CN105432969A - Production method of natural high-efficiency yolk color-improving agent for feed - Google Patents

Abstract

The invention discloses a production method of natural high-efficiency yolk color-improving agent for feed from discarded peels. The production method comprises the following steps: first preparing accessory ingredients, wherein the accessory ingredients comprise kaoline, sulfobutyl ether-beta-cyclodextrin and xylitol and the ratio of kaoline to sulfobutyl ether-beta-cyclodextrin to xylitol is 1.7: 1.3: 1.6; drying the mango peels, the orange peels, the bean residues, the waste mulberry silk and the America yellow volvox in the sun or by fire, then respectively crushing the mango peels, the orange peels, the bean residues, the waste mulberry silk and the America yellow volvox into coarse powder whose size is 60-80 meshes; preparing the following raw materials in parts by weight: 25-27 parts of mango-peel powder, 33-35 parts of orange-peel powder, 32-34 parts of bean-residue powder, 17-19 parts of waste mulberry silk, 6.5 parts of Danubi Synuropsis and 5 parts of accessory ingredients; mixing the coarse raw material powders, then mixing the mixed coarse raw material powders with the accessory ingredients; treating the mixture by a high-energy vibration mill, wherein the accelerated speed of the steel rod is 8-9g and the treatment time is 15-30 minutes; stopping the vibration mill for 2.5 minutes then treating again by the high-energy vibration mill, wherein the accelerated speed of the steel rod is 7.5g and the treatment time is 12-13 minutes, so that the raw materials experience two different solid-state mechanical chemical reactions; and screening the treated mixture by a 400-mesh screen so that the final product is obtained. The production method is capable of obviously reducing the bitterness of the raw materials, effectively dissolving the active ingredients in the raw materials, producing a natural yolk color-improving agent for feed, reducing the production cost of the enterprise and turning waste into treasure.

Description

The production method of the feeding yolk color improver of efficiency natural

Technical field

The present invention relates to the production method of producing the feeding yolk color improver of efficiency natural with discarded pericarp.

Background technology

Yolk color is one of most important project in egg product production target, the depth of yolk color, directly concerns mode of selling and the sales volume of commodity egg.Such as, the preserved egg that the added value such as salted egg, lime-preserved egg is higher, just requires that yolk color is comparatively dark, and the fresh egg of yolk color less than eight grades, can not export goods and earn foreign currency, even if market also can only be sold with lower price at home, profit is meagre, is difficult to enter high-end market.Pursue darker yolk color and the unreasonable consumption favourite hobby of non-consumer, darker yolk color shows wherein part nutritional labeling really more abundant (chemical industry such as tonyred, Carophyll red synthetic dyestuffs obtained except).Part natural colouring matter also can enrichment in birds, beasts and eggs, is one of present the heredity of filial generation in female generation, helps the advantage that mother's generation is inherited in filial generation in growing.And when the general level of the health of bird is poor, influenced with metabolism owing to ingesting, so yolk color is more shallow, the egg below level Four does not generally advise eating.Therefore the preference of consumer to dark yolk color has biology and nutrition basis.In yolk, main substance that show color is carotenoid, and multi-source is in plant.Carotenoid during bird assimilates food, provides vitamin and nutrition, and is enriched in yolk, makes up the deficiency self can not synthesizing carotenoid.

In order to save cost and improve yolk hyperchromic efficiency, the enterprise such as DSM, BASF develops different types of chemical industry synthesis yolk color improver in succession, and as Carophyll red, bolted rock is yellow, gold is glittering, Chinese blister beetle red pigment etc.These yolk color improvers are easy to use, and the more traditional natural products of price advantageously, and is easy to transport and stores.But increasing research shows in recent years, the pigment of chemical industry synthesis, there is potential health risk, even above several yolk color improver obtaining the usage license be also in succession proved to be have under given conditions cause consumer to suffer from diarrhoea, cause animal used as test slow poisoning, the effect such as carcinogenic.The multinational yolk color improver in succession limiting the use of or forbid synthesis.

Using natural plant composition as the agent of bird yolk color perfecting, food security can not only be ensured, the effect that also there is nutrition adjustment and supplement.If using the accessory substance of food processing industry or discarded object as main material production yolk color improver, then at the prerequisite decline low production cost ensureing result of use, total revenue can be increased.

Fruit process industry produces a large amount of pericarp, and most of pericarp becomes rubbish, and enterprise need bear the garbage transporting, the handling that surpass hundred yuan per ton, and therefore urban environment also bears burdens.Pericarp garbage conversion, if make full use of, such as feed addictive, can be become environmental benefit and economic benefit by pericarp.But the key problem that need solve is that in pericarp, active component animal absorptivity is not high, and pericarp palatability is poor, and high humidity is perishable.So process pericarp of employing new technology, the feeding yolk color improver of development of new has realistic meaning.

