CN105496868A - 一种含油的透明水性凝胶及制备方法 - Google Patents

一种含油的透明水性凝胶及制备方法 Download PDF

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CN105496868A
CN105496868A CN201510982114.5A CN201510982114A CN105496868A CN 105496868 A CN105496868 A CN 105496868A CN 201510982114 A CN201510982114 A CN 201510982114A CN 105496868 A CN105496868 A CN 105496868A
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侯剑峰
孙晋喜
秦福燕
林莉
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    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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Abstract

本发明公开了一种含油的透明水性凝胶及制备方法,该凝胶由A油相、B水相和C相混合制备而成,制得水包油透明凝胶体系。本发明提供的含油的透明水性凝胶,性能温和、肤感丝滑,保湿功效好。

Description

一种含油的透明水性凝胶及制备方法
技术领域
本发明涉及化妆品技术领域,特别涉及一种含油的透明水性凝胶及制备方法。
背景技术
目前市面的凝胶类护肤品繁多,主要以油包水或硅油包水为主,其缺点是铺展性比较差,外观不够新颖,而水性透明的凝胶体系,因不含有油分或含油量较少,肤感干涩,不滋润,含油的透明水性凝胶,会含有大量的表面活性剂,会产生刺激,且含油量不高,本发明因此而来。
发明内容
本发明目的之一是提供一种含油的透明水性凝胶,以解决现有技术中凝胶用后皮肤干涩、发痒等问题。
本发明的另一目的是提供一种含油的透明水性凝胶的制备方法。
基于上述问题,本发明提供的技术方案之一是:
一种含油的透明水性变色BB霜,由A相、B相和C相混合制备而成,
其中,A相为油相,按重量百分比包括以下组分:
硅油:9.00%~30.00%,
聚二甲基硅氧烷/乙烯基聚二甲基硅氧烷交联聚合物:0.50%~2.00%,
丙烯酸羟乙酯/丙烯酰二甲基牛磺酸钠共聚物:0.50~2.00%,
其中,B相为水相,按重量百分比包括以下组分:
纯化水:10.00%~77.00%
丙二醇:20.00%~50.00%,
1,3-丙二醇:1.00%~10.00%,
丙烯酰二甲基牛磺酸铵/VP共聚物:0.10%~2.00%;
其中,C相按照重量百分比包括以下组分:
香精:0.03%~0.5%,
PE9010:0.50%~1.00%,
藻提取物:0.50%~5.00%,
甜菜碱:0.50%~2.00%,
透明质酸钠:0.001%~0.05%;
以上各原料重量百分比之和为100%。
在其中的一个实施例中,所述硅油为环状硅油或低粘二甲基硅油。
本发明提供的另一技术方案是:
一种含油的透明水性凝胶的制备方法,包括以下步骤:
(1)将A相各组分按照用量份混合后加入油相锅中,以10~50rpm/min的转速搅拌10~60min至搅拌均匀;
(2)将B相各组分纯化水、丙二醇、1,3-丙二醇、丙烯酰二甲基牛磺酸铵/VP共聚物按照用量份依次加入真空乳化锅中,以30~35rpm/min的转速搅拌10~60min,保持真空,然后以2600~3100rpm/min的均质速度均质10~60min至混合均匀;
(3)将油相锅的原料通过过滤阀抽入真空乳化锅中,以25~35rpm/min的转速搅拌10~30min,形成均一透明凝胶;
(4)将C相各组分香精、PE9010、藻提取物、甜菜碱按照用量份依次加入真空乳化锅中,以10~50rpm/min的转速搅拌10~60min,搅拌均匀后出料送检;
(5)检测合格后灌装。
与现有技术相比,本发明的优点是:
1.采用本发明的技术方案,该凝胶为水包油透明凝胶体系,配方水相中加入多元醇、甜菜碱和透明质酸钠,可以提高产品的保湿功效;
2.采用本发明的技术方案,具有较高的含油量,但含有的表面活性剂少,性能温和、肤感丝滑。
具体实施方式
以下结合具体实施例对上述方案做进一步说明。应理解,这些实施例是用于说明本发明而不限于限制本发明的范围。实施例中采用的实施条件可以根据具体厂家的条件做进一步调整,未注明的实施条件通常为常规实验中的条件。
实施例1
本实施例中BB霜由A相、B相和C相混合制备而成,
A相为油相,按照重量辈分比包括以下组分:
环状硅油:13.5%,
聚二甲基硅氧烷/乙烯基聚二甲基硅氧烷交联聚合物:0.75%,
丙烯酸羟乙酯/丙烯酰二甲基牛磺酸钠共聚物:0.75%;
B相为水相,按照重量百分比包括以下组分:
纯化水:46.05%,
丙二醇:25.00%,
1,3-丙二醇:5.00%,
丙烯酰二甲基牛磺酸铵/VP共聚物:1.00%;
C相,按照重量百分比包括以下组分:
香精:0.10%,
PE9010(苯氧乙醇+乙基己基甘油):0.80%,
藻提取物:5.00%,
甜菜碱:2.00%,
透明质酸钠:0.05%。
本实施例中BB霜的制备方法为:
(1)将A相各组分按照用量份混合后加入油相锅中,以10~50rpm/min的转速搅拌10~60min至搅拌均匀;
(2)将B相各组分纯化水、丙二醇、1,3-丙二醇、丙烯酰二甲基牛磺酸铵/VP共聚物按照用量份依次加入真空乳化锅中,以30~35rpm/min的转速搅拌10~60min,保持真空,然后以2600~3100rpm/min的均质速度均质10~60min至混合均匀;
(3)将油相锅的原料通过过滤阀抽入真空乳化锅中,以25~35rpm/min的转速搅拌10~30min,形成均一透明凝胶;
(4)将C相各组分香精、PE9010、藻提取物、甜菜碱按照用量份依次加入真空乳化锅中,以10~50rpm/min的转速搅拌10~60min,搅拌均匀后出料送检;
(5)检测合格后灌装。
本例中制得的透明凝胶各项检测指标为:
膏体外观:透明凝胶;
气味:与香精气味一致;
稳定性:耐热50℃,1个月测试稳定;耐寒-15℃到-5℃,4次冻融,一个月低温稳定;
使用感:涂抹在皮肤上时,肤感丝滑,滋润保湿感强。
实施例2
本实施例中BB霜由A相、B相和C相混合制备而成,
A相为油相,按照重量辈分比包括以下组分:
低粘二甲基硅油:27%,
聚二甲基硅氧烷/乙烯基聚二甲基硅氧烷交联聚合物:1.5%,
丙烯酸羟乙酯/丙烯酰二甲基牛磺酸钠共聚物:1.5%;
B相为水相,按照重量百分比包括以下组分:
纯化水:26.20%,
丙二醇:30.00%,
1,3-丙二醇:10.00%,
丙烯酰二甲基牛磺酸铵/VP共聚物:0.10%;
C相,按照重量百分比包括以下组分:
香精:0.08%,
PE9010(苯氧乙醇+乙基己基甘油):0.60%,
藻提取物:2.00%,
甜菜碱:1.00%,
透明质酸钠:0.02%。
本实施例中的凝胶的制备方法与实施例1相同。
本例中制得的凝胶的各项检测指标为:
膏体外观:透明凝胶;
气味:与香精气味一致;
稳定性:耐热50℃,1个月测试稳定;耐寒-15℃到-5℃,4次冻融,一个月低温稳定;
使用感:涂抹在皮肤上时,肤感丝滑,滋润保湿感强。
上述实例只为说明本发明的技术构思及特点,其目的在于让熟悉此项技术的人是能够了解本发明的内容并据以实施,并不能以此限制本发明的保护范围。凡根据本发明精神实质所做的等效变换或修饰,都应涵盖在本发明的保护范围之内。

