CN105441190A - Pu'er-tea-fragrance-type tobacco essence and preparing method thereof - Google Patents
Pu'er-tea-fragrance-type tobacco essence and preparing method thereof Download PDFInfo
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- CN105441190A CN105441190A CN201510878023.7A CN201510878023A CN105441190A CN 105441190 A CN105441190 A CN 105441190A CN 201510878023 A CN201510878023 A CN 201510878023A CN 105441190 A CN105441190 A CN 105441190A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
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- General Chemical & Material Sciences (AREA)
- Tea And Coffee (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention provides a Pu'er-tea-fragrance-type tobacco essence and a preparing method thereof. The Pu'er-tea-fragrance-type tobacco essence is prepared from, by weight, 1-70 parts of Pu'er-tea extract, 1-15 parts of date jujube tincture, 0.1-1 part of vanillin, 10-40 parts of vanilla bean tincture, 0.01-1 part of damacscone beta, 1-25 parts of Yunyan tobacco extract, 0.01-1 part of coumarin and 1-20 parts of tonka bean tincture in proportion in an evenly-mixed mode, wherein the Pu'er-tea extract is obtained through ultrasonic extraction and macroporous resin separation. The Pu'er-tea-fragrance-type tobacco essence has good Pu'er-tea fragrance and the fresh and sweet mouthfeel, and the preparing method is easy, convenient, stable in product quality and capable of being widely applied to the field of tobaccos.
Description
Technical field
The invention belongs to flavouring essence for tobacco field, relate to a kind of flavouring essence for tobacco and preparation method thereof, particularly relate to flavouring essence for tobacco of a kind of Pu'er odor type and preparation method thereof.
Background technology
Leaf of Assam Tea, has another name called the blue or green tea in Yunnan, belongs to black tea.Leaf of Assam Tea shines blue or green tea for raw material with big-leaf species in yunnan, uses the blue or green tea method for making of sub-fermentation, from fermentation different points of make a living tea and ripe tea two kinds.Leaf of Assam Tea is always considered to a kind of beverage with health-care effect.The clinical trial certificate of domestic and international relevant expert, Leaf of Assam Tea have reduce blood fat, fat-reducing, antibacterial aid digestion, warm stomach, promote the production of body fluid, quench the thirst, the multiple efficacies such as removing toxic substances of sobering up.Can clearing stomach promote the production of body fluid, eliminate indigestion and phlegm, removing toxic substances of relieving the effect of alcohol, diuresis loose cold, relieving cough and reducing sputum, reduce lipid cholesterol.
In Field of Tobacco, tea flavor flavouring essence for tobacco kind is relatively single, is only divided into roughly black tea type and green tea type.In state-owned six large tea systems, modern tealeaves have hundreds of more than, the fragrance of different tealeaves is different.Develop the flavouring essence for tobacco of different tea perfume (or spice) for different tealeaves, the market of tea odor type tobacco essence product can be greatly enriched.
Summary of the invention
the technical problem solved:in state-owned six large tea systems, modern tealeaves have hundreds of more than, but tea flavor flavouring essence for tobacco kind is in the market relatively single.
technical scheme:for above-mentioned technical problem, the invention discloses the flavouring essence for tobacco of a kind of Pu'er odor type, the flavouring essence for tobacco of described Pu'er odor type consists of the following composition: Pu'er tea, jujube tincture, vanillin food grade,1000.000000ine mesh, vanilla bean tincture, second position damascone, yunyan extract, tonka bean camphor, black tonka-bean tincture.
Preferably, in the flavouring essence for tobacco of described a kind of Pu'er odor type, the parts by weight of each component are: Pu'er tea 1-70 part, jujube tincture 1-15 part, vanillin food grade,1000.000000ine mesh 0.1-1 part, vanilla bean tincture 10-40 part, second position damascone 0.01-1 part, yunyan extract 1-25 part, tonka bean camphor 0.01-1 part, black tonka-bean tincture 1-20 part.
