CN105505040A - Emulsion paint and preparation method thereof - Google Patents
Emulsion paint and preparation method thereof Download PDFInfo
- Publication number
- CN105505040A CN105505040A CN201511011570.1A CN201511011570A CN105505040A CN 105505040 A CN105505040 A CN 105505040A CN 201511011570 A CN201511011570 A CN 201511011570A CN 105505040 A CN105505040 A CN 105505040A
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- China
- Prior art keywords
- parts
- emulsion
- polyvinyl acetate
- stirring
- emulsion paint
- Prior art date
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D131/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an acyloxy radical of a saturated carboxylic acid, of carbonic acid, or of a haloformic acid; Coating compositions based on derivatives of such polymers
- C09D131/02—Homopolymers or copolymers of esters of monocarboxylic acids
- C09D131/04—Homopolymers or copolymers of vinyl acetate
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/02—Emulsion paints including aerosols
- C09D5/022—Emulsions, e.g. oil in water
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Dispersion Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Paints Or Removers (AREA)
Abstract
The invention discloses emulsion paint. The emulsion paint is prepared from the following raw materials in parts by weight: 15 to 25 parts of polyvinyl acetate emulsion, 10 to 15 parts of rutile titanium dioxide, 5 to 9 parts of lithopone, 2 to 6 parts of acrylonitrile, 6 to 9 parts of wollastonite powder, 7 to 9 parts of deionized water, 2 to 9 parts of tridecylic aldehyde and 2.5 to 7.4 parts of nonylphenol polyoxyethylene ether. Compared with an existing product, because of the addition of the polyvinyl acetate emulsion, the emulsion paint disclosed by the invention not only is healthy and environmental-friendly, but also is convenient in use; because of the addition of the rutile titanium dioxide and the lithopone, transportation and storage are convenient, and the emulsion paint is environmental-friendly and non-toxic because no preservative is added; because of the addition of the wollastonite powder and the tridecylic aldehyde, the drying speed is fast, fragrance can also be permanently maintained, and the air can be purified.
Description
Technical field
The present invention relates to a kind of emulsion paint and preparation method thereof, belong to building coating field.
Background technology
At present, the kind of the coating used in daily finishing is a lot, emulsion paint is one of current most popular wall decoration material, along with improving constantly of standard of living, people also just increase the requirement of finishing material thereupon, and existing coating variety is various, and what have is unfavorable for construction, some performances can not be satisfied the demand, and what also have is larger to the injury of human body.
Summary of the invention
For the deficiency that prior art exists, technical problem to be solved by this invention is, provides a kind of emulsion paint and preparation method thereof, solves the defect of currently available products, energy-conserving and environment-protective.
For solving the problems of the technologies described above, the technical scheme that the present invention takes is, a kind of emulsion paint, is made up of the raw material of following parts by weight: polyvinyl acetate emulsion 15-25 part, rutile titanium white powder 10-15 part, zinc sulfide white 5-9 part, vinyl cyanide 2-6 part, wollastonite powder 6-9 part, deionized water 7-9 part, tridecyl aldehyde 2-9 part and polyoxyethylene nonylphenol ether 2.5-7.4 part.
Optimize, above-mentioned emulsion paint, is made up of the raw material of following parts by weight: polyvinyl acetate emulsion 19 parts, 13 parts, rutile titanium white powder, 7 parts, zinc sulfide white, vinyl cyanide 5 parts, wollastonite powder 8 parts, deionized water 8 parts, tridecyl aldehyde 6 parts and polyoxyethylene nonylphenol ether 4.7 parts.
A preparation method for emulsion paint, comprises the following steps:
1) weigh according to formula, slowly poured in the agitator that rutile titanium white powder and zinc sulfide white are housed by the polyvinyl acetate emulsion of 60%, then add deionized water, stirring stirs evenly, then pours remaining polyvinyl acetate emulsion into, continues to stir until furnishing emulsion form;
2) then add vinyl cyanide and the wollastonite powder of formula ratio, stir under the speed of 50-60r/min, after stirring, heat gradually, when being heated to 75-85 DEG C, improving stirring velocity to 80-100r/min, stirring 13-15 minute;
3) add the tridecyl aldehyde of formula ratio again, keep stirring velocity to 80-100r/min, stir 15-20 minute;
4) after, cooling, when temperature drops to 55-65 DEG C, adds polyoxyethylene nonylphenol ether, and the stirring velocity of 1000r/min stirs 20min, mixes, is then cooled to room temperature and is finished product.
The present invention, compared with existing product, adds polyvinyl acetate emulsion, not only health environment-friendly but also easy to use; Add rutile titanium white powder and zinc sulfide white, transport and storage conveniently, and do not add any sanitas, environment-protecting asepsis; Add wollastonite powder and tridecyl aldehyde, rate of drying is fast, can also leave fragrance enduringly, purify air.
