CN105482698A - Wood board paint bright in gloss and preparing method of wood board paint - Google Patents
Wood board paint bright in gloss and preparing method of wood board paint Download PDFInfo
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- CN105482698A CN105482698A CN201510925227.1A CN201510925227A CN105482698A CN 105482698 A CN105482698 A CN 105482698A CN 201510925227 A CN201510925227 A CN 201510925227A CN 105482698 A CN105482698 A CN 105482698A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D193/00—Coating compositions based on natural resins; Coating compositions based on derivatives thereof
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/24—Crosslinking, e.g. vulcanising, of macromolecules
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K13/00—Use of mixtures of ingredients not covered by one single of the preceding main groups, each of these compounds being essential
- C08K13/02—Organic and inorganic ingredients
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/30—Sulfur-, selenium- or tellurium-containing compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/32—Phosphorus-containing compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2393/00—Characterised by the use of natural resins; Derivatives thereof
Abstract
The invention relates to a wood board paint bright in gloss and a preparing method of the wood board paint. The wood board paint is prepared from 60-65 parts of natural plant oleoresin, 10-15 parts of a natural plant oil-based mill base, 1-2 parts of a dispersing auxiliary, 1-2 parts of a defoaming agent, 2-3 parts of a thinning agent, 10-12 parts of roasted common coltsfoot flowers, 5-8 parts of fried radix platycodi, 10-12 parts of roasted stiff silkworms, 3-5 parts of unibract fritillary bulbs, 3-5 parts of roasted pericarpium papaveris, 1-2 parts of roasted scorpions, 4-5 grains of scented tea, 50-60 parts of epoxy organosilicone, 10-15 parts of a toughening agent, 1-2 parts of a coupling agent, 2-3 parts of a curing agent, 100-150 parts of ethyl cyanoacetate, 50-60 parts of solid formaldehyde, 2-3 parts of piperidine, 70-80 parts of methyl alcohol, 2-5 parts of cyclohexane, 1-3 parts of ethyl acetate, 2-5 parts of phosphorus pentoxide, 1-2 parts of sulfur dioxide and 1-3 parts of hydroquinone. The medicine is added, ground and mixed, so that organic compounds and free bodies released by the paint are diluted, and harm to the atmosphere and the human bodies is reduced; gel liquid is added and mixed into natural plant paint, a layer of protection film is additionally formed for reducing volatilization of the paint while even mixing is ensured, and the preservation effect of the paint is better.
Description
Technical field:
The present invention relates to a kind of coating, be specifically related to vivid plank japanning of gloss and preparation method thereof.
Background technology:
Paint is that one firmly can cover body surface, plays protection, decoration, mark and the chemical mixture coating of other special purposes.China's coating circle more authoritative " coating process " book is definition like this: " coating is a kind of material, and this material can be coated in article surface by different construction technologies, forms adhere well, has some strength, continuous print solid film.The film common name film of such formation, also known as paint film or coating."
Coating is generally made up of four parts such as filmogen, filler (color stuffing), solvent, auxiliary agents.According to performance requriements sometimes composition can slightly change, as varnish does not have can not have solvent in color stuffing, powder coating.
Belong to organic chemical industry's macromolecular material, the film formed belongs to macromolecular compound type.The classification of the Chemicals of passing through according to the modern times, coating belongs to fine chemical product.Modern coating is progressively becoming the polyfunctional engineering materials of a class, is an important industry in chemical industry.
Existing coating mostly is chemical coating, continuous volatile organic compound and episome in the process of smearing, and not only produces ozone pollution to air, people also can be made to produce headache, general paralysis, the harm such as anaemia.
Summary of the invention:
Technical problem to be solved by this invention is the defect overcoming prior art, plank japanning providing a kind of gloss vivid and preparation method thereof.
Technical problem to be solved by this invention realizes by the following technical solutions.
