WO2019119731A1 - Peripheral electric heating aerosol generating system containing tobacco particles - Google Patents

Peripheral electric heating aerosol generating system containing tobacco particles Download PDF

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Publication number
WO2019119731A1
WO2019119731A1 PCT/CN2018/088800 CN2018088800W WO2019119731A1 WO 2019119731 A1 WO2019119731 A1 WO 2019119731A1 CN 2018088800 W CN2018088800 W CN 2018088800W WO 2019119731 A1 WO2019119731 A1 WO 2019119731A1
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WIPO (PCT)
Prior art keywords
tobacco
heating
electric heating
cartridge
generating system
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PCT/CN2018/088800
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French (fr)
Chinese (zh)
Inventor
周顺
何庆
王成虎
张劲
王孝峰
张晓宇
张亚平
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安徽中烟工业有限责任公司
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Publication of WO2019119731A1 publication Critical patent/WO2019119731A1/en

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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24FSMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
    • A24F40/00Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
    • A24F40/40Constructional details, e.g. connection of cartridges and battery parts
    • A24F40/46Shape or structure of electric heating means
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/17Filters specially adapted for simulated smoking devices
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24FSMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
    • A24F40/00Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
    • A24F40/20Devices using solid inhalable precursors

Definitions

  • the invention relates to the technical field of tobacco products, in particular to a peripheral electric heating aerosol generating system comprising tobacco particles.
  • the heating non-burning tobacco product is a new type of tobacco product which relies on heating different forms of tobacco materials to produce smoke release effect. It was one of the important categories of new tobacco products since the 1980s.
  • the tobacco flavor is transmitted to consumers through the method of “heating without burning”, and its appearance and consumption mode are similar to those of traditional cigarettes, and the physiological and psychological needs of consumers are adapted and satisfied to some extent.
  • This "heating without burning” method allows the tobacco to be heated only at lower temperatures (generally below 500 ° C), avoiding the formation of tar and a large number of harmful compounds caused by high temperature combustion of the tobacco, and since there is substantially no sidestream smoke Gas, will not produce second-hand smoke, will not affect the public environment.
  • the electric heating non-combustion tobacco product has the advantages of controllable heating temperature, flexible heating mode, convenient use and fashion, and has higher attention, and is an important development direction of heating non-combustion tobacco products at home and abroad.
  • the technical core of heating non-combustion tobacco products mainly includes two aspects of heat source and smoke release material.
  • the heat source types are divided into three types: electric heating, carbon heating, and chemical reaction heating. Among them, electric heating and carbon heating have been applied to products such as “iQOS” of Philip Morris and Revo of Reynolds Tobacco.
  • the release material is a key factor affecting the smoking experience of heating non-combustible tobacco products.
  • the smoke release materials mainly include tobacco, tobacco, tobacco sheets and the like. These materials can release flue gas with tobacco characteristic aroma under different heating environments, but there are common defects such as uneven heating, easy carbonization, and inconvenient operation.
  • a peripheral electric heating aerosol generating system comprising tobacco particles, comprising an electrically heated tobacco rod and a cartridge inserted into the electrically heated tobacco rod,
  • the cartridge includes a metal sleeve, a filter section and a heating section, and the top end of the metal sleeve is open and the bottom end is sealed by a metal base, and the filter section and the heating section are arranged in an up-and-down arrangement inside the metal sleeve.
  • the bottom of the heating section is supported by a metal base, and the heating section is composed of tobacco particles, and the side wall of the metal sleeve has an inner vent hole at a position corresponding to the heating section;
  • the electric heating tobacco rod comprises a tobacco rod body, the upper portion of the tobacco rod body is provided with a receiving chamber with an open top end, and an electric heating assembly is arranged in the receiving chamber of the tobacco rod body, and the electric heating assembly comprises a distribution An annular heating piece of the inner side wall of the cavity, and a bottom heating piece distributed on the bottom wall of the accommodating cavity, and an outer vent hole is formed in the side wall of the accommodating cavity;
  • the tobacco particles are composed of the following mass percentages of raw materials:
  • the filter segment of the cartridge is a paper filter rod.
  • a battery for supplying power to the electric heating component is disposed inside the tobacco rod body, and the tobacco rod body is further provided with a charging interface for charging the battery.
  • a switch is further disposed on the body of the tobacco rod.
  • the accommodating cavity depth of the electrically heated tobacco rod is less than the axial length of the heating section of the cartridge.
  • the inner vent has a pore diameter smaller than a particle diameter of the tobacco particles.
  • the tobacco ultrafine powder is one or more selected from the group consisting of flue-cured tobacco, burley tobacco, oriental tobacco, expanded tobacco, and tobacco stem; and the particle size of the tobacco ultrafine powder is ⁇ 250 ⁇ m.
  • the other biomass powder is selected from one or more of tangerine peel, sandalwood, ebony, sarcophagus, sweet potato, chestnut, and malt; and the other biomass powder has a particle diameter of ⁇ 250 ⁇ m.
  • the mass of the other biomass powder accounts for ⁇ 20% of the mass of the tobacco ultrafine powder; the quality of the tobacco dry distillation accounts for 5-20% of the mass of the tobacco ultrafine powder.
  • the atomizing agent is selected from one or more of 1,2-propanediol, 1,3-butanediol, and glycerin;
  • the binder is selected from the group consisting of starch, xanthan gum, and carrageenan.
  • the preparation method of the tobacco dry distillation used in the invention is prepared by referring to the patent CN204579897U "a submicron smoke particle preparation device capable of improving the sensory quality of the electronic cigarette", and the specific preparation method is as follows:
  • At least one of flue-cured tobacco, burley tobacco, and oriental tobacco is used as a tobacco raw material, and is subjected to dry distillation at 200 to 400 ° C.
  • the distillate is collected by condensation, and concentrated under reduced pressure at 60 ° C to anhydrous steam. Distilled, the resulting residual product is the tobacco dry distillation.
  • the method for preparing tobacco particles of the present invention comprises the following steps:
  • Step 1 mixing the tobacco ultrafine powder and other biomass powders as a main ingredient, and mixing the tobacco dry matter, the atomizing agent, the binder and the tobacco flavor and fragrance according to the compounding amount as an auxiliary material;
  • the main material and the auxiliary material are wet-mixed (the atomizing agent may be used, and no other mixed medium is added) to obtain a premix;
  • Step 2 The premix obtained in the step 1 is subjected to baking alcoholization to obtain an alcoholate;
  • Step 3 extruding the alcoholate obtained in step 2 through an extruder to obtain an extrudate
  • Step 4 The extrudate obtained in the step 3 is subjected to spheronization granulation, and the water is removed by drying to obtain tobacco granules.
  • step 1 the mixing process is carried out by a high speed mixer, and the mixing conditions are: mixing time ⁇ 15 min; mixing speed ⁇ 500 rpm.
  • the conditions of the roasting alcoholization treatment are as follows: the atmosphere is continuously aerated with nitrogen; the temperature is 100-200 ° C; and the time is 2-4 h.
  • the premix is placed in a heatable, ventilated stainless steel tank for baking and alcoholization.
  • the process of step 2 can make the components in the premix more uniformly mixed on the one hand, and the Maillard reaction in the process of heating the alcoholization on the other hand can make the aroma of the product tobacco particle material more abundant, and remove the bad odor such as cyan gas;
  • this step also removes some of the moisture from the premix, facilitating extrusion and the sensory experience of the product.
  • the extrusion molding conditions are: extrusion temperature ⁇ 40 ° C; pore diameter of 0.5 - 0.8 mm; extrusion rate of 5 - 10 kg / h.
  • the pore diameter is preferably 0.7 mm.
  • the extruder employs a screen extruder or a variable density extruder (i.e., a screw extruder), preferably a variable density extruder.
  • the spheronization granulation adopts a high-speed spheronizer, and the spheronization speed is ⁇ 1000 rpm.
  • the drying adopts a temperature-controlled oven, preferably a tunnel type quick dryer, the drying temperature is 60-80 ° C, the drying time is ⁇ 1 h; preferably, the drying to the water content is ⁇ 5 wt%.
  • the tobacco particles prepared by the present invention are uniform spherical particles having a particle diameter of 0.5 to 0.8 mm.
  • the tobacco granule of the invention has uniform granules and pleasant scent, and can adjust the amount of the atomizing agent to be added according to the demand, and the amount of smoke fumes released is large, and the consumer can satisfy the satisfaction of smoking in the state of heating and non-combustion.
