zaocys, the Cortex Eucommiae, eupolyphage sece steleophaga, Herba Typhonii gigantei, Polyporus, Ootheca Mantidis, Flos Trollii, Cortex Phellodendri, Radix Scutellariae, Os Draconis, Os Tigris, hold back in vain, Radix Platycodonis is placed in a container, concoct with the Oleum Glycines of formula ratio; Wherein, concocting temperature is 35 DEG C, and concocted time is 70 hours;

S2, intermittent-heating is above-mentioned is equipped with the container concocting medicine, forms medicinal residues medicine liquid mixture;

First time heating: the process of preparing Chinese medicine medicine to 190 DEG C obtained with big fire heating S1; Be down to room temperature and continue immersion 24 hours, obtaining the first medicinal residues medicine liquid mixture;

Second time heating, with the described first medicinal residues medicine liquid mixture to 155 DEG C of moderate heat heating; Be down to room temperature and continue immersion 12 hours, obtaining the second medicinal residues medicine liquid mixture;

Third time heating, with the described second medicinal residues medicine liquid mixture to 100 DEG C of slow fire heating; Be down to room temperature and continue immersion 5 hours, obtaining final described medicinal residues medicine liquid mixture, for the process of S3 step.

S3, filter described medicinal residues medicine liquid mixture, filtering medicinal residues, obtain medicinal liquid;

S4, adopt the medicinal liquid to 140 DEG C that moderate heat heating S3 obtains, then, the crude drug of following formula ratio is added: Olibanum, Myrrha, Sanguis Draxonis and Colophonium in the medicinal liquid after heating, and continue at 140 DEG C and temper, temper while stir, the time of tempering is 100 minutes, start cooling after making the viscosity of medicinal liquid reach paste, obtain the first paste;

Wherein, Olibanum, Myrrha, Sanguis Draxonis and Colophonium are pretreated crude drug, and preprocess method is: sieve after being pulverized by crude drug Olibanum, obtain the Olibanum of powdered form;

Crude drug Myrrha is pulverized rear mistake 200 mesh sieve, obtain the Myrrha of powdered form;

Crude drug Sanguis Draxonis is pulverized rear mistake 200 mesh sieve, obtain the Sanguis Draxonis of powdered form;

Crude drug Colophonium is pulverized rear mistake 200 mesh sieve, obtain the Colophonium of powdered form;

S5, adopts the first paste to 160 DEG C that moderate heat heating S4 obtains, and then, adds the crude drug of following formula ratio: Plumbum preparatium, Calomelas, Pulvis Talci and Hydrocerussitum (Ceruse), obtain the second paste in the first paste after heating;

S6, adopts the second paste to 150 DEG C that moderate heat heating S5 obtains, and then, in the second paste after heating, add the Cera Flava of formula ratio, constantly stir, the heated and stirred time is 170 minutes, and the circular decorating film of through formation brownish black, preparation completes.

Preparation method embodiment 5:

Formula: Corium elephatis 55 weight portion; Flos Carthami 65 weight portion; Radix Notoginseng 65 weight portion; Herba speranskiae tuberculatae 55 weight portion; Radix Achyranthis Bidentatae 55 weight portion; Rhizoma Homalomenae 70 weight portion; Cortex schizophragmatis integrifolii radicis 60 weight portion; Crinis Carbonisatus 65 weight portion; Radix Saposhnikoviae 60 weight portion; Scolopendra 65 weight portion; Os Draconis 60 weight portion; Semen Strychni 70 weight portion; Zaocys 60 weight portion; The Cortex Eucommiae 65 weight portion; Eupolyphage sece steleophaga 70 weight portion; Herba Typhonii gigantei 60 weight portion; Polyporus 60 weight portion; Ootheca Mantidis 60 weight portion; Flos Trollii 65 weight portion; Cortex Phellodendri 70 weight portion; Radix Scutellariae 55 weight portion; Os Draconis 55 weight portion; Os Tigris 60 weight portion; Hold back 60 weight portions in vain; Radix Platycodonis 60 weight portion; Olibanum 55 weight portion; Myrrha 60 weight portion; Sanguis Draxonis 55 weight portion; Colophonium 60 weight portion; Plumbum preparatium 1500 weight portion; Calomelas 1.0 weight portion; Pulvis Talci 600 weight portion; Hydrocerussitum (Ceruse) 150 weight portion; Cera Flava 70 weight portion; Oleum Glycines 4500 weight portion.

