CN105462292A - Disperse dye composition and preparation method and application thereof - Google Patents
Disperse dye composition and preparation method and application thereof Download PDFInfo
- Publication number
- CN105462292A CN105462292A CN201510988977.3A CN201510988977A CN105462292A CN 105462292 A CN105462292 A CN 105462292A CN 201510988977 A CN201510988977 A CN 201510988977A CN 105462292 A CN105462292 A CN 105462292A
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- hydrogen
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- disperse dye
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- 0 *C(C=CC1=*C*2)=CC1=C2*=*[C@@](C(*C([N+]1[I-]C1)=O)C=C1C(N)N*)C=C1O Chemical compound *C(C=CC1=*C*2)=CC1=C2*=*[C@@](C(*C([N+]1[I-]C1)=O)C=C1C(N)N*)C=C1O 0.000 description 2
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0033—Blends of pigments; Mixtured crystals; Solid solutions
- C09B67/0046—Mixtures of two or more azo dyes
- C09B67/0051—Mixtures of two or more azo dyes mixture of two or more monoazo dyes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0071—Process features in the making of dyestuff preparations; Dehydrating agents; Dispersing agents; Dustfree compositions
- C09B67/0079—Azoic dyestuff preparations
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0071—Process features in the making of dyestuff preparations; Dehydrating agents; Dispersing agents; Dustfree compositions
- C09B67/008—Preparations of disperse dyes or solvent dyes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0071—Process features in the making of dyestuff preparations; Dehydrating agents; Dispersing agents; Dustfree compositions
- C09B67/0092—Dyes in solid form
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/16—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dispersed, e.g. acetate, dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/02—Material containing basic nitrogen
- D06P3/04—Material containing basic nitrogen containing amide groups
- D06P3/14—Wool
- D06P3/143—Wool using dispersed dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/02—Material containing basic nitrogen
- D06P3/04—Material containing basic nitrogen containing amide groups
- D06P3/24—Polyamides; Polyurethanes
- D06P3/26—Polyamides; Polyurethanes using dispersed dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/34—Material containing ester groups
- D06P3/36—Material containing ester groups using dispersed dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/34—Material containing ester groups
- D06P3/52—Polyesters
- D06P3/54—Polyesters using dispersed dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/70—Material containing nitrile groups
- D06P3/72—Material containing nitrile groups using dispersed dyestuffs
Landscapes
- Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Coloring (AREA)
Abstract
The invention relates to a disperse dye composition and a preparation method and application thereof. The disperse dye composition comprises two compounds of different structures as shown in formula I, at least one compound as shown in formula II and a compound as shown in formula III. The preparation method comprises the steps: uniformly mixing the compounds shown from formula I to formula III and additives, grinding, and spray drying to obtain the disperse dye composition. The disperse dye composition is used for dyeing a blended material of hydrophobic fibers or fibers. The disperse dye composition is good in color fastness and leveling property, good in washing fastness, fastness to rubbing, perspiration fastness, sublimation fastness and lifting power and also good in light fastness; and the preparation method is simple in process, low in cost and good in application prospect.
Description
Technical field
The invention belongs to nonionic dye field, particularly a kind of disperse dye composition and its preparation method and application.
Background technology
Dispersed dye are the water-soluble lower nonionic dyes of a class.Dispersed dye for the dyeing of cellulose acetate fibre, are called cellulose acetate dye the earliest.Along with the development of synthon, polyamide fibre, terylene occur in succession, especially terylene, high owing to having permutation degree, the characteristics such as fiber gap is few, and hydrophobicity is strong.This fiber will make swelling of fiber under high temperature, thermosol, and dyestuff just can enter fiber and upper dye.Along with the development of synthon, people it is also proposed new requirement to dyestuff, and dyestuff in the past has applied defect, and such as dye uptake is low, and fastness is difficult to allow people accept.
Therefore, need to develop a kind of can being suitable for and the new dye on multiclass fiber and its blended product.