Embodiment
embodiment 1
The present invention is a kind of emulsion paint, is made up of the raw material of following parts by weight: polyvinyl acetate emulsion 15 parts, 10 parts, rutile titanium white powder, 5 parts, zinc sulfide white, vinyl cyanide 2 parts, wollastonite powder 6 parts, deionized water 7 parts, tridecyl aldehyde 2 parts and polyoxyethylene nonylphenol ether 2.5 parts.
A preparation method for emulsion paint, comprises the following steps:
1) weigh according to formula, slowly poured in the agitator that rutile titanium white powder and zinc sulfide white are housed by the polyvinyl acetate emulsion of 60%, then add deionized water, stirring stirs evenly, then pours remaining polyvinyl acetate emulsion into, continues to stir until furnishing emulsion form;
2) then add vinyl cyanide and the wollastonite powder of formula ratio, stir under the speed of 50r/min, after stirring, heat gradually, when being heated to 75 DEG C, improving stirring velocity to 80r/min, stirring 13 minutes;
3) add the tridecyl aldehyde of formula ratio again, keep stirring velocity to 80r/min, stir 15 minutes;
4) after, cooling, when temperature drops to 55 DEG C, adds polyoxyethylene nonylphenol ether, and the stirring velocity of 1000r/min stirs 20min, mixes, is then cooled to room temperature and is finished product.
embodiment 2
The present invention is a kind of emulsion paint, is made up of the raw material of following parts by weight: polyvinyl acetate emulsion 25 parts, 15 parts, rutile titanium white powder, 9 parts, zinc sulfide white, vinyl cyanide 6 parts, wollastonite powder 9 parts, deionized water 9 parts, tridecyl aldehyde 9 parts and polyoxyethylene nonylphenol ether 7.4 parts.
A preparation method for emulsion paint, comprises the following steps:
1) weigh according to formula, slowly poured in the agitator that rutile titanium white powder and zinc sulfide white are housed by the polyvinyl acetate emulsion of 60%, then add deionized water, stirring stirs evenly, then pours remaining polyvinyl acetate emulsion into, continues to stir until furnishing emulsion form;
2) then add vinyl cyanide and the wollastonite powder of formula ratio, stir under the speed of 60r/min, after stirring, heat gradually, when being heated to 85 DEG C, improving stirring velocity to 100r/min, stirring 15 minutes;
3) add the tridecyl aldehyde of formula ratio again, keep stirring velocity to 100r/min, stir 20 minutes;
4) after, cooling, when temperature drops to 65 DEG C, adds polyoxyethylene nonylphenol ether, and the stirring velocity of 1000r/min stirs 20min, mixes, is then cooled to room temperature and is finished product.
embodiment 3
The present invention is a kind of emulsion paint, is made up of the raw material of following parts by weight: polyvinyl acetate emulsion 19 parts, 13 parts, rutile titanium white powder, 7 parts, zinc sulfide white, vinyl cyanide 5 parts, wollastonite powder 8 parts, deionized water 8 parts, tridecyl aldehyde 6 parts and polyoxyethylene nonylphenol ether 4.7 parts.
A preparation method for emulsion paint, comprises the following steps:
1) weigh according to formula, slowly poured in the agitator that rutile titanium white powder and zinc sulfide white are housed by the polyvinyl acetate emulsion of 60%, then add deionized water, stirring stirs evenly, then pours remaining polyvinyl acetate emulsion into, continues to stir until furnishing emulsion form;
2) then add vinyl cyanide and the wollastonite powder of formula ratio, stir under the speed of 55r/min, after stirring, heat gradually, when being heated to 78 DEG C, improving stirring velocity to 90r/min, stirring 14 minutes;
3) add the tridecyl aldehyde of formula ratio again, keep stirring velocity to 90r/min, stir 18 minutes;
4) after, cooling, when temperature drops to 58 DEG C, adds polyoxyethylene nonylphenol ether, and the stirring velocity of 1000r/min stirs 20min, mixes, is then cooled to room temperature and is finished product.
Contrasted by coating finished product in the coating finished product produced in above-described embodiment 1-3 and prior art, detected result is as follows:
The evaluation of application property is difficult to floating coating thickness for standard with obviously sagging during the thick painting of visual inspection generation with during scumbling;
Water-permeable evaluation is tested with reference to JISA6909;
Water tolerance evaluation is soaked in the warm water of 50 DEG C, to occur that the obvious albefaction time is for standard;
Freeze-thaw resistance evaluation is soaked 1 hour in 10 DEG C of water after coating is freezed 2h under-20 DEG C of environment, so repeatedly, to occur significantly ftractureing back number for standard;
Curing shrinkage rate is measured after 30 days in coating standing and drying.Through the interior wall paint that formula of the present invention and preparation technology obtain, there is excellent use properties and workability, the service requirements day by day improved can be met.