Preferred further, in the flavouring essence for tobacco of described Pu'er odor type, the parts by weight of each component are: Pu'er tea 50-70 part, jujube tincture 8-12 part, vanillin food grade,1000.000000ine mesh 0.2-0.6 part, vanilla bean tincture 10-20 part, second position damascone 0.02-0.05 part, yunyan extract 10-20 part, tonka bean camphor 0.02-0.05 part, black tonka-bean tincture 5-10 part.
Preferably, the flavouring essence for tobacco of described a kind of Pu'er odor type is Vandyke brown.
Preferably, the flavouring essence for tobacco of described a kind of Pu'er odor type, described Pu'er tea is the Pu'er tea obtained after macroporous resin is separated after puerh tea leaves ultrasonic extraction.
Preferably, the preparation method of described Pu'er tea comprises the following steps:
(1) in ultrasonic extraction tank, puerh tea leaves is added, add the mixed solvent be made up of ethanol, propylene glycol and water, feed liquid weight ratio is 1:5-1:15, opening device, and ultrasonic frequency is 20-200kHz, temperature remains on 50-90 DEG C, extraction time 20-90 minute, stops operation, and slightly pours out extracting solution after cooling, with strainer filtering, collect extracting solution; Remaining residue carries out second time with aforesaid method and extracts, collecting by filtration second time extracting solution;
(2) merge extracted twice liquid, concentrate on the rotary evaporator, thickening temperature 55-85 DEG C, vacuum tightness 0.005-0.01Mpa;
(3) distilled water diluting of enriched material 10-25 times of weight will obtained;
(4) diluent step (3) handled well makes it by D101 type macroporous adsorptive resins with the flow velocity of 1.5BV/h; After absorption terminates, rinse resin column with 5L distilled water with the flow velocity of 1.5BV/h; After flushing terminates, with the flow velocity of 1.0-1.5BV/h, with the aqueous ethanolic solution wash-out agent wash-out of the 20wt%-60wt% of 1.5-2.5BV, collect elutriant;
(5) concentrated on the rotary evaporator by the elutriant collected in step (4), thickening temperature 50-75 DEG C, vacuum tightness 0.005-0.01Mpa, being concentrated into density is 1.050-1.200, namely obtains Pu'er tea.
Preferably, in the preparation method of described Pu'er tea, puerh tea leaves is the common Pu'er raw tea tealeaves in market, and moisture content is 2wt%-8wt%.
Preferably, in the preparation method of described Pu'er tea, the part by weight of the mixed solvent of ethanol, propylene glycol and water composition is 40-60:10-20:20-50.
Preferably, in the preparation method of described Pu'er tea, D101 type macroporous adsorbent resin 95% alcohol immersion is spent the night, and with distilled water flushing extremely without after ethanol taste, then uses the solution soaking 4h of 4wt%NaOH, with distilled water flushing to neutral; Finally use the HCl solution soaking 4h of 4wt%, with distilled water flushing to neutral, dress post (5cm × 70cm) is for subsequent use.
The preparation method of the flavouring essence for tobacco of described a kind of Pu'er odor type, it is characterized in that, preparation method is: get Pu'er tea 1-70 part by weight, jujube tincture 1-15 part, vanillin food grade,1000.000000ine mesh 0.1-1 part, vanilla bean tincture 10-40 part, second position damascone 0.01-1 part, yunyan extract 1-25 part, tonka bean camphor 0.01-1 part, black tonka-bean tincture 1-20 part, is mixed to above-mentioned each composition evenly.
beneficial effect:the flavouring essence for tobacco of Pu'er odor type prepared by preparation method of the present invention, the soft exquisiteness of mouthfeel and pleasant impression is totally comfortable, have the distinctive faint scent of Leaf of Assam Tea, and the preparation method of described flavouring essence for tobacco is easy, constant product quality, can be widely used in cigarette product.
Embodiment
Below in conjunction with specific embodiment, the present invention is further described.
