CN100412139C - Disperse dye composition - Google Patents
Disperse dye composition Download PDFInfo
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- CN100412139C CN100412139C CNB2006100531044A CN200610053104A CN100412139C CN 100412139 C CN100412139 C CN 100412139C CN B2006100531044 A CNB2006100531044 A CN B2006100531044A CN 200610053104 A CN200610053104 A CN 200610053104A CN 100412139 C CN100412139 C CN 100412139C
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- China
- Prior art keywords
- dyestuff
- formula
- dye composition
- disperse dye
- iii
- Prior art date
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- 239000000203 mixture Substances 0.000 title claims abstract description 35
- 239000000986 disperse dye Substances 0.000 title claims abstract description 29
- 239000000975 dye Substances 0.000 claims abstract description 129
- 150000001875 compounds Chemical class 0.000 claims description 26
- 229910052739 hydrogen Inorganic materials 0.000 claims description 12
- 239000001257 hydrogen Substances 0.000 claims description 12
- 150000002431 hydrogen Chemical class 0.000 claims description 8
- 239000002131 composite material Substances 0.000 claims description 6
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims description 6
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 4
- -1 methoxyl group Chemical group 0.000 claims description 4
- 125000000449 nitro group Chemical group [O-][N+](*)=O 0.000 claims description 4
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 2
- ODFJOVXVLFUVNQ-UHFFFAOYSA-N acetarsol Chemical compound CC(=O)NC1=CC([As](O)(O)=O)=CC=C1O ODFJOVXVLFUVNQ-UHFFFAOYSA-N 0.000 claims description 2
- 239000000460 chlorine Substances 0.000 claims description 2
- 229910052801 chlorine Inorganic materials 0.000 claims description 2
- 125000004093 cyano group Chemical group *C#N 0.000 claims description 2
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 claims description 2
- 229910052736 halogen Inorganic materials 0.000 claims description 2
- 150000002367 halogens Chemical class 0.000 claims description 2
- 238000004043 dyeing Methods 0.000 abstract description 6
- 239000004744 fabric Substances 0.000 abstract description 6
- 229920000728 polyester Polymers 0.000 abstract description 3
- 239000002657 fibrous material Substances 0.000 abstract 1
- 210000004243 sweat Anatomy 0.000 abstract 1
- 238000005406 washing Methods 0.000 abstract 1
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
- 239000012752 auxiliary agent Substances 0.000 description 6
- 239000000047 product Substances 0.000 description 6
- 239000002270 dispersing agent Substances 0.000 description 5
- 238000002156 mixing Methods 0.000 description 5
- 238000002360 preparation method Methods 0.000 description 5
- 239000007859 condensation product Substances 0.000 description 4
- 239000006185 dispersion Substances 0.000 description 4
- 229920005552 sodium lignosulfonate Polymers 0.000 description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- 238000009833 condensation Methods 0.000 description 3
- 230000005494 condensation Effects 0.000 description 3
- 238000001035 drying Methods 0.000 description 3
- 238000005507 spraying Methods 0.000 description 3
- KTHUKEZOIFYPEH-UHFFFAOYSA-N 1-benzylnaphthalene Chemical compound C=1C=CC2=CC=CC=C2C=1CC1=CC=CC=C1 KTHUKEZOIFYPEH-UHFFFAOYSA-N 0.000 description 2
- 229920001732 Lignosulfonate Polymers 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- NVVZQXQBYZPMLJ-UHFFFAOYSA-N formaldehyde;naphthalene-1-sulfonic acid Chemical compound O=C.C1=CC=C2C(S(=O)(=O)O)=CC=CC2=C1 NVVZQXQBYZPMLJ-UHFFFAOYSA-N 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 235000019357 lignosulphonate Nutrition 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 239000004576 sand Substances 0.000 description 2
- 239000000080 wetting agent Substances 0.000 description 2
- WODGMMJHSAKKNF-UHFFFAOYSA-N 2-methylnaphthalene-1-sulfonic acid Chemical compound C1=CC=CC2=C(S(O)(=O)=O)C(C)=CC=C21 WODGMMJHSAKKNF-UHFFFAOYSA-N 0.000 description 1
- 229920004933 Terylene® Polymers 0.000 description 1
- 229920004935 Trevira® Polymers 0.000 description 1