Preparation technology:

S1, by the Corium elephatis of formula ratio, Flos Carthami, Radix Notoginseng, Herba speranskiae tuberculatae, Radix Achyranthis Bidentatae, Rhizoma Homalomenae, Cortex schizophragmatis integrifolii radicis, Crinis Carbonisatus, Radix Saposhnikoviae, Scolopendra, Os Draconis, Semen Strychni, Zaocys, the Cortex Eucommiae, eupolyphage sece steleophaga, Herba Typhonii gigantei, Polyporus, Ootheca Mantidis, Flos Trollii, Cortex Phellodendri, Radix Scutellariae, Os Draconis, Os Tigris, hold back in vain, Radix Platycodonis is placed in a container, concoct with the Oleum Glycines of formula ratio; Wherein, concocting temperature is 45 DEG C, and concocted time is 75 hours;

S2, intermittent-heating is above-mentioned is equipped with the container concocting medicine, forms medicinal residues medicine liquid mixture;

First time heating: the process of preparing Chinese medicine medicine to 185 DEG C obtained with big fire heating S1; Be down to room temperature and continue immersion 25 hours, obtaining the first medicinal residues medicine liquid mixture;

Second time heating, with the described first medicinal residues medicine liquid mixture to 155 DEG C of moderate heat heating; Be down to room temperature and continue immersion 13 hours, obtaining the second medicinal residues medicine liquid mixture;

Third time heating, with the described second medicinal residues medicine liquid mixture to 90 DEG C of slow fire heating; Be down to room temperature and continue immersion 6 hours, obtaining final described medicinal residues medicine liquid mixture, for the process of S3 step.

S3, filter described medicinal residues medicine liquid mixture, filtering medicinal residues, obtain medicinal liquid;

S4, adopt the medicinal liquid to 150 DEG C that moderate heat heating S3 obtains, then, the crude drug of following formula ratio is added: Olibanum, Myrrha, Sanguis Draxonis and Colophonium in the medicinal liquid after heating, and continue at 150 DEG C and temper, temper while stir, the time of tempering is 120 minutes, start cooling after making the viscosity of medicinal liquid reach paste, obtain the first paste;

Wherein, Olibanum, Myrrha, Sanguis Draxonis and Colophonium are pretreated crude drug, and preprocess method is: sieve after being pulverized by crude drug Olibanum, obtain the Olibanum of powdered form;

Crude drug Myrrha is pulverized rear mistake 200 mesh sieve, obtain the Myrrha of powdered form;

Crude drug Sanguis Draxonis is pulverized rear mistake 200 mesh sieve, obtain the Sanguis Draxonis of powdered form;

Crude drug Colophonium is pulverized rear mistake 200 mesh sieve, obtain the Colophonium of powdered form;

S5, adopts the first paste to 140 DEG C that moderate heat heating S4 obtains, and then, adds the crude drug of following formula ratio: Plumbum preparatium, Calomelas, Pulvis Talci and Hydrocerussitum (Ceruse), obtain the second paste in the first paste after heating;

S6, adopts the second paste to 150 DEG C that moderate heat heating S5 obtains, and then, in the second paste after heating, add the Cera Flava of formula ratio, constantly stir, the heated and stirred time is 160 minutes, and the circular decorating film of through formation brownish black, preparation completes.

