CN105505584A - Extraction method of cape jasmine flower essential oil - Google Patents

Extraction method of cape jasmine flower essential oil Download PDF

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Publication number
CN105505584A
CN105505584A CN201510876062.3A CN201510876062A CN105505584A CN 105505584 A CN105505584 A CN 105505584A CN 201510876062 A CN201510876062 A CN 201510876062A CN 105505584 A CN105505584 A CN 105505584A
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CN
China
Prior art keywords
flower
essential oil
capa jasmine
capa
cape jasmine
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201510876062.3A
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Chinese (zh)
Inventor
魏玉宝
魏洁琼
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
ZHENJIANG DANTU DISTRICT NANSHAN XIYUAN TEA PROFESSIONAL COOPERATIVES
Original Assignee
ZHENJIANG DANTU DISTRICT NANSHAN XIYUAN TEA PROFESSIONAL COOPERATIVES
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by ZHENJIANG DANTU DISTRICT NANSHAN XIYUAN TEA PROFESSIONAL COOPERATIVES filed Critical ZHENJIANG DANTU DISTRICT NANSHAN XIYUAN TEA PROFESSIONAL COOPERATIVES
Priority to CN201510876062.3A priority Critical patent/CN105505584A/en
Publication of CN105505584A publication Critical patent/CN105505584A/en
Pending legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/02—Recovery or refining of essential oils from raw materials
    • C11B9/025—Recovery by solvent extraction
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/02—Recovery or refining of essential oils from raw materials
    • C11B9/022—Refining
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/02—Recovery or refining of essential oils from raw materials
    • C11B9/027—Recovery of volatiles by distillation or stripping

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Fats And Perfumes (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

The invention relates to an extraction method of cape jasmine flower essential oil and belongs to the technical field of processing of agricultural products. The cape jasmine flower essential oil can clear heat, purge pathogenic fire, cool blood and stop bleeding. The fragrance of the cape jasmine flower essential oil is faint and pleasant and is especially suitable for Chinese. The cape jasmine flower essential oil is extracted with a microwave extraction-vapor distillation method; the method comprises the following steps collection, transportation and storage, microwave extraction, a vapor distillation method, refinement and the like, the cape jasmine flower essential oil can be effectively extracted, and the blank of the market can be filled up. The extraction method comprises collection of cape jasmine flowers, transportation and storage, pre-treatment, microwave extraction, vapor distillation extraction, refinement and the like.

Description

A kind of extracting method of flower of Capa Jasmine essential oil
Technical field
The present invention relates to a kind of extracting method of flower of Capa Jasmine essential oil, belong to technical field of agricultural product process.
Background technology
Flower of Capa Jasmine (formal name used at school: Gardeniajasminoides), originates in China, and cultivating and growing is comparatively easy, containing volatile oil, comprises jasmal, phanteine, another containing pigment glucoside, C6H14O6 etc.Flower of Capa Jasmine essential oil heat-clearing and fire-purging, cooling blood for hemostasis.Flower of Capa Jasmine essential oil fragrance is simple and elegant pleasant, is especially applicable to Chinese's odor type.
Although flower of Capa Jasmine is more in China, the flower of Capa Jasmine florescence is of short duration, not easily retains, and market flower of Capa Jasmine essential oil is comparatively rare.The present invention, with microwave extracting-extraction by steam distillation flower of Capa Jasmine essential oil, relates to technique and comprises: gather, transport with preservation, microwave extracting, steam distillation and refine etc. step, effectively can extract flower of Capa Jasmine essential oil, fill a hole in the market.
Summary of the invention
The present invention, with microwave extracting-extraction by steam distillation cape jasmine anthosin, relates to technique and comprises: collect, transport with preservation, microwave extracting, steam distillation and refine etc. step, effectively can extract flower of Capa Jasmine essential oil, fill a hole in the market.Summary of the invention comprises: the collection of flower of Capa Jasmine, transport is with preservation, pre-treatment, microwave extracting, water vapour distillation and refine.
Embodiment
1. collect: the flower of Capa Jasmine gathering open 1-2 days is raw material, lucifuge, insulation;
2. transport and preservation: the flower of Capa Jasmine collected is sealed low temperature-2 DEG C and is transported to preservation in freezer, for subsequent use;
3. pre-treatment: it is in the ethanolic soln of 70% that the flower of Capa Jasmine of collecting preservation is soaked in mass concentration, stirs 1 hour at 40-50 DEG C, and cooling, collects pretreated flower of Capa Jasmine petal
4. microwave extracting: pretreated flower of Capa Jasmine petal being placed in mass concentration is that the ethanol of 75-80% carries out microwave extracting, arranging microwave output power is 400w, 10 minutes microwave time was set, filtering flower of Capa Jasmine petal residue after cooling, collect extracting solution, and by extracting solution concentrating under reduced pressure, deliver to gas chromatograph and detect without ethanol.
5. water vapour distillation: add water in water vapor distillation apparatus, is heated to boiling, then adds step 4 and obtain extracting solution, reflux, collects distillation fraction, naturally cooling; The distillation fraction collected is joined in rectifier unit, is heated to boiling reflux, collect the rectifying cut of 90 DEG C to 95 DEG C.
6. refining: the flower of Capa Jasmine rectifying cut obtained by water vapour distillation is cooled to 2-5 DEG C, join in the ethyl acetate of same temperature and the mixed solution of water, this temperature is kept to stir, stratification, collected organic layer, in organic layer, add anhydrous magnesium sulfate and stir, leave standstill, filter, filtrate reduced in volume, deliver to gas chromatograph and detect no solvent residue, obtain flower of Capa Jasmine essential oil.

