CN105496906A - Aloe and konjac glucomannan facial mask and preparation method thereof - Google Patents

Aloe and konjac glucomannan facial mask and preparation method thereof Download PDF

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Publication number
CN105496906A
CN105496906A CN201610063469.9A CN201610063469A CN105496906A CN 105496906 A CN105496906 A CN 105496906A CN 201610063469 A CN201610063469 A CN 201610063469A CN 105496906 A CN105496906 A CN 105496906A
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Prior art keywords
aloe
preparation
konjac glucomannan
rhizoma amorphophalli
membrane
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CN201610063469.9A
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CN105496906B (en
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庞杰
王敏
穆若郡
马真
黄荣勋
谭小丹
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Zhuhai Jijia century Daily Chemical Co., Ltd
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Fujian Agriculture and Forestry University
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Dermatology (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Engineering & Computer Science (AREA)
  • Biotechnology (AREA)
  • Botany (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Cosmetics (AREA)

Abstract

The invention relates to an aloe and konjac glucomannan facial mask and a preparation method thereof. The preparation method of the aloe konjac glucomannan facial mask comprises the steps of preparation of an aloe extract, preparation of a film agent, compounding of konjac glucomannan and xanthan gum, preparation of a film, stripping soaking, sterilization and packaging. The superior film-forming property, water-retaining property, water absorbability and antibiotic property of konjac glucomannan and the anti-inflammatory, whitening and moisturizing functions of aloe are fully utilized to prepare the aloe and konjac glucomannan facial mask, so that the prepared aloe and konjac glucomannan facial mask has not only excellent fitting property but also favorable water replenishing and whitening effects, is healthy, environment-friendly and fashionable. The cost of the konjac glucomannan complex gum is lower than that of traditional algin products, the raw materials are nontoxic and healthy, and the aloe and konjac glucomannan facial mask is suitable for people of various skin; as a small quantity of konjac glucomannan is added into the film agent, the viscosity is increased, the probability of dripping during use is low, much convenience and safety are achieved and the effect is remarkable.

