CN105520192B - A kind of preparation method and application of cigarette filter-tip additive agent - Google Patents
A kind of preparation method and application of cigarette filter-tip additive agent Download PDFInfo
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- CN105520192B CN105520192B CN201610075660.5A CN201610075660A CN105520192B CN 105520192 B CN105520192 B CN 105520192B CN 201610075660 A CN201610075660 A CN 201610075660A CN 105520192 B CN105520192 B CN 105520192B
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/067—Use of materials for tobacco smoke filters characterised by functional properties
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- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Fats And Perfumes (AREA)
Abstract
The present invention is a kind of preparation method and device of cigarette filter-tip additive agent.Method is that the spice material cracked will be needed to bring fragrance component into cracking reaction stove by carrier gas stream and material storage container, and required volatile fragrance component is held in liquid storage tank；Carry out while cooperateing with cracking reaction, the fragrant ingredient of cracking of generation to be deposited the granular materials absorption in bed, form additives of filter tip granular materials in same pyrolysis furnace.The granular materials that equipment used by this method can be needed for one-step shaping filter tip simultaneously, it is easy to operation, and raw material dosage is saved very much, it can strictly control production cost.
Description
Technical field
The present invention relates to technical field of cigarettes, specifically a kind of preparation method and application of cigarette filter-tip additive agent.
Background technology
In recent years, there is deeper change in cigarette filter, from common single cellulose acetate filter, to
Filter tip and Flavoring filter direction develop made of polynary filter tip, multiple material.These novel filter tips are just gradually rolled up
The favor of cigarette manufacturer and consumer.Flavoring processing is carried out in filter tip is commonly known as non-burning flavoring, that is, the fragrance being added
Without burning, the oral cavity of consumer is directly eluted by flue gas.This method has that materials'use amount is few, and method is directly etc. excellent
Gesture.But cigarette smoke is a kind of product of burning, therefore directly cigarette smoke can be caused one by the way of non-burning flavoring
Determine uncoordinated in degree, especially tobacco this perfume is influenced more prominent.Therefore, it is necessary to consider to the fragrance component in filter tip
Certain class burning processing is carried out, to increase flue gas harmony, this perfume of prominent tobacco.
Invention content
The object of the present invention is to provide a kind of preparation method and application of cigarette filter-tip additive agent, by tobacco aromaticss and/or
The method that tobacco leaf uses thermal cracking carries out the fragrant extraction of cracking by mixing synergistic effect, and the cracking perfume (or spice) ingredient of generation is deposited
Granular materials absorption in bed, forms additives of filter tip granular materials.This method can be needed for one-step shaping filter tip granular material
Material, it is easy to operation, and raw material dosage is saved very much, it can strictly control production cost.
The present invention is realized by following technical proposal：A kind of preparation method of cigarette filter-tip additive agent, by following each step
Suddenly：
（1）The reaction bed that the spice material cracked will be needed to be put into pyrolysis furnace, will be placed on as the granular materials of adsorbent
In the deposition bed of pyrolysis furnace；
（2）Carrier gas stream needed for opening, and by material storage container, required volatile fragrance component is held in liquid storage tank,
Carrier gas stream brings fragrance component into cracking reaction stove；
（3）It opens cracking reaction stove and collaboration cracking reaction is carried out to the various substances in stove；
（4）Wait for that cracking reaction takes out the granular materials in deposition bed up to cigarette filter-tip additive agent after the completion.
Step（2）Carrier gas in described is one kind in nitrogen, nitrogen oxygen atmosphere, helium.
The spice material is one or more of tobacco leaf, agalloch eaglewood, peppermint grass.
The granular materials of the adsorbent is one or more in activated carbon, diatomite, porous paper material.
The volatile fragrance component held in liquid storage tank is one or more of Rosa Damascana, geranium oil.
Preferred 600-1000 DEG C of pyrolysis furnace reaction temperature, to approach the actual temperature of cigarette burning, heating rate 200-
400 DEG C/min, reaction time 5-10min.
Carrier gas speed, liquid storage tank temperature and cracking furnace temperature and heating rate are unlimited, are subject to needs of production.
The step（2）In material storage container required fragrance can be housed, fragrance can not also be filled according to required.