- 125000000129 anionic group Chemical group 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- YDEXUEFDPVHGHE-GGMCWBHBSA-L disodium;(2r)-3-(2-hydroxy-3-methoxyphenyl)-2-[2-methoxy-4-(3-sulfonatopropyl)phenoxy]propane-1-sulfonate Chemical compound [Na+].[Na+].COC1=CC=CC(C[C@H](CS([O-])(=O)=O)OC=2C(=CC(CCCS([O-])(=O)=O)=CC=2)OC)=C1O YDEXUEFDPVHGHE-GGMCWBHBSA-L 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000005020 polyethylene terephthalate Substances 0.000 description 1
- 238000007639 printing Methods 0.000 description 1
- 238000005070 sampling Methods 0.000 description 1
- 238000001694 spray drying Methods 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
- 239000003643 water by type Substances 0.000 description 1
- 238000009941 weaving Methods 0.000 description 1
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- Coloring (AREA)
Abstract
A disperse dye composition consisting essentially of: 1-40 wt% of one or more dyes A shown in formula , 10-70 wt% of one or more dyes B shown in formula (II), 10-50 wt% of one or more dyes C shown in formula (III) and 1-35 wt% of one or more dyes D shown in formula (IV). When the disperse dye composition is used for dyeing polyester fiber materials, dark blue to black dyed fabrics with bright color, good dispersibility, sun resistance, washing resistance, sweat resistance and other excellent performances can be obtained by adjusting the proportion of different components.
Description
(1) technical field
The present invention relates to disperse dye composition, relate in particular to the disperse dye composition of a kind of terylene and BLENDED FABRIC thereof printing and dyeing usefulness.
(2) background technology
Along with the fast development of the new fiber of polyester in recent years and people to the raising that textiles requires, correspondingly, dyeing behavior, environmental-protecting performance that dyestuff itself has are also had higher requirement.Promptly require dyestuff that high lifting force and every fastness of dyeing are arranged.Particularly widely used blue-black dye species, become one of industry research emphasis, but, still can not satisfy the demands fully aspect the application performances such as lifting force and dyefastness from existing composite dye species such as patent JP2005-036071, US2004339252, described prescription dyestuffs such as JP11-158402, US6562082.
(3) summary of the invention
For addressing the above problem, the invention provides a kind of disperse dye composition, by its dispersed dye that are configured to, every fastness excellent property, composite effect is remarkable.
The technical solution adopted for the present invention to solve the technical problems is: a kind of disperse dye composition, basically form by following component: weight percentage be 1 ~ 40% one or more suc as formula the dyestuff A shown in (I), weight percentage be 10 ~ 70% one or more suc as formula the dyestuff B shown in (II), weight percentage be 10 ~ 50% one or more suc as formula the dyestuff C shown in (III), weight percentage be 1 ~ 35% one or more suc as formula the dyestuff D shown in (IV), above weight percentage is based on the total amount of dyestuff A, B, C, D.
In the formula (I), X
1Be NH or O; R
1For-C
3H
6OCH
3,-C
3H
6OC
2H
5Or-C
3H
6OC
2H
4OCH
3
In the formula (II), R
2, R
3Independent separately be hydrogen ,-OCOCH
3Or-OCOCH
2CH
3R
6Be hydrogen, methyl or kharophen;
In the formula (III), X
2, X
3Independent separately is hydrogen, chlorine, cyano group or nitro; Y
1Be methyl, methoxyl group, NHCONH
2, NHCOCH
3Or NHCOCH
2CH
3R
4For hydrogen ,-CH
2COOCH
3Or-CH
2COOCH
2CH
3R
5Be methyl or ethyl;
In the formula (IV), R
9Be hydrogen, C
1～C
4Alkyl or C
3H
6OCH
3R
10, R
11Independent separately but be not simultaneously hydrogen, halogen, nitro ,-COOC
2H
4OC
2H
4OCH
3,-OSO
2-Ph ,-OSO
2N (CH
3)
2,-OSO
2-CH
3,-CO-Ph or-CO-Ph-Cl.
Preferably, based on dyestuff A, dyestuff B, dyestuff C, dyestuff D, the weight percentage of described dyestuff A is 5 ~ 25%, and the weight percentage of described dyestuff B is 15 ~ 50%, the weight percentage of described dyestuff C is 20 ~ 45%, and the weight percentage of described dyestuff D is 5 ~ 25%.
