CN105440830B - Scrubbable interior wall coating of a kind of low viscosity height covering height and preparation method thereof - Google Patents
Scrubbable interior wall coating of a kind of low viscosity height covering height and preparation method thereof Download PDFInfo
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- CN105440830B CN105440830B CN201510955783.3A CN201510955783A CN105440830B CN 105440830 B CN105440830 B CN 105440830B CN 201510955783 A CN201510955783 A CN 201510955783A CN 105440830 B CN105440830 B CN 105440830B
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D131/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an acyloxy radical of a saturated carboxylic acid, of carbonic acid, or of a haloformic acid; Coating compositions based on derivatives of such polymers
- C09D131/02—Homopolymers or copolymers of esters of monocarboxylic acids
- C09D131/04—Homopolymers or copolymers of vinyl acetate
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/14—Paints containing biocides, e.g. fungicides, insecticides or pesticides
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
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Abstract
The present invention relates to a kind of low viscosity height to cover high scrubbable interior wall coating, it is formulated by following components:Water, hydroxyethyl cellulose, inorganic thixotropic thickening agent, bentonite, water-soluble multifunctional auxiliary agent, dispersant, wetting agent, diatomite, titanium dioxide, 800 mesh coarse whitings, talcum powder, calcined kaolin, lotion, antifreeze, coalescents, antifoaming agent, thickener, Antisepticize and mildew preventive.Beneficial effects of the present invention:There is coating of the present invention the high of high-class product to cover, its contrast ratio is more than 0.95;High scrubbing resistance;A painting construction can be done without being watered, and in fitting up or overhauling, only needs roller coating one time, reduces construction times;Paint film property is excellent, and feel is good;Labor cost has not only been saved, has reduced the construction time, and also reduce transportation cost;Storage stability is good at a low viscosity for coating of the present invention.
Description
Technical field
The present invention relates to decorative paint fields, and in particular to a kind of low viscosity height cover high scrubbable interior wall coating and its
Preparation method.
Background technology
The considerations of for storage stability, the viscosity of interior wall coating is usually in 100~120ku or so at present, because low viscous
The coating of degree frequently can lead to coating storage layered and sedimentation phenomenon.But construct optimum viscosity generally in 75~85ku, so
30%~50% water would generally be converted when normal construction.And it is watered the covering power that will seriously reduce coating and scrubbing resistance etc. is every
Performance.So using current interior wall coating, normal construction technique is that a priming paint adds 2 times finishing coats, to ensure the covering of construction
Property with paint film strength.
Invention content
Invention provides a kind of low viscosity height and covers high scrubbable high-class product interior wall coating, its viscosity is low, covering is good and
Scrub resistance is good, its long term storage does not settle, and without being watered when normal construction, roller coating is only needed finishing to can be completed or turn over for one time
It repaiies, it is possible to reduce the construction time.
Technical scheme is as follows:A kind of high scrubbable interior wall coating of low viscosity height covering, is pressed by following components
It is formulated according to following parts by weight:
Further, the hydroxyethyl cellulose is the water dissolvable cellulose ether of nonionic.
Further, the inorganic thixotropic thickening agent is the gel particle based on aluminum magnesium silicate.
Further, the bentonite uses the aqueous viscous mine based on montmorillonite.
Further, the water-soluble multifunctional auxiliary agent uses 2-amino-2-methyl-1-propanol.
Further, the dispersant uses sodium polycarboxylate salt form dispersant.
Further, the wetting agent is environment-friendly type non-ionic emulsifier wetting agent.
Further, the antifoaming agent is nonionic antifoaming agent or organic silicon defoamer.
Further, the diatomite SiO2 contents >=:89.6.
Further, the titanium dioxide is anatase thpe white powder or rutile type titanium white.
Further, the talcum powder is 1250 mesh talcum powder.
Further, the antifreezing agent is 1,2-PD.
Further, the coalescents use 2,2,4- trimethyl -1,3 pentanediol mono isobutyrates.
Further, the thickener is association thickener.
Further, the sterilization antiseptic uses isothiazolinone disinfecting agent.