Description

Aloe Rhizoma amorphophalli glucomannan facial film and preparation method thereof
Technical field
The present invention relates to a kind of cosmetics and preparation method thereof, be specifically related to a kind of Aloe Rhizoma amorphophalli glucomannan facial film and preparation method thereof, belong to cosmetic field.
Background technology
Facial film is the indispensable cosmetic product of women of liking to be beautiful in the modern times, and facial film pattern is in the market single, mostly is mounted facial film, and general mounted facial film in use cannot fit tightly various shape of face, easy landing; In addition, mostly the main material of mounted facial film popular on market is non-woven fabrics, and production cost is higher, and non-woven fabrics absorption affinity is not enough, and essence easily drips.Compared with mounted facial film, paste daubing-type facial mask easily meets the needs of various shape of face, but cream pack product in the market adds too much chemicals in process of production usually, like this, not only can damage skin, also can be detrimental to health.Self-made face pack, use safety, but manufacturing process is more time-consuming, and due to raw material problem, effect is often not good.
Application number is patent of invention " a kind of aloe face pack " (applying date: 2014.10.04) of 201410518587.5, with Margarita powder 6% ~ 10%, Aloe 2% ~ 5%, asiaticoside 1% ~ 5%, the facial film of the weight proportion making of Cucumber 1% ~ 6%, whole production technology is simple, non-stimulated, be applicable to sensitive skin and use, but Margarita powder cost is high, essence viscosity is little, easily drips during use.
Application number is patent of invention " a kind of konjac facial mask " (applying date: 2008.11.24) of 200810158986.X, and face pack prescription is Rhizoma amorphophalli 15 ~ 20%, Kaolin 10 ~ 12%, zinc oxide 1.8 ~ 2.0%, ethanol 4.0 ~ 6.0%, sodium alginate 2.0 ~ 3.0%, carboxymethyl cellulose 0.8 ~ 1.0%, ermine oil 2.0 ~ 2.2%, propylene glycol 3.0 ~ 4.0%, antiseptic 0.01 ~ 0.03%, essence 0.3 ~ 0.6%, surplus are deionized water.This facial film has good oxidation resistance, and energy slowing down skin aging, but complicated component, be not suitable for sensitive-skinned crowd, and cost is higher.
Along with expanding economy, improving constantly of rhythm of life, the requirement of people to cosmetics has developed into the aspect of healthy facility, environment-friendly high-efficiency, but on market, most of facial film can not meet these requirements simultaneously.
Summary of the invention
The object of this invention is to provide a kind of Aloe Rhizoma amorphophalli glucomannan facial film and preparation method thereof.The present invention with Rhizoma amorphophalli glucomannan and Aloe for main material, utilize the film property of Rhizoma amorphophalli glucomannan, water-retaining property, water absorption, the antiinflammatory of antibiotic property and Aloe, whitening, moisture-keeping functions, and be aided with other thickening agents (xanthan gum), synergist (sodium carboxymethyl cellulose), make film-formation result good, pliability is good, skin of more easily fitting, easy cleaning, there is whitening and moisture-keeping functions, mounted facial film easy to use.
The object of the invention is to be achieved through the following technical solutions.
The preparation method of Aloe Rhizoma amorphophalli glucomannan facial film of the present invention, is characterized in that preparation process is as follows:
(1) preparation of Aloe extract: after the Aloe of drying is pulverized with pulverizer, put into 60 DEG C of vacuum drying oven baking 12h, cross 80 mesh sieves, obtain Aloe fine powder, get the Aloe fine powder after 10g oven dry, add the ethanol 40mL that volume ratio is 50%, supersound extraction 30min, ultrasonic temperature 30 DEG C, extracting solution heating in water bath volatilizes, be placed on drying under reduced pressure 1h in drying baker, obtain Aloe extractum;
(2) preparation of membrane: get 10 ~ 15g Aloe extractum, add 0.3 ~ 0.5g Rhizoma amorphophalli glucomannan, 0.5 ~ 1g hydroxy methocel, 100mL deionized water, heat in 50 DEG C of water-baths, heat while stirring uniformly viscous liquid, use 0.1mol/L sodium pyrophosphate solution, regulate pH to be 5 ~ 6, room temperature cools, obtain membrane, for subsequent use;
(3) Rhizoma amorphophalli glucomannan and xanthan gum composite: get 350 ~ 400mL distilled water and be placed in water-bath and be heated to 90 DEG C, take again 0.3 ~ 0.5g xanthan gum and 0.3 ~ 0.5g Rhizoma amorphophalli glucomannan mixing add, stir 10 ~ 12min with the rotating speed of 300r/min simultaneously, be cooled to room temperature, leave standstill swelling 4 ~ 4.5h, obtain product glue, for subsequent use;
(4) preparation of film: product glue uniform application step (3) obtained is on mould, and thickness is 1.5 ~ 2mm, leaves standstill 15 ~ 20min, obtains shaping membrane;
(5) demoulding soaks: shaping membrane step (4) obtained immerses in the membrane of step (2), swelling absorption 10 ~ 15min;
(6) sterilization packaging: the shaping membrane after step (5) being soaked, sterilization, packaging, be finished product.
Advantage of the present invention and beneficial effect: the antiinflammatory of the excellent film property that the present invention takes full advantage of that Rhizoma amorphophalli glucomannan has, water-retaining property, water absorption, antibiotic property and Aloe, whitening, moisture-keeping functions, preparation Aloe Rhizoma amorphophalli glucomannan facial film, product had both had good stickiness, also there is good moisturizing white-skinned face function, healthy, environmental protection, and fashion.The alginate jelly series products that Rhizoma amorphophalli glucomannan compound gel cost uses lower than tradition, the nontoxic health of raw material, is applicable to the crowd of all kinds of skin; Add a small amount of Rhizoma amorphophalli glucomannan in membrane and increase viscosity, not easily drip during use, convenient and safe, effect is remarkable.