  • the combination of tobacco dry distillation and tobacco powder can significantly improve the sensory quality of the flue gas, so that the flue gas has excellent uniformity, aroma, concentration and strength; and the selective addition of other biomass powder can impart a unique aroma to the flue gas. Taste.
  • Particle formulation aroma concentration Energize Overview Smoke + dry distillation spice A+ A++ A+ A+ Smoke A- A- A A-
  • the present invention provides a peripheral electrically heated aerosol generating system comprising tobacco particles which, by heating the tobacco particles, produces an effect similar to conventional cigarettes.
  • the shell of the cartridge is surrounded by a metal sleeve and a metal base to form a bottom closed space, and the tobacco particles of the heating section are sealed and filled in the space, and the cartridge is matched with the electric heating rod, and the cartridge is directly used after being used.
  • the electric heating rod is taken out, and the smoke releasing material of the cartridge does not remain in the electric heating rod, and does not pollute the electric heating rod. Therefore, the electric heating rod is not required to be cleaned, the use is very convenient, and the cartridge is replaced. There is no fire hazard after abandonment.
  • Figure 1 is a schematic view showing the entire structure of the present invention.
  • FIG. 2 is a schematic structural view of a cartridge of the present invention.
  • Figure 3 is a schematic view showing the structure of an electrically heated tobacco rod of the present invention.
  • Figure 4 is a comparison of the flue gas release rates of the tobacco particulate material prepared in Example 1 with other smoke releasing materials such as tobacco flakes and soot in a heat-non-combustible state (350 ° C).
  • Figure 5 is a comparison of the amount of smoke released from the tobacco particulate material prepared in Example 1 and other smoke releasing materials such as tobacco flakes and soot in a non-combustible state (350 ° C).
  • the tobacco particulate material has obvious advantages over the flue gas release rate and the flue gas release amount of the tobacco flakes and the smoke. Under the same conditions, the tobacco particulate material is heated and not combusted. The smoke is released faster and the smoke is released more.
  • Figure 6 is a comparison of the flue gas release rates of the tobacco particulate material prepared in Example 2 with other smoke releasing materials such as tobacco flakes and soot in a heat-non-combustible state (350 ° C).
  • Figure 7 is a comparison of the amount of smoke released from the tobacco particulate material prepared in Example 2 with other smoke releasing materials such as tobacco flakes and soot in a non-combustible state (350 ° C).
  • the tobacco particulate material has obvious advantages over the flue gas release rate and the flue gas release amount of the tobacco flakes and the smoke. Under the same conditions, the tobacco particulate material is heated and not combusted. The smoke is released faster and the smoke is released more.
  • the embodiment discloses a peripheral electric heating aerosol generating system including tobacco particles, comprising an electric heating tobacco rod 1 and a cartridge 2 inserted into the electric heating tobacco rod 1.
  • the cartridge 2 includes a metal sleeve 21, a filter section 22 and a heating section 23.
  • the top end of the metal sleeve 21 is open and the bottom end is sealed by a metal base 24, and the filter section 22 and the heating section 23 are arranged one above the other in the metal sleeve 21.
  • the bottom of the heating section 23 is supported by the metal base 24, and the heating section 23 is composed of tobacco particles.
  • the side wall of the metal sleeve 21 is provided with an inner vent hole 25 at the position corresponding to the heating section 23, and the inner vent hole 25 is provided.
  • the pore size is smaller than the particle size of the tobacco particles to avoid leakage of the tobacco particles.
  • the electrically heated tobacco rod 1 comprises a tobacco rod body 11 having an upper portion of the upper portion of the tobacco rod body 11 with an open top end, the receiving chamber 12 having a depth smaller than the axial length of the heating portion 23 of the cartridge 2.
  • An electric heating assembly is disposed in the accommodating chamber 12 of the tobacco rod body 11.
  • the electric heating assembly includes an annular heating piece 13 distributed on the inner side wall of the accommodating chamber 12, and a bottom heating piece 14 distributed on the bottom wall of the accommodating chamber 12, accommodating the chamber 12.
  • An outer venting opening 15 is defined in the side wall of the cavity; a battery for supplying power to the electric heating component is disposed inside the tobacco rod body 11, and the charging rod 16 is further provided with a charging interface 16 for charging the battery;
  • a switch 17 is also provided on the 11 for opening and closing the electric heating assembly.
  • the cartridge 2 is inserted into the accommodating chamber 12 of the electric heating rod 1 from the top to the bottom, and the side wall of the heating section 23 of the cartridge 2 is heated by the annular heating piece 13, and the heating section 23 of the cartridge 2 is passed through the bottom heating sheet 14. Heat the bottom.
  • the material of the filter section 22 of the cartridge 2 can be selected from the group consisting of cellulose acetate filter rod, paper filter rod, activated carbon, aluminum foil, polylactic acid non-woven fabric, polylactic acid film, modified polylactic acid non-woven fabric and modified polylactic acid film.
  • the material of the metal sleeve 21 and the metal base 24 may be at least one selected from the group consisting of copper, aluminum, aluminum alloy, iron, and stainless steel.
  • the cartridge 2 is inserted into the accommodating chamber 12 of the electric heating rod 1 from top to bottom, and the side wall of the heating section 23 of the cartridge 2 is heated by the annular heating sheet 13 through the bottom heating sheet 14 to the cartridge 2
  • the bottom of the heating section 23 is heated to cause the tobacco particles to generate smoke for suction.
  • the periphery and the bottom of the heating section 23 are simultaneously heated, and the heating is more uniform.
  • This embodiment produces an effect similar to a conventional cigarette by heating the tobacco particulate material to generate smoke.
  • the tobacco granule material is sealed in the cartridge 2, and the used electric heating rod 1 is not left and polluted after use, and the electric heating rod 1 is not required to be cleaned, and the rod 2 is replaced and discarded without causing fire hazard.
  • the tobacco particles are composed of the following mass percentages of raw materials:
  • the preparation method of the tobacco dry distillation used in the invention is prepared by referring to the patent CN204579897U "a submicron smoke particle preparation device capable of improving the sensory quality of the electronic cigarette", and the specific preparation method is as follows:
  • At least one of flue-cured tobacco, burley tobacco, and oriental tobacco is used as a tobacco raw material, and is subjected to dry distillation at 200 to 400 ° C.
  • the distillate is collected by condensation, and concentrated under reduced pressure at 60 ° C to anhydrous steam. Distilled, the resulting residual product is the tobacco dry distillation.
  • Step 1 Take flue-cured tobacco powder, sieve with 250 ⁇ m sieve, weigh 600g as main ingredient; weigh 50g of flue-cured tobacco dry distillation, 240g of glycerol, 60g of propylene glycol, 20g of guar gum, 10g of gelatin, maltodextrin 10 g, tobacco flavors and fragrances (mint) 10 g in a stirred tank, stirred at 1000 rpm for 15 min as an auxiliary material; the main ingredient was added to the auxiliary material under stirring, and stirring was continued at 1000 rpm for 1 h at room temperature to obtain a premix.
  • mint tobacco flavors and fragrances
  • Step 2 Pour the premix into a heated, ventilated stainless steel reaction tank, continuously pass nitrogen gas from the upper vent hole of the tank, and keep the pores open; the alcoholization temperature is 120 ° C, and the alcoholization time is 2 h. Alcohol.
  • Step 3 After the alcoholate was cooled to room temperature, it was sent to a screw extruder for extrusion molding at an extrusion rate of 5 kg/h and a pore diameter of 0.7 mm to obtain an extrudate.
  • Step 4 The extrudate obtained in step 3 is sent to a high-speed rounding machine for spheronization and granulation at a speed of 2000 rpm to obtain a wet granular material having a particle diameter of 0.7 mm, placed in a temperature-controlled oven, and dried at 80 ° C to a water content in the granules. The rate was 5 wt%, which gave the desired tobacco particles.
  • the flue gas release rate (Fig. 4) and the flue gas release rate (Fig. 5) of the tobacco particulate material and other smoke releasing materials such as tobacco sheets and cigarettes in a non-combustible state (Fig. 4) were compared by a cone calorimeter (Fig. 5). It can be seen from the figure that the tobacco particulate material has obvious advantages over the flue gas release rate and the flue gas release amount of the tobacco flakes and the smoke. Under the same conditions, the tobacco particulate material is smoked under heating and non-combustion conditions. The gas is released faster and the amount of smoke released is greater.
  • the tobacco granules of the present embodiment have a fast release rate of flue gas and a sufficient release amount in the state of heating and non-combustion, and have a distinctive flue-cured style characteristic, accompanied by a lightness of the mint, a strong sense of flue gas, and good comfort.