Embodiment 1
(1) pre-treatment of macroporous resin column: D101 type macroporous adsorbent resin 95% alcohol immersion is spent the night, with distilled water flushing extremely without after ethanol taste, then uses the solution soaking 4h of 4%NaOH, with distilled water flushing to neutral; Finally use the HCl solution soaking 4h of 4%, with distilled water flushing to neutral, dress post (5cm × 70cm) is for subsequent use;
(2) in ultrasonic extraction tank, puerh tea leaves is added, add the mixed solvent that weight ratio is ethanol, propylene glycol and water=40:15:50, feed liquid weight ratio is 1:5, opening device, and ultrasonic frequency is 20kHz, temperature remains on 50 DEG C, 20 minutes extraction times, stop operation, slightly pour out extracting solution after cooling, with strainer filtering, collect extracting solution; Remaining residue carries out second time with aforesaid method and extracts, collecting by filtration second time extracting solution;
(3) merge extracted twice liquid, concentrate on the rotary evaporator, thickening temperature 55 DEG C, vacuum tightness 0.01Mpa;
(4) distilled water diluting of enriched material 10 times of weight will obtained;
(5) diluent step (4) handled well makes it by D101 type macroporous adsorptive resins with the flow velocity of 1.5BV/h; After absorption terminates, rinse resin column with 5L distilled water with the flow velocity of 1.5BV/h; After flushing terminates, with the flow velocity of 1.0BV/h, with the aqueous ethanolic solution wash-out agent wash-out of the 40wt% of 1.5BV, collect elutriant;
(6) concentrated on the rotary evaporator by the elutriant collected in step (5), thickening temperature 50 DEG C, vacuum tightness 0.01Mpa, being concentrated into density is 1.150, namely obtains Pu'er tea;
(7) Pu'er tea 50 parts is got, jujube tincture 8 parts, vanillin food grade,1000.000000ine mesh 0.2 part, vanilla bean tincture 15 parts, second position damascone 0.02 part, yunyan extract 10 parts, tonka bean camphor 0.02 part, black tonka-bean tincture 10 parts, is mixed to above-mentioned each composition evenly, obtains Pu'er odor type flavouring essence for tobacco A.
Embodiment 2
(1) pre-treatment of macroporous resin column is identical with embodiment 1;
(2) in ultrasonic extraction tank, puerh tea leaves is added, add the mixed solvent that weight ratio is ethanol, propylene glycol and water=50:20:30, feed liquid weight ratio is 1:10, opening device, and ultrasonic frequency is 80kHz, temperature remains on 70 DEG C, 40 minutes extraction times, stop operation, slightly pour out extracting solution after cooling, with strainer filtering, collect extracting solution; Remaining residue carries out second time with aforesaid method and extracts, collecting by filtration second time extracting solution;
(3) merge extracted twice liquid, concentrate on the rotary evaporator, thickening temperature 60 DEG C, vacuum tightness 0.005Mpa;
(4) distilled water diluting of enriched material 15 times of weight will obtained;
(5) diluent step (4) handled well makes it by D101 type macroporous adsorptive resins with the flow velocity of 1.5BV/h; After absorption terminates, rinse resin column with 5L distilled water with the flow velocity of 1.5BV/h; After flushing terminates, with the flow velocity of 1.5BV/h, with the aqueous ethanolic solution wash-out agent wash-out of the 50wt% of 2.5BV, collect elutriant;
(6) concentrated on the rotary evaporator by the elutriant collected in step (5), thickening temperature 50 DEG C, vacuum tightness 0.01Mpa, being concentrated into density is 1.050, namely obtains Pu'er tea;
(7) Pu'er tea 60 parts is got, jujube tincture 10 parts, vanillin food grade,1000.000000ine mesh 0.4 part, vanilla bean tincture 20 parts, second position damascone 0.04 part, yunyan extract 15 parts, tonka bean camphor 0.05 part, black tonka-bean tincture 8 parts, is mixed to above-mentioned each composition evenly, obtains Pu'er odor type flavouring essence for tobacco B.