Summary of the invention

The object of this invention is to provide the method for producing the feeding yolk color improver of efficiency natural with discarded pericarp, solve the selection of raw material and the optimum formula of each material rate and auxiliary agent ratio, carotenoid composition in efficient release pericarp, significantly reduces pericarp bitter taste; Active component in efficient stripping pericarp, produces natural feeding yolk color improver, realizes turning waste into wealth, develop a circular economy.

For achieving the above object, the technical solution used in the present invention is: the production method of the feeding yolk color improver of efficiency natural, the first step, and auxiliary agent is prepared, and auxiliary agent is kaolin: sulfobutyl ether-beta-cyclodextrin: xylitol=1.7: 1.3: 1.6;

Second step, mangrove bark, orange peel, bean dregs, silkworm waste silk, the yellow volvox in America are dried or dried, and water content, 10 ~ 13%, is crushed to 60 ~ 80 object meal respectively;

3rd step, gets the raw materials ready by following weight portion: mangrove bark powder 25-27 part, orange peel powder 33-35 part, okara powder 32-34 part, silkworm waste silk 17-19 part, reaches and exerts analogy Synura 6.5 parts, auxiliary agent 5 parts; Each raw material meal mixing is mixed with auxiliary agent again;

4th step; the mixture high energy vibration mill 3rd step obtained processes; under cool cycles water temperature 19 ~ 21 DEG C, frequency 16Hz, rod iron acceleration 8 ~ 9g; processing time 15 ~ 30min, then shuts down 2.5min, then with rod iron acceleration 7.5g; process 12 ~ 13min; there is twice different solid-state machinery chemical reaction in each raw material, crosses 400 mesh sieves, obtain finished product.

Each raw material optimization formula is: 26 parts, mangrove bark powder, 34 parts, orange peel powder, okara powder 33 parts, 18 parts, silkworm waste silk, reaches and exerts analogy Synura 5.2 parts, auxiliary agent 9 parts.

The invention has the beneficial effects as follows: the selection of raw material of the present invention and the best of breed of each material rate and auxiliary agent ratio, and use high energy vibration to grind process raw material, one is that the carotenoid composition enabling to contain in raw material efficiently discharges, and bitter taste significantly reduces, and palatability meets the requirement of feed industry; Two is that the natural scents of plant micropowder fully discharges, and is beneficial to following process; Three is that raw material includes the efficient stripping of active component, and assimilation effect comparatively meal significantly improves, and is beneficial to animal uptake and accumulation, and yolk yellow valency obviously rises, and can improve laying rate and average egg weight simultaneously; Four is that production technology is simple, easy to use, significantly reduces the raw material production cost of prior art, make mangrove bark, orange peel is applicable to being processed into natural feeding yolk color improver, realize recycling economy and sustainable development, for enterprise brings economic benefit, and alleviate environmental protection pressure.

Formula Raw part by weight is very important, and reason is:

1. the particularity of the mutual ratio of various composition

Containing multiple types carrotene and Tea Polyphenols in mangrove bark, yolk color can be made to deepen, but ratio is too high, wherein pectin composition is too much, affects laying hen metabolism.If orange peel consumption is too high, then yellow component is too much, and yolk color is only yellow intensification, and colourimetric number can only reach about 8, and distance export standard 11 still has significance difference distance; If bean dregs too high levels, then fibre composition is many, the easy agglomerate caking of material, more difficult processing, and intractability strengthens; The glycine of more than 40% and the silk gum of more than 10% in silkworm waste silk, greatly can promote natural colouring matter enrichment in yolk, but the fibroin being wrapped in silk gum inside is water-soluble poor, addition is excessive, easily swells block in the narrow crook of alimentary canal.

To sum up, the ratio of orange peel, bean dregs, mangrove bark, silkworm waste silk has significant particularity, it is one of innovative point of this technology, if only by rule of thumb or general knowledge slightly join, obviously the bright yolk color that yellow red dichromatism has concurrently cannot be obtained under low cost, tractable prerequisite, the product obtained may be only partially yellow, easily disperses (difficulty infiltrates or throws something and feeds) or easily caking, easily adhesion, easily corruption, difficult storage or mixing.

2. auxiliary agent ratio particularity

Auxiliary agent of the present invention is by kaolin: sulfobutyl ether-beta-cyclodextrin: xylitol=1.5:1.3:2.1 forms, not common equal proportion mixing, selects the foundation of this special ratios to be summarized as follows:

Sulfobutyl ether-beta-cyclodextrin is the one that in shitosan compounds, cross-linking effect is best, and short solubility property is good, but cost is higher; The large then high cost of addition, addition little then target substance bag is insufficient.It is as osmotic pressure regulator, antioxidant synergist that xylitol one of acts in the present invention, and the too high absorption efficiency that causes on the contrary of ratio reduces, and content is too low is difficult to onset again.Kaolin is one of sorbefacient key assistant, and too high levels makes preparation block in the agglomerating formation that namely absorbs water of alimentary canal leading portion, affects bioavailability.So the selection of three kinds of auxiliary agent raw materials and the relative scale of upper person are one of main innovate point of the present invention, the simple general knowledge not with the industry just can draw.