  • Step 1 Weigh 350g of flue-cured tobacco powder sieved through a 250 ⁇ m sieve, 150g of burley tobacco powder, 50g of dried tangerine peel powder, 50g of ebony powder in a stirred tank, stir at a speed of 500rpm for 20min, as the main material; weigh the flue-cured tobacco separately 70 g of dry distillation, 10 g of burley tobacco dry distillation, 250 g of glycerin, 20 g of xanthan gum, 10 g of gelatin, 40 g of flavors and flavors of tobacco (fruity flavor, cocoa), and stirred in a stirred tank at 1000 rpm for 15 min. Excipients; adding the main ingredient to the auxiliary material under stirring, stirring at 1000 rpm for 1 h at room temperature to obtain a premix.
  • Step 2 Pour the premix into a heatable and ventilated stainless steel reaction tank, continuously pass nitrogen gas from the upper vent hole of the tank, and keep the pores open; the alcoholization temperature is 100 ° C, and the alcoholization time is 4 h. Alcohol.
  • Step 3 After the alcoholate was cooled to room temperature, it was sent to a screw extruder for extrusion molding at an extrusion rate of 6 kg/h and a pore diameter of 0.8 mm to obtain an extrudate.
  • Step 4 The extrudate obtained in step 3 is sent to a high-speed rounding machine for spheronization granulation at a rotational speed of 1500 rpm to obtain a wet granular material having a particle diameter of 0.8 mm, placed in a temperature-controlled oven, and dried at 80 ° C to a water content in the granules. The rate was 3 wt%, which gave the desired tobacco particles.
  • the flue gas release rate (Fig. 6) and the flue gas release rate (Fig. 6) of the tobacco particulate material and other smoke releasing materials such as tobacco sheets and cigarettes in a non-combustion state (Fig. 6) were compared by a cone calorimeter (Fig. 7). It can be seen from the figure that the tobacco particulate material has obvious advantages over the flue gas release rate and the flue gas release amount of the tobacco flakes and the smoke. Under the same conditions, the tobacco particulate material is smoked under heating and non-combustion conditions. The gas is released faster and the amount of smoke released is greater.
  • the tobacco granule material of the present embodiment has a fast release rate of flue gas and a sufficient amount of release in the state of heating and non-combustion, and has remarkable mixed tobacco style characteristics, and combines the aroma of dried tangerine peel and ebony, and the smoke has a strong sense of satisfaction and good comfort. .

Abstract

Disclosed is a peripheral electric heating aerosol generating system containing tobacco particles, comprising an electric heating tobacco stem and a cartridge inserted in the electric heating tobacco stem. The cartridge comprises a metal sleeve, a filter section and a heating section. The top of the metal sleeve is provided with an opening, and the bottom of the metal sleeve is sealed by means of a metal base. The filter section and the heating section are vertically arranged in a cavity inside the metal sleeve. The bottom of the heating section is supported by the metal base, and the heating section is formed by the tobacco particles. The electric heating tobacco stem comprises a tobacco stem body. The upper portion of the tobacco stem body is provided with a containing cavity. An electric heating assembly is provided in the containing cavity of the tobacco stem body. The electric heating assembly comprises an annular heating piece and a bottom heating piece. The cartridge is inserted in the containing cavity of the electric heating tobacco stem, and the side wall and bottom of the heating section of the cartridge are heated by means of the annular heating piece and the bottom heating piece. The present invention has the advantages that the tobacco particles are sealed in the cartridge, the electric heating tobacco stem is not polluted, and fire hazards cannot be caused after the cartridge is replaced and discarded.

Description

一种包含烟草颗粒的外围电加热气雾产生系统Peripheral electric heating aerosol generating system comprising tobacco particles 技术领域Technical field
本发明涉及烟草制品技术领域,尤其涉及的是一种包含烟草颗粒的外围电加热气雾产生系统。The invention relates to the technical field of tobacco products, in particular to a peripheral electric heating aerosol generating system comprising tobacco particles.
背景技术Background technique
近年来,随着《烟草控制框架公约》的颁布与实施,各国政府的烟草管控措施日趋严格,对烟草的监管立法愈加严格,控烟和反烟的呼声越来越强烈,国内外市场竞争压力持续增大;同时,随着人们生活水平的不断提高,人们更加注重自己的身心健康和环境保护,对烟草有了新的认识。In recent years, with the promulgation and implementation of the Framework Convention on Tobacco Control, tobacco control measures of various governments have become stricter, and the regulatory legislation on tobacco has become stricter. The voices of tobacco control and anti-smoking have become stronger and stronger, and the competitive pressures in domestic and foreign markets continue. At the same time, with the continuous improvement of people's living standards, people pay more attention to their physical and mental health and environmental protection, and have a new understanding of tobacco.
诸如上述原因使传统卷烟的发展受到越来越多的制约,据2011年统计数据显示,在世界范围内卷烟产销量有所下降的同时,其他类型烟草制品呈现快速增长趋势,世界烟草市场产品结构不断发生深刻变化,积极发展全系列烟草制品逐渐成为各个跨国烟草公司的战略取向。目前,市场上已出现了三种主要的新型烟草制品类型:加热不燃烧型烟草制品、电子烟和无烟气烟草制品。For the above reasons, the development of traditional cigarettes is subject to more and more constraints. According to statistics from 2011, while cigarette production and sales have declined worldwide, other types of tobacco products have shown a rapid growth trend, and the world tobacco market product structure. Constantly undergoing profound changes, and actively developing a full range of tobacco products has gradually become the strategic orientation of various multinational tobacco companies. At present, three major new types of tobacco products have emerged on the market: heating non-combustible tobacco products, electronic cigarettes and smokeless tobacco products.
其中,加热不燃烧烟草制品是一种靠加热不同形式的烟草材料产生释烟效果的新型烟草制品,始于20世纪80年代,是新型烟草制品的重要品类之一。一般通过“加热不燃烧”的方式将烟草香味传递给消费者,其外观与消费方式上也与传统卷烟相似,在一定程度上适应和满足了消费者的生理需要和心理需求。这种“加热不燃烧”的方式,使烟草只在较低的温度下(一般低于500℃)被加热,避免了烟草高温燃烧导致的焦油和大量有害化合物生成,而且由于基本没有侧流烟气,不会产生二手烟气,不会对公共环境产生影响。近年来众多烟草制造企业、研究机构都看到了加热不燃烧烟草制品的巨大潜力,重金投入这一领域,并收获颇丰。其中,电加热不燃烧烟草制品由于具有加热温度可控、加热方式灵活、使用方便时尚等优点,具有更高的关注度,是当前国内外加热不燃烧烟草制品的重要发展方向。Among them, the heating non-burning tobacco product is a new type of tobacco product which relies on heating different forms of tobacco materials to produce smoke release effect. It was one of the important categories of new tobacco products since the 1980s. Generally, the tobacco flavor is transmitted to consumers through the method of “heating without burning”, and its appearance and consumption mode are similar to those of traditional cigarettes, and the physiological and psychological needs of consumers are adapted and satisfied to some extent. This "heating without burning" method allows the tobacco to be heated only at lower temperatures (generally below 500 ° C), avoiding the formation of tar and a large number of harmful compounds caused by high temperature combustion of the tobacco, and since there is substantially no sidestream smoke Gas, will not produce second-hand smoke, will not affect the public environment. In recent years, many tobacco manufacturing companies and research institutes have seen great potential for heating non-combustible tobacco products, and have invested heavily in this field, and have gained a lot. Among them, the electric heating non-combustion tobacco product has the advantages of controllable heating temperature, flexible heating mode, convenient use and fashion, and has higher attention, and is an important development direction of heating non-combustion tobacco products at home and abroad.