Embodiment 3
(1) pre-treatment of macroporous resin column is identical with embodiment 1;
(2) in ultrasonic extraction tank, puerh tea leaves is added, add the mixed solvent that weight ratio is ethanol, propylene glycol and water=60:10:20, feed liquid weight ratio is 1:15, opening device, and ultrasonic frequency is 200kHz, temperature remains on 90 DEG C, 90 minutes extraction times, stop operation, slightly pour out extracting solution after cooling, with strainer filtering, collect extracting solution; Remaining residue carries out second time with aforesaid method and extracts, collecting by filtration second time extracting solution;
(3) merge extracted twice liquid, concentrate on the rotary evaporator, thickening temperature 85 DEG C, vacuum tightness 0.01Mpa;
(4) distilled water diluting of enriched material 20 times of weight will obtained;
(5) diluent step (4) handled well makes it by D101 type macroporous adsorptive resins with the flow velocity of 1.5BV/h; After absorption terminates, rinse resin column with 5L distilled water with the flow velocity of 1.5BV/h; After flushing terminates, with the flow velocity of 1.0BV/h, with the aqueous ethanolic solution wash-out agent wash-out of the 60wt% of 1.5BV, collect elutriant;
(6) concentrated on the rotary evaporator by the elutriant collected in step (5), thickening temperature 50 DEG C, vacuum tightness 0.01Mpa, being concentrated into density is 1.20, namely obtains Pu'er tea;
(7) Pu'er tea 70 parts is got, jujube tincture 12 parts, vanillin food grade,1000.000000ine mesh 0.6 part, vanilla bean tincture 10 parts, second position damascone 0.05 part, yunyan extract 20 parts, tonka bean camphor 0.02 part, black tonka-bean tincture 5 parts, is mixed to above-mentioned each composition evenly, obtains Pu'er odor type flavouring essence for tobacco C.
Embodiment 4
Preparation method's step (1) to (6) is with embodiment 3, Pu'er tea 1 part is got in step (7), jujube tincture 15 parts, vanillin food grade,1000.000000ine mesh 0.1 part, vanilla bean tincture 10 parts, second position damascone 0.01 part, yunyan extract 25 parts, tonka bean camphor 0.01 part, black tonka-bean tincture 20 parts, above-mentioned each composition is mixed to evenly, obtains Pu'er odor type flavouring essence for tobacco D.
Embodiment 5
Preparation method's step (1) to (6) is with embodiment 3, Pu'er tea 70 parts is got in step (7), jujube tincture 1 part, vanillin food grade,1000.000000ine mesh 1 part, vanilla bean tincture 40 parts, second position damascone 1 part, yunyan extract 1 part, coumarin 1 part, black tonka-bean tincture 1 part, above-mentioned each composition is mixed to evenly, obtains Pu'er odor type flavouring essence for tobacco E.
The smoking result of the flavouring essence for tobacco of embodiment 1 to 5
The flavouring essence for tobacco A of Pu'er odor type embodiment 1 prepared, adds in flue-cured tobacco pipe tobacco according to the 0.5wt% of cigarette shreds weight and makes tobacco product.Smoking result shows, compared with blank cigarette, the cigarette adding Pu'er odor type flavouring essence for tobacco has unique Leaf of Assam Tea delicate fragrance when aspirating, and perfume quantity increases, and hamony is good, and pleasant impression is improved, and promotes the production of body fluid obviously.
The flavouring essence for tobacco B of Pu'er odor type embodiment 2 prepared, adds in flue-cured tobacco pipe tobacco according to the 0.1wt% of cigarette shreds weight and makes tobacco product.Smoking result shows, compared with blank cigarette, the cigarette adding Pu'er odor type flavouring essence for tobacco has obvious Leaf of Assam Tea delicate fragrance when aspirating, and with fresh and sweet note, fragrance exquisiteness is soft, covers assorted gas, reduces and stimulates, and hamony is better, and pleasant impression promotes the production of body fluid Hui Tian.
The flavouring essence for tobacco C of Pu'er odor type embodiment 3 prepared, adds in flue-cured tobacco pipe tobacco according to the 1wt% of cigarette shreds weight and makes tobacco product.Smoking result shows, compared with blank cigarette, the cigarette adding Pu'er odor type flavouring essence for tobacco has obvious Leaf of Assam Tea delicate fragrance, plentiful of fragrance when aspirating, and overall stimulation has decline, and hamony is better, and pleasant impression is clean.
