CN105463466A - Polishing liquid for stainless steel mechanical equipment and preparing method of polishing liquid - Google Patents
Polishing liquid for stainless steel mechanical equipment and preparing method of polishing liquid Download PDFInfo
- Publication number
- CN105463466A CN105463466A CN201510806959.9A CN201510806959A CN105463466A CN 105463466 A CN105463466 A CN 105463466A CN 201510806959 A CN201510806959 A CN 201510806959A CN 105463466 A CN105463466 A CN 105463466A
- Authority
- CN
- China
- Prior art keywords
- parts
- stainless steel
- polishing liquid
- mechanical means
- polishing fluid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23F—NON-MECHANICAL REMOVAL OF METALLIC MATERIAL FROM SURFACE; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL; MULTI-STEP PROCESSES FOR SURFACE TREATMENT OF METALLIC MATERIAL INVOLVING AT LEAST ONE PROCESS PROVIDED FOR IN CLASS C23 AND AT LEAST ONE PROCESS COVERED BY SUBCLASS C21D OR C22F OR CLASS C25
- C23F3/00—Brightening metals by chemical means
- C23F3/04—Heavy metals
Abstract
The invention discloses polishing liquid for stainless steel mechanical equipment and a preparing method of the polishing liquid. The polishing liquid is composed of, by weight, 5 parts to 18 parts of alkylphenol polyoxyethylene, 8 parts to 22 parts of citric acid, 25 parts to 35 parts of silicone emulsion, 1 part to 8 parts of trichloroacetic acid and 5 parts to 15 parts of sodium diethyldithiocarbamate. The trichloroacetic acid is added into the sodium diethyldithiocarbamate, and microwave processing is carried out to obtain mixed liquid A; the alkylphenol ethoxylates and the citric acid are placed in silicone emulsion, heated in a sealed manner, and then cooled, the mixed liquid A is added, after seal stirring, the mixing liquid is cooled to be at the room temperature; and the polishing liquid for the stainless steel mechanical equipment is obtained. The lubricating performance, the cooling performance and the penetration performance are good, the price is low, the preservative effect is good, the polishing liquid is suitable for mirror polishing of the stainless steel mechanical equipment, and the surface of the mechanical equipment reaches 8k mirror surface smooth finish.
Description
Technical field
The present invention relates to a kind of polishing fluid, specifically a kind of polishing fluid and preparation method thereof of the mechanical means for stainless steel.
Background technology
Mechanical means major part adopts stainless steel.It is high that stainless steel has hardness, wear resistance is good, good erosion resistance, the characteristics such as excellent outward appearance and life-span length, the high-quality mirror polish of surface of stainless steel product ensures that it is widely used in one of key factor of the industries such as building, automotive industry, shipbuilding, marine device, mechanical means and chemical device, and the proportioning of surface of stainless steel product polishing material is the key that surface of stainless steel product reaches specular quality.Polishing material has good degreasing, antirust, cleans and performance of adding lustre to, and Stainless Steel Products can be made to exceed original gloss.Existing stainless steel materials mirror polish material, often adopts buffing wax, rubbing paste etc., and it all can not be suitable for large surperficial sheet material polishing.Buffing wax, rubbing paste etc. are applicable to the polishing of foundry goods and structural part, and be characterized in a kind of dry grinding agent, it is difficult to be evenly distributed in the large-area surface of stainless steel.And adopt dry grinding agent to carry out polishing to stainless steel plate, its thermal distortion is larger.And its price is costly, and wherein operation is more in the fabrication process, the abrasive material of mixing containing impure granularity.Existing stainless steel mirror polishing material contain impurity or polishing fluid irregular time, the surface imperfection such as " small particles ", " draw circle " and " orange peel " can be caused during polishing.
Summary of the invention
The object of the present invention is to provide that a kind of lubricity, cost are low, impregnability good, the polishing fluid of the mechanical means for stainless steel of favorable anti-corrosion effect and preparation method thereof, to solve the problem proposed in above-mentioned background technology.