Summary of the invention
Technical problem to be solved by this invention is to provide a kind of disperse dye composition and its preparation method and application, and this disperse dye composition has good degree of fixation, level-dyeing property; There is good washing fastness, fastness to rubbing, color fastness to perspiration, fastness to sublimation and lifting force, in addition, light fastness also especially good; Preparation method's technique is simple, and cost is low, has a good application prospect.
A kind of disperse dye composition of the present invention, comprises the compound shown in two formula I with different structure
With the compound shown at least one formula II
With the compound shown in a formula III
Wherein,
R
1hydrogen, (C
1-C
4) alkyl or halogen;
R
2hydrogen or (C
1-C
4) alkyl;
R
3to R
6independently be selected from (C
1-C
4) alkyl, (CH
2)
n-O-(C
1-C
4) alkyl, (CH
2)
n-O-CO-(C
1-C
4) alkyl, (CH
2)
n-COO-(C
1-C
4) alkyl, (CH
2)
n-phenyl or (CH
2)
n-COO (CH
2)
m-CO-(C
1-C
4) alkyl;
X
1-X
6independently be selected from hydrogen, halogen, nitro, cyano group, carbonyl, SCN or CO-NR
2r
3;
Y
1hydrogen, (C
1-C
4) alkyl, replacement (C
1-C
4) alkyl, (C
2-C
4) thiazolinyl or (CH
2)
m-phenyl;
Y
2hydrogen, (C
1-C
4) alkyl or (C
1-C
4) alkoxyl group;
Y
3hydrogen, (C
1-C
4) alkyl or (C
1-C
4) alkoxyl group;
Above n and m is 1,2,3 or 4 respectively.
Preferably, R described in general structure
1hydrogen, (C
1-C
2) alkyl or halogen;
R
2hydrogen or (C
1-C
2) alkyl;
R
3to R
6independently be selected from (C
1-C
2) alkyl, (CH
2)
n-COO-(C
1-C
2) alkyl, (CH
2)
n-phenyl or (CH
2)
n-COO (CH
2)
m-CO-(C
1-C
2) alkyl;
X
1and X
2independently be selected from hydrogen, nitro, cyano group, bromine or chlorine;
X
3-X
5independently be selected from hydrogen, nitro, bromine or chlorine;
X
6nitro or cyano group;
Y
1(C
1-C
4) alkyl or (CH
2)
m-phenyl;
Y
2hydrogen or (C
1-C
2) alkyl;
Y
3hydrogen, (C
1-C
2) alkyl or (C
1-C
2) alkoxyl group;
Above n and m is 1 or 2 respectively.
Preferred, R described in general structure
1hydrogen or methyl;
R
2methyl or ethyl;
R
3to R
6independently be selected from (C
1-C
2) alkyl, (CH
2)
n-COO-(C
1-C
2) alkyl, (CH
2)
n-phenyl or (CH
2)
n-COO (CH
2)
m-CO-(C
1-C
2) alkyl;
X
1and X
2independently be selected from hydrogen, nitro, cyano group, bromine or chlorine;
X
3and X
6it is nitro;
X
4and X
5independently be selected from nitro, bromine or chlorine;
Y
1(CH
2)
m-phenyl;
Y
2hydrogen or methyl;
Y
3hydrogen, methoxy or ethoxy;
Above n and m is 1 or 2 respectively.
Most preferred, R described in general structure
1hydrogen;
R
2methyl or ethyl;
R
3to R
6independently be selected from (CH
2)
n-COO-(C
1-C
2) alkyl;
X
1and X
2independently be selected from hydrogen, nitro, cyano group, bromine or chlorine;
X
3and X
6it is nitro;
X
4and X
5independently be selected from nitro, bromine or chlorine;
Y
1(CH
2)
m-phenyl;
Y
2hydrogen or methyl;
Y
3it is methoxyl group;
Above n and m is 1 or 2 respectively.