Preparing device used in above-mentioned cigarette filter-tip additive agent is：Including three liquid storage tank, pyrolysis furnace and deposition bed masters
Want component；
It is equipped with liquid entrance above the liquid storage tank, can be used for being packed into or pouring out liquid, lower section is filled equipped with temperature control
It sets, for the liquid in liquid storage tank is heated or freezed, there is admission line and outlet pipe in liquid storage tank；Crack furnace middle end
Equipped with one layer with porous reaction bed, upper and lower side has pipeline to be connected；Being connected with the pipeline of pyrolysis furnace lower end above deposition bed,
The position of deposition bed side on the lower is connected with the pipeline above pyrolysis furnace by bend pipe；The liquid storage tank and between pyrolysis furnace
Also it is connected using pipeline.
The pyrolysis furnace sheet is heated as controllable temperature, is had opening in the position of reaction bed, can be opened cleaning or replacement
Reaction bed.It can change gas phase and liquid phase ingredient by adjusting two methods of flow rate of carrier gas and liquid storage tank temperature control in preparation process
Conveying capacity.
The reaction bed be porous flat plate, to make liquid pyrolysis product flow downward out, aperture it can be selected that so that
Cracked residue without falling into the deposition bed of lower section subject to.
Reaction bed upper and lower has tubular opening, the liquid product that cracking reaction generates that can be oozed from the hole of reaction bed
Go out, and deposition bed is flowed into along lower end nozzle；The gaseous products of generation are passed through deposition after upper end tube nozzle is flowed out with carrier gas, along pipeline
The other end of bed, the same granular materials absorption being deposited on bed.
The outlet port of the liquid storage tank admission line will be less than the height of outlet pipe, to ensure that gas can pass through
Liquid internal in liquid storage tank.
The deposition bed also is provided with raw material inlet and outlet, to facilitate the placement and taking-up of raw material in deposition bed, and can
For exhaust gas to be discharged.
Gained cigarette filter-tip additive agent is added with the feed postition of convention filter sorbing material into filter stick, and addition is to roll up
Subject to cigarette sensory evaluation is optimal, the addition of general every cigarette is 5~30mg
The present invention has the advantage that and good effect is：
The present invention makes a variety of fragrance components mix and cooperate in pyrolysis furnace to split by the way of carrier gas conveying
Solution reaction, the fragrant product of two kinds of cracking of liquid and gas of generation.The fragrant ingredient of cracking can be deposited the suction of the granular materials on bed
It is attached.Entire production process one-pass molding, it is simple and practicable, production of cigarettes cost can be greatly reduced.Prepared granular material
Material can solve the flue gas coordination sex chromosome mosaicism that common non-burning flavoring is brought after cigarette filter is added, this perfume of tobacco is prominent.
Description of the drawings
Fig. 1 preparation facilities structural schematic diagrams of the present invention.
In figure, 1 is pyrolysis furnace, and 2 be reaction bed, 3 deposition beds, 4 liquid storage tanks, the 5 liquid perfume original to be stored in liquid storage tank
Material, 6 and 14 be the conduit that the fragrant ingredient of cracking is transferred to deposition bed from pyrolysis furnace, and 7 and 13 be carrier gas conduit, and 8 are open for deposition bed,
9 are open for pyrolysis furnace, and 10 are open for liquid storage tank, and 11 be temperature regulating device, 12 solid or liquid to be loaded in deposition bed.
Specific implementation mode
With reference to embodiment, the present invention will be further described.
Embodiment 1
（1）20g Zimbabwe tobacco leaf is put into cracking reaction stove, and places 40 mesh of 500g in the deposition bed of lower section
The active carbon particle of size；
（2）Select nitrogen as carrier gas stream, control carries air-flow velocity as 120ml/min, and the storage by filling geraniol
Liquid pool, wherein liquid storage tank temperature are controlled at 50 DEG C, and geraniol is brought into cracking reaction stove using nitrogen carrier gas stream；
（3）It opens cracking reaction stove and collaboration cracking reaction is carried out to the various substances in stove, control cracking temperature is 800
DEG C, heating rate is 300 DEG C/min, and the cracking reaction time is 5min；
（4）After the completion of waiting for cracking reaction, the active carbon particle material in deposition bed is taken out, cigarette filter is added after cooling,
Addition is 10mg/ branch.
Final cigarette product obtained, this perfume of flue gas tobacco is prominent, and flue gas harmony enhancing, organoleptic quality obtains obviously
It is promoted.