Claims (5)

1. an extracting method for flower of Capa Jasmine essential oil, is characterized in that: flower of Capa Jasmine essential oil heat-clearing and fire-purging, cooling blood for hemostasis;
Flower of Capa Jasmine essential oil fragrance is simple and elegant pleasant, is especially applicable to Chinese's odor type;
Invention with microwave extracting-extraction by steam distillation cape jasmine anthosin, relate to technique and comprise: collect, transport with preservation, microwave extracting, steam distillation and refine etc. step, effectively can extract flower of Capa Jasmine essential oil, fill a hole in the market; Summary of the invention comprises: 1. the collection of Cape jasmine flower; 2. transport and preservation; 3. pre-treatment; 4. microwave extracting; 5. water vapour distillation; 6. refine.
2. the method according to claims 1, it is characterized in that: described pre-treatment refers to: it is in the ethanolic soln of 70% that the flower of Capa Jasmine of collecting preservation is soaked in mass concentration, stir 1 hour at 40-50 DEG C, cooling, collects pretreated flower of Capa Jasmine petal.
3. the method according to claims 1, it is characterized in that: described microwave extracting refers to: pretreated flower of Capa Jasmine petal being placed in mass concentration is that the ethanol of 75-80% carries out microwave extracting, arranging microwave output power is 400w, 10 minutes microwave time was set, filtering flower of Capa Jasmine petal residue after cooling, collect extracting solution, and by extracting solution concentrating under reduced pressure, deliver to gas chromatograph and detect without ethanol.
4. the method according to claims 1, is characterized in that: described water vapour distillation refers to: in water vapor distillation apparatus, add water, is heated to boiling, then adds step 4 and obtain extracting solution, reflux, collects distillation fraction, naturally cooling; The distillation fraction collected is joined in rectifier unit, is heated to boiling reflux, collect the rectifying cut of 90 DEG C to 95 DEG C.
5. the method according to claims 1, it is characterized in that: described the refining of flower of Capa Jasmine essential oil refers to: the flower of Capa Jasmine rectifying cut obtained by water vapour distillation is cooled to 2-5 DEG C, joins in the ethyl acetate of same temperature and the mixed solution of water, keeps this temperature to stir, stratification, collected organic layer, adds anhydrous magnesium sulfate and stirs in organic layer, leaves standstill, filter, filtrate reduced in volume, delivers to gas chromatograph and detects no solvent residue, obtain flower of Capa Jasmine essential oil.
CN201510876062.3A 2015-12-03 2015-12-03 Extraction method of cape jasmine flower essential oil Pending CN105505584A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201510876062.3A CN105505584A (en) 2015-12-03 2015-12-03 Extraction method of cape jasmine flower essential oil

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201510876062.3A CN105505584A (en) 2015-12-03 2015-12-03 Extraction method of cape jasmine flower essential oil

Publications (1)

Publication Number Publication Date
CN105505584A true CN105505584A (en) 2016-04-20

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Family Applications (1)

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CN201510876062.3A Pending CN105505584A (en) 2015-12-03 2015-12-03 Extraction method of cape jasmine flower essential oil

Country Status (1)

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CN (1) CN105505584A (en)