Described dyestuff A is one or more in the compound shown in the formula (I-1) ~ (I-3) preferably:
Described dyestuff B is one or more in the compound shown in the formula (II-1) ~ (II-4) preferably:
Described dyestuff C is one or more in the compound shown in the formula (III-1) ~ (III-9) preferably:
Described dyestuff D is one or more in the compound shown in the formula (IV-1) ~ (IV-7) preferably:
Most preferred: described disperse dye composition is by the dyestuff B shown in the dyestuff A shown in the formula (I-1), the formula (II-1), the dyestuff C shown in the formula (III-1), and the dyestuff D shown in the formula (IV-1) forms; Perhaps: described disperse dye composition is made up of dyestuff A, dyestuff B, dyestuff C, dyestuff D, wherein dyestuff A is the compound shown in the formula (I-1), dyestuff B is a combination of compounds shown in compound shown in the formula (II-1) and the formula (II-2), dyestuff C is the compound shown in the formula (III-1), and dyestuff D is a combination of compounds shown in compound shown in the formula (IV-1) and the formula (IV-2); Perhaps described disperse dye composition is by the dyestuff B shown in the dyestuff A shown in the formula (I-1), the formula (II-1), the dyestuff C shown in the formula (III-1), and the dyestuff D shown in formula (IV-1) and the formula (IV-2) forms.
Dyestuff with disperse dye composition allotment of the present invention can obtain the tone by dark blue-Hei.
Because the singularity of dye industry is difficult to also there is no need to make pure product, can have the impurity in some preparation process usually, also allows to contain the physics impurity of a spot of moisture content and trace when disperse dye composition of the present invention is made finished product.
When utilizing composition of the present invention to prepare dispersed dye, it is synthetic that employed dyestuff A, dyestuff B, dyestuff C and dyestuff D can know the ground mode by those skilled in the art easily, wherein dyestuff A, B, C, D also can also can adopt the commercial goods respectively with reference to the method preparation of introducing among patent US4904796, US4211696, US5550217, the JP10-077583.
Utilize composition preparation dispersed dye of the present invention, generally need to add auxiliary agent during application and disperse.For example that structural formula (I), (II), (III) and structural formula (IV) is represented dyestuff carries out corpusculed with pulverizers such as sand mill or shredders after mixing by above-mentioned proportioning in the presence of auxiliary agent, water or other wetting agent; Dyestuff that also can structural formula (I), (II), (III) and structural formula (IV) is represented carries out mixing with above-mentioned ratio after corpusculed is handled with pulverizers such as sand mill or shredders respectively in the presence of auxiliary agent, water or other wetting agent in addition.Usually, auxiliary agent is 0.8～5: 1 with the ratio of former dyestuff weight.
Described auxiliary agent is dispersed dye dispersion agent commonly used, diffusants etc. when composite, one of preferred following or its several mixture arbitrarily: anionic dispersing agents such as naphthalene sulfonic acidformaldehyde condensation product, alkyl naphthalene sulfonic acid formaldehyde condensation products, benzyl naphthalene sulfonic formaldehyde condensation compound, sulfonated lignin.Particularly, naphthalene sulfonic acidformaldehyde condensation product such as dispersing agent NNO, alkyl naphthalene sulfonic acid formaldehyde condensation products such as Dispersant MF (condensation compound of methyl naphthalene sulfonic acid and formaldehyde), benzyl naphthalene sulfonic formaldehyde condensation compound such as dispersing agent CNF etc., sulfonated lignin such as sodium lignosulfonate (as commercial dispersants Reax 83A, Reax 85A) etc.
Disperse dye composition of the present invention, the liquid state after can corpusculed, emulsifiable paste attitude or with spray-drying process etc. carry out dried powdery, graininess is supplied with dyeing.When dying Polyester Fibers,, can obtain to have that coloured light is gorgeous by adjusting proportion among different with disperse dye composition of the present invention, premium propertiess such as good dispersity, sun-proof, washable, perspiration resistance dark blue to black dyeing and weaving thing.
(5) embodiment
Below in conjunction with specific embodiment the present invention is further described, but protection scope of the present invention is not limited to this.