Preparation method embodiment 6:

Formula: Corium elephatis 65 weight portion; Flos Carthami 50 weight portion; Radix Notoginseng 70 weight portion; Herba speranskiae tuberculatae 65 weight portion; Radix Achyranthis Bidentatae 65 weight portion; Rhizoma Homalomenae 60 weight portion; Cortex schizophragmatis integrifolii radicis 65 weight portion; Crinis Carbonisatus 70 weight portion; Radix Saposhnikoviae 65 weight portion; Scolopendra 60 weight portion; Os Draconis 65 weight portion; Semen Strychni 65 weight portion; Zaocys 65 weight portion; The Cortex Eucommiae 50 weight portion; Eupolyphage sece steleophaga 50 weight portion; Herba Typhonii gigantei 65 weight portion; Polyporus 70 weight portion; Ootheca Mantidis 60 weight portion; Flos Trollii 70 weight portion; Cortex Phellodendri 65 weight portion; Radix Scutellariae 65 weight portion; Os Draconis 55 weight portion; Os Tigris 65 weight portion; Hold back 60 weight portions in vain; Radix Platycodonis 55 weight portion; Olibanum 55 weight portion; Myrrha 55 weight portion; Sanguis Draxonis 65 weight portion; Colophonium 70 weight portion; Plumbum preparatium 2000 weight portion; Calomelas 0.9 weight portion; Pulvis Talci 900 weight portion; Hydrocerussitum (Ceruse) 250 weight portion; Cera Flava 65 weight portion; Oleum Glycines 4500 weight portion.

Preparation technology:

S1, by the Corium elephatis of formula ratio, Flos Carthami, Radix Notoginseng, Herba speranskiae tuberculatae, Radix Achyranthis Bidentatae, Rhizoma Homalomenae, Cortex schizophragmatis integrifolii radicis, Crinis Carbonisatus, Radix Saposhnikoviae, Scolopendra, Os Draconis, Semen Strychni, Zaocys, the Cortex Eucommiae, eupolyphage sece steleophaga, Herba Typhonii gigantei, Polyporus, Ootheca Mantidis, Flos Trollii, Cortex Phellodendri, Radix Scutellariae, Os Draconis, Os Tigris, hold back in vain, Radix Platycodonis is placed in a container, concoct with the Oleum Glycines of formula ratio; Wherein, concocting temperature is 50 DEG C, and concocted time is 65 hours;

S2, intermittent-heating is above-mentioned is equipped with the container concocting medicine, forms medicinal residues medicine liquid mixture;

First time heating: the process of preparing Chinese medicine medicine to 195 DEG C obtained with big fire heating S1; Be down to room temperature and continue immersion 23 hours, obtaining the first medicinal residues medicine liquid mixture;

Second time heating, with the described first medicinal residues medicine liquid mixture to 150 DEG C of moderate heat heating; Be down to room temperature and continue immersion 14 hours, obtaining the second medicinal residues medicine liquid mixture;

Third time heating, with the described second medicinal residues medicine liquid mixture to 80 DEG C of slow fire heating; Be down to room temperature and continue immersion 5 hours, obtaining final described medicinal residues medicine liquid mixture, for the process of S3 step.

S3, filter described medicinal residues medicine liquid mixture, filtering medicinal residues, obtain medicinal liquid;

S4, adopt the medicinal liquid to 160 DEG C that moderate heat heating S3 obtains, then, the crude drug of following formula ratio is added: Olibanum, Myrrha, Sanguis Draxonis and Colophonium in the medicinal liquid after heating, and continue at 160 DEG C and temper, temper while stir, the time of tempering is 130 minutes, start cooling after making the viscosity of medicinal liquid reach paste, obtain the first paste;

Wherein, Olibanum, Myrrha, Sanguis Draxonis and Colophonium are pretreated crude drug, and preprocess method is: sieve after being pulverized by crude drug Olibanum, obtain the Olibanum of powdered form;

Crude drug Myrrha is pulverized rear mistake 200 mesh sieve, obtain the Myrrha of powdered form;