Detailed description of the invention

Provide embodiment below to elaborate to the present invention.

Embodiment 1 first step, auxiliary agent is prepared; Kaolin: sulfobutyl ether-beta-cyclodextrin: xylitol=1.7: 1.3: 1.6;

Second step, mangrove bark, orange peel, bean dregs, silkworm waste silk, the yellow volvox in America are dried or dried, and water content, 10 ~ 13%, is crushed to 60 ~ 80 object meal respectively;

3rd step, taking raw material (formula one) is by weight: 34 parts, orange peel powder, okara powder 33 parts, 26 parts, mangrove bark powder, and 18 parts, silkworm waste silk, reaches and exert analogy Synura 5.2 parts, auxiliary agent 5 parts; Each raw material meal mixing is mixed with auxiliary agent again;

4th step; high energy vibration mill is used by raw material after mixing to process; under cool cycles water temperature 19 ~ 21 DEG C, frequency 16Hz, rod iron acceleration 8 ~ 9g; processing time 15 ~ 30min, then shuts down 2.5min, then with rod iron acceleration 7.5g; processing time 12 ~ 13min; there is twice different solid-state machinery chemical reaction in each raw material, crosses 400 mesh sieves, obtain finished product.This product is rich in vitamin C, lutein, carotenoid, as the feeding yolk color improver of laying hen.

Embodiment 2, method for making are with embodiment 1, and parts by weight of raw materials (formula two) is: 33 parts, orange peel powder, okara powder 32 parts, 25 parts, mangrove bark powder, and 17 parts, silkworm waste silk reaches and exerts analogy Synura 5.2 parts, auxiliary agent 9 parts.

Embodiment 3, method for making are with embodiment 1, and parts by weight of raw materials (formula three) is: 35 parts, orange peel powder, okara powder 34 parts, 27 parts, mangrove bark powder, and 19 parts, silkworm waste silk reaches and exerts analogy Synura 5.2 parts, auxiliary agent 9 parts.

Using method: be added in laying hen adequate diet with product 2 ~ 3% ratio of the present invention, uses continuously and can significantly increase yolk yellow valency in more than 3 days, have no adverse effects to other physical signs of laying hen.

In order to check effect of the present invention, in April, 2013 has carried out following test in fine chemistry industry National Key Laboratory of Dalian University of Technology of Liaoning Province:

Test material: the present invention fills a prescription one, three kinds of products of formula two, formula three, control group, with orange peel, bean dregs, mangrove bark, the yellow volvox equal proportion mixing in America, compares with laying hen adequate diet simultaneously.

Testing index:

Yolk yellow valency: the blue brown laying hen in sea, 120/experimental group.Every day receives egg, is broken by egg in glass culture dish, and ware lower berth adularescent ground paper, as background, uses Roche yolk colorimetric fan to carry out colorimetric under fluorescent light.(1 → 14, color from shallow to deep).

Experimental result sees the following form (7 days):

Test shows: product of the present invention, as natural feeding yolk color improver, significantly can improve the yolk color of laying hen.From yolk yellow valency, fill a prescription one group and reach 13.36, significantly improve than control group and adequate diet group.Given prominence to by the visible practicality of the present invention of experimental result, effect is obvious, can carry out considerable economic benefit for breeding layer chicken industrial belt.

Claims (3)

1. the production method of the feeding yolk color improver of efficiency natural, is characterized in that:

The first step, auxiliary agent is prepared, and auxiliary agent is kaolin: sulfobutyl ether-beta-cyclodextrin: xylitol=1.7: 1.3: 1.6;

Second step, mangrove bark, orange peel, bean dregs, silkworm waste silk, the yellow volvox in America are dried or dried, and water content, 10 ~ 13%, is crushed to 60 ~ 80 object meal respectively;

3rd step, gets the raw materials ready by following weight portion: 25 ~ 27 parts, mangrove bark powder, 33 ~ 35 parts, orange peel powder, okara powder 32 ~ 34 parts, 17 ~ 19 parts, silkworm waste silk, reaches and exerts analogy Synura 6.5 parts, auxiliary agent 5 parts; Each raw material meal mixing is mixed with auxiliary agent again;

4th step; the raw mixture high energy vibration mill 3rd step obtained processes; under cool cycles water temperature 19 ~ 21 DEG C, frequency 16Hz, rod iron acceleration 8 ~ 9g; processing time 15 ~ 30min, then shuts down 2.5min, then with rod iron acceleration 7.5g; processing time 12 ~ 13min; there is twice different solid-state machinery chemical reaction in each raw material, crosses 400 mesh sieves, obtain finished product.

2. efficiency natural feeding yolk color improver production method as claimed in claim 1, each raw material optimization formula is: 26 parts, mangrove bark powder, 34 parts, orange peel powder, okara powder 33 parts, 18 parts, silkworm waste silk, reaches and exerts analogy Synura 5.2 parts, auxiliary agent 9 parts.

3. the product that obtains of efficiency natural feeding yolk color improver production method as claimed in claim 1.