Embodiment 1
Dyestuff A, the dyestuff B of 45.8 gram formulas (II-1), dyestuff C, the dyestuff D of 8.4 gram formulas (IV-1) of 33.5 gram formulas (III-1), 195 sodium lignosulfonates that restrain with 12.3 gram formulas (I-1), after adding water and piece together mixing, grind dispersion with shredder, spraying drying, the dyestuff that gets product, this dyestuff can offer the good mazarine of the every fastness ability of fabric.
Embodiment 2
Dyestuff A, the dyestuff B of 39 gram formulas (II-1), dyestuff B, the dyestuff C of 31 gram formulas (III-1) of 6 gram formulas (II-2), dyestuff D, the dyestuff D of 7 gram formulas (IV-2) of 10 gram formulas (IV-1), 200 sodium lignosulfonates that restrain with 7 gram formulas (I-1), after adding water and piece together mixing, grind dispersion with shredder, spraying drying, the dyestuff that gets product, this dyestuff can offer the good aterrimus of the every fastness ability of fabric.
Embodiment 3～10
According to the preparation method shown in the embodiment 1,2, described disperse dye composition is pieced together dyestuff A, dyestuff B, dyestuff C, dyestuff D mixed by the continuous data of table 1.
Table 1
| Embodiment | Each composition weight of dyestuff (gram) | Auxiliary agent (gram) | Pure water (gram) | Tone |
| Embodiment 3 | (I-1)∶(II-1)∶(III-2)∶(IV-1)＝5∶20∶17.5∶ 7.5 | 120 | 220 | Dark blue |
| Embodiment 4 | (I-2)∶(II-3)∶(III-5)∶(IV-4)＝7.5∶25∶15∶ 2.5 | 120 | 220 | Dark blue |
| Embodiment 5 | (I-3)∶(II-4)∶(III-9)∶(IV-6)＝5∶22.5∶20∶ 2.5 | 120 | 220 | Dark blue |
| Embodiment 6 | (I-1)∶(II-2)∶(III-6)∶(IV-2)＝10∶17.5∶15∶ 7.5 | 120 | 220 | Dark blue |
| Embodiment 7 | (I-1)∶(II-1)∶(III-1)∶(IV-1)∶(IV-2)＝6∶ 21∶13∶6∶4 | 120 | 220 | Black |
| Embodiment 8 | (I-1)∶(II-1)∶(II-4)∶(III-2)∶(IV-1)∶(IV- 7)＝3∶15∶10∶13∶5∶4 | 120 | 220 | Black |
| Embodiment 9 | (I-2)∶(II-2)∶(II-4)∶(III-6)∶(IV-2)∶(IV- 4)＝5∶10∶12∶15∶5∶3 | 120 | 220 | Black |
| Embodiment 10 | (I-3)∶(II-2)∶(II-3)∶(III-9)∶(IV-3)∶(IV- 6)＝6∶9∶11∶14∶5∶5 | 120 | 220 | Black |
Embodiment 11 ~ 19
Preparation method according to embodiment 1, the structure of the defined dyestuff A of each substituting group, dyestuff B, dyestuff C, dyestuff A is as shown in table 2, described composite dye mixture is pieced together dyestuff A, dyestuff B, dyestuff C by the continuous data shown in the table 3 mixed, gets the dyestuff finished product.
Table 2
Table 3
Embodiment 20
Dyestuff A, dyestuff B, the dyestuff C of 40 gram formulas (III-1) of 30 gram formulas (II-1), dyestuff D, the dyestuff D of 10 gram formulas (IV-2) of 10 gram formulas (IV-1), 200 sodium lignosulfonates that restrain with 10 gram formulas (I-1), after adding water and piece together mixing, grind dispersion with shredder, spraying drying, the dyestuff that gets product, this dyestuff can offer the good aterrimus of the every fastness ability of fabric.
Embodiment 21
Respectively getting 0.5 dispersed dye that make of gram embodiment 1～20 is dispersed in 500 ml waters, mix with 60 milliliters water after drawing 20 milliliters, transferring dye bath PH with acetic acid is 5, be warming up to 70 ℃ put into simultaneously 2 the gram trevira dye, in 30 minutes, be warmed up to 130 ℃ by 70 ℃, be incubated 30 minutes, begin sampling when being cooled to 90 ℃.Observe sample cloth coloured light, adopt that GB GB/T3921-1997, GB/T3920-1997, GB/T3922-1997, GB/T8427-1998 test respectively that it is washable, 4～5 grades of rub resistances, colour fastness to perspiration; 6～7 grades of sun-resistant fastness.