Preferably, described disperse dye composition comprise the compound shown in two formula I with different structure and one there is the compound shown in formula II and one there is the compound shown in formula III.
Most preferred, described disperse dye composition comprises the compound shown in formula I-1
With the compound shown in formula I-2
With the compound shown in formula II-1
With the compound shown in formula III-1
Disperse dye composition of the present invention also comprises auxiliary agent; Wherein, auxiliary agent is dispersion agent and/or diffusant.
Described auxiliary agent is one or more in naphthalene sulfonic acidformaldehyde condensation product, sulfonated lignin, alkyl naphthalene sulfonic acid formaldehyde condensation products.
Described naphthalene sulfonic acidformaldehyde condensation product is one or more in dispersing agent NNO, Dispersant MF, dispersing agent CNF.
The compounds content shown in formula I that two described structures are different is respectively the 0.5-10% of dye composite total mass separately, preferred 1-5%; Compounds content shown in described formula II is the 5-45% of dye composite total mass, preferred 10-35%; Compounds content shown in described formula III is the 0.5-5% of dye composite total mass, preferred 1-3%; All the other are auxiliary agent.The mass ratio of the compound shown in formula I that two structures are different is 1:5-5:1.
Further, described formula I-1 compounds content is the 0.5-10% of dyestuff total mass, preferred 1-5%; Described formula I-2 compounds content is the 0.5-10% of dyestuff total mass, preferred 1-5%, more preferably 1.2%; Described formula II-1 compounds content is the 5-45% of dyestuff total amount, preferred 10-35%; Described formula III-1 compounds content is the 0.5-5% of dyestuff total amount, preferred 1-3%; All the other are auxiliary agent.The mass ratio of the compound shown in formula I-1 and formula I-2 is 1:5-5:1.
Another aspect of the present invention, is to provide a kind of aqueous solution of dyeing, comprises above-mentioned disperse dye composition, and in the described aqueous solution, the content of dye composite is 0.001% to 20%, and preferably 0.005% to 16%.
The preparation method of a kind of disperse dye composition of the present invention, comprising:
Compound shown in formula I to formula III mixed with auxiliary agent and grinds, then carrying out spraying dry, to obtain final product.
The application of a kind of disperse dye composition of the present invention, described disperse dye composition is applied to the dyeing of the blend of hydrophobic fibre or fiber.
Described hydrophobic fibre or blend include but not limited to: cellulose acetate fibre, cotton, nylon, trevira, acrylic fibers, wool, spandex.Described textile materials or its blend can be thread, bulk fibre, yarn or form that is woven or knit goods.
The preparation method of compound of the present invention method can prepare disclosed in referenced patent CN101522816, JP58152056 and EP5551779.
beneficial effect
Disperse dye composition of the present invention has good degree of fixation, level-dyeing property; There is good washing fastness, fastness to rubbing, color fastness to perspiration, fastness to sublimation and lifting force, in addition, light fastness also especially good; Preparation method's technique is simple, and cost is low, has a good application prospect.
Embodiment
Below in conjunction with specific embodiment, set forth the present invention further.Should be understood that these embodiments are only not used in for illustration of the present invention to limit the scope of the invention.In addition should be understood that those skilled in the art can make various changes or modifications the present invention, and these equivalent form of values fall within the application's appended claims limited range equally after the content of having read the present invention's instruction.
Embodiment 1
By formula (I-1) 4.5g, formula (I-2) 1.2g, formula (II-1) 31.7g, formula (III-1) 1.9g and Dispersant MF 60.7g adds water after blending, use shredder grinding distribution, then carry out spraying dry, obtain dark blue dyes composition.
Embodiment 2
By formula (I-1) 5g, formula (I-2) 2.3g, formula (II-2) 34.9g, formula (III-1) 0.9g and dispersion agent NNO56.9g adds water after blending, use shredder grinding distribution, then carry out spraying dry, obtain mazarine to black dye composition.