加热不燃烧烟草制品的技术核心主要包括热源和释烟材料两个方面。热源类型分为电加热、碳加热以及化学反应加热三种类型,其中电加热和碳加热两种热源已经应用于产品,如菲莫烟草公司的“iQOS”和雷诺烟草公司的“Revo”。释烟材料是影响加热不燃烧烟草制品抽吸体验的关键因素,目前所开发的释烟材料主要包括烟丝、烟末、烟草薄片等。这些材料在不同的加热环境下能够释放具有烟草特征香气的烟气,但普遍存在受热不均匀、易碳化、操作不便等缺陷。其中烟丝和烟末由于难以添加雾化剂,存在烟雾量小、发烟不均匀、易焦化等问题;而“iQOS”所用的烟草薄片虽然解决了发烟量问题,但制造工艺复杂,设备成本 昂贵,可调控性不强,且烟气中存在较重的烧纸味,影响口感,同时,现有产品在使用后,释烟材料由于焦化、碳化、粘结等原因会残留于电加热组件上,需要配套专门的工具对加热组件进行清洁,而且该类产品,与传统卷烟一样,在使用完抛弃后存在安全火灾隐患。因此,开发一种操作简便、雾化效果好、无需清洁、对环境友好的新型电加热气雾产生系统,对于新型烟草制品开发是非常有意义的。The technical core of heating non-combustion tobacco products mainly includes two aspects of heat source and smoke release material. The heat source types are divided into three types: electric heating, carbon heating, and chemical reaction heating. Among them, electric heating and carbon heating have been applied to products such as “iQOS” of Philip Morris and Revo of Reynolds Tobacco. The release material is a key factor affecting the smoking experience of heating non-combustible tobacco products. Currently, the smoke release materials mainly include tobacco, tobacco, tobacco sheets and the like. These materials can release flue gas with tobacco characteristic aroma under different heating environments, but there are common defects such as uneven heating, easy carbonization, and inconvenient operation. Among them, tobacco and tobacco are difficult to add atomizing agent, and there are problems such as small amount of smoke, uneven smoking, and easy coking; while the tobacco sheet used in "iQOS" solves the problem of smoke generation, the manufacturing process is complicated and the equipment cost is low. Expensive, not controllable, and there is a heavy burning paper smell in the flue gas, affecting the taste. At the same time, after the existing products are used, the smoke releasing material will remain on the electric heating component due to coking, carbonization, bonding and the like. Special tools are needed to clean the heating components, and this kind of product, like traditional cigarettes, has a safety fire hazard after use. Therefore, the development of a new type of electric heating aerosol generating system with simple operation, good atomization effect, no need for cleaning and environmental friendliness is very meaningful for the development of new tobacco products.
发明内容Summary of the invention
本发明的目的在于克服现有技术的不足,提供了一种包含烟草颗粒的外围电加热气雾产生系统。It is an object of the present invention to overcome the deficiencies of the prior art and to provide a peripheral electrically heated aerosol generating system comprising tobacco particles.
本发明是通过以下技术方案实现的:The invention is achieved by the following technical solutions:
一种包含烟草颗粒的外围电加热气雾产生系统,包括电加热烟杆和插入电加热烟杆内的烟弹,A peripheral electric heating aerosol generating system comprising tobacco particles, comprising an electrically heated tobacco rod and a cartridge inserted into the electrically heated tobacco rod,
所述烟弹包括金属套管、过滤段和加热段,所述金属套管顶端敞口、底端通过一个金属底座密封,所述过滤段和加热段呈上下排列设置在金属套管内部的空腔内,所述加热段底部依靠金属底座来支撑,所述加热段由烟草颗粒组成,所述金属套管侧壁在对应加热段的位置上开有内通气孔;The cartridge includes a metal sleeve, a filter section and a heating section, and the top end of the metal sleeve is open and the bottom end is sealed by a metal base, and the filter section and the heating section are arranged in an up-and-down arrangement inside the metal sleeve. Inside the cavity, the bottom of the heating section is supported by a metal base, and the heating section is composed of tobacco particles, and the side wall of the metal sleeve has an inner vent hole at a position corresponding to the heating section;
所述电加热烟杆包括烟杆本体,所述烟杆本体上部设有顶端敞口的容纳腔,所述烟杆本体的容纳腔内设有电加热组件,所述电加热组件包括分布在容纳腔内侧壁的环形加热片、以及分布在容纳腔底壁的底部加热片,所述容纳腔侧壁上开有外通气孔;The electric heating tobacco rod comprises a tobacco rod body, the upper portion of the tobacco rod body is provided with a receiving chamber with an open top end, and an electric heating assembly is arranged in the receiving chamber of the tobacco rod body, and the electric heating assembly comprises a distribution An annular heating piece of the inner side wall of the cavity, and a bottom heating piece distributed on the bottom wall of the accommodating cavity, and an outer vent hole is formed in the side wall of the accommodating cavity;
所述烟弹从上往下插入所述电加热烟杆的容纳腔内,通过所述环形加热片对烟弹的加热段侧壁进行加热,通过所述底部加热片对烟弹的加热段底部进行加热;Inserting the cartridge into the receiving cavity of the electric heating rod from top to bottom, heating the side wall of the heating section of the cartridge through the annular heating sheet, and passing the bottom heating piece to the bottom of the heating section of the cartridge Heating;
所述烟草颗粒由以下质量百分比的原料构成:The tobacco particles are composed of the following mass percentages of raw materials:
烟草超微粉末40-60%,其他生物质粉末0-10%,烟草干馏物5-10%,雾化剂20-40%,粘结剂1-5%,余量为烟用香精香料。Tobacco ultrafine powder 40-60%, other biomass powder 0-10%, tobacco dry distillation 5-10%, atomizing agent 20-40%, binder 1-5%, the balance is tobacco flavors and fragrances.
进一步的,所述烟弹的过滤段为纸质滤棒。Further, the filter segment of the cartridge is a paper filter rod.
进一步的,所述烟杆本体内部设置有用于对电加热组件进行供电的电池,所述烟杆本体上还设有用于对电池进行充电的充电接口。Further, a battery for supplying power to the electric heating component is disposed inside the tobacco rod body, and the tobacco rod body is further provided with a charging interface for charging the battery.
进一步的,所述烟杆本体上还设有开关。Further, a switch is further disposed on the body of the tobacco rod.
进一步的,所述电加热烟杆的容纳腔深度小于所述烟弹的加热段的轴向长度。Further, the accommodating cavity depth of the electrically heated tobacco rod is less than the axial length of the heating section of the cartridge.
进一步的,所述内通气孔的孔径小于所述烟草颗粒的颗粒粒径。Further, the inner vent has a pore diameter smaller than a particle diameter of the tobacco particles.
进一步的,所述烟草超微粉末选自烤烟、白肋烟、香料烟、膨胀烟、烟梗中的一种或几种;所述烟草超微粉末的粒径≤250μm。Further, the tobacco ultrafine powder is one or more selected from the group consisting of flue-cured tobacco, burley tobacco, oriental tobacco, expanded tobacco, and tobacco stem; and the particle size of the tobacco ultrafine powder is ≤250 μm.
进一步的,所述其他生物质粉末选自陈皮、檀皮、乌梅、石斛、红薯、板栗、麦芽中的一种或几种;所述其他生物质粉末的粒径≤250μm。Further, the other biomass powder is selected from one or more of tangerine peel, sandalwood, ebony, sarcophagus, sweet potato, chestnut, and malt; and the other biomass powder has a particle diameter of ≤250 μm.
进一步的,所述其他生物质粉末的质量占烟草超微粉末质量的比例≤20%;所述烟草干馏物的质量占烟草超微粉末质量的5-20%。Further, the mass of the other biomass powder accounts for ≤20% of the mass of the tobacco ultrafine powder; the quality of the tobacco dry distillation accounts for 5-20% of the mass of the tobacco ultrafine powder.
进一步的,所述雾化剂选自1,2-丙二醇、1,3-丁二醇、丙三醇中的一种或几种;所述粘结剂选自淀粉、黄原胶、卡拉胶、明胶、瓜尔胶、麦芽糊精中的一种或几种。Further, the atomizing agent is selected from one or more of 1,2-propanediol, 1,3-butanediol, and glycerin; the binder is selected from the group consisting of starch, xanthan gum, and carrageenan. One or more of gelatin, guar gum, and maltodextrin.
本发明中使用的烟草干馏物的制备方法参考专利CN204579897U“一种可提升电子烟感官质量的亚微米烟颗粒制备装置”制备得到,具体制备方法如下:The preparation method of the tobacco dry distillation used in the invention is prepared by referring to the patent CN204579897U "a submicron smoke particle preparation device capable of improving the sensory quality of the electronic cigarette", and the specific preparation method is as follows:
在无氧气氛下,将烤烟、白肋烟、香料烟中的至少一种作为烟草原料,在200-400℃下进行干馏,馏出物经冷凝后收集,60℃减压浓缩至无水蒸气蒸出,所得残留产物即为烟草干馏物。In an oxygen-free atmosphere, at least one of flue-cured tobacco, burley tobacco, and oriental tobacco is used as a tobacco raw material, and is subjected to dry distillation at 200 to 400 ° C. The distillate is collected by condensation, and concentrated under reduced pressure at 60 ° C to anhydrous steam. Distilled, the resulting residual product is the tobacco dry distillation.
