CN105462536A - 一种水性硅烷改性聚氨酯粘合剂及其制备方法 - Google Patents
一种水性硅烷改性聚氨酯粘合剂及其制备方法 Download PDFInfo
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- CN105462536A CN105462536A CN201510916178.5A CN201510916178A CN105462536A CN 105462536 A CN105462536 A CN 105462536A CN 201510916178 A CN201510916178 A CN 201510916178A CN 105462536 A CN105462536 A CN 105462536A
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- 239000004432 silane-modified polyurethane Substances 0.000 title claims abstract description 40
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- 239000007767 bonding agent Substances 0.000 title abstract 5
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 29
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims abstract description 24
- 239000006087 Silane Coupling Agent Substances 0.000 claims abstract description 14
- 239000003822 epoxy resin Substances 0.000 claims abstract description 12
- 229920000647 polyepoxide Polymers 0.000 claims abstract description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000008367 deionised water Substances 0.000 claims abstract description 6
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 6
- 239000004721 Polyphenylene oxide Substances 0.000 claims abstract description 5
- 239000002253 acid Substances 0.000 claims abstract description 5
- 229920000570 polyether Polymers 0.000 claims abstract description 5
- 239000002994 raw material Substances 0.000 claims abstract description 3
- 238000006243 chemical reaction Methods 0.000 claims description 26
- ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 claims description 21
- 229920001730 Moisture cure polyurethane Polymers 0.000 claims description 20
- AZYRZNIYJDKRHO-UHFFFAOYSA-N 1,3-bis(2-isocyanatopropan-2-yl)benzene Chemical compound O=C=NC(C)(C)C1=CC=CC(C(C)(C)N=C=O)=C1 AZYRZNIYJDKRHO-UHFFFAOYSA-N 0.000 claims description 14
- 238000003756 stirring Methods 0.000 claims description 13
- UKLDJPRMSDWDSL-UHFFFAOYSA-L [dibutyl(dodecanoyloxy)stannyl] dodecanoate Chemical compound CCCCCCCCCCCC(=O)O[Sn](CCCC)(CCCC)OC(=O)CCCCCCCCCCC UKLDJPRMSDWDSL-UHFFFAOYSA-L 0.000 claims description 12
- 150000002009 diols Chemical class 0.000 claims description 12
- 229920000909 polytetrahydrofuran Polymers 0.000 claims description 12
- OMIGHNLMNHATMP-UHFFFAOYSA-N 2-hydroxyethyl prop-2-enoate Chemical compound OCCOC(=O)C=C OMIGHNLMNHATMP-UHFFFAOYSA-N 0.000 claims description 10
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 10
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 claims description 10
- 238000004945 emulsification Methods 0.000 claims description 10
- IQPQWNKOIGAROB-UHFFFAOYSA-N isocyanate group Chemical group [N-]=C=O IQPQWNKOIGAROB-UHFFFAOYSA-N 0.000 claims description 10
- 239000000203 mixture Substances 0.000 claims description 10
- PTBDIHRZYDMNKB-UHFFFAOYSA-N 2,2-Bis(hydroxymethyl)propionic acid Chemical compound OCC(C)(CO)C(O)=O PTBDIHRZYDMNKB-UHFFFAOYSA-N 0.000 claims description 7
- ZPOLNCDBPYJDSE-UHFFFAOYSA-N 3-[4-[bis(2-chloroethyl)amino]phenyl]-2-formamidopropanoic acid Chemical compound O=CNC(C(=O)O)CC1=CC=C(N(CCCl)CCCl)C=C1 ZPOLNCDBPYJDSE-UHFFFAOYSA-N 0.000 claims description 7