Embodiment 2
（1）10g agalloch eaglewood clasts are put into cracking reaction stove, and placement 50 mesh of 700g is big in the deposition bed of lower section
Small active carbon particle；
（2）Select nitrogen as carrier gas stream, it is 60ml/min that control, which carries air-flow velocity, and by filling Rosa Damascana
Liquid storage tank, wherein liquid storage tank temperature are controlled at 60 DEG C.Rosa Damascana is brought into cracking reaction stove using nitrogen carrier gas stream；
（3）It opens cracking reaction stove and collaboration cracking reaction is carried out to the various substances in stove, control cracking temperature is 700
DEG C, heating rate is 200 DEG C/min, and the cracking reaction time is 10min；
（4）After the completion of waiting for cracking reaction, the active carbon particle material in deposition bed is taken out, cigarette filter is added after cooling,
Addition is 10mg/ branch.
Final cigarette product obtained, flue gas agalloch eaglewood taste and rose scent are apparent, the enhancing of flue gas harmony, organoleptic quality
It is obviously improved.
Embodiment 3
（1）By 30g fannings leaf slag and Zimbabwe's tobacco leaf（Respectively account for 50%）It is put into cracking reaction stove, and in the heavy of lower section
The active carbon particle of 40 mesh sizes of 1000g is placed on product bed；
（2）It is 10% to select containing nitrogen（Volume fraction）Nitrogen oxygen atmosphere as carrier gas stream, control carries air-flow velocity and is
300ml/min is directly entered pyrolysis furnace after empty liquid storage tank；
（3）It opens cracking reaction stove and collaboration cracking reaction is carried out to the various substances in stove, control cracking temperature is 600
DEG C, heating rate is 400 DEG C/min, and the cracking reaction time is 10min；
（4）After the completion of waiting for cracking reaction, the active carbon particle material in deposition bed is taken out, cigarette filter is added after cooling,
Addition is 5mg/ branch.
Final cigarette product obtained, this perfume of flue gas tobacco is prominent, and tea smell is apparent, the enhancing of flue gas harmony, sense organ
Quality is obviously improved.
Embodiment 4
（1）The Yuxi 10g cigarette pipe tobacco is put into cracking reaction stove, and placement 35 mesh of 600g is big in the deposition bed of lower section
Small activated carbon and montmorillonite hybrid particles；
（2）It is 20% to select containing nitrogen（Volume fraction）Nitrogen oxygen atmosphere as carrier gas stream, control carries air-flow velocity and is
100ml/min, and by filling the liquid storage tank for having dissolved Yuxi cigarette and being formulated required flavor sugar materials aqueous solution, the control of liquid storage tank temperature
At 80 DEG C, Rosa Damascana is brought into cracking reaction stove using carrier gas stream；
（3）It opens cracking reaction stove and collaboration cracking reaction is carried out to the various substances in stove, control cracking temperature is 900
DEG C, heating rate is 300 DEG C/min, and the cracking reaction time is 5min；
（4）After the completion of waiting for cracking reaction, the activated carbon and montmorillonite mixing particulate material in deposition bed are taken out, is added after cooling
Enter cigarette filter, addition is 5mg/ branch.
When preparing cigarette, tobacco content in cigarette is reduced, increases the usage amount of the filler materials such as thin slice, stem.
Final obtained cigarette product, Yuxi cigarette perfume taste protrudes in flue gas, and flue gas harmony is good, organoleptic quality with it is normal
Yuxi cigarette is close, and it is notable to reduce cost effect.
Embodiment 5
（1）15g nanmu clasts are put into cracking reaction stove, and place 35 mesh sizes of 300g in the deposition bed of lower section
Active carbon particle and 200g350 mesh sizes diatomite particle；
（2）It selects containing helium as carrier gas stream, control carries air-flow velocity as 200ml/min, and the storage by filling pure water
Liquid pool, wherein liquid storage tank temperature are controlled at 80 DEG C.Vapor is brought into cracking reaction stove using carrier gas stream；
（3）It opens cracking reaction stove and collaboration cracking reaction is carried out to the various substances in stove, control cracking temperature is 1000
DEG C, heating rate is 300 DEG C/min, and the cracking reaction time is 5min；After the completion of waiting for cracking reaction, the mixing in deposition bed is taken out
Granular materials, is added cigarette filter after cooling, addition is 30mg/ branch.
Final cigarette product obtained, flue gas root of Aucklandia lappa Decne taste is apparent, and flue gas harmony enhancing, organoleptic quality is obviously carried
It rises.