Embodiment 3
By formula (I-1) 1.0g, formula (I-2) 4.2g, formula (II-1) 20.4g, formula (III-2) 3g and dispersion agent sodium lignosulfonate 71.4g adds water after blending, use shredder grinding distribution, then carry out spraying dry, obtain mazarine to black dye composition.
Embodiment 4
By formula (I-3) 0.5g, formula (I-2) 6.0g, formula (II-1) 40.0g, formula (III-1) 4.5g and Dispersant MF 49.0g adds water after blending, use shredder grinding distribution, then carry out spraying dry, obtain mazarine to black dye composition.
Embodiment 5
By formula (I-1) 1.0g, formula (I-4) 4.8g, formula (II-3) 10.9g, formula (III-1) 2.5g and Dispersant MF 80.8g adds water after blending, use shredder grinding distribution, then carry out spraying dry, obtain mazarine to black dye composition.
Embodiment 6
By formula (I-5) 3.5g, formula (I-4) 2.0g, formula (II-3) 40.0g, formula (III-1) 1.0g and Dispersant MF 53.5g adds water after blending, use shredder grinding distribution, then carry out spraying dry, obtain mazarine to black dye composition.
Embodiment 7
By formula (I-1) 5.0g, formula (I-2) 5.0g, formula (II-1) 10.0g, formula (III-1) 3.0g and Dispersant MF 77.0g adds water after blending, use shredder grinding distribution, then carry out spraying dry, obtain mazarine to black dye composition.
Embodiment 8
By formula (I-1) 1.0g, formula (I-2) 5.0g, formula (II-1) 35.0g, formula (III-1) 3.0g and Dispersant MF 56.0g adds water after blending, use shredder grinding distribution, then carry out spraying dry, obtain mazarine to black dye composition.
Embodiment 9
By formula (I-1) 0.5g, formula (I-2) 7.6g, formula (II-1) 39.5g, formula (III-1) 4.1g and Dispersant MF 48.3g adds water after blending, use shredder grinding distribution, then carry out spraying dry, obtain mazarine to black dye composition.
Embodiment 10
Respectively get the dispersed dye that 2.0g embodiment 1 ~ 9 is obtained, the dispersed dye suspension that concentration is 2g/L is made into respectively with water, get the water mixing of 2ml and 8ml, regulate dye bath pH to be 5 with acetic acid, be then warming up to 60 DEG C, put into 2g filamentary material as shown in the table simultaneously respectively and carry out high-temperature pressure dyeing, 130 DEG C are warmed up in 30 minutes, be incubated 30 minutes, cooling, sampling.Detect dye uptake.And respectively according to the colour fastness to rubbing of GB relevant regulations testing example 1-9, water-fastness colour fastness, colour fasteness to sunlight and color fastness to sublimation.
Table 1
Table 2
Table 3
Claims (10)
1. a disperse dye composition, is characterized in that: comprise the compound shown in two formula I with different structure
With the compound shown at least one formula II
With the compound shown in a formula III
Wherein,
R
1hydrogen, (C
1-C
4) alkyl or halogen;
R
2hydrogen or (C
1-C
4) alkyl;
R
3to R
6independently be selected from (C
1-C
4) alkyl, (CH
2)
n-O-(C
1-C
4) alkyl, (CH
2)
n-O-CO-(C
1-C
4) alkyl, (CH
2)
n-COO-(C
1-C
4) alkyl, (CH
2)
n-phenyl or (CH
2)
n-COO (CH
2)
m-CO-(C
1-C
4) alkyl;
X
1-X
6independently be selected from hydrogen, halogen, nitro, cyano group, carbonyl, SCN or CO-NR
2r
3;
Y
1hydrogen, (C
1-C
4) alkyl, replacement (C
1-C
4) alkyl, (C
2-C
4) thiazolinyl or (CH
2)
m-phenyl;
Y
2hydrogen, (C
1-C
4) alkyl or (C
1-C
4) alkoxyl group;
Y
3hydrogen, (C
1-C
4) alkyl or (C
1-C
4) alkoxyl group;
Above n and m is 1,2,3 or 4 respectively.