Claims (10)
1. disperse dye composition, form by following component basically:
Weight percentage be 1～40% one or more suc as formula the dyestuff A shown in (I), weight percentage be 10～70% one or more suc as formula the dyestuff B shown in (II), weight percentage be 10～50% one or more suc as formula the dyestuff C shown in (III), weight percentage be 1～35% one or more suc as formula the dyestuff D shown in (IV), above weight percentage is based on the total amount of dyestuff A, B, C, D:
In the formula (I), X
1For-NH or O; R
1For-C
3H
6OCH
3,-C
3H
6OC
2H
5Or-C
3H
6OC
2H
4OCH
3
In the formula (II), R
2, R
3Independent separately be hydrogen ,-OCOCH
3Or-OCOCH
2CH
3R
6Be hydrogen, methyl or kharophen;
In the formula (III), X
2, X
3Independent separately is hydrogen, chlorine, cyano group or nitro; Y
1Be methyl, methoxyl group, NHCONH
2, NHCOCH
3Or NHCOCH
2CH
3R
4For hydrogen ,-CH
2COOCH
3Or-CH
2COOCH
2CH
3R
5Be methyl or ethyl;
In the formula (IV), R
9Be hydrogen, C
1～C
4Alkyl or C
3H
6OCH
3R
10, R
11Independent separately but be not simultaneously hydrogen, halogen, nitro ,-COOC
2H
4OC
2H
4OCH
3,-OSO
2-Ph ,-OSO
2N (CH
3)
2,-OSO
2-CH
3,-CO-Ph or-CO-Ph-Cl.
2. disperse dye composition as claimed in claim 1, it is characterized in that: based on dyestuff A, dyestuff B, dyestuff C, dyestuff D, the weight percentage of described dyestuff A is 5～25%, the weight percentage of described dyestuff B is 15～50%, the weight percentage of described dyestuff C is 20～45%, and the weight percentage of described dyestuff D is 5～25%.
3. disperse dye composition as claimed in claim 1 or 2 is characterized in that: described dyestuff A is selected from one or more in the compound shown in the formula (I-1)～(I-3):
4. disperse dye composition as claimed in claim 1 or 2 is characterized in that: described dyestuff B is selected from one or more in the compound shown in the formula (II-1)～(II-4):
5. disperse dye composition as claimed in claim 1 or 2 is characterized in that: described dyestuff C is selected from one or more in the compound shown in the formula (III-1)～(III-9):
6. disperse dye composition as claimed in claim 1 or 2 is characterized in that: described dyestuff D is selected from one or more in the compound shown in the formula (IV-1)～(IV-7):
7. disperse dye composition as claimed in claim 6 is characterized in that: described dyestuff A is selected from one or more in the compound shown in the formula (I-1)～(I-3):
Described dyestuff B is selected from one or more in the compound shown in the formula (II-1)～(II-4):
Described dyestuff C is selected from one or more in the compound shown in the formula (III-1)～(III-9):
8. disperse dye composition as claimed in claim 7 is characterized in that: described composite disperse dye composition is made up of the dyestuff D shown in the dyestuff B shown in the dyestuff A shown in the formula (I-1), the formula (II-1), the dyestuff C shown in the formula (III-1), the formula (IV-1).
9. disperse dye composition as claimed in claim 7 is characterized in that: described composite disperse dye composition is made up of dyestuff A, dyestuff B, dyestuff C, dyestuff D; Described dyestuff A is the compound shown in the formula (I-1), described dyestuff B is a combination of compounds shown in compound shown in the formula (II-1) and the formula (II-2), described dyestuff C is the compound shown in the formula (III-1), and described dyestuff D is a combination of compounds shown in compound shown in the formula (IV-1) and the formula (IV-2).