A kind of low viscosity height covers the preparation method of high scrubbable interior wall coating, it is characterised in that:It include below according to
The step of sequence carries out:
(1) 18-26 parts of part water are added in dispersion cylinder, then sequentially add 0.2~0.3 under 350-550r/min rotating speeds
Part hydroxyethyl cellulose, 0.1~0.3 part of thixotropic thickening agent, 0.1~0.3 part of bentonite and 0.1~0.2 part of water-soluble multifunctional help
After agent, 1-5min is stirred;
(2) rotating speed is then improved to 800-1000r/min, sequentially adds 0.7~0.8 part of dispersant, 0.3~0.4 part of profit
Humectant, 0.3~0.5 part of antifoaming agent, 3~4 parts of diatomite, 15~18 parts of titanium dioxides, 4~6 parts of talcum powder, 9~10 parts of calcinings are high
After ridge soil and 3~5 part of 800 mesh coarse whiting, improves again under rotating speed to 1800-2000r/min rotating speeds and disperses 15-20min,
(3) fineness is detected after, when fineness≤60 μm, is reduced rotating speed to 1000-1200r/min rotating speeds, is sequentially added 16
~19 parts of lotions, 0.6~0.7 part of coalescents, 0.8~1.2 portion of antifreeze, 0.3~0.5 part of antifoaming agent, 0.8~1.2 part it is anti-
Rotten mould inhibitor, 1~1.2 part of thickener and remaining water, dispersion 15-20min are uniform to mixing liquid.
Beneficial effects of the present invention:There is coating of the present invention the high of high-class product to cover, its contrast ratio is more than 0.95;It is high resistance to
It cleans;A painting construction can be done without being watered, and in fitting up or overhauling, only needs roller coating one time, reduces construction times;
Paint film property is excellent, and feel is good;Not only saved labor cost, reduced the construction time, and also reduce transport at
This;Storage stability is good at a low viscosity for coating of the present invention.
Specific implementation mode
Embodiment 1
A kind of preparation method being used to prepare the interior wall coating that the low viscosity height covers, it includes following sequentially carrying out
Step:
(1) 18 parts of water are added in dispersion cylinder, 0.2 part of hydroxyethyl cellulose, 0.3 is sequentially added under 450r/min rotating speeds
After part thixotropic thickening agent, 0.3 part of bentonite and 0.1 part of water-soluble multifunctional auxiliary agent, 2min is stirred;
(2) improve rotating speed to 900r/min after, sequentially add 0.7 part of aqueous dispersion, 0.3 part of aqueous wetting agent, 0.3 part
After aqueous defoamer, 3 parts of diatomite, 18.0 parts of titanium dioxides, 4 parts of talcum powder, 9 parts of kaolin and 3 parts of coarse whitings, rotating speed is improved again
Disperse 17.5min under to 1900r/min rotating speeds, whether detect fineness later≤60 μm, step is continued to execute if fineness≤60 μm
Suddenly (3);
(3) reduce sequentially added under rotating speed to 1100r/min rotating speeds 16 parts of VAE lotions, 0.6 part of coalescents, 1.2 parts it is anti-
After freezing agent, 0.5 part of aqueous defoamer, 0.8 part of sterilization antiseptic, 1 part of thickener and 20 parts of water, dispersion 17.5min to mixed liquor
Body is uniform.
Embodiment 2
A kind of preparation method for being used to prepare the low viscosity height and covering interior wall coating, it includes the following step sequentially carried out
Suddenly:
(1) 20 parts of water are added in dispersion cylinder, 0.3 part of hydroxyethyl cellulose, 0.2 is sequentially added under 390r/min rotating speeds
After part thixotropic thickening agent, 0.2 part of bentonite and 0.2 part of water-soluble multifunctional auxiliary agent, 2min is stirred;
(2) improve rotating speed to 900r/min after, sequentially add 0.8 part of aqueous dispersion, 0.4 part of aqueous wetting agent, 0.5 part
After aqueous defoamer, 4 parts of diatomite, 15.0 parts of titanium dioxides, 5 parts of talcum powder, 10 parts of kaolin and 4 parts of coarse whitings, improves turn again
Disperse 20min under speed to 1800r/min rotating speeds, whether detect fineness later≤60 μm, step is continued to execute if fineness≤60 μm
Suddenly (3);
(3) reduce sequentially added under rotating speed to 1200r/min rotating speeds 17 parts of VAE lotions, 0.6 part of coalescents, 1.2 parts it is anti-
After freezing agent, 0.3 part of aqueous defoamer, 0.8 part of sterilization antiseptic, 1.2 parts of thickeners and 16 parts of water, dispersion 10min to mixed liquor
Body is uniform.