本发明的烟草颗粒的制备方法,包括如下步骤:The method for preparing tobacco particles of the present invention comprises the following steps:
步骤1:将烟草超微粉末和其他生物质粉末按配比量混合后作为主料,将烟草干馏物、雾化剂、粘结剂和烟用香精香料按配比量混合后作为辅料;将所述主料和所述辅料进行湿法混合(有雾化剂就可以,不再外加其他混合介质),得到预混物;Step 1: mixing the tobacco ultrafine powder and other biomass powders as a main ingredient, and mixing the tobacco dry matter, the atomizing agent, the binder and the tobacco flavor and fragrance according to the compounding amount as an auxiliary material; The main material and the auxiliary material are wet-mixed (the atomizing agent may be used, and no other mixed medium is added) to obtain a premix;
步骤2:将步骤1得到的预混物进行烘焙醇化处理,得到醇化物;Step 2: The premix obtained in the step 1 is subjected to baking alcoholization to obtain an alcoholate;
步骤3:将步骤2所得醇化物通过挤出机挤出成型,得到挤出物;Step 3: extruding the alcoholate obtained in step 2 through an extruder to obtain an extrudate;
步骤4:将步骤3所得挤出物进行滚圆造粒,干燥除去水份,即可获得烟草颗粒。Step 4: The extrudate obtained in the step 3 is subjected to spheronization granulation, and the water is removed by drying to obtain tobacco granules.
其中,步骤1中,混合的过程通过高速搅拌机进行,混合条件为:混合时间≥15min;混合转速≥500rpm。Wherein, in step 1, the mixing process is carried out by a high speed mixer, and the mixing conditions are: mixing time ≥ 15 min; mixing speed ≥ 500 rpm.
步骤2中,烘焙醇化处理的条件为:气氛条件为氮气连续通气;温度为100-200℃;时间为2-4h。烘焙醇化处理时,预混物置于可加热、可通气的不锈钢罐中进行烘培醇化处理。步骤2的过程一方面能够让预混物中各组分混合更加均匀,另一方面加热醇化过程中的梅拉德反应能够使产物烟草颗粒材料香气更加丰富,同时去除青杂气等不良气味;此外,该步骤还可去除预混物中的部分水份,有利于挤出成型和产物的感官体验。In the step 2, the conditions of the roasting alcoholization treatment are as follows: the atmosphere is continuously aerated with nitrogen; the temperature is 100-200 ° C; and the time is 2-4 h. For the aromatization treatment, the premix is placed in a heatable, ventilated stainless steel tank for baking and alcoholization. The process of step 2 can make the components in the premix more uniformly mixed on the one hand, and the Maillard reaction in the process of heating the alcoholization on the other hand can make the aroma of the product tobacco particle material more abundant, and remove the bad odor such as cyan gas; In addition, this step also removes some of the moisture from the premix, facilitating extrusion and the sensory experience of the product.
步骤3中,挤出成型的条件为:挤出温度≤40℃;孔直径为0.5-0.8mm;挤出速率为5-10kg/h。孔直径优选为0.7mm。所述挤出机采用筛网式挤出机或可变密度式挤出机(即螺杆挤出机),优选采用可变密度式挤出机。In the step 3, the extrusion molding conditions are: extrusion temperature ≤ 40 ° C; pore diameter of 0.5 - 0.8 mm; extrusion rate of 5 - 10 kg / h. The pore diameter is preferably 0.7 mm. The extruder employs a screen extruder or a variable density extruder (i.e., a screw extruder), preferably a variable density extruder.
步骤4中,所述滚圆造粒采用高速滚圆机,滚圆转速≥1000rpm。所述干燥采用控温烘箱,优选采用隧道式快速烘干机,干燥温度为60-80℃,干燥时间≤1h;优选干燥至含水率≤5wt%。In step 4, the spheronization granulation adopts a high-speed spheronizer, and the spheronization speed is ≥1000 rpm. The drying adopts a temperature-controlled oven, preferably a tunnel type quick dryer, the drying temperature is 60-80 ° C, the drying time is ≤ 1 h; preferably, the drying to the water content is ≤ 5 wt%.
本发明制备的烟草颗粒为均匀的球状颗粒,颗粒直径为0.5-0.8mm。The tobacco particles prepared by the present invention are uniform spherical particles having a particle diameter of 0.5 to 0.8 mm.
本发明的烟草颗粒,颗粒度均匀,嗅香愉悦,能够根据需求调节雾化剂的添加量,所释放的烟气烟雾量大,在加热不燃烧状态下能够提供消费者类似吸烟的满足感。烟草干馏物和烟草粉末的配合使用可以显著提升烟气感官品质,使烟气具有优异的均匀性、香气、浓度和劲头;且其他生物质粉末的选择性加入能够赋予烟气以独特的香味和口感。The tobacco granule of the invention has uniform granules and pleasant scent, and can adjust the amount of the atomizing agent to be added according to the demand, and the amount of smoke fumes released is large, and the consumer can satisfy the satisfaction of smoking in the state of heating and non-combustion. The combination of tobacco dry distillation and tobacco powder can significantly improve the sensory quality of the flue gas, so that the flue gas has excellent uniformity, aroma, concentration and strength; and the selective addition of other biomass powder can impart a unique aroma to the flue gas. Taste.
表1 烟草颗粒材料感官评价表(使用配套电加热烟具评价)Table 1 Sensory evaluation form of tobacco granules (evaluation using matching electric heating smoking ware)
颗粒配方组成Particle formulation 香气aroma 浓度concentration 劲头Energize 综合评价Overview
烟末+干馏香料Smoke + dry distillation spice A+A+ A++A++ A+A+ A+A+
烟末Smoke A-A- A-A- AA A-A-
本发明相比现有技术具有以下优点:The present invention has the following advantages over the prior art:
本发明提供的一种包含烟草颗粒的外围电加热气雾产生系统,通过加热烟草颗粒产生烟雾,能够产生类似于传统卷烟的效果。其烟弹外壳由金属套管和金属底座围成一个底部封闭的空间,加热段的烟草颗粒密封填装在该空间内,该烟弹与电加热烟杆配合,使用后将该烟弹直接从电加热烟杆内取出,烟弹的释烟材料完全不会残留在电加热烟杆内,不会污染电加热烟杆,因此无须对电加热烟杆进行清洁,使用非常方便,且烟弹更换抛弃后不会产生火灾隐患。The present invention provides a peripheral electrically heated aerosol generating system comprising tobacco particles which, by heating the tobacco particles, produces an effect similar to conventional cigarettes. The shell of the cartridge is surrounded by a metal sleeve and a metal base to form a bottom closed space, and the tobacco particles of the heating section are sealed and filled in the space, and the cartridge is matched with the electric heating rod, and the cartridge is directly used after being used. The electric heating rod is taken out, and the smoke releasing material of the cartridge does not remain in the electric heating rod, and does not pollute the electric heating rod. Therefore, the electric heating rod is not required to be cleaned, the use is very convenient, and the cartridge is replaced. There is no fire hazard after abandonment.
附图说明DRAWINGS
图1是本发明的整体结构示意图。BRIEF DESCRIPTION OF THE DRAWINGS Figure 1 is a schematic view showing the entire structure of the present invention.
图2是本发明的烟弹的结构示意图。2 is a schematic structural view of a cartridge of the present invention.
图3是本发明的电加热烟杆的结构示意图。Figure 3 is a schematic view showing the structure of an electrically heated tobacco rod of the present invention.
图4是实施例1制备的烟草颗粒材料与其他释烟材料如烟草薄片、烟末在加热不燃烧状态下(350℃)的烟气释放速率比较。Figure 4 is a comparison of the flue gas release rates of the tobacco particulate material prepared in Example 1 with other smoke releasing materials such as tobacco flakes and soot in a heat-non-combustible state (350 ° C).
图5是实施例1制备的烟草颗粒材料与其他释烟材料如烟草薄片、烟末在加热不燃烧状态下(350℃)的烟气释放量比较。Figure 5 is a comparison of the amount of smoke released from the tobacco particulate material prepared in Example 1 and other smoke releasing materials such as tobacco flakes and soot in a non-combustible state (350 ° C).
从图4、5中可以看出,烟草颗粒材料较烟草薄片和烟末的烟气释放速率和烟气释放量均具有明显的优势,在同等条件下,该烟草颗粒材料在加热不燃烧状态下烟气释放更快,烟气释放量更大。It can be seen from Figures 4 and 5 that the tobacco particulate material has obvious advantages over the flue gas release rate and the flue gas release amount of the tobacco flakes and the smoke. Under the same conditions, the tobacco particulate material is heated and not combusted. The smoke is released faster and the smoke is released more.