Claims (3)

1.一种含油的透明水性凝胶,其特征在于:由A相、B相和C相混合制备而成,
其中,A相为油相,按重量百分比包括以下组分:
硅油:9.00%~30.00%,
聚二甲基硅氧烷/乙烯基聚二甲基硅氧烷交联聚合物:0.50%~2.00%,
丙烯酸羟乙酯/丙烯酰二甲基牛磺酸钠共聚物:0.50~2.00%;
其中,B相为水相,按重量百分比包括以下组分:
纯化水:10.00%~77.00%
丙二醇:20.00%~50.00%,
1,3-丙二醇:1.00%~10.00%,
丙烯酰二甲基牛磺酸铵/VP共聚物:0.10%~2.00%;
其中,C相按照重量百分比包括以下组分:
香精:0.03%~0.5%,
PE9010:0.50%~1.00%,
藻提取物:0.50%~5.00%,
甜菜碱:0.50%~2.00%,
透明质酸钠:0.001%~0.05%;
以上各原料重量百分比之和为100%。
2.根据权利要求1所述的含油的透明水性变色BB霜,其特征在于:所述硅油为环状硅油或低粘二甲基硅油。
3.一种含油的透明水性凝胶的制备方法,其特征在于包括以下步骤:
(1)将A相各组分按照用量份混合后加入油相锅中,以10~50rpm/min的转速搅拌10~60min至搅拌均匀;
(2)将B相各组分纯化水、丙二醇、1,3-丙二醇、丙烯酰二甲基牛磺酸铵/VP共聚物按照用量份依次加入真空乳化锅中,以30~35rpm/min的转速搅拌10~60min,保持真空,然后以2600~3100rpm/min的均质速度均质10~60min至混合均匀;
(3)将油相锅的原料通过过滤阀抽入真空乳化锅中,以25~35rpm/min的转速搅拌10~30min,形成均一透明凝胶;
(4)将C相各组分香精、PE9010、藻提取物、甜菜碱按照用量份依次加入真空乳化锅中,以10~50rpm/min的转速搅拌10~60min,搅拌均匀后出料送检;
(5)检测合格后灌装。
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