For achieving the above object, the invention provides following technical scheme:
For a polishing fluid for the mechanical means of stainless steel, be made up of the following raw material according to weight part: alkylphenol polyoxyethylene 5-18 part, citric acid 8-22 part, silicone emulsion 25-35 part, trichoroacetic acid(TCA) 1-8 part, Thiocarb 5-15 part.
As the further scheme of the present invention: the polishing fluid of the described mechanical means for stainless steel, be made up of the following raw material according to weight part: alkylphenol polyoxyethylene 12-15 part, citric acid 13-18 part, silicone emulsion 28-32 part, trichoroacetic acid(TCA) 4-6 part, Thiocarb 8-12 part.
As the further scheme of the present invention: the polishing fluid of the described mechanical means for stainless steel, be made up of the following raw material according to weight part: alkylphenol polyoxyethylene 14 parts, citric acid 15 parts, silicone emulsion 30 parts, trichoroacetic acid(TCA) 5 parts, Thiocarb 10 parts.
The preparation method of the polishing fluid of the described mechanical means for stainless steel, is made up of following steps:
1) insert in Thiocarb by trichoroacetic acid(TCA), microwave treatment, microwave treatment conditions is: adjustment microwave frequency is 1000-1200MHz, and microwave heating power is 90-110W, and microwave treatment time is 0.5-2h, obtains mixed liquor A for subsequent use;
2) insert in silicone emulsion by alkylphenol polyoxyethylene, citric acid, heated sealed, to 70-80 DEG C, stirs 0.3-0.8h, be cooled to 50-60 DEG C, add mixed liquor A again, 1-2h is stirred in sealing, is down to the polishing fluid that namely room temperature obtains the mechanical means for stainless steel.
Compared with prior art, the invention has the beneficial effects as follows:
Lubricity of the present invention, cost are low, impregnability good, favorable anti-corrosion effect, are suitable for the mirror polish of the mechanical means of stainless steel, and its surface can be made to reach 8k mirror-finishing.The present invention can reduce the wearing and tearing of polishing abrasive tool, improve the life-span of grinding tool, and equipment surface can not leave too much polishing fluid, can also improve polishing efficiency.
Embodiment
Below in conjunction with the embodiment of the present invention, be clearly and completely described the technical scheme in the embodiment of the present invention, obviously, described embodiment is only the present invention's part embodiment, instead of whole embodiments.Based on the embodiment in the present invention, those of ordinary skill in the art, not making the every other embodiment obtained under creative work prerequisite, belong to the scope of protection of the invention.
The present invention can be used in stainless steel 304,316 sheet materials, and thickness, at 1.0-12mm, carries out mirror polish.
When implementing of the present invention, the stainless steel materials surface that will process contacts with the embodiment of the present invention, and the duration of contact of glazed surface and polishing fluid sufficiently, to produce enough polishing effects, uses during polishing fluid and wants suitable shake, make polishing fluid even.
Embodiment 1
In the embodiment of the present invention, for a polishing fluid for the mechanical means of stainless steel, be made up of the following raw material according to weight part: alkylphenol polyoxyethylene 5 parts, citric acid 8 parts, silicone emulsion 25 parts, trichoroacetic acid(TCA) 1 part, Thiocarb 5 parts.Inserted by trichoroacetic acid(TCA) in Thiocarb, microwave treatment, microwave treatment conditions is: adjustment microwave frequency is 1000MHz, and microwave heating power is 90W, and microwave treatment time is 0.5h, obtains mixed liquor A for subsequent use.Insert in silicone emulsion by alkylphenol polyoxyethylene, citric acid, heated sealed to 70 DEG C, stir 0.3h, be cooled to 50 DEG C, then add mixed liquor A, 1h is stirred in sealing, is down to the polishing fluid that namely room temperature obtains the mechanical means for stainless steel.
In embodiment 1, stainless steel materials used is 1.5mm austenite 304 stainless steel, and polishing time is 1.8 hours, every square metre, plate surface evenness≤5.Its luminance brightness is 20 °, 135060 °, and 630 detecting instruments are luminance brightness detector, GB4550 or same quasi-instrument.