Embodiment 6
（1）The wizened bacterium clast that 15g dries is put into cracking reaction stove, and 500g is placed in the deposition bed of lower section
The active carbon particle of 35 mesh sizes；
（2）It selects containing helium as carrier gas stream, control carries air-flow velocity as 100ml/min, and the storage by filling pure water
Liquid pool, wherein liquid storage tank temperature are controlled at 90 DEG C, and vapor is brought into cracking reaction stove using carrier gas stream；
（3）It opens cracking reaction stove and collaboration cracking reaction is carried out to the various substances in stove, control cracking temperature is 850
DEG C, heating rate is 200 DEG C/min, and the cracking reaction time is 10min；After the completion of waiting for cracking reaction, take out mixed in deposition bed
Granular materials is closed, cigarette filter is added after cooling, addition is 10mg/ branch.
Final cigarette product obtained, flue gas bacterium is aromatic strongly fragrant, and flue gas harmony enhancing, organoleptic quality is obviously carried
It rises.
Above-described embodiment equipment therefor is as shown in Figure 1, including the liquid storage tank 4 described in liquid storage tank 4, pyrolysis furnace 1 and deposition bed 3
Bottom is equipped with temperature control heating device 11, and for the liquid in liquid storage tank is heated or freezed, top is led equipped with two carrier gas
Pipe, respectively air induction conduit 7 and outtake tube 13, the wherein end of air induction conduit 7 will be less than the position of outtake tube 13, and set
There is the entrance 10 for facilitating and being packed into or pour out liquid, can be used for being packed into or pouring out liquid；The upper and lower side of pyrolysis furnace 1, which is equipped with, leads
Pipe, wherein top conduit 14 be used for crack generate gas phase composition transfer, lower section conduit 6 be used for crack generation liquid phase at
The transfer divided；The upper end of deposition bed 3 is connected with the conduit 6 of 1 lower end of pyrolysis furnace, the bend pipe of 3 side of deposition bed and 1 upper end of pyrolysis furnace
14 are connected；Deposition bed 3 is equipped with opening 8 for exhaust gas to be discharged and launches or take out solid-state/liquid-absorbant.Liquid storage tank and and split
Also it is connected using pipeline between solution stove.In the pyrolysis furnace 1 be equipped with reaction bed 2, stage casing be equipped with opening, can open cleaning or
Replace reaction bed；The reaction bed 2 is porous flat plate structure, and to make liquid pyrolysis product flow downward out, aperture can be with
Selection so that cracked residue without falling into the deposition bed of lower section subject to.
Above-mentioned all pipelines are stainless steel, and wall thickness is 2mm.Liquid storage tank 4, reaction bed 2, deposition bed 3 are
Stainless steel, wall thickness are 2mm.Pyrolysis furnace sheet is heated as controllable temperature, and other structures are produced with existing pyrolysis furnace in the market
Based on product.
Application method：By required liquid charging stock（Room temperature liquid material can be by freezing so that it becomes liquid）, essential oil it is logical
It crosses liquid storage tank opening 10 to be fitted into liquid storage tank 4, it is desirable that its liquid level covers the height of air inlet carrier gas conduit 7, but is no more than airborne
Then the height of airway 13 closes liquid storage tank opening 10.Solid material is put into via pyrolysis furnace opening 9 on reaction bed 2, and
Close pyrolysis furnace opening 9.By selected absorbent（Solid/liquid）It is fitted into deposition bed via deposition bed opening 8, it is desirable that it is high
Degree covers the height of lateral conduits 14, and deposition bed opening 8 can not be closed.
Liquid storage tank temperature regulating device 11 is first opened, after so that liquid storage tank temperature is dropped to the temperature of setting, is passed through carrier gas stream.Ventilation
Make after a period of time carrier gas full of pyrolysis furnace, deposition bed and between pipeline after, be then turned on pyrolysis furnace.The duration of ventilation
It can voluntarily be selected according to actually required, generally 10 minutes or so.
Pyrolysis furnace is opened, sets cracking temperature, heating rate and reaction time, and start to warm up.It waits after the completion of reacting,
Carrier gas stream can be closed, its cooled to room temperature is made.Product goes out to take out from deposition bed opening 8.
Complete unit after use, can be dismantled and be cleaned, to prevent the influence between different products.
The device can easily, scale carry out the extraction of embedded non-burning flavoring material, easy to operate, convenient
Cleaning and displacement, and raw material dosage is saved very much, it can strictly control production cost.
Claims (10)
1. a kind of preparation method of cigarette filter-tip additive agent, it is characterised in that：It follows these steps to carry out：
（1）The reaction bed that the spice material cracked will be needed to be put into pyrolysis furnace, will be placed on cracking as the granular materials of adsorbent
In the deposition bed of stove；
（2）Carrier gas stream needed for opening, and by material storage container, required volatile fragrance component, carrier gas are held in liquid storage tank
Stream brings fragrance component into cracking reaction stove；
（3）It opens cracking reaction stove and collaboration cracking reaction is carried out to the various substances in stove；
（4）Wait for that cracking reaction takes out the granular materials in deposition bed up to cigarette filter-tip additive agent after the completion.