Cited By (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106221933A (en) * 2016-08-26 2016-12-14 广西灏源盛世生物科技有限公司 A kind of extraction process for Juniperus rigida Sieb.et Zucc. quintessence oil
CN106244326A (en) * 2016-08-26 2016-12-21 广西灏源盛世生物科技有限公司 A kind of Herba Cymbopogonis Citrari extraction of essential oil processing technique
CN106281703A (en) * 2016-08-26 2017-01-04 广西灏源盛世生物科技有限公司 A kind of extracting method of Bergamot
CN106318630A (en) * 2016-08-26 2017-01-11 广西灏源盛世生物科技有限公司 Method for extracting Arabian jasmine flower essential oil
CN106350221A (en) * 2016-08-26 2017-01-25 广西灏源盛世生物科技有限公司 Processing technique for extracting Cinnamomum camphora essential oil
CN106590019A (en) * 2016-10-21 2017-04-26 南阳理工学院 Odor source analysis and removal method of gardenia yellow pigment
CN109777623A (en) * 2019-03-15 2019-05-21 宁夏师范学院 A kind of method that microwave-assisted steam distillation extracts Rosemary Oil
CN109797044A (en) * 2017-11-16 2019-05-24 镇江市丹徒区南山溪园茶叶专业合作社 A kind of extracting method of jasmine essential oil
CN110373269A (en) * 2019-07-05 2019-10-25 福建省农业科学院作物研究所 A method of cape jasmine flower essential oil is prepared with waste liquid
CN110591823A (en) * 2019-09-29 2019-12-20 河南中医药大学 Extraction and separation method of gardenia volatile oil
CN112056613A (en) * 2020-09-07 2020-12-11 广西中烟工业有限责任公司 Preparation method of cigarette filter stick with gardenia fragrance
CN112293744A (en) * 2020-11-18 2021-02-02 河北中烟工业有限责任公司 Extraction method of fresh lotus flower syrup
CN114032146A (en) * 2021-11-25 2022-02-11 浙江骄栀科技有限公司 Fine filtering device for extracting gardenia essential oil and fine filtering method thereof
CN117297988A (en) * 2023-11-29 2023-12-29 江西中妆检验检测中心有限公司 Amino acid facial cleanser and preparation method thereof

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104164302A (en) * 2014-09-04 2014-11-26 南京标科生物科技有限公司 Extraction method of gardenia jasminoides volatile oil
CN104312732A (en) * 2014-11-20 2015-01-28 邯郸学院 Extraction method for fructus forsythia volatile oil

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104164302A (en) * 2014-09-04 2014-11-26 南京标科生物科技有限公司 Extraction method of gardenia jasminoides volatile oil
CN104312732A (en) * 2014-11-20 2015-01-28 邯郸学院 Extraction method for fructus forsythia volatile oil

Cited By (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106244326A (en) * 2016-08-26 2016-12-21 广西灏源盛世生物科技有限公司 A kind of Herba Cymbopogonis Citrari extraction of essential oil processing technique
CN106281703A (en) * 2016-08-26 2017-01-04 广西灏源盛世生物科技有限公司 A kind of extracting method of Bergamot
CN106318630A (en) * 2016-08-26 2017-01-11 广西灏源盛世生物科技有限公司 Method for extracting Arabian jasmine flower essential oil
CN106350221A (en) * 2016-08-26 2017-01-25 广西灏源盛世生物科技有限公司 Processing technique for extracting Cinnamomum camphora essential oil
CN106221933A (en) * 2016-08-26 2016-12-14 广西灏源盛世生物科技有限公司 A kind of extraction process for Juniperus rigida Sieb.et Zucc. quintessence oil
CN106590019B (en) * 2016-10-21 2021-07-27 南阳理工学院 Method for analyzing and removing peculiar smell source of gardenia yellow pigment
CN106590019A (en) * 2016-10-21 2017-04-26 南阳理工学院 Odor source analysis and removal method of gardenia yellow pigment
CN109797044A (en) * 2017-11-16 2019-05-24 镇江市丹徒区南山溪园茶叶专业合作社 A kind of extracting method of jasmine essential oil
CN109777623A (en) * 2019-03-15 2019-05-21 宁夏师范学院 A kind of method that microwave-assisted steam distillation extracts Rosemary Oil
CN110373269A (en) * 2019-07-05 2019-10-25 福建省农业科学院作物研究所 A method of cape jasmine flower essential oil is prepared with waste liquid
CN110591823A (en) * 2019-09-29 2019-12-20 河南中医药大学 Extraction and separation method of gardenia volatile oil
CN112056613A (en) * 2020-09-07 2020-12-11 广西中烟工业有限责任公司 Preparation method of cigarette filter stick with gardenia fragrance
CN112293744A (en) * 2020-11-18 2021-02-02 河北中烟工业有限责任公司 Extraction method of fresh lotus flower syrup
CN114032146A (en) * 2021-11-25 2022-02-11 浙江骄栀科技有限公司 Fine filtering device for extracting gardenia essential oil and fine filtering method thereof
CN117297988A (en) * 2023-11-29 2023-12-29 江西中妆检验检测中心有限公司 Amino acid facial cleanser and preparation method thereof

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Application publication date: 20160420