Embodiment 3
A kind of preparation method for being used to prepare the low viscosity height and covering interior wall coating, it includes the following step sequentially carried out
Suddenly:
(1) 17 parts of water are added in dispersion cylinder, 0.3 part of hydroxyethyl cellulose, 0.1 is sequentially added under 400r/min rotating speeds
After part thixotropic thickening agent, 0.3 part of bentonite and 0.1 part of water-soluble multifunctional auxiliary agent, 4min is stirred;
(2) improve rotating speed to 900r/min after, sequentially add 0.8 part of aqueous dispersion, 0.4 part of aqueous wetting agent, 0.4 part
After aqueous defoamer, 4 parts of diatomite, 16.0 parts of titanium dioxides, 5 parts of talcum powder, 10 parts of kaolin and 3 parts of coarse whitings, improves turn again
Disperse 16min under speed to 1900r/min rotating speeds, whether detect fineness later≤60 μm, step is continued to execute if fineness≤60 μm
Suddenly (3);
(3) reduce sequentially added under rotating speed to 1000r/min rotating speeds 16 parts of VAE lotions, 0.6 part of coalescents, 1.2 parts it is anti-
After freezing agent, 0.4 part of aqueous defoamer, 0.8 part of sterilization antiseptic, 1 part of thickener and 21 parts of water, dispersion 16min to mixing liquid
Uniformly.
Embodiment 4
A kind of preparation method being used to prepare the interior wall coating that the low viscosity height covers, it includes following sequentially carrying out
Step:
(1) 26 parts of water are added in dispersion cylinder, 0.2 part of hydroxyethyl cellulose, 0.1 is sequentially added under 350r/min rotating speeds
After part thixotropic thickening agent, 0.2 part of bentonite and 0.2 part of water-soluble multifunctional auxiliary agent, 5min is stirred;
(2) improve rotating speed to 900r/min after, sequentially add 0.8 part of aqueous dispersion, 0.3 part of aqueous wetting agent, 0.3 part
After aqueous defoamer, 3 parts of diatomite, 15.0 parts of titanium dioxides, 4 parts of talcum powder, 9 parts of kaolin and 3 parts of coarse whitings, rotating speed is improved again
Disperse 15min under to 1900r/min rotating speeds, whether detect fineness later≤60 μm, step is continued to execute if fineness≤60 μm
(3);
(3) reduce sequentially added under rotating speed to 1100r/min rotating speeds 16 parts of VAE lotions, 0.7 part of coalescents, 1.2 parts it is anti-
After freezing agent, 0.5 part of aqueous defoamer, 0.8 part of sterilization antiseptic, 1.1 parts of thickeners and 22 parts of water, dispersion 17.5min to mixing
Liquid is uniform.
Embodiment 5
A kind of preparation method being used to prepare the interior wall coating that the low viscosity height covers, it includes following sequentially carrying out
Step:
(1) 18 parts of water are added in dispersion cylinder, 0.23 part of hydroxy ethyl fiber is then sequentially added under 350r/min rotating speeds
After element, 0.1 part of thixotropic thickening agent, 0.1 part of bentonite and 0.1 part of water-soluble multifunctional auxiliary agent, 1min is stirred;
(2) rotating speed is then improved to 800r/min, sequentially adds 0.7 part of dispersant, 0.3 part of wetting agent, 0.3 part of defoaming
After agent, 3 parts of diatomite, 15 parts of titanium dioxides, 4 parts of talcum powder, 9 parts of calcined kaolins and 3 part of 800 mesh coarse whiting, rotating speed is improved again
Disperse 15min under to 1800r/min rotating speeds, detect fineness later, when fineness≤60 μm, continues to execute step (3);
(3) reduce rotating speed to 1000r/min rotating speeds under, sequentially add 16 parts of lotions, 0.6 part of coalescents, 0.8 part it is freeze proof
Agent, 0.3 part of antifoaming agent, 0.8 part of Antisepticize and mildew preventive, 1 part of thickener and remaining water, dispersion 15-20min are equal to mixing liquid
It is even.