10. disperse dye composition as claimed in claim 7, it is characterized in that: described disperse dye composition is by the dyestuff B shown in the dyestuff A shown in the formula (I-1), the formula (II-1), dyestuff C shown in the formula (III-1), the dyestuff D shown in formula (IV-1) and the formula (IV-2) forms.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2006100531044A CN100412139C (en) | 2006-08-23 | 2006-08-23 | Disperse dye composition |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2006100531044A CN100412139C (en) | 2006-08-23 | 2006-08-23 | Disperse dye composition |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1939980A CN1939980A (en) | 2007-04-04 |
| CN100412139C true CN100412139C (en) | 2008-08-20 |
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|---|---|---|---|
| CNB2006100531044A Expired - Fee Related CN100412139C (en) | 2006-08-23 | 2006-08-23 | Disperse dye composition |
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Families Citing this family (12)
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|---|---|---|---|---|
| CN101289414B (en) * | 2007-04-16 | 2012-05-09 | 阮伟刚 | Monoazo compounds, preparation method and uses thereof |
| CN101955691B (en) * | 2010-08-26 | 2013-12-25 | 浙江龙盛集团股份有限公司 | Dispersed deep blue dye composition |
| CN105087183A (en) * | 2010-11-12 | 2015-11-25 | 宝洁公司 | Thienylazo dye and clothes washing and caring composition with same |
| CN102220031B (en) * | 2011-04-15 | 2013-12-11 | 浙江闰土股份有限公司 | Black-and-blue series disperse dye composition |
| CN103044967B (en) * | 2012-12-25 | 2014-08-13 | 浙江闰土股份有限公司 | Dispersed black dye composition, dispersed black dye, and preparation method and application thereof |
| CN103602095B (en) * | 2013-09-10 | 2016-04-20 | 江苏亚邦染料股份有限公司 | One class Monoazo type dispersed dye, preparation method and application |
| CN103881412A (en) * | 2014-03-22 | 2014-06-25 | 浙江山峪染料化工有限公司 | Mono-azo disperse dye compound and preparation method thereof |
| CN104974552B (en) * | 2015-07-31 | 2017-01-11 | 杭州福莱蒽特精细化工有限公司 | Disperse sapphire blue dye composition with high color fastness |
| CN106566282B (en) * | 2016-10-12 | 2019-03-08 | 浙江龙盛集团股份有限公司 | A kind of high fastness disperse dye composition and dye preparations |
| CN111718600B (en) * | 2020-06-30 | 2021-10-08 | 浙江龙盛集团股份有限公司 | Disperse turquoise blue dye composition and dye product |
| CN111718599B (en) * | 2020-06-30 | 2021-10-08 | 浙江龙盛集团股份有限公司 | Disperse turquoise blue dye composition and dye product |
| CN111718602B (en) * | 2020-06-30 | 2021-10-08 | 浙江龙盛集团股份有限公司 | Disperse turquoise blue dye composition and dye product |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0042535A1 (en) * | 1980-06-21 | 1981-12-30 | Bayer Ag | Mixtures of dyes, process for their manufacture and for dyeing hydrophobic fibres |
| JPH11158402A (en) * | 1997-11-28 | 1999-06-15 | Sumitomo Chem Co Ltd | Disperse dye composition and method for coloring hydrophobic material therewith |
| US6562082B1 (en) * | 1998-01-05 | 2003-05-13 | Basf Aktiengesellschaft | Disperse dye mixture |
| JP2005036071A (en) * | 2003-07-18 | 2005-02-10 | Dystar Japan Ltd | Disperse dye mixture suitable for dyeing polylactic acid fiber |
-
2006
- 2006-08-23 CN CNB2006100531044A patent/CN100412139C/en not_active Expired - Fee Related
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0042535A1 (en) * | 1980-06-21 | 1981-12-30 | Bayer Ag | Mixtures of dyes, process for their manufacture and for dyeing hydrophobic fibres |
| JPH11158402A (en) * | 1997-11-28 | 1999-06-15 | Sumitomo Chem Co Ltd | Disperse dye composition and method for coloring hydrophobic material therewith |
| US6562082B1 (en) * | 1998-01-05 | 2003-05-13 | Basf Aktiengesellschaft | Disperse dye mixture |
| JP2005036071A (en) * | 2003-07-18 | 2005-02-10 | Dystar Japan Ltd | Disperse dye mixture suitable for dyeing polylactic acid fiber |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1939980A (en) | 2007-04-04 |
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