2. a kind of disperse dye composition according to claim 1, is characterized in that: described R
1hydrogen, (C
1-C
2) alkyl or halogen;
R
2hydrogen or (C
1-C
2) alkyl;
R
3to R
6independently be selected from (C
1-C
2) alkyl, (CH
2)
n-COO-(C
1-C
2) alkyl, (CH
2)
n-phenyl or (CH
2)
n-COO (CH
2)
m-CO-(C
1-C
2) alkyl;
X
1and X
2independently be selected from hydrogen, nitro, cyano group, bromine or chlorine;
X
3-X
5independently be selected from hydrogen, nitro, bromine or chlorine;
X
6nitro or cyano group;
Y
1(C
1-C
4) alkyl or (CH
2)
m-phenyl;
Y
2hydrogen or (C
1-C
2) alkyl;
Y
3hydrogen, (C
1-C
2) alkyl or (C
1-C
2) alkoxyl group;
Above n and m is 1 or 2 respectively.
3. a kind of disperse dye composition according to claim 2, is characterized in that: described R
1hydrogen or methyl;
R
2methyl or ethyl;
R
3to R
6independently be selected from (C
1-C
2) alkyl, (CH
2)
n-COO-(C
1-C
2) alkyl, (CH
2)
n-phenyl or (CH
2)
n-COO (CH
2)
m-CO-(C
1-C
2) alkyl;
X
1and X
2independently be selected from hydrogen, nitro, cyano group, bromine or chlorine;
X
3and X
6it is nitro;
X
4and X
5independently be selected from nitro, bromine or chlorine;
Y
1(CH
2)
m-phenyl;
Y
2hydrogen or methyl;
Y
3hydrogen, methoxy or ethoxy;
Above n and m is 1 or 2 respectively.
4. a kind of disperse dye composition according to claim 3, is characterized in that: described R
1hydrogen;
R
2methyl or ethyl;
R
3to R
6independently be selected from (CH
2)
n-COO-(C
1-C
2) alkyl;
X
1and X
2independently be selected from hydrogen, nitro, cyano group, bromine or chlorine;
X
3and X
6it is nitro;
X
4and X
5independently be selected from nitro, bromine or chlorine;
Y
1(CH
2)
m-phenyl;
Y
2hydrogen or methyl;
Y
3it is methoxyl group;
Above n and m is 1 or 2 respectively.
5. a kind of disperse dye composition according to claim 1, is characterized in that: comprise the compound shown in formula I-1
With the compound shown in formula I-2
With the compound shown in formula II-1
With the compound shown in formula III-1
6. a kind of disperse dye composition according to claim 1, is characterized in that: also comprise auxiliary agent; Wherein, auxiliary agent is dispersion agent and/or diffusant.
7. a kind of disperse dye composition according to claim 6, is characterized in that: described auxiliary agent is one or more in naphthalene sulfonic acidformaldehyde condensation product, sulfonated lignin, alkyl naphthalene sulfonic acid formaldehyde condensation products.
8. a kind of disperse dye composition according to claim 6, is characterized in that: the compounds content shown in formula I that two described structures are different is respectively the 0.5-10% of dye composite total mass separately; Compounds content shown in described formula II is the 5-45% of dye composite total mass; Compounds content shown in described formula III is the 0.5-5% of dye composite total mass; All the other are auxiliary agent.
9. a preparation method for disperse dye composition as claimed in claim 1, comprising:
Compound shown in formula I to formula III mixed with auxiliary agent and grinds, then carrying out spraying dry, to obtain final product.
10. an application for disperse dye composition as claimed in claim 1, is characterized in that: described disperse dye composition is applied to the dyeing of the blend of hydrophobic fibre or fiber.