The flavouring essence for tobacco D of Pu'er odor type embodiment 4 prepared, adds in flue-cured tobacco pipe tobacco according to the 1wt% of cigarette shreds weight and makes tobacco product.Smoking result shows, compared with blank cigarette, the cigarette adding Pu'er odor type flavouring essence for tobacco has Leaf of Assam Tea delicate fragrance when aspirating, and fragrance is plentiful, and overall stimulation declines to some extent, and hamony is better, and pleasant impression is clean.
The flavouring essence for tobacco E of Pu'er odor type embodiment 5 prepared, adds in flue-cured tobacco pipe tobacco according to the 1wt% of cigarette shreds weight and makes tobacco product.Smoking result shows, compared with blank cigarette, the cigarette adding Pu'er odor type flavouring essence for tobacco has significant Leaf of Assam Tea delicate fragrance when aspirating, and fragrance is sent out thoroughly, and overall stimulation declines to some extent, and hamony is better, and pleasant impression is clean.
Smoking result shows, the flavouring essence for tobacco smoking result of embodiment 1 is best, and the flavouring essence for tobacco of embodiment 2 and embodiment 3 takes second place, and the flavouring essence for tobacco smoking result of embodiment 4 and embodiment 5 is also better, but lower than the smoking result of embodiment 2 and embodiment 3.
More than to invention has been elaboration; the present invention is understood for helping; but embodiments of the present invention are not restricted to the described embodiments; any do not deviate from the principle of the invention under do change, modification, substitute, combination, simplify; all should be the substitute mode of equivalence, be included within protection scope of the present invention.
Claims (9)
1. a flavouring essence for tobacco for Pu'er odor type, is characterized in that, the flavouring essence for tobacco of described Pu'er odor type consists of the following composition: Pu'er tea, jujube tincture, vanillin food grade,1000.000000ine mesh, vanilla bean tincture, second position damascone, yunyan extract, tonka bean camphor, black tonka-bean tincture.
2. the flavouring essence for tobacco of a kind of Pu'er according to claim 1 odor type, it is characterized in that, in the flavouring essence for tobacco of described Pu'er odor type, the parts by weight of each component are: Pu'er tea 1-70 part, jujube tincture 1-15 part, vanillin food grade,1000.000000ine mesh 0.1-1 part, vanilla bean tincture 10-40 part, second position damascone 0.01-1 part, yunyan extract 1-25 part, tonka bean camphor 0.01-1 part, black tonka-bean tincture 1-20 part.
3. the flavouring essence for tobacco of a kind of Pu'er according to claim 1 odor type, it is characterized in that, in the flavouring essence for tobacco of described Pu'er odor type, the parts by weight of each component are: Pu'er tea 50-70 part, jujube tincture 8-12 part, vanillin food grade,1000.000000ine mesh 0.2-0.6 part, vanilla bean tincture 10-20 part, second position damascone 0.02-0.05 part, yunyan extract 10-20 part, tonka bean camphor 0.02-0.05 part, black tonka-bean tincture 5-10 part.
4. the flavouring essence for tobacco of a kind of Pu'er according to claim 1 odor type, it is characterized in that, described flavouring essence for tobacco is Vandyke brown.
