CN105415465B - A kind of preparation method of willow writing brush penholder - Google Patents

A kind of preparation method of willow writing brush penholder Download PDF

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Publication number
CN105415465B
CN105415465B CN201510794857.XA CN201510794857A CN105415465B CN 105415465 B CN105415465 B CN 105415465B CN 201510794857 A CN201510794857 A CN 201510794857A CN 105415465 B CN105415465 B CN 105415465B
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CN
China
Prior art keywords
willow
hours
penholder
preparation
plate
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201510794857.XA
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Chinese (zh)
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CN105415465A (en
Inventor
朱建青
朱凯
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Bengbu Shenlong Pencils Co Ltd
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Bengbu Shenlong Pencils Co Ltd
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Priority to CN201510794857.XA priority Critical patent/CN105415465B/en
Publication of CN105415465A publication Critical patent/CN105415465A/en
Application granted granted Critical
Publication of CN105415465B publication Critical patent/CN105415465B/en
Expired - Fee Related legal-status Critical Current
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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K3/00Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
    • B27K3/02Processes; Apparatus
    • B27K3/08Impregnating by pressure, e.g. vacuum impregnation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K5/00Treating of wood not provided for in groups B27K1/00, B27K3/00
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27MWORKING OF WOOD NOT PROVIDED FOR IN SUBCLASSES B27B - B27L; MANUFACTURE OF SPECIFIC WOODEN ARTICLES
    • B27M3/00Manufacture or reconditioning of specific semi-finished or finished articles

Abstract

The present invention relates to writing brush technical field, and in particular to a kind of preparation method of willow writing brush penholder, comprises the following steps:Selection;Alkalescence immersion;Acidity immersion;Vulcanization;Heat is steamed;Processing;Penholder density and glossiness produced by the present invention are all improved, and are unlikely to deteriorate, and thoroughly sterilization, and without preservative, environment protection health uses good hand touch.