图6是实施例2制备的烟草颗粒材料与其他释烟材料如烟草薄片、烟末在加热不燃烧状态下(350℃)的烟气释放速率比较。Figure 6 is a comparison of the flue gas release rates of the tobacco particulate material prepared in Example 2 with other smoke releasing materials such as tobacco flakes and soot in a heat-non-combustible state (350 ° C).
图7是实施例2制备的烟草颗粒材料与其他释烟材料如烟草薄片、烟末在加热不燃烧状态下(350℃)的烟气释放量比较。Figure 7 is a comparison of the amount of smoke released from the tobacco particulate material prepared in Example 2 with other smoke releasing materials such as tobacco flakes and soot in a non-combustible state (350 ° C).
从图6、7中可以看出,烟草颗粒材料较烟草薄片和烟末的烟气释放速率和烟气释放量均具有明显的优势,在同等条件下,该烟草颗粒材料在加热不燃烧状态下烟气释放更快,烟气释放量更大。It can be seen from Figures 6 and 7 that the tobacco particulate material has obvious advantages over the flue gas release rate and the flue gas release amount of the tobacco flakes and the smoke. Under the same conditions, the tobacco particulate material is heated and not combusted. The smoke is released faster and the smoke is released more.
图中标号:1电加热烟杆,11烟杆本体,12容纳腔,13环形加热片,14底部加热片,15外通气孔,16充电接口,17开关,2烟弹,21金属套管,22过滤段,23加热段,24金属底座,25内通气孔。In the figure: 1 electric heating rod, 11 rod body, 12 housing cavity, 13 ring heating piece, 14 bottom heating piece, 15 outer vent, 16 charging interface, 17 switch, 2 cartridge, 21 metal sleeve, 22 filter section, 23 heating section, 24 metal base, 25 inner vent.
具体实施方式Detailed ways
下面对本发明的实施例作详细说明,本实施例在以本发明技术方案为前提下进行实施,给出了详细的实施方式和具体的操作过程,但本发明的保护范围不限于下述的实施例。The embodiments of the present invention are described in detail below. The present embodiment is implemented on the premise of the technical solution of the present invention, and detailed implementation manners and specific operation procedures are given, but the scope of protection of the present invention is not limited to the following implementation. example.
参见图1至图3,本实施例公开了一种包含烟草颗粒的外围电加热气雾产生系统,包括电加热烟杆1和插入电加热烟杆1内的烟弹2,Referring to FIG. 1 to FIG. 3, the embodiment discloses a peripheral electric heating aerosol generating system including tobacco particles, comprising an electric heating tobacco rod 1 and a cartridge 2 inserted into the electric heating tobacco rod 1.
烟弹2包括金属套管21、过滤段22和加热段23,金属套管21顶端敞口、底端通过一个金属底座24密封,过滤段22和加热段23呈上下排列设置在金属套管21内部的空腔内,加热段23底部依靠金属底座24来支撑,加热段23由烟草颗粒组成,金属套管21侧壁在对应加热段23的位置上开有内通气孔25,内通气孔25的孔径小于烟草颗粒的颗粒粒径,以避免烟草颗粒漏出来。The cartridge 2 includes a metal sleeve 21, a filter section 22 and a heating section 23. The top end of the metal sleeve 21 is open and the bottom end is sealed by a metal base 24, and the filter section 22 and the heating section 23 are arranged one above the other in the metal sleeve 21. In the inner cavity, the bottom of the heating section 23 is supported by the metal base 24, and the heating section 23 is composed of tobacco particles. The side wall of the metal sleeve 21 is provided with an inner vent hole 25 at the position corresponding to the heating section 23, and the inner vent hole 25 is provided. The pore size is smaller than the particle size of the tobacco particles to avoid leakage of the tobacco particles.
电加热烟杆1包括烟杆本体11,烟杆本体11上部设有顶端敞口的容纳腔12,容纳腔12深度小于烟弹2的加热段23的轴向长度。烟杆本体11的容纳腔12内设有电加热组件,电加热组件包括分布在容纳腔12内侧壁的环形加热片13、以及分布在容纳腔12底壁的底部加热片14,容纳腔12的腔体侧壁上开有外通气孔15;烟杆本体11内部设置有用于对电加热组件进行供电的电池,烟杆本体11上还设有用于对电池进行充电的充电接口16;烟杆本体11上还设有开关17,用于对电加热组件的启闭。The electrically heated tobacco rod 1 comprises a tobacco rod body 11 having an upper portion of the upper portion of the tobacco rod body 11 with an open top end, the receiving chamber 12 having a depth smaller than the axial length of the heating portion 23 of the cartridge 2. An electric heating assembly is disposed in the accommodating chamber 12 of the tobacco rod body 11. The electric heating assembly includes an annular heating piece 13 distributed on the inner side wall of the accommodating chamber 12, and a bottom heating piece 14 distributed on the bottom wall of the accommodating chamber 12, accommodating the chamber 12. An outer venting opening 15 is defined in the side wall of the cavity; a battery for supplying power to the electric heating component is disposed inside the tobacco rod body 11, and the charging rod 16 is further provided with a charging interface 16 for charging the battery; A switch 17 is also provided on the 11 for opening and closing the electric heating assembly.
烟弹2从上往下插入电加热烟杆1的容纳腔12内,通过环形加热片13对烟弹2的加热段23侧壁进行加热,通过底部加热片14对烟弹2的加热段23底部进行加热。The cartridge 2 is inserted into the accommodating chamber 12 of the electric heating rod 1 from the top to the bottom, and the side wall of the heating section 23 of the cartridge 2 is heated by the annular heating piece 13, and the heating section 23 of the cartridge 2 is passed through the bottom heating sheet 14. Heat the bottom.
其中,烟弹2的过滤段22所用材料可选择醋酸纤维滤棒、纸质滤棒、活性炭、铝箔、聚乳酸无纺布、聚乳酸薄膜、改性聚乳酸无纺布、改性聚乳酸薄膜中的种。金属套管21和金属底座24的材料可选择铜、铝、铝合金、铁、不锈钢中的至少一种。The material of the filter section 22 of the cartridge 2 can be selected from the group consisting of cellulose acetate filter rod, paper filter rod, activated carbon, aluminum foil, polylactic acid non-woven fabric, polylactic acid film, modified polylactic acid non-woven fabric and modified polylactic acid film. The species in it. The material of the metal sleeve 21 and the metal base 24 may be at least one selected from the group consisting of copper, aluminum, aluminum alloy, iron, and stainless steel.
使用时,将烟弹2从上往下插入电加热烟杆1的容纳腔12内,通过环形加热片13对烟弹2的加热段23侧壁进行加热,通过底部加热片14对烟弹2的加热段23底部进行加热,使烟草颗粒产生烟雾进行抽吸。本实施例实现了加热段23的外围和底部同时加热,加热更均匀。In use, the cartridge 2 is inserted into the accommodating chamber 12 of the electric heating rod 1 from top to bottom, and the side wall of the heating section 23 of the cartridge 2 is heated by the annular heating sheet 13 through the bottom heating sheet 14 to the cartridge 2 The bottom of the heating section 23 is heated to cause the tobacco particles to generate smoke for suction. In this embodiment, the periphery and the bottom of the heating section 23 are simultaneously heated, and the heating is more uniform.
本实施例通过加热烟草颗粒材料产生烟雾,能够产生类似于传统卷烟的效果。烟草颗粒 材料密封于烟弹2中,使用完不会残留和污染电加热烟杆1,不需要对电加热烟杆1进行清洁,且烟弹2更换抛弃后不会产生火灾隐患。This embodiment produces an effect similar to a conventional cigarette by heating the tobacco particulate material to generate smoke. The tobacco granule material is sealed in the cartridge 2, and the used electric heating rod 1 is not left and polluted after use, and the electric heating rod 1 is not required to be cleaned, and the rod 2 is replaced and discarded without causing fire hazard.
其中,烟草颗粒由以下质量百分比的原料构成:Among them, the tobacco particles are composed of the following mass percentages of raw materials:
烟草超微粉末40-60%,其他生物质粉末0-10%,烟草干馏物5-10%,雾化剂20-40%,粘结剂1-5%,余量为烟用香精香料。Tobacco ultrafine powder 40-60%, other biomass powder 0-10%, tobacco dry distillation 5-10%, atomizing agent 20-40%, binder 1-5%, the balance is tobacco flavors and fragrances.