- HNJBEVLQSNELDL-UHFFFAOYSA-N pyrrolidin-2-one Chemical compound O=C1CCCN1 HNJBEVLQSNELDL-UHFFFAOYSA-N 0.000 claims description 7
- 239000003153 chemical reaction reagent Substances 0.000 claims description 6
- 230000006837 decompression Effects 0.000 claims description 5
- 230000018044 dehydration Effects 0.000 claims description 5
- 238000006297 dehydration reaction Methods 0.000 claims description 5
- 229910052757 nitrogen Inorganic materials 0.000 claims description 5
- 238000010992 reflux Methods 0.000 claims description 5
- 150000002334 glycols Chemical class 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 4
- 238000013019 agitation Methods 0.000 claims description 2
- 238000010438 heat treatment Methods 0.000 claims description 2
- 239000003643 water by type Substances 0.000 claims description 2
- 239000000853 adhesive Substances 0.000 abstract description 11
- 230000001070 adhesive effect Effects 0.000 abstract description 11
- 229920002635 polyurethane Polymers 0.000 abstract description 9
- 239000004814 polyurethane Substances 0.000 abstract description 9
- 230000032683 aging Effects 0.000 abstract description 6
- 238000005187 foaming Methods 0.000 abstract description 3
- 230000002209 hydrophobic effect Effects 0.000 abstract description 3
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 abstract 2
- SECXISVLQFMRJM-UHFFFAOYSA-N N-Methylpyrrolidone Chemical compound CN1CCCC1=O SECXISVLQFMRJM-UHFFFAOYSA-N 0.000 abstract 2
- GETQZCLCWQTVFV-UHFFFAOYSA-N trimethylamine Chemical compound CN(C)C GETQZCLCWQTVFV-UHFFFAOYSA-N 0.000 abstract 2
- 238000009835 boiling Methods 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 125000005442 diisocyanate group Chemical group 0.000 abstract 1
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 abstract 1
- 229920005749 polyurethane resin Polymers 0.000 abstract 1
- 239000000758 substrate Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 description 7
- QVYARBLCAHCSFJ-UHFFFAOYSA-N butane-1,1-diamine Chemical compound CCCC(N)N QVYARBLCAHCSFJ-UHFFFAOYSA-N 0.000 description 3
- 238000007711 solidification Methods 0.000 description 3
- 230000008023 solidification Effects 0.000 description 3
- 229920002803 thermoplastic polyurethane Polymers 0.000 description 3
- 239000011230 binding agent Substances 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000004134 energy conservation Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 230000008719 thickening Effects 0.000 description 1
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J175/00—Adhesives based on polyureas or polyurethanes; Adhesives based on derivatives of such polymers
- C09J175/04—Polyurethanes
- C09J175/08—Polyurethanes from polyethers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/08—Processes
- C08G18/10—Prepolymer processes involving reaction of isocyanates or isothiocyanates with compounds having active hydrogen in a first reaction step
- C08G18/12—Prepolymer processes involving reaction of isocyanates or isothiocyanates with compounds having active hydrogen in a first reaction step using two or more compounds having active hydrogen in the first polymerisation step
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/40—High-molecular-weight compounds