Crude drug Sanguis Draxonis is pulverized rear mistake 200 mesh sieve, obtain the Sanguis Draxonis of powdered form;

Crude drug Colophonium is pulverized rear mistake 200 mesh sieve, obtain the Colophonium of powdered form;

S5, adopts the first paste to 150 DEG C that moderate heat heating S4 obtains, and then, adds the crude drug of following formula ratio: Plumbum preparatium, Calomelas, Pulvis Talci and Hydrocerussitum (Ceruse), obtain the second paste in the first paste after heating;

S6, adopts the second paste to 160 DEG C that moderate heat heating S5 obtains, and then, in the second paste after heating, add the Cera Flava of formula ratio, constantly stir, the heated and stirred time is 180 minutes, and the circular decorating film of through formation brownish black, preparation completes.

Test example 1

This test example is for investigating the remarkable result of step S2 technique of the present invention:

It is sample 1 that the removing toxic substances and promoting tissue regeneration black powder prepared with preparation method embodiment 2 of the present invention pastes;

Formula and other technological parameters are all identical with preparation method embodiment 2 technological parameter, and the mode of heating only changing step S2 carries out the preparation of plaster, is specially:

Adopt the process of preparing Chinese medicine medicine to 195 DEG C that big fire heating S1 obtains; Be down to room temperature and continue immersion 50 hours, obtaining the medicinal residues medicine liquid mixture described in S2, the plaster prepared thus is sample 2;

Adopt the process of preparing Chinese medicine medicine to 90 DEG C that little fire heating S1 obtains; Be down to room temperature and continue immersion 50 hours, obtaining the medicinal residues medicine liquid mixture described in S2, the plaster prepared thus is sample 3;

Adopt the process of preparing Chinese medicine medicine to 140 DEG C that moderate heat heating S1 obtains; Be down to room temperature and continue immersion 50 hours, obtaining the medicinal residues medicine liquid mixture described in S2, the plaster prepared thus is sample 4.

Choose 100 routine patients, wherein, male patient 50 example, female patient 50 example, age distribution interval is 25 years old-75 years old; Treatment time is as shown in table 1 with treatment situation:

Table 1

Wherein, healing refers to: after treatment, symptom and objective determination display, and conditions disappears, and recovers work capacity completely, and Continuous Observation more than 3 years, no longer recur.

Effectively to refer to: after treatment, cardinal symptom is clearly better, and disease phenomenon obviously reduces, and Continuous Observation 26 months not developing deeply.

Except to cure and effective, it is invalid to be, and invalidly refers to: after treatment, and after cardinal symptom and objective determination, disease phenomenon is without improving and deterioration person rapidly.

As can be seen from Table 1, the removing toxic substances and promoting tissue regeneration black powder that the present invention adopts intermittent-heating method to prepare pastes, and is obviously greater than the preparation-obtained plaster of other non-batch heating means to the effective percentage (namely cure rate adds obvious effective rate) of above-mentioned all kinds of symptom.

Test example 2

The removing toxic substances and promoting tissue regeneration black powder prepared with preparation method embodiment 1 of the present invention pastes as subjects, and using method is: be attached to patient's afflicted area; Within every 2 days, change once new removing toxic substances and promoting tissue regeneration black powder to paste.

For each case shown in table 1, all choose 100 routine patients, wherein, male patient 50 example, female patient 50 example, age distribution interval is 25 years old-75 years old; Treatment time is as shown in table 2 with treatment situation:

Table 2: test example

Wherein, healing refers to: after treatment, symptom and objective determination display, and conditions disappears, and recovers work capacity completely, and Continuous Observation more than 3 years, no longer recur.

Effectively to refer to: after treatment, cardinal symptom is clearly better, and disease phenomenon obviously reduces, and Continuous Observation 26 months not developing deeply.