Embodiment 6
(1) 26 parts of part water are added in dispersion cylinder, 0.3 part of hydroxy ethyl fiber is then sequentially added under 550r/min rotating speeds
After element, 0.3 part of thixotropic thickening agent, 0.3 part of bentonite and 0.2 part of water-soluble multifunctional auxiliary agent, 5min is stirred;
(2) rotating speed is then improved to 1000r/min, sequentially adds 0.8 part of dispersant, 0.4 part of wetting agent, 0.5 part of defoaming
After agent, 4 parts of diatomite, 18 parts of titanium dioxides, 6 parts of talcum powder, 10 parts of calcined kaolins and 5 part of 800 mesh coarse whiting, rotating speed is improved again
Disperse 20min under to 2000r/min rotating speeds, detect fineness later, when fineness≤60 μm, continues to execute step (3);
(3) reduce rotating speed to 1200r/min rotating speeds under, sequentially add 19 parts of lotions, 0.7 part of coalescents, 1.2 parts it is freeze proof
Agent, 0.5 part of antifoaming agent, 1.2 parts of Antisepticize and mildew preventives, 1.2 parts of thickeners and remaining water, dispersion 20min are equal to mixing liquid
It is even.
In the above various embodiments:
The water uses ordinary tap water;
The hydroxyethyl cellulose is preferably the sub- 250HBR across dragon production;
The inorganic thixotropic thickening agent is the ATT 40 of BASF
The bentonite is preferably the BT-6000 of U.S.'s Mei Nuokai Chemical Manufactures;
The water-soluble multifunctional auxiliary agent is preferably the AMP-95 of Tao Shi productions;
The aqueous dispersion is preferably the SN5040 of Nuo Puke productions;
The aqueous wetting agent is preferably the 2405 of Hai Run productions;
The aqueous defoamer is preferably the A10 of CF246 and the Hai Chuan production of Blackburn production;
The diatomite is preferably Celite celite499
The titanium dioxide is preferably the BLR-699 of one hundred profit connection production;
The talcum powder is preferably 1250 mesh talcum powder of the rich power production of the rising sun;
The kaolin is preferably the kaolin for covering west production;
The calcium carbonate is preferably 800 mesh coarse whitings of agriculture-countryside-farmer's production;
The lotion is preferably the RS-998AF lotions of Ahmedabad richness production;
The coalescents are preferably the Texanol of Yi Shiman productions;
The antifreezing agent is preferably the propylene glycol of Shandong Depew Chemical Manufacture;
The sterilization antiseptic is preferably the RS of Troy production;
The RM8W of the preferred ROHM AND HAAS of thickener.
According to GB/T9756-2009 in each embodiment for the interior wall coating that low viscosity height prepared by the present invention covers
《Resin latex dope》The certified products standard and HJ2537-2014 of finishing coat《People's Republic of China's National Environmental is protected
Shield standard》Property indices measured by interior wall coating gloss (60 °≤10 ° finishing coats) and for example following table institute of technical indicator
Show:
Every experimental data of various embodiments of the present invention is more than GB/T9756-2009《Resin latex dope》
The high-class product standard and HJ2537-2014 of finishing coat《People's Republic of China's state environment protecting standard》(60 ° of interior wall coating gloss
≤ 10 ° of finishing coats) high-class product requirement.