Embodiment 2
In the embodiment of the present invention, for a polishing fluid for the mechanical means of stainless steel, be made up of the following raw material according to weight part: alkylphenol polyoxyethylene 18 parts, citric acid 22 parts, silicone emulsion 35 parts, trichoroacetic acid(TCA) 8 parts, Thiocarb 15 parts.Inserted by trichoroacetic acid(TCA) in Thiocarb, microwave treatment, microwave treatment conditions is: adjustment microwave frequency is 1200MHz, and microwave heating power is 110W, and microwave treatment time is 2h, obtains mixed liquor A for subsequent use.Insert in silicone emulsion by alkylphenol polyoxyethylene, citric acid, heated sealed to 80 DEG C, stir 0.8h, be cooled to 60 DEG C, then add mixed liquor A, 2h is stirred in sealing, is down to the polishing fluid that namely room temperature obtains the mechanical means for stainless steel.
In embodiment 2, stainless steel materials used is 2mm austenite 304 stainless steel, and polishing time is 1.3 hours, every square metre, plate surface evenness≤5.Its luminance brightness is 20 °, 134060 °, and 620 detecting instruments are luminance brightness detector, GB4550 or same quasi-instrument.
Embodiment 3
In the embodiment of the present invention, for a polishing fluid for the mechanical means of stainless steel, be made up of the following raw material according to weight part: alkylphenol polyoxyethylene 12 parts, citric acid 13 parts, silicone emulsion 28 parts, trichoroacetic acid(TCA) 4 parts, Thiocarb 8 parts.Inserted by trichoroacetic acid(TCA) in Thiocarb, microwave treatment, microwave treatment conditions is: adjustment microwave frequency is 1100MHz, and microwave heating power is 95W, and microwave treatment time is 1h, obtains mixed liquor A for subsequent use.Insert in silicone emulsion by alkylphenol polyoxyethylene, citric acid, heated sealed to 73 DEG C, stir 0.4h, be cooled to 53 DEG C, then add mixed liquor A, 1.2h is stirred in sealing, is down to the polishing fluid that namely room temperature obtains the mechanical means for stainless steel.
In embodiment 3, stainless steel materials used is 3mm austenite 304 stainless steel, and polishing time is 0.9 hour, every square metre, plate surface evenness≤5.Its luminance brightness is 20 °, 137060 °, and 635 detecting instruments are luminance brightness detector, GB4550 or same quasi-instrument.
Embodiment 4
In the embodiment of the present invention, for a polishing fluid for the mechanical means of stainless steel, be made up of the following raw material according to weight part: alkylphenol polyoxyethylene 15 parts, citric acid 18 parts, silicone emulsion 32 parts, trichoroacetic acid(TCA) 6 parts, Thiocarb 12 parts.Inserted by trichoroacetic acid(TCA) in Thiocarb, microwave treatment, microwave treatment conditions is: adjustment microwave frequency is 1100MHz, and microwave heating power is 105W, and microwave treatment time is 1.5h, obtains mixed liquor A for subsequent use.Insert in silicone emulsion by alkylphenol polyoxyethylene, citric acid, heated sealed, to 70-80 DEG C, stirs 0.7h, is cooled to 57 DEG C, then adds mixed liquor A, and 1.7h is stirred in sealing, is down to the polishing fluid that namely room temperature obtains the mechanical means for stainless steel.
In embodiment 4, stainless steel materials used is 5mm austenite 316 stainless steel, and polishing time is 0.8 hour, every square metre, plate surface evenness≤5.Its luminance brightness is 20 °, 137060 °, and 635 detecting instruments are luminance brightness detector, GB4550 or same quasi-instrument.
Embodiment 5
In the embodiment of the present invention, for a polishing fluid for the mechanical means of stainless steel, be made up of the following raw material according to weight part: alkylphenol polyoxyethylene 14 parts, citric acid 15 parts, silicone emulsion 30 parts, trichoroacetic acid(TCA) 5 parts, Thiocarb 10 parts.Inserted by trichoroacetic acid(TCA) in Thiocarb, microwave treatment, microwave treatment conditions is: adjustment microwave frequency is 1100MHz, and microwave heating power is 100W, and microwave treatment time is 1.2h, obtains mixed liquor A for subsequent use.Insert in silicone emulsion by alkylphenol polyoxyethylene, citric acid, heated sealed, to 70-80 DEG C, stirs 0.6h, is cooled to 55 DEG C, then adds mixed liquor A, and 1.5h is stirred in sealing, is down to the polishing fluid that namely room temperature obtains the mechanical means for stainless steel.