2. the preparation method of cigarette filter-tip additive agent according to claim 1, it is characterised in that：Step（1）Described in
Spice material is one kind in tobacco leaf, agalloch eaglewood, peppermint grass.
3. the preparation method of cigarette filter-tip additive agent according to claim 1, it is characterised in that：Step（1）Described in
The granular materials of adsorbent is one or more of activated carbon, diatomite, porous paper material.
4. the preparation method of cigarette filter-tip additive agent according to claim 1, it is characterised in that：Step（2）Described in
Carrier gas is one kind in nitrogen, nitrogen oxygen atmosphere, helium.
5. the preparation method of cigarette filter-tip additive agent according to claim 1, it is characterised in that：Step（2）Described in
The volatile fragrance component held in liquid storage tank is one kind in Rosa Damascana, geranium oil.
6. the preparation method of cigarette filter-tip additive agent according to claim 1, it is characterised in that：Pyrolysis furnace reaction temperature is excellent
600-1000 DEG C is selected, heating rate is 200-400 DEG C/min, reaction time 5-10min.
7. a kind of device being used to prepare cigarette filter-tip additive agent described in claim 1, it is characterised in that the device includes storage
Three liquid pool, pyrolysis furnace and deposition bed critical pieces；Liquid entrance is equipped with above the liquid storage tank, can be used for being packed into or
Liquid is poured out, there is air inlet pipe in lower section equipped with temperature regulating device for the liquid in liquid storage tank is heated or freezed in liquid storage tank
Road and outlet pipe；It cracks furnace middle end and is equipped with one layer with porous reaction bed, upper and lower side has pipeline to be connected；Above deposition bed with
The pipeline of pyrolysis furnace lower end is connected, and the position of deposition bed side on the lower is connected with the pipeline above pyrolysis furnace by bend pipe；It is described
Liquid storage tank and between pyrolysis furnace also using pipeline be connected.
8. the device according to claim 7 for being used to prepare cigarette filter-tip additive agent, it is characterised in that：The pyrolysis furnace
This is heated as controllable temperature, has opening in the position of reaction bed, can be opened cleaning or be replaced reaction bed.
9. the device according to claim 7 for being used to prepare cigarette filter-tip additive agent, it is characterised in that：The reaction bed
It is porous flat plate, to make liquid pyrolysis product flow downward out, aperture it can be selected that so that cracked residue is without falling into lower section
Subject to deposition bed.
10. the device according to claim 7 for being used to prepare cigarette filter-tip additive agent, it is characterised in that：Above and below reaction bed
Fang Jun has tubular opening, the liquid product that cracking reaction generates that can be oozed out from the hole of reaction bed, and is flowed into along lower end nozzle
Deposition bed；The gaseous products of generation are passed through the other end of deposition bed along pipeline after upper end tube nozzle is flowed out with carrier gas, are equally sunk
Granular materials absorption on product bed.
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| CN201610075660.5A CN105520192B (en) | 2016-02-03 | 2016-02-03 | A kind of preparation method and application of cigarette filter-tip additive agent |
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| CN201610075660.5A CN105520192B (en) | 2016-02-03 | 2016-02-03 | A kind of preparation method and application of cigarette filter-tip additive agent |
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| CN105520192B true CN105520192B (en) | 2018-11-09 |
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Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106539124B (en) * | 2016-10-20 | 2018-05-29 | 云南中烟工业有限责任公司 | A kind of preparation method of cigarette filter tip additive |
| CN108627584A (en) * | 2018-05-16 | 2018-10-09 | 云南中烟工业有限责任公司 | The detection device and detection method of the aromatic amine burst size of a kind of nanometer of filter tip |
| CN108918699A (en) * | 2018-05-16 | 2018-11-30 | 云南中烟工业有限责任公司 | A kind of detection method of the aldehyde material the amount of migration of nanometer of filter tip |
| CN108663451A (en) * | 2018-05-16 | 2018-10-16 | 云南中烟工业有限责任公司 | The detection method of tea component the amount of migration in a kind of special flavoring filter stick |
| CN110577093B (en) * | 2019-08-08 | 2021-02-26 | 武汉市艺茂机械有限公司 | Intermittent type formula granule powder adds device |
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