本发明中使用的烟草干馏物的制备方法参考专利CN204579897U“一种可提升电子烟感官质量的亚微米烟颗粒制备装置”制备得到,具体制备方法如下:The preparation method of the tobacco dry distillation used in the invention is prepared by referring to the patent CN204579897U "a submicron smoke particle preparation device capable of improving the sensory quality of the electronic cigarette", and the specific preparation method is as follows:
在无氧气氛下,将烤烟、白肋烟、香料烟中的至少一种作为烟草原料,在200-400℃下进行干馏,馏出物经冷凝后收集,60℃减压浓缩至无水蒸气蒸出,所得残留产物即为烟草干馏物。In an oxygen-free atmosphere, at least one of flue-cured tobacco, burley tobacco, and oriental tobacco is used as a tobacco raw material, and is subjected to dry distillation at 200 to 400 ° C. The distillate is collected by condensation, and concentrated under reduced pressure at 60 ° C to anhydrous steam. Distilled, the resulting residual product is the tobacco dry distillation.
实施例1:Example 1:
本实施例中烟草颗粒的制备方法如下:The preparation method of the tobacco granules in this embodiment is as follows:
步骤1:取烤烟烟草粉末,用250μm筛网过筛,称取600g作为主料;分别称取烤烟烟草干馏物50g、丙三醇240g、丙二醇60g,瓜尔胶20g、明胶10g、麦芽糊精10g、烟用香精香料(薄荷香)10g于搅拌釜中,于1000rpm转速下搅拌15min,作为辅料;搅拌下向辅料中加入主料,室温下继续1000rpm转速下搅拌1h,得到预混物。Step 1: Take flue-cured tobacco powder, sieve with 250μm sieve, weigh 600g as main ingredient; weigh 50g of flue-cured tobacco dry distillation, 240g of glycerol, 60g of propylene glycol, 20g of guar gum, 10g of gelatin, maltodextrin 10 g, tobacco flavors and fragrances (mint) 10 g in a stirred tank, stirred at 1000 rpm for 15 min as an auxiliary material; the main ingredient was added to the auxiliary material under stirring, and stirring was continued at 1000 rpm for 1 h at room temperature to obtain a premix.
步骤2:将预混物倒入可加热、可通气的不锈钢反应罐中,从罐体上部通气孔中连续通入氮气,并保留出气孔为打开状态;醇化温度120℃,醇化时间2h,得到醇化物。Step 2: Pour the premix into a heated, ventilated stainless steel reaction tank, continuously pass nitrogen gas from the upper vent hole of the tank, and keep the pores open; the alcoholization temperature is 120 ° C, and the alcoholization time is 2 h. Alcohol.
步骤3:待醇化物冷却至室温后,送入螺杆挤出机中进行挤压成型,挤出速率5kg/h,孔直径0.7mm,获得挤出物。Step 3: After the alcoholate was cooled to room temperature, it was sent to a screw extruder for extrusion molding at an extrusion rate of 5 kg/h and a pore diameter of 0.7 mm to obtain an extrudate.
步骤4:将步骤3所得挤出物送入高速滚圆机进行滚圆造粒,转速2000rpm,得到粒径为0.7mm的湿颗粒材料,放入控温烘箱中,80℃下烘干至颗粒中含水率为5wt%,即得所需烟草颗粒。Step 4: The extrudate obtained in step 3 is sent to a high-speed rounding machine for spheronization and granulation at a speed of 2000 rpm to obtain a wet granular material having a particle diameter of 0.7 mm, placed in a temperature-controlled oven, and dried at 80 ° C to a water content in the granules. The rate was 5 wt%, which gave the desired tobacco particles.
利用锥形量热仪比较了该烟草颗粒材料与其他释烟材料如烟草薄片、烟末在加热不燃烧状态下(350℃)的烟气释放速率(图4)和烟气释放量(图5),从图中可以看出,烟草颗粒材料较烟草薄片和烟末的烟气释放速率和烟气释放量均具有明显的优势,在同等条件下,该烟草颗粒材料在加热不燃烧状态下烟气释放更快,烟气释放量更大。The flue gas release rate (Fig. 4) and the flue gas release rate (Fig. 5) of the tobacco particulate material and other smoke releasing materials such as tobacco sheets and cigarettes in a non-combustible state (Fig. 4) were compared by a cone calorimeter (Fig. 5). It can be seen from the figure that the tobacco particulate material has obvious advantages over the flue gas release rate and the flue gas release amount of the tobacco flakes and the smoke. Under the same conditions, the tobacco particulate material is smoked under heating and non-combustion conditions. The gas is released faster and the amount of smoke released is greater.
本实施例的烟草颗粒在加热不燃烧状态下,烟气释放速率快,释放量充足,具有显著的烤烟风格特征,并伴随轻若薄荷凉感,烟气满足感强,舒适性好。The tobacco granules of the present embodiment have a fast release rate of flue gas and a sufficient release amount in the state of heating and non-combustion, and have a distinctive flue-cured style characteristic, accompanied by a lightness of the mint, a strong sense of flue gas, and good comfort.
实施例2:Example 2:
本实施例中烟草颗粒的制备方法如下:The preparation method of the tobacco granules in this embodiment is as follows:
步骤1:分别称取经250μm筛网过筛的烤烟烟草粉末350g、白肋烟烟草粉末150g、陈皮粉末50g、乌梅粉末50g于搅拌釜中,转速500rpm搅拌20min,作为主料;分别称取烤烟烟草干馏物70g,白肋烟烟草干馏物10g、丙三醇250g、黄原胶20g、明胶10g、烟用香精香料(果香、可可香)40g于搅拌釜中,于1000rpm转速下搅拌15min,作为辅料;搅拌下向辅料中加入主料,室温下继续1000rpm转速下搅拌1h,得到预混物。Step 1: Weigh 350g of flue-cured tobacco powder sieved through a 250μm sieve, 150g of burley tobacco powder, 50g of dried tangerine peel powder, 50g of ebony powder in a stirred tank, stir at a speed of 500rpm for 20min, as the main material; weigh the flue-cured tobacco separately 70 g of dry distillation, 10 g of burley tobacco dry distillation, 250 g of glycerin, 20 g of xanthan gum, 10 g of gelatin, 40 g of flavors and flavors of tobacco (fruity flavor, cocoa), and stirred in a stirred tank at 1000 rpm for 15 min. Excipients; adding the main ingredient to the auxiliary material under stirring, stirring at 1000 rpm for 1 h at room temperature to obtain a premix.
步骤2:将预混物倒入可加热、可通气的不锈钢反应罐中,从罐体上部通气孔中连续通入氮气,并保留出气孔为打开状态;醇化温度100℃,醇化时间4h,得到醇化物。Step 2: Pour the premix into a heatable and ventilated stainless steel reaction tank, continuously pass nitrogen gas from the upper vent hole of the tank, and keep the pores open; the alcoholization temperature is 100 ° C, and the alcoholization time is 4 h. Alcohol.
步骤3:待醇化物冷却至室温后,送入螺杆挤出机中进行挤压成型,挤出速率6kg/h,孔直径0.8mm,获得挤出物。Step 3: After the alcoholate was cooled to room temperature, it was sent to a screw extruder for extrusion molding at an extrusion rate of 6 kg/h and a pore diameter of 0.8 mm to obtain an extrudate.
步骤4:将步骤3所得挤出物送入高速滚圆机进行滚圆造粒,转速1500rpm,得到粒径为0.8mm的湿颗粒材料,放入控温烘箱中,80℃下烘干至颗粒中含水率为3wt%,即得所需烟草颗粒。Step 4: The extrudate obtained in step 3 is sent to a high-speed rounding machine for spheronization granulation at a rotational speed of 1500 rpm to obtain a wet granular material having a particle diameter of 0.8 mm, placed in a temperature-controlled oven, and dried at 80 ° C to a water content in the granules. The rate was 3 wt%, which gave the desired tobacco particles.