Invalidly to refer to: after treatment, after cardinal symptom and objective determination, disease phenomenon is without improvement and deterioration person rapidly.

Such as:

Zhao so-and-so, man, 55 years old, left arm is injured festered, in the past few years through hospitalize diagnosis there is no effect, need to do amputation.Through curing completely with after two courses for the treatment of of this plaster, do not need amputation.

Jiang, female, 38 years old, lump in breast hypertrophy, fully recovered with after two courses for the treatment of of this plaster.

Grandson so-and-so, female, 58 years old, suffers from uremia three plus siges, fully recovers with after this plaster three course for the treatment of.

By analytical table 2, average total effective rate is: 98.44%.

Same test that the removing toxic substances and promoting tissue regeneration black powder exchange premium prepared preparation method embodiment 2-6 of the present invention is capable, result of the test is similar.

The above is only the preferred embodiment of the present invention; it should be pointed out that for those skilled in the art, under the premise without departing from the principles of the invention; can also make some improvements and modifications, these improvements and modifications also should look protection scope of the present invention.

Claims (10)

1. a removing toxic substances and promoting tissue regeneration black powder pastes, it is characterized in that, comprise following crude drug: Corium elephatis, Flos Carthami, Radix Notoginseng, Herba speranskiae tuberculatae, Radix Achyranthis Bidentatae, Rhizoma Homalomenae, Cortex schizophragmatis integrifolii radicis, Crinis Carbonisatus, Radix Saposhnikoviae, Scolopendra, Os Draconis, Semen Strychni, Zaocys, the Cortex Eucommiae, eupolyphage sece steleophaga, Herba Typhonii gigantei, Polyporus, Ootheca Mantidis, Flos Trollii, Cortex Phellodendri, Radix Scutellariae, Os Draconis, Os Tigris, hold back in vain, Radix Platycodonis, Olibanum, Myrrha, Sanguis Draxonis, Colophonium, Plumbum preparatium, Calomelas, Pulvis Talci, Hydrocerussitum (Ceruse), Cera Flava and Oleum Glycines.

2. removing toxic substances and promoting tissue regeneration black powder according to claim 1 pastes, and it is characterized in that, the weight portion of each crude drug is:

Corium elephatis 50 ~ 70 weight portion; Flos Carthami 50 ~ 70 weight portion; Radix Notoginseng 50 ~ 70 weight portion; Herba speranskiae tuberculatae 50 ~ 70 weight portion; Radix Achyranthis Bidentatae 50 ~ 70 weight portion; Rhizoma Homalomenae 50 ~ 70 weight portion; Cortex schizophragmatis integrifolii radicis 50 ~ 70 weight portion; Crinis Carbonisatus 50 ~ 70 weight portion; Radix Saposhnikoviae 50 ~ 70 weight portion; Scolopendra 50 ~ 70 weight portion; Os Draconis 50 ~ 70 weight portion; Semen Strychni 50 ~ 70 weight portion; Zaocys 50 ~ 70 weight portion; The Cortex Eucommiae 50 ~ 70 weight portion; Eupolyphage sece steleophaga 50 ~ 70 weight portion; Herba Typhonii gigantei 50 ~ 70 weight portion; Polyporus 50 ~ 70 weight portion; Ootheca Mantidis 50 ~ 70 weight portion; Flos Trollii 50 ~ 70 weight portion; Cortex Phellodendri 50 ~ 70 weight portion; Radix Scutellariae 50 ~ 70 weight portion; Os Draconis 50 ~ 70 weight portion; Os Tigris 50 ~ 70 weight portion; Hold back 50 ~ 70 weight portions in vain; Radix Platycodonis 50 ~ 70 weight portion; Olibanum 50 ~ 70 weight portion; Myrrha 50 ~ 70 weight portion; Sanguis Draxonis 50 ~ 70 weight portion; Colophonium 50 ~ 70 weight portion; Plumbum preparatium 1500 ~ 2500 weight portion; Calomelas 0.1 ~ 1.0 weight portion; Pulvis Talci 500 ~ 900 weight portion; Hydrocerussitum (Ceruse) 100 ~ 300 weight portion; Cera Flava 50 ~ 80 weight portion; Oleum Glycines 4000 ~ 6000 weight portion.