The Aloe Rhizoma amorphophalli glucomannan facial film made is carried out use test:
(1) pH value
Pick intermediate materials product glue of the present invention with the reagent paper of pH, observe the change of its color, contrast pH value parameter sees its acid-base value.The pH recording product glue, all between 5 ~ 6, belongs to gentle non-irritating.
(2) product glue
This product product glue is clear viscous shape, British plain spirits.
(3) wettability
After using this product, foaming micelle is sprinkling upon the user that lies low on the face uniformly, and then user is stood up uprightly, the foaming micelle number that observation remains on the face.The person that uses this product, residual foaming micelle number is more, illustrate this product use after the moist degree of skin strong.
(4) veneer degree
When using this product, below the lip of this product person, the laminating degree of the keypoint part such as wing of nose both sides is good, and veneer degree is satisfactory for result.
(5) moisturizing degree
Adopt moisture testing apparatus to measure to use before this product, just used, use latter 2 hours, the skin moisture value of this three phases.Result shows, instant moisturizing degree and the lasting moisturizing degree of this facial film are all better than mask product general on the market.
(6) whitening effect
Adopt the method for observing, observe using before this product, use latter 1 month, use the whitening skin degree of latter 3 months.Through observing, after using product of the present invention, whitening effect is remarkable, and NIP, lasting use obviously can improve face skin.Facial film of the present invention and commercially available facial film compare, and result is as shown in table 1.
Table 1 Aloe Rhizoma amorphophalli glucomannan facial film compares with other facial films
The comparative result of table 1 shows, Aloe Rhizoma amorphophalli glucomannan facial film of the present invention is better than other facial films.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is described in further detail.
The preparation method of embodiment 1, a kind of Aloe Rhizoma amorphophalli glucomannan facial film
A preparation method for Aloe Rhizoma amorphophalli glucomannan facial film, comprises the following steps:
(1) preparation of Aloe extract: after being pulverized with pulverizer by the Aloe of drying, puts into 60 DEG C of vacuum drying oven baking 12h, crosses 80 mesh sieves, obtain Aloe fine powder, get the Aloe fine powder after 10g oven dry, add the ethanol 40mL that volume ratio is 50%, supersound extraction 30min, ultrasonic temperature 30 DEG C; Extracting solution heating in water bath volatilizes, and is placed on drying under reduced pressure 1h in drying baker, obtains Aloe extractum, for subsequent use;
(2) preparation of membrane: get 15g Aloe extractum, add 0.3g Rhizoma amorphophalli glucomannan, 1g hydroxy methocel, 100ml deionized water, heat in 50 DEG C of water-baths, heat while stirring uniformly viscous liquid, use 0.1mol/L sodium pyrophosphate solution, regulate pH to be 5, room temperature cools, obtain membrane, for subsequent use;
(3) Rhizoma amorphophalli glucomannan and xanthan gum composite: get 400mL distilled water and be placed in water-bath and be heated to 90 DEG C, the Rhizoma amorphophalli glucomannan mixing taking 0.5g xanthan gum and 0.5g again adds, and stirs 10min simultaneously, be cooled to room temperature with the rotating speed of 300r/min, leave standstill swelling 4h, obtain product glue for subsequent use;
(4) preparation of film: spread upon uniformly on mould by the glue that step (3) obtains, thickness is about 2mm, and standing 18min obtains shaping membrane;
(5) demoulding soaks: in the membrane that shaping membrane immersion step (2) step (4) obtained obtains, swelling absorption 15min;
(6) sterilization packaging: the molding facial film after step (5) being soaked, sterilization, packaging, be finished product.
The preparation method of embodiment 2 one kinds of Aloe Rhizoma amorphophalli glucomannan facial films
A preparation method for Aloe Rhizoma amorphophalli glucomannan facial film, comprises the following steps:
(1) preparation of Aloe extract: after being pulverized with pulverizer by the Aloe of drying, puts into 60 DEG C of vacuum drying oven baking 12h, crosses 80 mesh sieves, obtain Aloe fine powder, get the Aloe fine powder after 10g oven dry, add 50% ethanol 40mL, supersound extraction 30min, ultrasonic temperature 30 DEG C; Extracting solution heating in water bath volatilizes, and is placed on drying under reduced pressure 1h in drying baker, obtains Aloe extractum, for subsequent use;
(2) preparation of membrane: get 10g Aloe extractum, add 0.5g Rhizoma amorphophalli glucomannan, 0.5g hydroxy methocel, 100mL deionized water, heat in 50 DEG C of water-baths, heat while stirring uniformly viscous liquid, use 0.1mol/L sodium pyrophosphate solution, regulate pH to be 5, room temperature cools, obtain membrane, for subsequent use;
(3) Rhizoma amorphophalli glucomannan and xanthan gum composite: get 400mL distilled water and be placed in water-bath and be heated to 90 DEG C, the Rhizoma amorphophalli glucomannan mixing taking 0.5g xanthan gum and 0.5g again adds, and stirs 10min simultaneously, be cooled to room temperature with the rotating speed of 300r/min, leave standstill swelling 4h, obtain product glue for subsequent use;
(4) preparation of film: the glue (3) obtained spreads upon on mould uniformly, thickness 2mm, leaves standstill 20min;
(5) demoulding soaks: in the membrane that shaping membrane immersion step (2) step (4) obtained obtains, swelling absorption 15min;
(6) sterilization packaging: by forming surface membrane sterilization, packaging after the immersion of step (5), be finished product.
The foregoing is only preferred embodiment of the present invention, all equalizations done according to the present patent application the scope of the claims change and modify, and all should belong to covering scope of the present invention.