- C08G18/4009—Two or more macromolecular compounds not provided for in one single group of groups C08G18/42 - C08G18/64
- C08G18/4045—Mixtures of compounds of group C08G18/58 with other macromolecular compounds
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/65—Low-molecular-weight compounds having active hydrogen with high-molecular-weight compounds having active hydrogen
- C08G18/66—Compounds of groups C08G18/42, C08G18/48, or C08G18/52
- C08G18/6633—Compounds of group C08G18/42
- C08G18/6659—Compounds of group C08G18/42 with compounds of group C08G18/34
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/65—Low-molecular-weight compounds having active hydrogen with high-molecular-weight compounds having active hydrogen
- C08G18/66—Compounds of groups C08G18/42, C08G18/48, or C08G18/52
- C08G18/6666—Compounds of group C08G18/48 or C08G18/52
- C08G18/6692—Compounds of group C08G18/48 or C08G18/52 with compounds of group C08G18/34
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/67—Unsaturated compounds having active hydrogen
- C08G18/671—Unsaturated compounds having only one group containing active hydrogen
- C08G18/672—Esters of acrylic or alkyl acrylic acid having only one group containing active hydrogen
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/72—Polyisocyanates or polyisothiocyanates
- C08G18/74—Polyisocyanates or polyisothiocyanates cyclic
- C08G18/76—Polyisocyanates or polyisothiocyanates cyclic aromatic
- C08G18/7614—Polyisocyanates or polyisothiocyanates cyclic aromatic containing only one aromatic ring
- C08G18/7628—Polyisocyanates or polyisothiocyanates cyclic aromatic containing only one aromatic ring containing at least one isocyanate or isothiocyanate group linked to the aromatic ring by means of an aliphatic group
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Adhesives Or Adhesive Processes (AREA)
- Polyurethanes Or Polyureas (AREA)
Abstract
Description
固含量/% | 45 | 拉伸强度/MPa | 50 |
平均粒径/μm | <0.15 | 断裂伸长率/% | 500 |
粘度(为增稠)/mPa.s | 200 | 邵氏A硬度 | 55 |
表面张力/N.m-1 | 55 | PH值 | 6.8 |
Claims (7)
Priority Applications (1)
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CN201510916178.5A CN105462536B (zh) | 2015-12-11 | 2015-12-11 | 一种水性硅烷改性聚氨酯粘合剂及其制备方法 |
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CN201510916178.5A CN105462536B (zh) | 2015-12-11 | 2015-12-11 | 一种水性硅烷改性聚氨酯粘合剂及其制备方法 |
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CN105462536A true CN105462536A (zh) | 2016-04-06 |
CN105462536B CN105462536B (zh) | 2019-02-12 |
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Cited By (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105950030A (zh) * | 2016-06-15 | 2016-09-21 | 安徽扬帆充气游乐设备制造有限公司 | 一种充气船艇用复合胶黏剂 |
CN105950029A (zh) * | 2016-06-15 | 2016-09-21 | 安徽扬帆充气游乐设备制造有限公司 | 一种充气船艇用耐水胶黏剂 |
CN106085254A (zh) * | 2016-06-15 | 2016-11-09 | 安徽扬帆充气游乐设备制造有限公司 | 一种高性能充气船艇用胶黏剂 |
CN109880512A (zh) * | 2019-02-18 | 2019-06-14 | 南京信息工程大学 | 硅烷改性聚氨酯防水涂料及其制备方法 |
CN111394050A (zh) * | 2020-05-18 | 2020-07-10 | 南京信息工程大学 | 一种水性eva封装聚氨酯粘合剂及其生产工艺 |
CN111484790A (zh) * | 2020-05-18 | 2020-08-04 | 南京信息工程大学 | 一种公路隧道喷涂吸音涂料及其制备方法 |
CN112226196A (zh) * | 2020-11-02 | 2021-01-15 | 南京工业大学 | 一种水性聚氨酯粘合剂及其制备方法 |