利用锥形量热仪比较了该烟草颗粒材料与其他释烟材料如烟草薄片、烟末在加热不燃烧状态下(350℃)的烟气释放速率(图6)和烟气释放量(图7),从图中可以看出,烟草颗粒材料较烟草薄片和烟末的烟气释放速率和烟气释放量均具有明显的优势,在同等条件下,该烟草颗粒材料在加热不燃烧状态下烟气释放更快,烟气释放量更大。The flue gas release rate (Fig. 6) and the flue gas release rate (Fig. 6) of the tobacco particulate material and other smoke releasing materials such as tobacco sheets and cigarettes in a non-combustion state (Fig. 6) were compared by a cone calorimeter (Fig. 7). It can be seen from the figure that the tobacco particulate material has obvious advantages over the flue gas release rate and the flue gas release amount of the tobacco flakes and the smoke. Under the same conditions, the tobacco particulate material is smoked under heating and non-combustion conditions. The gas is released faster and the amount of smoke released is greater.
本实施例的烟草颗粒材料在加热不燃烧状态下,烟气释放速率快,释放量充足,具有显著的混合型烟草风格特征,并融合陈皮、乌梅的香气,烟气满足感强,舒适性好。The tobacco granule material of the present embodiment has a fast release rate of flue gas and a sufficient amount of release in the state of heating and non-combustion, and has remarkable mixed tobacco style characteristics, and combines the aroma of dried tangerine peel and ebony, and the smoke has a strong sense of satisfaction and good comfort. .
以上仅为本发明的较佳实施例而已,并不用以限制本发明,凡在本发明的精神和原则之内所作的任何修改、等同替换和改进等,均应包含在本发明的保护范围之内。The above are only the preferred embodiments of the present invention, and are not intended to limit the present invention. Any modifications, equivalents, and improvements made within the spirit and scope of the present invention should be included in the scope of the present invention. Inside.

Claims (10)

  1. 一种包含烟草颗粒的外围电加热气雾产生系统,其特征在于:包括电加热烟杆和插入电加热烟杆内的烟弹,A peripheral electric heating aerosol generating system comprising tobacco particles, comprising: an electrically heated tobacco rod and a cartridge inserted into the electrically heated tobacco rod,
    所述烟弹包括金属套管、过滤段和加热段,所述金属套管顶端敞口、底端通过一个金属底座密封,所述过滤段和加热段呈上下排列设置在金属套管内部的空腔内,所述加热段底部依靠金属底座来支撑,所述加热段由烟草颗粒组成,所述金属套管侧壁在对应加热段的位置上开有内通气孔;The cartridge includes a metal sleeve, a filter section and a heating section, and the top end of the metal sleeve is open and the bottom end is sealed by a metal base, and the filter section and the heating section are arranged in an up-and-down arrangement inside the metal sleeve. Inside the cavity, the bottom of the heating section is supported by a metal base, and the heating section is composed of tobacco particles, and the side wall of the metal sleeve has an inner vent hole at a position corresponding to the heating section;
    所述电加热烟杆包括烟杆本体,所述烟杆本体上部设有顶端敞口的容纳腔,所述烟杆本体的容纳腔内设有电加热组件,所述电加热组件包括分布在容纳腔内侧壁的环形加热片、以及分布在容纳腔底壁的底部加热片,所述容纳腔侧壁上开有外通气孔;The electric heating tobacco rod comprises a tobacco rod body, the upper portion of the tobacco rod body is provided with a receiving chamber with an open top end, and an electric heating assembly is arranged in the receiving chamber of the tobacco rod body, and the electric heating assembly comprises a distribution An annular heating piece of the inner side wall of the cavity, and a bottom heating piece distributed on the bottom wall of the accommodating cavity, and an outer vent hole is formed in the side wall of the accommodating cavity;
    所述烟弹从上往下插入所述电加热烟杆的容纳腔内,通过所述环形加热片对烟弹的加热段侧壁进行加热,通过所述底部加热片对烟弹的加热段底部进行加热;Inserting the cartridge into the receiving cavity of the electric heating rod from top to bottom, heating the side wall of the heating section of the cartridge through the annular heating sheet, and passing the bottom heating piece to the bottom of the heating section of the cartridge Heating;
    所述烟草颗粒由以下质量百分比的原料构成:The tobacco particles are composed of the following mass percentages of raw materials:
    烟草超微粉末40-60%,其他生物质粉末0-10%,烟草干馏物5-10%,雾化剂20-40%,粘结剂1-5%,余量为烟用香精香料。Tobacco ultrafine powder 40-60%, other biomass powder 0-10%, tobacco dry distillation 5-10%, atomizing agent 20-40%, binder 1-5%, the balance is tobacco flavors and fragrances.
  2. 如权利要求1所述的一种包含烟草颗粒的外围电加热气雾产生系统,其特征在于:所述烟弹的过滤段为纸质滤棒。A peripheral electrically heated aerosol generating system comprising tobacco particles according to claim 1 wherein the filter section of the cartridge is a paper filter plug.
  3. 如权利要求1所述的一种包含烟草颗粒的外围电加热气雾产生系统,其特征在于:所述烟杆本体内部设置有用于对电加热组件进行供电的电池,所述烟杆本体上还设有用于对电池进行充电的充电接口。A peripheral electric heating aerosol generating system comprising tobacco particles according to claim 1, wherein the tobacco rod body is internally provided with a battery for supplying power to the electric heating assembly, and the tobacco rod body is further A charging interface for charging the battery is provided.
  4. 如权利要求3所述的一种包含烟草颗粒的外围电加热气雾产生系统,其特征在于:所述烟杆本体上还设有开关。A peripheral electric heating aerosol generating system comprising tobacco particles according to claim 3, wherein the tobacco rod body is further provided with a switch.
  5. 如权利要求1所述的一种包含烟草颗粒的外围电加热气雾产生系统,其特征在于:所述电加热烟杆的容纳腔深度小于所述烟弹的加热段的轴向长度。A peripheral electrically heated aerosol generating system comprising tobacco particles according to claim 1 wherein said electrically heated tobacco rod has a receiving chamber depth that is less than an axial length of said heated section of said cartridge.
  6. 如权利要求1所述的一种包含烟草颗粒的外围电加热气雾产生系统,其特征在于:所述内通气孔的孔径小于所述烟草颗粒的颗粒粒径。A peripheral electrically heated aerosol generating system comprising tobacco particles according to claim 1 wherein said inner vent has a pore size smaller than a particle size of said tobacco particles.
  7. 如权利要求1所述的一种包含烟草颗粒的外围电加热气雾产生系统,其特征在于:所述烟草超微粉末选自烤烟、白肋烟、香料烟、膨胀烟、烟梗中的一种或几种;所述烟草超微粉末的粒径≤250μm。A peripheral electric heating aerosol generating system comprising tobacco particles according to claim 1, wherein said tobacco ultrafine powder is selected from the group consisting of flue-cured tobacco, burley tobacco, oriental tobacco, expanded tobacco, and tobacco stem. One or more; the tobacco ultrafine powder has a particle size of ≤250 μm.
  8. 如权利要求1所述的一种包含烟草颗粒的外围电加热气雾产生系统,其特征在于:所述其他生物质粉末选自陈皮、檀皮、乌梅、石斛、红薯、板栗、麦芽中的一种或几种;所述其他生物质粉末的粒径≤250μm。A peripheral electric heating aerosol generating system comprising tobacco particles according to claim 1, wherein said other biomass powder is selected from the group consisting of dried tangerine peel, sandalwood, ebony, sarcophagus, sweet potato, chestnut, and malt. One or more; the other biomass powder has a particle size of ≤250 μm.
  9. 如权利要求1所述的一种包含烟草颗粒的外围电加热气雾产生系统,其特征在于:所述其他生物质粉末的质量占烟草超微粉末质量的比例≤20%;所述烟草干馏物的质量占烟草超微粉末质量的5-20%。A peripheral electric heating aerosol generating system comprising tobacco particles according to claim 1, wherein: said other biomass powder has a mass ratio of tobacco ultrafine powder of ≤ 20%; said tobacco dry distillation The quality accounts for 5-20% of the quality of the ultrafine powder of tobacco.
  10. 如权利要求1所述的一种包含烟草颗粒的外围电加热气雾产生系统,其特征在于:A peripheral electric heating aerosol generating system comprising tobacco particles according to claim 1 wherein:
    所述雾化剂选自1,2-丙二醇、1,3-丁二醇、丙三醇中的一种或几种;The atomizing agent is selected from one or more of 1,2-propanediol, 1,3-butanediol, and glycerin;
    所述粘结剂选自淀粉、黄原胶、卡拉胶、明胶、瓜尔胶、麦芽糊精中的一种或几种。The binder is selected from one or more of starch, xanthan gum, carrageenan, gelatin, guar gum, and maltodextrin.
PCT/CN2018/088800 2017-12-22 2018-05-29 Peripheral electric heating aerosol generating system containing tobacco particles WO2019119731A1 (en)

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