In embodiment 5, stainless steel materials used is 8mm austenite 316 stainless steel, and polishing time is 0.5 hour, every square metre, plate surface evenness≤5.Its luminance brightness is 20 °, 137060 °, and 635 detecting instruments are luminance brightness detector, GB4550 or same quasi-instrument.
To those skilled in the art, obviously the invention is not restricted to the details of above-mentioned one exemplary embodiment, and when not deviating from spirit of the present invention or essential characteristic, the present invention can be realized in other specific forms.Therefore, no matter from which point, all should embodiment be regarded as exemplary, and be nonrestrictive, scope of the present invention is limited by claims instead of above-mentioned explanation, and all changes be therefore intended in the implication of the equivalency by dropping on claim and scope are included in the present invention.
In addition, be to be understood that, although this specification sheets is described according to embodiment, but not each embodiment only comprises an independently technical scheme, this narrating mode of specification sheets is only for clarity sake, those skilled in the art should by specification sheets integrally, and the technical scheme in each embodiment also through appropriately combined, can form other embodiments that it will be appreciated by those skilled in the art that.
Claims (4)
1. the polishing fluid for the mechanical means of stainless steel, it is characterized in that, be made up of the following raw material according to weight part: alkylphenol polyoxyethylene 5-18 part, citric acid 8-22 part, silicone emulsion 25-35 part, trichoroacetic acid(TCA) 1-8 part, Thiocarb 5-15 part.
2. the polishing fluid of the mechanical means for stainless steel according to claim 1, it is characterized in that, be made up of the following raw material according to weight part: alkylphenol polyoxyethylene 12-15 part, citric acid 13-18 part, silicone emulsion 28-32 part, trichoroacetic acid(TCA) 4-6 part, Thiocarb 8-12 part.
3. the polishing fluid of the mechanical means for stainless steel according to claim 2, it is characterized in that, be made up of the following raw material according to weight part: alkylphenol polyoxyethylene 14 parts, citric acid 15 parts, silicone emulsion 30 parts, trichoroacetic acid(TCA) 5 parts, Thiocarb 10 parts.
4., according to the preparation method of the polishing fluid of the arbitrary described mechanical means for stainless steel of claim 1-3, it is characterized in that, be made up of following steps:
1) insert in Thiocarb by trichoroacetic acid(TCA), microwave treatment, microwave treatment conditions is: adjustment microwave frequency is 1000-1200MHz, and microwave heating power is 90-110W, and microwave treatment time is 0.5-2h, obtains mixed liquor A for subsequent use;
2) insert in silicone emulsion by alkylphenol polyoxyethylene, citric acid, heated sealed, to 70-80 DEG C, stirs 0.3-0.8h, be cooled to 50-60 DEG C, add mixed liquor A again, 1-2h is stirred in sealing, is down to the polishing fluid that namely room temperature obtains the mechanical means for stainless steel.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510806959.9A CN105463466A (en) | 2015-11-22 | 2015-11-22 | Polishing liquid for stainless steel mechanical equipment and preparing method of polishing liquid |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510806959.9A CN105463466A (en) | 2015-11-22 | 2015-11-22 | Polishing liquid for stainless steel mechanical equipment and preparing method of polishing liquid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105463466A true CN105463466A (en) | 2016-04-06 |
Family
ID=55601614
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510806959.9A Pending CN105463466A (en) | 2015-11-22 | 2015-11-22 | Polishing liquid for stainless steel mechanical equipment and preparing method of polishing liquid |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105463466A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109097779A (en) * | 2018-08-28 | 2018-12-28 | 常州大学 | A kind of electrolytic copper foil titanium cathode roller chemical polishing solution and polishing method |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101016440A (en) * | 2006-02-08 | 2007-08-15 | 罗门哈斯电子材料Cmp控股股份有限公司 | Multi-component barrier polishing solution |