CN113249081A (zh) * | 2021-07-15 | 2021-08-13 | 中国科学院过程工程研究所 | 一种聚氨酯胶膜及其制备方法和应用 |
CN115466591A (zh) * | 2022-10-19 | 2022-12-13 | 张丽君 | 一种水性聚氨酯粘合剂及其制备工艺 |
CN115975525A (zh) * | 2023-01-30 | 2023-04-18 | 开普洛克(苏州)材料科技有限公司 | 一种含有改性胶粘剂的可回收保护膜 |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103881640A (zh) * | 2014-03-27 | 2014-06-25 | 山东华诚高科胶粘剂有限公司 | 一种用于软包装复合的单组份水性聚氨酯胶的制备方法 |
-
2015
- 2015-12-11 CN CN201510916178.5A patent/CN105462536B/zh active Active
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103881640A (zh) * | 2014-03-27 | 2014-06-25 | 山东华诚高科胶粘剂有限公司 | 一种用于软包装复合的单组份水性聚氨酯胶的制备方法 |
Non-Patent Citations (1)
Title |
---|
刘益军: "《聚氨酯原料及助剂手册》", 31 January 2013 * |
Cited By (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105950030A (zh) * | 2016-06-15 | 2016-09-21 | 安徽扬帆充气游乐设备制造有限公司 | 一种充气船艇用复合胶黏剂 |
CN105950029A (zh) * | 2016-06-15 | 2016-09-21 | 安徽扬帆充气游乐设备制造有限公司 | 一种充气船艇用耐水胶黏剂 |
CN106085254A (zh) * | 2016-06-15 | 2016-11-09 | 安徽扬帆充气游乐设备制造有限公司 | 一种高性能充气船艇用胶黏剂 |
CN109880512A (zh) * | 2019-02-18 | 2019-06-14 | 南京信息工程大学 | 硅烷改性聚氨酯防水涂料及其制备方法 |
CN111394050A (zh) * | 2020-05-18 | 2020-07-10 | 南京信息工程大学 | 一种水性eva封装聚氨酯粘合剂及其生产工艺 |
CN111484790A (zh) * | 2020-05-18 | 2020-08-04 | 南京信息工程大学 | 一种公路隧道喷涂吸音涂料及其制备方法 |
CN112226196A (zh) * | 2020-11-02 | 2021-01-15 | 南京工业大学 | 一种水性聚氨酯粘合剂及其制备方法 |
CN113249081A (zh) * | 2021-07-15 | 2021-08-13 | 中国科学院过程工程研究所 | 一种聚氨酯胶膜及其制备方法和应用 |
CN113249081B (zh) * | 2021-07-15 | 2021-10-08 | 中国科学院过程工程研究所 | 一种聚氨酯胶膜及其制备方法和应用 |
CN115466591A (zh) * | 2022-10-19 | 2022-12-13 | 张丽君 | 一种水性聚氨酯粘合剂及其制备工艺 |
CN115466591B (zh) * | 2022-10-19 | 2024-01-12 | 珠海固瑞泰复合材料有限公司 | 一种水性聚氨酯粘合剂及其制备工艺 |
CN115975525A (zh) * | 2023-01-30 | 2023-04-18 | 开普洛克(苏州)材料科技有限公司 | 一种含有改性胶粘剂的可回收保护膜 |
CN115975525B (zh) * | 2023-01-30 | 2023-10-20 | 开普洛克(苏州)材料科技有限公司 | 一种含有改性胶粘剂的可回收保护膜 |
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Effective date of registration: 20191224 Address after: 201507, 3, No. two, No. 2-20, West Road, Industrial Development Zone, Cao Jing Town, Shanghai, Jinshan District Patentee after: YOUXING SHARK (SHANGHAI) TECHNOLOGY CO.,LTD. Address before: The Olympic Avenue in Jianye District of Nanjing city of Jiangsu Province, No. 69 210019 Patentee before: Nanjing University of Information Science and Technology |
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Denomination of invention: A water-based silane modified polyurethane adhesive and its preparation method Effective date of registration: 20230509 Granted publication date: 20190212 Pledgee: Shanghai Rural Commercial Bank Co.,Ltd. Jinshan sub branch Pledgor: YOUXING SHARK (SHANGHAI) TECHNOLOGY CO.,LTD. Registration number: Y2023310000176 |
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Granted publication date: 20190212 Pledgee: Shanghai Rural Commercial Bank Co.,Ltd. Jinshan sub branch Pledgor: YOUXING SHARK (SHANGHAI) TECHNOLOGY CO.,LTD. Registration number: Y2023310000176 |
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Denomination of invention: A waterborne silane modified polyurethane adhesive and its preparation method Granted publication date: 20190212 Pledgee: Shanghai Rural Commercial Bank Co.,Ltd. Jinshan sub branch Pledgor: YOUXING SHARK (SHANGHAI) TECHNOLOGY CO.,LTD. Registration number: Y2024310000529 |