Claims (2)
1. a kind of low viscosity height covers high scrubbable interior wall coating, it is characterised in that:By following components according to following parts by weight
It is formulated:
The hydroxyethyl cellulose is the water-soluble cellulose ether of nonionic;
The inorganic thixotropic thickening agent is the gel particle based on aluminum magnesium silicate;
The bentonite is the aqueous viscous mine based on montmorillonite;
The water-soluble multifunctional auxiliary agent is 2-amino-2-methyl-1-propanol;
The dispersant is sodium polycarboxylate salt form dispersant;
The wetting agent is environment-friendly type non-ionic emulsifier wetting agent;
The antifoaming agent is nonionic antifoaming agent or organic silicon defoamer;
SiO in the diatomite2Content >=89.6%;The titanium dioxide is anatase thpe white powder or rutile type titanium white;It is described
Talcum powder is 1250 mesh talcum powder;The antifreezing agent is 1,2-PD;The coalescents are 2,2,4- trimethyls -1,3 penta
Monoisobutyrate;The thickener is association thickener;The sterilization antiseptic is isothiazolinone disinfecting agent.
2. a kind of low viscosity height according to claim 1 covers the preparation method of high scrubbable interior wall coating, feature
It is:It includes the steps that following sequentially carrying out:
(1) 18-26 parts of water are added in dispersion cylinder, 0.2~0.3 part of hydroxyl second is then sequentially added under 350-550r/min rotating speeds
After base cellulose, 0.1~0.3 part of thixotropic thickening agent, 0.1~0.3 part of bentonite and 0.1~0.2 part of water-soluble multifunctional auxiliary agent, stir
Mix 1-5min;
(2) then improve rotating speed to 800-1000r/min, sequentially add 0.7~0.8 part of dispersant, 0.3~0.4 part of wetting agent,
0.3-0.5 parts of antifoaming agent, 3~4 parts of diatomite, 15~18 parts of titanium dioxides, 4~6 parts of talcum powder, 9~10 parts of calcined kaolins and 3
After~5 part of 800 mesh coarse whiting, improves again under rotating speed to 1800-2000r/min rotating speeds and disperses 15-20min,
(3) and then detection fineness reduces rotating speed to 1000-1200r/min, sequentially adds 16~19 parts of breasts when fineness≤60 μm
Liquid, 0.6~0.7 part of coalescents, 0.8~1.2 portion of antifreeze, 0.3~0.5 part of antifoaming agent, 0.8~1.2 part of Antisepticize and mildew preventive
Afterwards and remaining water, dispersion 15-20min are uniform to mixing liquid.
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CN107502091A (en) * | 2017-08-31 | 2017-12-22 | 苏州仲勉装饰有限公司 | A kind of preparation method of washable interior wall coating |
CN107815252A (en) * | 2017-12-01 | 2018-03-20 | 湘江涂料科技有限公司 | A kind of environmental protection coating material of a construction molding and preparation method thereof |
CN112280396B (en) * | 2020-10-20 | 2022-04-08 | 嘉宝莉化工集团股份有限公司 | High-covering washable one-time painting waterborne interior wall paint |
CN113122095A (en) * | 2021-04-21 | 2021-07-16 | 浙江华德新材料有限公司 | High-solid low-viscosity aqueous composition for one-time coating |
CN113789089A (en) * | 2021-09-16 | 2021-12-14 | 湖北三棵树新材料科技有限公司 | Freezing-resistant and quick-recovery exterior wall coating and preparation method thereof |
CN113736304A (en) * | 2021-10-13 | 2021-12-03 | 贵州柯维建材开发有限公司 | Paint formula for inner and outer wall construction and processing technology |
CN113861778A (en) * | 2021-10-14 | 2021-12-31 | 浙江大学杭州国际科创中心 | High-scrubbing-resistance environment-friendly building coating and preparation method thereof |
CN115820018A (en) * | 2022-11-30 | 2023-03-21 | 河北昊泽化工有限公司 | Preparation method and production equipment of coating with extremely strong scrubbing resistance |
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CN1709995A (en) * | 2005-06-10 | 2005-12-21 | 华南理工大学 | Scrubbing-tolerant internal wall emulsion coating and its preparing method |
CN101619181B (en) * | 2009-07-31 | 2011-04-06 | 广东嘉宝莉化工集团有限公司 | Soft hand feel coating and preparation method thereof |
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CN103834242A (en) * | 2013-12-25 | 2014-06-04 | 杨昌富 | Anti-scratch emulsion paint for interior wall |
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