| CN103590044A (en) * | 2013-11-06 | 2014-02-19 | 天津圳鹏清洗技术开发有限公司 | Metal polishing agent and preparation method thereof |
| CN104131291A (en) * | 2014-07-01 | 2014-11-05 | 蚌埠市高华电子有限公司 | Novel composite metal polishing fluid and preparation method thereof |
| CN104830234A (en) * | 2015-04-23 | 2015-08-12 | 深圳杰明纳微电子科技有限公司 | A-directional sapphire mobile phone cover plate polishing solution and preparation method thereof |
| CN105038606A (en) * | 2015-06-16 | 2015-11-11 | 盐城工学院 | Special polishing solution for gallium oxide substrate polishing and preparation method thereof |
-
2015
- 2015-11-22 CN CN201510806959.9A patent/CN105463466A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101016440A (en) * | 2006-02-08 | 2007-08-15 | 罗门哈斯电子材料Cmp控股股份有限公司 | Multi-component barrier polishing solution |
| CN103590044A (en) * | 2013-11-06 | 2014-02-19 | 天津圳鹏清洗技术开发有限公司 | Metal polishing agent and preparation method thereof |
| CN104131291A (en) * | 2014-07-01 | 2014-11-05 | 蚌埠市高华电子有限公司 | Novel composite metal polishing fluid and preparation method thereof |
| CN104830234A (en) * | 2015-04-23 | 2015-08-12 | 深圳杰明纳微电子科技有限公司 | A-directional sapphire mobile phone cover plate polishing solution and preparation method thereof |
| CN105038606A (en) * | 2015-06-16 | 2015-11-11 | 盐城工学院 | Special polishing solution for gallium oxide substrate polishing and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109097779A (en) * | 2018-08-28 | 2018-12-28 | 常州大学 | A kind of electrolytic copper foil titanium cathode roller chemical polishing solution and polishing method |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101392149B (en) | Water-soluble solid polishing wax | |
| CN106281045A (en) | A kind of nano material formula for precision stainless steel polishing and preparation technology thereof | |
| CN108165178A (en) | A kind of mobile phone metal rear shell antiscuffing paste | |
| CN111647356A (en) | Diamond polishing solution and preparation method thereof | |
| CN102965668B (en) | Polishing solution for processing stainless steel plate material 8K mirror surface | |
| CN104130714B (en) | A kind of mixed polishing solution being applicable to metal containing abrasive material and preparation method thereof | |
| CN108034293A (en) | A kind of water-based metal baking vanish | |
| CN105463466A (en) | Polishing liquid for stainless steel mechanical equipment and preparing method of polishing liquid | |
| CN101875818A (en) | Polishing liquid used for stainless steel mirror surface and preparation method | |
| CN103773246A (en) | Liquid polishing wax composition | |
| CN103659551A (en) | Ultra-precision polishing method for stainless steel metal product | |
| CN105199610B (en) | A kind of sapphire polishing composition and preparation method thereof | |
| CN109468579B (en) | Mold targeting surface treatment method based on vacuum heat treatment and boronizing agent | |
| CN107304348A (en) | A kind of method that microwave heating prepares diamond paste | |
| CN105950844A (en) | Quenching oil dedicated to small module gears and preparation method of quenching oil | |
| CN107629846A (en) | A kind of honing oil | |
| CN109338368A (en) | A kind of polishing fluid and preparation method thereof | |
| CN107385386A (en) | A kind of high rigidity, high infiltration rate and big infiltration layer salt bath B-V co-penetrant and co-penetration technology | |
| CN110283571A (en) | A kind of modified new type abrasive in surface | |
| CN103881588A (en) | Raw material and preparation method of multifunctional brightener | |
| CN104131286B (en) | Metal-polishing liquid that a kind of steady quality polishing efficiency is high and preparation method thereof | |
| CN106675755A (en) | Glass grinding fluid capable of effectively dispersing boron carbide grinding material and preparation method of glass grinding fluid | |
| CN107022727B (en) | A kind of heating means of the big substance titanium base of big thickness | |
| CN105968270B (en) | A kind of composite ceramic water-reducing agent and preparation method thereof | |
| CN109554710A (en) | A kind of acid decoating liquid and obstacles in quit containing titanium coating |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20160406 |