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|---|---|---|---|
| CN201510988977.3A CN105462292A (en) | 2015-12-24 | 2015-12-24 | Disperse dye composition and preparation method and application thereof |
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|---|---|---|---|
| CN201510988977.3A CN105462292A (en) | 2015-12-24 | 2015-12-24 | Disperse dye composition and preparation method and application thereof |
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|---|---|
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ID=55600475
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106867274A (en) * | 2016-12-31 | 2017-06-20 | 浙江龙盛集团股份有限公司 | A kind of dispersion red dye composition and dye preparations |
Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB909843A (en) * | 1959-02-10 | 1962-11-07 | Ici Ltd | New monoazo dyestuffs containing ester groups |
| US4548613A (en) * | 1984-05-18 | 1985-10-22 | American Hoechst Corporation | Yellow disperse dyestuff mixtures and dyeing process |
| CN1886466A (en) * | 2003-12-10 | 2006-12-27 | 克莱里安特财务(Bvi)有限公司 | Disperse dyes |
| CN101273095A (en) * | 2005-06-09 | 2008-09-24 | 克莱里安特财务(Bvi)有限公司 | Disperse azo dyes and mixtures comprising these disperse azo dyes |
| CN101522816A (en) * | 2006-10-27 | 2009-09-02 | 德意志戴斯达纺织品及染料两合公司 | Disperse dyes, their preparation and their use |
| US20100281629A1 (en) * | 2007-09-22 | 2010-11-11 | DyStar Colours Deustschland GmbH | Azo dyes for dyeing and printing hydrophobic materials |
| US20140123407A1 (en) * | 2011-01-15 | 2014-05-08 | Dystar Colours Distribution Gmbh | Disperse dye mixtures, their preparation and use |
| CN104919006A (en) * | 2013-01-14 | 2015-09-16 | 德司达染料分销有限公司 | AOX-free navy and black disperse dye mixtures |
-
2015
- 2015-12-24 CN CN201510988977.3A patent/CN105462292A/en active Pending
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB909843A (en) * | 1959-02-10 | 1962-11-07 | Ici Ltd | New monoazo dyestuffs containing ester groups |
| US4548613A (en) * | 1984-05-18 | 1985-10-22 | American Hoechst Corporation | Yellow disperse dyestuff mixtures and dyeing process |
| CN1886466A (en) * | 2003-12-10 | 2006-12-27 | 克莱里安特财务(Bvi)有限公司 | Disperse dyes |
| CN101273095A (en) * | 2005-06-09 | 2008-09-24 | 克莱里安特财务(Bvi)有限公司 | Disperse azo dyes and mixtures comprising these disperse azo dyes |
| CN101522816A (en) * | 2006-10-27 | 2009-09-02 | 德意志戴斯达纺织品及染料两合公司 | Disperse dyes, their preparation and their use |
| US20100281629A1 (en) * | 2007-09-22 | 2010-11-11 | DyStar Colours Deustschland GmbH | Azo dyes for dyeing and printing hydrophobic materials |
| US20140123407A1 (en) * | 2011-01-15 | 2014-05-08 | Dystar Colours Distribution Gmbh | Disperse dye mixtures, their preparation and use |
| CN104919006A (en) * | 2013-01-14 | 2015-09-16 | 德司达染料分销有限公司 | AOX-free navy and black disperse dye mixtures |
| CN105102547A (en) * | 2013-01-14 | 2015-11-25 | 德司达染料分销有限公司 | High wet fast disperse dye mixtures |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106867274A (en) * | 2016-12-31 | 2017-06-20 | 浙江龙盛集团股份有限公司 | A kind of dispersion red dye composition and dye preparations |
| CN106867274B (en) * | 2016-12-31 | 2019-06-28 | 浙江龙盛集团股份有限公司 | A kind of dispersion red dye composition and dye preparations |
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