5. the flavouring essence for tobacco of a kind of Pu'er according to claim 1 odor type, it is characterized in that, the preparation method of described Pu'er tea comprises the following steps: (1) adds puerh tea leaves in ultrasonic extraction tank, add the mixed solvent be made up of ethanol, propylene glycol and water, feed liquid weight ratio is 1:5-1:15, opening device, ultrasonic frequency is 20-200kHz, temperature remains on 50-90 DEG C, extraction time 20-90 minute, stops operation, and slightly pours out extracting solution after cooling, with strainer filtering, collect extracting solution; Remaining residue carries out second time with aforesaid method and extracts, collecting by filtration second time extracting solution; (2) merge extracted twice liquid, concentrate on the rotary evaporator, thickening temperature 55-85 DEG C, vacuum tightness 0.005-0.01Mpa; (3) distilled water diluting of enriched material 10-25 times of weight will obtained; (4) diluent step (3) handled well makes it by D101 type macroporous adsorptive resins with the flow velocity of 1.5BV/h; After absorption terminates, rinse resin column with 5L distilled water with the flow velocity of 1.5BV/h; After flushing terminates, with the flow velocity of 1.0-1.5BV/h, with the aqueous ethanolic solution wash-out agent wash-out of the 20wt%-60wt% of 1.5-2.5BV, collect elutriant; (5) concentrated on the rotary evaporator by the elutriant collected in step (4), thickening temperature 50-75 DEG C, vacuum tightness 0.005-0.01Mpa, being concentrated into density is 1.050-1.200, namely obtains Pu'er tea.
6. the flavouring essence for tobacco of a kind of Pu'er according to claim 5 odor type, is characterized in that, described puerh tea leaves is the common Pu'er raw tea tealeaves in market, and moisture content is 2wt%-8wt%.
7. the flavouring essence for tobacco of a kind of Pu'er according to claim 5 odor type, is characterized in that, the part by weight of the mixed solvent of described ethanol, propylene glycol and water composition is 40-60:10-20:20-50.
8. the flavouring essence for tobacco of a kind of Pu'er according to claim 5 odor type, it is characterized in that, described D101 type macroporous adsorbent resin 95% alcohol immersion is spent the night, with distilled water flushing extremely without after ethanol taste, use the solution soaking 4h of 4wt%NaOH again, with distilled water flushing to neutral; Finally use the HCl solution soaking 4h of 4wt%, with distilled water flushing to neutral, dress post (5cm × 70cm) is for subsequent use.
9. the preparation method of the flavouring essence for tobacco of a kind of Pu'er according to claim 2 odor type, it is characterized in that, preparation method is: get Pu'er tea 1-70 part by weight, jujube tincture 1-15 part, vanillin food grade,1000.000000ine mesh 0.1-1 part, vanilla bean tincture 10-40 part, second position damascone 0.01-1 part, yunyan extract 1-25 part, tonka bean camphor 0.01-1 part, black tonka-bean tincture 1-20 part, is mixed to above-mentioned each composition evenly.
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| CN108251216A (en) * | 2018-01-18 | 2018-07-06 | 云南中烟工业有限责任公司 | A kind of preparation method and application of the Pu'er tea absolute oil containing the fragrant component of Viscμm articulatum Burm f cause |
| CN108893196A (en) * | 2018-07-27 | 2018-11-27 | 鹰潭中投科技有限公司 | A kind of tobacco aromaticss formula of fresh breath and preparation method thereof |
| CN111035061A (en) * | 2019-12-30 | 2020-04-21 | 福建中烟工业有限责任公司 | Composition for cigarettes, preparation method and application thereof |
| CN114223933A (en) * | 2022-02-11 | 2022-03-25 | 云南中烟工业有限责任公司 | Method for preparing tobacco by co-fermenting white spirit and Pu' er tea characteristic extract |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108251216A (en) * | 2018-01-18 | 2018-07-06 | 云南中烟工业有限责任公司 | A kind of preparation method and application of the Pu'er tea absolute oil containing the fragrant component of Viscμm articulatum Burm f cause |
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| CN111035061A (en) * | 2019-12-30 | 2020-04-21 | 福建中烟工业有限责任公司 | Composition for cigarettes, preparation method and application thereof |
| CN114223933A (en) * | 2022-02-11 | 2022-03-25 | 云南中烟工业有限责任公司 | Method for preparing tobacco by co-fermenting white spirit and Pu' er tea characteristic extract |
| CN114223933B (en) * | 2022-02-11 | 2022-11-04 | 云南中烟工业有限责任公司 | Method for preparing tobacco by co-fermenting white spirit and Pu' er tea characteristic extracts |
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