Claims (4)

1. a preparation method for Aloe Rhizoma amorphophalli glucomannan facial film, is characterized in that preparation process is as follows:
(1) preparation of Aloe extract: after being pulverized with pulverizer by the Aloe of drying, puts into 60 DEG C of vacuum drying oven baking 12h, crosses 80 mesh sieves, obtain Aloe fine powder; Get the Aloe fine powder after 10g oven dry, add the ethanol 40mL that volume ratio is 50%, supersound extraction 30min, ultrasonic temperature 30 DEG C, extracting solution heating in water bath volatilizes, and is placed on drying under reduced pressure 1h in drying baker, obtains Aloe extractum;
(2) preparation of membrane: get 10 ~ 15g Aloe extractum, add 0.3 ~ 0.5g Rhizoma amorphophalli glucomannan, 0.5 ~ 1g hydroxy methocel, 100mL deionized water, heat in 50 DEG C of water-baths, heat while stirring uniformly viscous liquid, use 0.1mol/L sodium pyrophosphate solution, regulate pH to be 5 ~ 6, room temperature cools, obtain membrane, for subsequent use;
(3) Rhizoma amorphophalli glucomannan and xanthan gum composite: get 350 ~ 400mL distilled water and be placed in water-bath and be heated to 90 DEG C, take again 0.3 ~ 0.5g xanthan gum and 0.3 ~ 0.5g Rhizoma amorphophalli glucomannan mixing add, stir 10 ~ 12min with the rotating speed of 300r/min simultaneously, be cooled to room temperature, leave standstill swelling 4 ~ 4.5h, obtain product glue, for subsequent use;
(4) preparation of film: product glue uniform application step (3) obtained is on mould, and thickness is 1.5 ~ 2mm, leaves standstill 15 ~ 20min, obtains shaping membrane;
(5) demoulding soaks: shaping membrane step (4) obtained immerses in the membrane of step (2), swelling absorption 10 ~ 15min;
(6) sterilization packaging: the shaping membrane after step (5) being soaked, sterilization, packaging, be finished product.
2. the preparation method of a kind of Aloe Rhizoma amorphophalli glucomannan facial film according to claim 1, it is characterized in that the preparation of described membrane: get 15g Aloe extractum, add 0.3g Rhizoma amorphophalli glucomannan, 1g hydroxy methocel, 100mL deionized water, heat in 50 DEG C of water-baths, heat while stirring uniformly viscous liquid, uses 0.1mol/L sodium pyrophosphate solution, pH is regulated to be 5, room temperature cools, and obtains membrane, for subsequent use.
3. the preparation method of a kind of Aloe Rhizoma amorphophalli glucomannan facial film according to claim 1, it is characterized in that the preparation of described film: spread upon uniformly on mould by glue, thickness is about 2mm, standing 18min obtains shaping membrane.
4. the Aloe Rhizoma amorphophalli glucomannan facial film prepared by the either method described in claim 1-3.
CN201610063469.9A 2016-01-29 2016-01-29 Aloe konjaku glucomannan facial mask and preparation method thereof Active CN105496906B (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107362115A (en) * 2017-08-22 2017-11-21 安徽省中日农业环保科技有限公司 A kind of preparation method of the anti-acne essence containing aloe extract
CN110123720A (en) * 2019-06-15 2019-08-16 福建农林大学 A kind of konjaku glucomannan care face cream and preparation method thereof
CN110200885A (en) * 2019-06-26 2019-09-06 武汉芘芘薇莎生物科技有限公司 A kind of konjac facial mask base fabric and preparation method thereof and konjac facial mask
CN111686058A (en) * 2020-07-13 2020-09-22 富源县金地魔芋种业有限公司 Formed konjak mask and preparation method thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102389380A (en) * 2011-09-07 2012-03-28 福建农林大学 Konjac glucomannan eye mask and preparation method thereof
FR2997406A1 (en) * 2012-10-25 2014-05-02 Basf Beauty Care Solutions F HYALURONATE AND GLUCOMANNAN POLYMER
CN104306280A (en) * 2014-09-23 2015-01-28 青岛康和食品有限公司 Aloe facial mask

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102389380A (en) * 2011-09-07 2012-03-28 福建农林大学 Konjac glucomannan eye mask and preparation method thereof
FR2997406A1 (en) * 2012-10-25 2014-05-02 Basf Beauty Care Solutions F HYALURONATE AND GLUCOMANNAN POLYMER
CN104306280A (en) * 2014-09-23 2015-01-28 青岛康和食品有限公司 Aloe facial mask

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107362115A (en) * 2017-08-22 2017-11-21 安徽省中日农业环保科技有限公司 A kind of preparation method of the anti-acne essence containing aloe extract
CN110123720A (en) * 2019-06-15 2019-08-16 福建农林大学 A kind of konjaku glucomannan care face cream and preparation method thereof
CN110200885A (en) * 2019-06-26 2019-09-06 武汉芘芘薇莎生物科技有限公司 A kind of konjac facial mask base fabric and preparation method thereof and konjac facial mask
WO2020258740A1 (en) * 2019-06-26 2020-12-30 武汉芘芘薇莎生物科技有限公司 Konjac face mask base cloth and preparation method therefor, and konjac face mask
CN111686058A (en) * 2020-07-13 2020-09-22 富源县金地魔芋种业有限公司 Formed konjak mask and preparation method thereof

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