3. removing toxic substances and promoting tissue regeneration black powder according to claim 2 pastes, and it is characterized in that, the weight portion of each crude drug is:

Corium elephatis 60 weight portion; Flos Carthami 60 weight portion; Radix Notoginseng 60 weight portion; Herba speranskiae tuberculatae 60 weight portion; Radix Achyranthis Bidentatae 60 weight portion; Rhizoma Homalomenae 60 weight portion; Cortex schizophragmatis integrifolii radicis 60 weight portion; Crinis Carbonisatus 60 weight portion; Radix Saposhnikoviae 60 weight portion; Scolopendra 60 weight portion; Os Draconis 60 weight portion; Semen Strychni 60 weight portion; Zaocys 60 weight portion; The Cortex Eucommiae 60 weight portion; Eupolyphage sece steleophaga 60 weight portion; Herba Typhonii gigantei 60 weight portion; Polyporus 60 weight portion; Ootheca Mantidis 60 weight portion; Flos Trollii 60 weight portion; Cortex Phellodendri 60 weight portion; Radix Scutellariae 60 weight portion; Os Draconis 60 weight portion; Os Tigris 60 weight portion; Hold back 60 weight portions in vain; Radix Platycodonis 60 weight portion; Olibanum 60 weight portion; Myrrha 60 weight portion; Sanguis Draxonis 60 weight portion; Colophonium 60 weight portion; Plumbum preparatium 2000 weight portion; Calomelas 0.5 weight portion; Pulvis Talci 700 weight portion; Hydrocerussitum (Ceruse) 200 weight portion; Cera Flava 65 weight portion; Oleum Glycines 5000 weight portion.

4. a preparation method for removing toxic substances and promoting tissue regeneration black powder subsides, is characterized in that, comprise the following steps:

S1, by the Corium elephatis of formula ratio, Flos Carthami, Radix Notoginseng, Herba speranskiae tuberculatae, Radix Achyranthis Bidentatae, Rhizoma Homalomenae, Cortex schizophragmatis integrifolii radicis, Crinis Carbonisatus, Radix Saposhnikoviae, Scolopendra, Os Draconis, Semen Strychni, Zaocys, the Cortex Eucommiae, eupolyphage sece steleophaga, Herba Typhonii gigantei, Polyporus, Ootheca Mantidis, Flos Trollii, Cortex Phellodendri, Radix Scutellariae, Os Draconis, Os Tigris, hold back in vain, Radix Platycodonis is placed in a container, concoct with the Oleum Glycines of formula ratio; Wherein, concocting temperature is 30 ~ 50 DEG C, and concocted time is 60 ~ 80 hours;

S2, intermittent-heating is above-mentioned is equipped with the container concocting medicine, forms medicinal residues medicine liquid mixture;

S3, filter described medicinal residues medicine liquid mixture, filtering medicinal residues, obtain medicinal liquid;

S4, adopt medicinal liquid to 140 ~ 160 DEG C that moderate heat heating S3 obtains, then, the crude drug of following formula ratio is added: Olibanum, Myrrha, Sanguis Draxonis and Colophonium in the medicinal liquid after heating, and continue at 140 ~ 160 DEG C and temper, temper while stir, start cooling after making the viscosity of medicinal liquid reach paste, obtain the first paste;

S5, adopts the first paste to 140 ~ 160 DEG C that moderate heat heating S4 obtains, and then, adds the crude drug of following formula ratio: Plumbum preparatium, Calomelas, Pulvis Talci and Hydrocerussitum (Ceruse), obtain the second paste in the first paste after heating;

S6, adopts the second paste to 140 ~ 160 DEG C that moderate heat heating S5 obtains, and then, adds the Cera Flava of formula ratio, constantly stir in the second paste after heating, and the circular decorating film of through formation brownish black, preparation completes.