Can find out, the indices of coating of the present invention, considerably beyond GB, has higher ultimate compression strength and cohesive strength, water-tolerant.Compared with existing product, add polyvinyl acetate emulsion, not only health environment-friendly but also easy to use; Add rutile titanium white powder and zinc sulfide white, transport and storage conveniently, and do not add any sanitas, environment-protecting asepsis; Add wollastonite powder and tridecyl aldehyde, rate of drying is fast, can also leave fragrance enduringly, purify air.
To the above-mentioned explanation of the disclosed embodiments, professional and technical personnel in the field are realized or uses the present invention.To be apparent for those skilled in the art to the multiple amendment of these embodiments, General Principle as defined herein can without departing from the spirit or scope of the present invention, realize in other embodiments.Therefore, the present invention can not be restricted to these embodiments shown in this article, but will meet the widest scope consistent with principle disclosed herein and features of novelty.
Claims (3)
1. an emulsion paint, is characterized in that: be made up of the raw material of following parts by weight: polyvinyl acetate emulsion 15-25 part, rutile titanium white powder 10-15 part, zinc sulfide white 5-9 part, vinyl cyanide 2-6 part, wollastonite powder 6-9 part, deionized water 7-9 part, tridecyl aldehyde 2-9 part and polyoxyethylene nonylphenol ether 2.5-7.4 part.
2. emulsion paint according to claim 1, is made up of the raw material of following parts by weight: polyvinyl acetate emulsion 19 parts, 13 parts, rutile titanium white powder, 7 parts, zinc sulfide white, vinyl cyanide 5 parts, wollastonite powder 8 parts, deionized water 8 parts, tridecyl aldehyde 6 parts and polyoxyethylene nonylphenol ether 4.7 parts.
3. the preparation method of the emulsion paint according to claims 1 or 2, comprises the following steps:
1) weigh according to formula, slowly poured in the agitator that rutile titanium white powder and zinc sulfide white are housed by the polyvinyl acetate emulsion of 60%, then add deionized water, stirring stirs evenly, then pours remaining polyvinyl acetate emulsion into, continues to stir until furnishing emulsion form;
2) then add vinyl cyanide and the wollastonite powder of formula ratio, stir under the speed of 50-60r/min, after stirring, heat gradually, when being heated to 75-85 DEG C, improving stirring velocity to 80-100r/min, stirring 13-15 minute;
3) add the tridecyl aldehyde of formula ratio again, keep stirring velocity to 80-100r/min, stir 15-20 minute;
4) after, cooling, when temperature drops to 55-65 DEG C, adds polyoxyethylene nonylphenol ether, and the stirring velocity of 1000r/min stirs 20min, mixes, is then cooled to room temperature and is finished product.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201511011570.1A CN105505040A (en) | 2015-12-30 | 2015-12-30 | Emulsion paint and preparation method thereof |
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CN201511011570.1A CN105505040A (en) | 2015-12-30 | 2015-12-30 | Emulsion paint and preparation method thereof |
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CN105505040A true CN105505040A (en) | 2016-04-20 |
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CN201511011570.1A Pending CN105505040A (en) | 2015-12-30 | 2015-12-30 | Emulsion paint and preparation method thereof |
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Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1793248A (en) * | 2005-12-31 | 2006-06-28 | 天津绿屋涂料有限公司 | Internal and external wall lastex paint containing whey protein and production process thereof |
CN102153933A (en) * | 2011-05-13 | 2011-08-17 | 华东理工大学 | Preparation method for vibration-damping and noise-reducing coating composition |
CN103897522A (en) * | 2014-03-27 | 2014-07-02 | 桂林市和鑫防水装饰材料有限公司 | Water-based environment-friendly non-toxic and harmless elastic waterproof emulsion and preparation method thereof |
CN104140722A (en) * | 2014-07-29 | 2014-11-12 | 南京师范大学 | Needle-shaped wollastonite filling modification emulsion coating formula |
CN104877481A (en) * | 2015-04-29 | 2015-09-02 | 苏州市湘园特种精细化工有限公司 | Polyvinyl acetate coating and preparation method thereof |
-
2015
- 2015-12-30 CN CN201511011570.1A patent/CN105505040A/en active Pending
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1793248A (en) * | 2005-12-31 | 2006-06-28 | 天津绿屋涂料有限公司 | Internal and external wall lastex paint containing whey protein and production process thereof |
CN102153933A (en) * | 2011-05-13 | 2011-08-17 | 华东理工大学 | Preparation method for vibration-damping and noise-reducing coating composition |
CN103897522A (en) * | 2014-03-27 | 2014-07-02 | 桂林市和鑫防水装饰材料有限公司 | Water-based environment-friendly non-toxic and harmless elastic waterproof emulsion and preparation method thereof |
CN104140722A (en) * | 2014-07-29 | 2014-11-12 | 南京师范大学 | Needle-shaped wollastonite filling modification emulsion coating formula |
CN104877481A (en) * | 2015-04-29 | 2015-09-02 | 苏州市湘园特种精细化工有限公司 | Polyvinyl acetate coating and preparation method thereof |
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Application publication date: 20160420 |
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