Description

A kind of preparation method of willow writing brush penholder
Technical field:
The present invention relates to writing brush technical field, and in particular to a kind of preparation method of willow writing brush penholder.
Background technology:
Material for making writing brush penholder is a lot, slightly and classifying has:Metal class:Gold, silver, copper, stainless steel tube;
Wood type:Hardwood, ebony, nanmu, the penholder that sandalwood etc. is made, mostly wooden hard, decorative pattern beauty is individually It is wooden to have special fragrance, it is first-class penholder material;
Bamboo class;Bai Zhuguan, square bamboo trunk, black bamboo pipe, bamboo palm pipe, mottled bamboo pipe, bamboo of the Ladies of the Xiang pipe and horsewhip bamboo trunk etc..Note:Tear is done Blood goes out, and drips bamboo spotting, and the bamboo of the Ladies of the Xiang product valency of Ming and Qing is high, has imitative product, calls its " boiling hot prince wife ", i.e., burn spot with flatiron on Bai Zhu Trace;
Animal class:Rhinoceros, ivory;
Porcelain class:Blue and white, under-glaze red, powder enamel etc.;
Plastic:Sticking plaster;
Other:Jade, hawksbill turtle, enamel etc.;Note:The beautiful pen pipe in ancient times is all made with the Khotan jade for originating from Xinjiang Tianshan, is divided into White jade, sapphire, topaz, jasper, the kind such as black jade, color is beautiful, and matter is thin, is available for collecting and appreciate treasure, also reality enamel pipe, with copper smoothness scape Safe indigo plant glazing, which is fired, to be formed, and penholder is heavier, magnificent attractive in appearance, mostly admires pen.
Except timber, bamboo class, plastics, the penholder of other materials involves great expense, and plastics are poor using feel, conventional still wood Material, and good timber cost is equally expensive, the manufacturing process of common timber penholder make it that penholder feel is poor, easily broken, yielding, And preservative is with the addition of, not environmentally.
The content of the invention:
The technical problems to be solved by the invention be to overcome existing technological deficiency provide it is a kind of it is with low cost, using hand The preparation method for the willow writing brush penholder felt.
The technical problems to be solved by the invention are realized using following technical scheme:
A kind of preparation method of willow writing brush penholder, it is characterised in that comprise the following steps:
(1) selection:5-10 willow raw material is chosen, then carries out cutting into willow plate;
(2) alkalescence immersion:Willow plate is immersed in soda ash solution 9-15 hours, temperature control is in 130-140 DEG C, pressure Control is taken out and soaked 1-2 hours using deionized water in 3-4MPa, then is rinsed 20-30 minutes, carries out low temperature drying, dries temperature Degree is at 30-40 DEG C;
(3) acid immersion:Dried willow plate is put into sealing acidification pool, uniformly 5-9% is put into acidification pool Hydrochloric acid solution, is increased to 120-130 DEG C, pressure rise to 2-3MPa after 9-12 hours, adds 9- by the temperature of acidification pool 12% acetum, pressure rise to 5-6MPa, the time is 6-7 hours, is then taken out, and uses deionized water rinsing 1-2 hours;
(4) vulcanize:Willow plate is added into vulcanizing tank, temperature control is in 175 DEG C -185 DEG C, Stress control 1MPa- in tank 1.2MPa, curing time control were at -6 hours 5 hours;
(5) heat is steamed:Willow plate after vulcanization is put into drying chamber and carries out hot steaming processing, is kept at 50-60 DEG C of low temperature 30-40 hours;Kept for 16-20 hour at 130-150 DEG C of high temperature again, while the spraying steam into drying room, makes willow plate holding 5- 10% moisture content;Kept for 40-50 hours at 60-70 DEG C of low temperature;
(6) process:The penholder of model needed for willow plate is processed into, then sanding and polishing processing;
Further, described steam includes the raw material of following weight percents:1-2% polyhydroxyalkanoates, 0.5- 1% isocyanates, 0.2-0.5% silicone oil, 1-2% castor oil, remaining is water;
Described steam preparation method is:Above-mentioned each raw material is mixed to be put into evaporating dish and heated, steam is produced.
It is of the invention thorough by lignin in willow and cellulose modified so that oxidation Decomposition occurs for willow, so as to reduce willow Hygroscopicity so that the swelling capacity of timber declines, and hydrophobicity is improved;
Obtained penholder is unlikely to deform, bent, and willow can be planted, and growth period is short, sustainability, with certain economic society Can benefit;
Penholder density and glossiness produced by the present invention are all improved, and are unlikely to deteriorate, and thoroughly sterilization, without anti-corrosion Agent, environment protection health uses good hand touch.
Embodiment:
In order that the technical means, the inventive features, the objects and the advantages of the present invention are easy to understand, enter below One step illustrates the present invention.
In embodiment:A kind of preparation method of willow writing brush penholder, it is characterised in that comprise the following steps:
(1) selection:5-10 willow raw material is chosen, then carries out cutting into willow plate;
(2) alkalescence immersion:Willow plate is immersed in soda ash solution 9-15 hours, temperature control is in 130-140 DEG C, pressure Control is taken out and soaked 1-2 hours using deionized water in 3-4MPa, then is rinsed 20-30 minutes, carries out low temperature drying, dries temperature Degree is at 30-40 DEG C;
(3) acid immersion:Dried willow plate is put into sealing acidification pool, uniformly 5-9% is put into acidification pool Hydrochloric acid solution, is increased to 120-130 DEG C, pressure rise to 2-3MPa after 9-12 hours, adds 9- by the temperature of acidification pool 12% acetum, pressure rise to 5-6MPa, the time is 6-7 hours, is then taken out, and uses deionized water rinsing 1-2 hours;
(4) vulcanize:Willow plate is added into vulcanizing tank, temperature control is in 175 DEG C -185 DEG C, Stress control 1MPa- in tank 1.2MPa, curing time control were at -6 hours 5 hours;
(5) heat is steamed:Willow plate after vulcanization is put into drying chamber and carries out hot steaming processing, is kept at 50-60 DEG C of low temperature 30-40 hours;Kept for 16-20 hour at 130-150 DEG C of high temperature again, while the spraying steam into drying room, makes willow plate holding 5- 10% moisture content;Kept for 40-50 hours at 60-70 DEG C of low temperature;
(6) process:The penholder of model needed for willow plate is processed into, then sanding and polishing processing;
Steam includes the raw material of following weight percents:1-2% polyhydroxyalkanoates, 0.5-1% isocyanates, 0.2- 0.5% silicone oil, 1-2% castor oil, remaining is water;
Steam preparation method is:Above-mentioned each raw material is mixed to be put into evaporating dish and heated, steam is produced.
The general principle and principal character and advantages of the present invention of the present invention has been shown and described above.The technology of the industry Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the simply explanation described in above-described embodiment and specification is originally The principle of invention, without departing from the spirit and scope of the present invention, various changes and modifications of the present invention are possible, these changes Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its Equivalent thereof.