5. the preparation method of removing toxic substances and promoting tissue regeneration black powder subsides according to claim 4, is characterized in that, in S1, concocting temperature is 40 DEG C, and concocted time is 72 hours.

6. the preparation method of removing toxic substances and promoting tissue regeneration black powder subsides according to claim 4, it is characterized in that, in S2, the number of times of intermittent-heating is 3 times, and S2 is specially:

First time heating: process of preparing Chinese medicine medicine to 180 ~ 195 DEG C obtained with big fire heating S1; Be down to room temperature and continue immersion 22 ~ 26 hours, obtaining the first medicinal residues medicine liquid mixture;

Second time heating, with described first medicinal residues medicine liquid mixture to 140 ~ 160 DEG C of moderate heat heating; Be down to room temperature and continue immersion 10 ~ 14 hours, obtaining the second medicinal residues medicine liquid mixture;

Third time heating, with described second medicinal residues medicine liquid mixture to 80 ~ 100 DEG C of slow fire heating; Be down to room temperature and continue immersion 5 ~ 7 hours, obtaining final described medicinal residues medicine liquid mixture, for the process of S3 step.

7. the preparation method of removing toxic substances and promoting tissue regeneration black powder subsides according to claim 6, it is characterized in that, in S2, the number of times of intermittent-heating is 3 times, and S2 is specially:

First time heating: the process of preparing Chinese medicine medicine to 190 DEG C obtained with big fire heating S1; Be down to room temperature and continue immersion 24 hours, obtaining the first medicinal residues medicine liquid mixture;

Second time heating, with the described first medicinal residues medicine liquid mixture to 150 DEG C of moderate heat heating; Be down to room temperature and continue immersion 12 hours, obtaining the second medicinal residues medicine liquid mixture;

Third time heating, with the described second medicinal residues medicine liquid mixture to 90 DEG C of slow fire heating; Be down to room temperature and continue immersion 6 hours, obtaining final described medicinal residues medicine liquid mixture, for the process of S3 step.

8. the preparation method of removing toxic substances and promoting tissue regeneration black powder subsides according to claim 4, it is characterized in that, in S4, described Olibanum, Myrrha, Sanguis Draxonis and Colophonium are pretreated crude drug;

Preprocess method is:

Sieve after crude drug Olibanum is pulverized, obtain the Olibanum of powdered form;

Sieve after crude drug Myrrha is pulverized, obtain the Myrrha of powdered form;

Sieve after crude drug Sanguis Draxonis is pulverized, obtain the Sanguis Draxonis of powdered form;

Sieve after crude drug Colophonium is pulverized, obtain the Colophonium of powdered form;

The Olibanum of described powdered form, the Myrrha of powdered form, the Sanguis Draxonis of powdered form and the Colophonium of powdered form are the crude drug that S4 uses.

9. the removing toxic substances and promoting tissue regeneration black powder according to claim 8 preparation method of pasting, is characterized in that, describedly crude drug Olibanum is pulverized rear mistake 200 mesh sieve; Describedly crude drug Myrrha is pulverized rear mistake 200 mesh sieve; Describedly crude drug Sanguis Draxonis is pulverized rear mistake 200 mesh sieve; Describedly crude drug Colophonium is pulverized rear mistake 200 mesh sieve.

10. the removing toxic substances and promoting tissue regeneration black powder according to claim 4 preparation method of pasting, is characterized in that, in S4, described in time of tempering be 90 ~ 150 minutes;

In S6, after adding Cera Flava, the heated and stirred time is 150 ~ 200 minutes;

After S6, also comprise:

S7, the circular decorating film of the brownish black obtained by S6 is coated on non-woven fibre cloth, obtains removing toxic substances and promoting tissue regeneration black powder and pastes.