The plank japanning that gloss is vivid, it is characterized in that: comprise natural phant oiliness resin 60-65 part, natural phant oiliness mill base 10-15 part, dispersing auxiliary 1-2 part, defoamer 1-2 part, thinner 2-3 part, honey-fried FLOS FARFARAE 10-12 part, fry balloonflower root 5-8 part, process stiff silkworm 10-12 part, Unibract Fritillary Bulb 3-5 part, process Poppy capsule 3-5 part, process scorpio 1-2 part, jasmine tea 4-5 grain, epoxy organosilicon: 50-60 part, toughner: 10-15 part, coupling agent: 1-2 part, solidifying agent: 2-3 part, ethyl cyanoacetate: 100-150 part, solid formaldehyde: 50-60 part, piperidines: 2-3 part, methyl alcohol: 70-80 part, hexanaphthene: 2-5 part, ethyl acetate: 1-3 part, Vanadium Pentoxide in FLAKES: 2-5 part, sulfurous gas 1-2 part, Resorcinol: 1-3 part.。
The plank japanning preparation method that gloss is vivid, is characterized in that: specifically comprise the following steps:
Add in reactor by natural oil resin, under the effect of orgnometallic catalyst, heating and controlling crosslinking temperature is 110 DEG C-130 DEG C, and pressure is 0.2MPa-0.25MPa, stirring velocity is 30-50 rev/min, and mixing 30-60 minute, to color even, transparent, viscosity obviously increases, then lowers the temperature;
Add dispersing auxiliary and natural phant oiliness mill base is uniformly mixed, obtain mixture;
By the honey-fried FLOS FARFARAE in constitutive material, fry balloonflower root, process stiff silkworm, Unibract Fritillary Bulb, process Poppy capsule and process scorpio, put into matrass, add the clear water of 5 times, boiling, to the water evaporate to dryness in matrass, collect water vapour, water vapour liquefies again; Jasmine tea is put into boiling water to soak, the water yield is 300ml simultaneously, and soak 5-8 minute, filtered water, obtains jasmine tea water; Again the water vapour collected is mixed with jasmine tea water;
Pour into after mixing in mixture, leave standstill 2 hours, heat 1 hour for 60-70 DEG C, cool 1 hour, heat 20 minutes for 66-72 DEG C, then leave standstill 1 hour, add thinner, stand-by;
Get epoxy organosilicon, toughner, coupling agent mixing completely dissolve after, add solidifying agent and make work in-process glue;
Get solid formaldehyde simultaneously, piperidines, methyl alcohol adds in a flask, heating, stirs, dissolve, then dropped in reactor, reactor is warming up to 90 DEG C, add ethyl cyanoacetate, heat 2 hours, then recycling design methyl alcohol, to temperature 120 DEG C, stop heating, add hexanaphthene, ethyl acetate mixing, reflux dewatering, temperature rises to 125 DEG C, and discharging obtains condensation polymer;
By condensation polymer and the mixing of work in-process glue, proportion is 100:20-50, adds 5-10 part promotor, is warming up to 90 DEG C, and heating duration can obtain copolymerization sizing agent in 1 hour;
Get 1-2 part Vanadium Pentoxide in FLAKES and add copolymerization sizing agent, be heated to 190 DEG C-200 DEG C, carry out cracking under vacuum tightness 0.1MPa, obtain crude monomer;
In crude monomer, add remaining Vanadium Pentoxide in FLAKES, Resorcinol, sulfurous gas, stir in reactor, temperature control 80-100 DEG C, vacuum tightness collects the product that cut is 70-80 DEG C under being 0.1MPa, obtains smart monomer;
Getting smart monomer, to add massfraction be the dioctyl phthalate (DOP) of 1%-2%, the mixture of lucite powder, adds defoamer, obtain required paint.
Beneficial effect of the present invention is: natural phant oiliness resin reduces micromolecular content after crosslinking Treatment, improves macromolecular content, and water tolerance and thermotolerance are all applauded; Add medicine ground and mixed simultaneously; the organic compound of dilution paint release and episome; reduce the harm to air and human body; colloidal liquid mixing is added in crude vegetal paint; while guarantee mixes; for the volatilization reducing paint strengthens layer protecting film, make paint preservation effect better, the time is longer.
Embodiment:
The technique means realized to make the present invention, creation characteristic, reaching object and effect is easy to understand, below in conjunction with specific embodiment, setting forth the present invention further.
Specific embodiment 1: the plank japanning that gloss is vivid, comprise natural phant oiliness resin 60 parts, natural phant oiliness mill base 10 parts, dispersing auxiliary 1 part, defoamer 1 part, thinner 2 parts, honey-fried FLOS FARFARAE 10 parts, fry balloonflower root 5 parts, process stiff silkworm 10 parts, Unibract Fritillary Bulb 3 parts, process Poppy capsule 3 parts, process scorpio 1 part, jasmine tea 4, epoxy organosilicon: 50 parts, toughner: 10 parts, coupling agent: 1 part, solidifying agent: 2 parts, ethyl cyanoacetate: 100 parts, solid formaldehyde: 50 parts, piperidines: 2 parts, methyl alcohol: 70 parts, hexanaphthene: 2 parts, ethyl acetate: 1 part, Vanadium Pentoxide in FLAKES: 2 parts, sulfurous gas 1 part, Resorcinol: 1 part.