Claims (2)

1. a kind of preparation method of willow writing brush penholder, it is characterised in that comprise the following steps:
(1) selection:5-10 willow raw material is chosen, then carries out cutting into willow plate;
(2) alkalescence immersion:Willow plate is immersed in soda ash solution 9-15 hours, temperature control is in 130-140 DEG C, Stress control In 3-4MPa, take out and soaked 1-2 hours using deionized water, then rinse 20-30 minutes, carry out low temperature drying, drying temperature exists 30-40℃;
(3) acid immersion:Dried willow plate is put into sealing acidification pool, uniformly 5-9% hydrochloric acid is put into acidification pool Solution, is increased to 120-130 DEG C, pressure rise to 2-3MPa after 9-12 hours, adds 9-12% vinegar by the temperature of acidification pool Acid solution, pressure rise to 5-6MPa, the time is 6-7 hours, is then taken out, and uses deionized water rinsing 1-2 hours;
(4) vulcanize:Willow plate is added into vulcanizing tank, in tank temperature control 175 DEG C -185 DEG C, Stress control 1MPa-1.2MPa, sulphur Change processing time control at -6 hours 5 hours;
(5) heat is steamed:Willow plate after vulcanization is put into drying chamber and carries out hot steaming processing, 30-40 is kept at 50-60 DEG C of low temperature Hour;Kept for 16-20 hour at 130-150 DEG C of high temperature again, while the spraying steam into drying room, contains willow plate holding 5-10% Water rate;Kept for 40-50 hours at 60-70 DEG C of low temperature;
(6) process:The penholder of model needed for willow plate is processed into, then sanding and polishing processing.
2. the preparation method of a kind of willow writing brush penholder according to claim 1, it is characterised in that described steam includes The raw material of following weight percents:1-2% polyhydroxyalkanoates, 0.5-1% isocyanates, 0.2-0.5% silicone oil, 1-2% Castor oil, remaining is water;
Described steam preparation method is:Above-mentioned each raw material is mixed to be put into evaporating dish and heated, steam is produced.
CN201510794857.XA 2015-11-17 2015-11-17 A kind of preparation method of willow writing brush penholder Expired - Fee Related CN105415465B (en)

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Application Number Priority Date Filing Date Title
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Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107127854B (en) * 2017-05-18 2018-11-23 阜南县星光工艺品有限公司 A kind of softening method of bark
CN107297803A (en) * 2017-05-18 2017-10-27 阜南县星光工艺品有限公司 A kind of softening mold-proof method of timber
CN108501149A (en) * 2018-04-10 2018-09-07 绩溪县上庄老胡开文墨厂 A kind of preparation method of willow writing brush penholder
CN108340460A (en) * 2018-04-10 2018-07-31 绩溪县上庄老胡开文墨厂 A kind of preparation method of willow writing brush penholder
CN114888913B (en) * 2022-05-13 2023-07-18 安徽德润工艺品有限公司 Production process method for in-situ crosslinking self-toughening braided wicker

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101264679A (en) * 2008-04-30 2008-09-17 周觉民 Rattan bamboo plus material and preparation method thereof
CN102225563A (en) * 2011-04-27 2011-10-26 信和光伏硅材料(福建)有限公司 Method for cleaning treatment of wood chip
CN102699970A (en) * 2012-05-22 2012-10-03 浙江庆元欧迪实业有限公司 Modified production method and modified production device for poplar pencil board

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101264679A (en) * 2008-04-30 2008-09-17 周觉民 Rattan bamboo plus material and preparation method thereof
CN102225563A (en) * 2011-04-27 2011-10-26 信和光伏硅材料(福建)有限公司 Method for cleaning treatment of wood chip
CN102699970A (en) * 2012-05-22 2012-10-03 浙江庆元欧迪实业有限公司 Modified production method and modified production device for poplar pencil board

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