Specific embodiment 2: the plank japanning that gloss is vivid, comprise natural phant oiliness resin 65 parts, natural phant oiliness mill base 15 parts, dispersing auxiliary 2 parts, defoamer 2 parts, thinner 3 parts, honey-fried FLOS FARFARAE 12 parts, fry balloonflower root 8 parts, process stiff silkworm 12 parts, Unibract Fritillary Bulb 5 parts, process Poppy capsule 5 parts, process scorpio 2 parts, jasmine tea 5, epoxy organosilicon: 60 parts, toughner: 15 parts, coupling agent: 2 parts, solidifying agent: 3 parts, ethyl cyanoacetate: 150 parts, solid formaldehyde: 60 parts, piperidines: 3 parts, methyl alcohol: 80 parts, hexanaphthene: 5 parts, ethyl acetate: 3 parts, Vanadium Pentoxide in FLAKES: 5 parts, sulfurous gas 2 parts, Resorcinol: 3 parts.
The plank japanning preparation method that gloss is vivid, specifically comprises the following steps:
Add in reactor by natural oil resin, under the effect of orgnometallic catalyst, heating and controlling crosslinking temperature is 110 DEG C-130 DEG C, and pressure is 0.2MPa-0.25MPa, stirring velocity is 30-50 rev/min, and mixing 30-60 minute, to color even, transparent, viscosity obviously increases, then lowers the temperature;
Add dispersing auxiliary and natural phant oiliness mill base is uniformly mixed, obtain mixture;
By the honey-fried FLOS FARFARAE in constitutive material, fry balloonflower root, process stiff silkworm, Unibract Fritillary Bulb, process Poppy capsule and process scorpio, put into matrass, add the clear water of 5 times, boiling, to the water evaporate to dryness in matrass, collect water vapour, water vapour liquefies again; Jasmine tea is put into boiling water to soak, the water yield is 300ml simultaneously, and soak 5-8 minute, filtered water, obtains jasmine tea water; Again the water vapour collected is mixed with jasmine tea water;
Pour into after mixing in mixture, leave standstill 2 hours, heat 1 hour for 60-70 DEG C, cool 1 hour, heat 20 minutes for 66-72 DEG C, then leave standstill 1 hour, add thinner, stand-by;
Get epoxy organosilicon, toughner, coupling agent mixing completely dissolve after, add solidifying agent and make work in-process glue;
Get solid formaldehyde simultaneously, piperidines, methyl alcohol adds in a flask, heating, stirs, dissolve, then dropped in reactor, reactor is warming up to 90 DEG C, add ethyl cyanoacetate, heat 2 hours, then recycling design methyl alcohol, to temperature 120 DEG C, stop heating, add hexanaphthene, ethyl acetate mixing, reflux dewatering, temperature rises to 125 DEG C, and discharging obtains condensation polymer;
By condensation polymer and the mixing of work in-process glue, proportion is 100:20-50, adds 5-10 part promotor, is warming up to 90 DEG C, and heating duration can obtain copolymerization sizing agent in 1 hour;
Get 1-2 part Vanadium Pentoxide in FLAKES and add copolymerization sizing agent, be heated to 190 DEG C-200 DEG C, carry out cracking under vacuum tightness 0.1MPa, obtain crude monomer;
In crude monomer, add remaining Vanadium Pentoxide in FLAKES, Resorcinol, sulfurous gas, stir in reactor, temperature control 80-100 DEG C, vacuum tightness collects the product that cut is 70-80 DEG C under being 0.1MPa, obtains smart monomer;
Getting smart monomer, to add massfraction be the dioctyl phthalate (DOP) of 1%-2%, the mixture of lucite powder, adds defoamer, obtain required paint.
More than show and describe ultimate principle of the present invention, principal character and advantage of the present invention.The technician of the industry should understand; the present invention is not restricted to the described embodiments; what describe in above-described embodiment and specification sheets just illustrates principle of the present invention; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications, and these changes and improvements all fall in the claimed scope of the invention.Application claims protection domain is defined by appending claims and equivalent thereof.
Claims (2)
1. the plank japanning that gloss is vivid, it is characterized in that: comprise natural phant oiliness resin 60-65 part, natural phant oiliness mill base 10-15 part, dispersing auxiliary 1-2 part, defoamer 1-2 part, thinner 2-3 part, honey-fried FLOS FARFARAE 10-12 part, fry balloonflower root 5-8 part, process stiff silkworm 10-12 part, Unibract Fritillary Bulb 3-5 part, process Poppy capsule 3-5 part, process scorpio 1-2 part, jasmine tea 4-5 grain, epoxy organosilicon: 50-60 part, toughner: 10-15 part, coupling agent: 1-2 part, solidifying agent: 2-3 part, ethyl cyanoacetate: 100-150 part, solid formaldehyde: 50-60 part, piperidines: 2-3 part, methyl alcohol: 70-80 part, hexanaphthene: 2-5 part, ethyl acetate: 1-3 part, Vanadium Pentoxide in FLAKES: 2-5 part, sulfurous gas 1-2 part, Resorcinol: 1-3 part.
2. according to claim 1, the plank japanning that gloss is vivid, is characterized in that: specifically comprise the following steps:
Add in reactor by natural oil resin, under the effect of orgnometallic catalyst, heating and controlling crosslinking temperature is 110 DEG C-130 DEG C, and pressure is 0.2MPa-0.25MPa, stirring velocity is 30-50 rev/min, and mixing 30-60 minute, to color even, transparent, viscosity obviously increases, then lowers the temperature;
Add dispersing auxiliary and natural phant oiliness mill base is uniformly mixed, obtain mixture;
By the honey-fried FLOS FARFARAE in constitutive material, fry balloonflower root, process stiff silkworm, Unibract Fritillary Bulb, process Poppy capsule and process scorpio, put into matrass, add the clear water of 5 times, boiling, to the water evaporate to dryness in matrass, collect water vapour, water vapour liquefies again; Jasmine tea is put into boiling water to soak, the water yield is 300ml simultaneously, and soak 5-8 minute, filtered water, obtains jasmine tea water; Again the water vapour collected is mixed with jasmine tea water;
Pour into after mixing in mixture, leave standstill 2 hours, heat 1 hour for 60-70 DEG C, cool 1 hour, heat 20 minutes for 66-72 DEG C, then leave standstill 1 hour, add thinner, stand-by;
Get epoxy organosilicon, toughner, coupling agent mixing completely dissolve after, add solidifying agent and make work in-process glue;
Get solid formaldehyde simultaneously, piperidines, methyl alcohol adds in a flask, heating, stirs, dissolve, then dropped in reactor, reactor is warming up to 90 DEG C, add ethyl cyanoacetate, heat 2 hours, then recycling design methyl alcohol, to temperature 120 DEG C, stop heating, add hexanaphthene, ethyl acetate mixing, reflux dewatering, temperature rises to 125 DEG C, and discharging obtains condensation polymer;
By condensation polymer and the mixing of work in-process glue, proportion is 100:20-50, adds 5-10 part promotor, is warming up to 90 DEG C, and heating duration can obtain copolymerization sizing agent in 1 hour;
Get 1-2 part Vanadium Pentoxide in FLAKES and add copolymerization sizing agent, be heated to 190 DEG C-200 DEG C, carry out cracking under vacuum tightness 0.1MPa, obtain crude monomer;
In crude monomer, add remaining Vanadium Pentoxide in FLAKES, Resorcinol, sulfurous gas, stir in reactor, temperature control 80-100 DEG C, vacuum tightness collects the product that cut is 70-80 DEG C under being 0.1MPa, obtains smart monomer;
Getting smart monomer, to add massfraction be the dioctyl phthalate (DOP) of 1%-2%, the mixture of lucite powder, adds defoamer, obtain required paint.
Priority Applications (1)
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CN201510925227.1A CN105482698A (en) | 2015-12-11 | 2015-12-11 | Wood board paint bright in gloss and preparing method of wood board paint |
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CN201510925227.1A CN105482698A (en) | 2015-12-11 | 2015-12-11 | Wood board paint bright in gloss and preparing method of wood board paint |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107538705A (en) * | 2017-08-04 | 2018-01-05 | 安徽博泰塑业科技有限公司 | Polyethylene particle and synthetic fibers composite pipe expressing technique |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101735729A (en) * | 2008-11-06 | 2010-06-16 | 夏栋 | Crude vegetal paint |
JP2013237739A (en) * | 2012-05-14 | 2013-11-28 | Isamu Hatake | Aqueous anti-ultraviolet agent, coating material having anti-ultraviolet property, and material having anti-ultraviolet property |
JP2014132069A (en) * | 2012-12-05 | 2014-07-17 | Otani Toryo Kk | Moose coating material for aqueous woodwork |
-
2015
- 2015-12-11 CN CN201510925227.1A patent/CN105482698A/en active Pending
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101735729A (en) * | 2008-11-06 | 2010-06-16 | 夏栋 | Crude vegetal paint |
JP2013237739A (en) * | 2012-05-14 | 2013-11-28 | Isamu Hatake | Aqueous anti-ultraviolet agent, coating material having anti-ultraviolet property, and material having anti-ultraviolet property |
JP2014132069A (en) * | 2012-12-05 | 2014-07-17 | Otani Toryo Kk | Moose coating material for aqueous woodwork |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107538705A (en) * | 2017-08-04 | 2018-01-05 | 安徽博泰塑业科技有限公司 | Polyethylene particle and synthetic fibers composite pipe expressing technique |
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