CN105384966A - Coconut oil-calcium carbonate activating agent - Google Patents
Coconut oil-calcium carbonate activating agent Download PDFInfo
- Publication number
- CN105384966A CN105384966A CN201510755915.8A CN201510755915A CN105384966A CN 105384966 A CN105384966 A CN 105384966A CN 201510755915 A CN201510755915 A CN 201510755915A CN 105384966 A CN105384966 A CN 105384966A
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- Prior art keywords
- parts
- calcium carbonate
- resin
- coconut oil
- activating agent
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K9/00—Use of pretreated ingredients
- C08K9/04—Ingredients treated with organic substances
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/24—Acids; Salts thereof
- C08K3/26—Carbonates; Bicarbonates
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K9/00—Use of pretreated ingredients
- C08K9/02—Ingredients treated with inorganic substances
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K9/00—Use of pretreated ingredients
- C08K9/04—Ingredients treated with organic substances
- C08K9/06—Ingredients treated with organic substances with silicon-containing compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K9/00—Use of pretreated ingredients
- C08K9/08—Ingredients agglomerated by treatment with a binding agent
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/24—Acids; Salts thereof
- C08K3/26—Carbonates; Bicarbonates
- C08K2003/265—Calcium, strontium or barium carbonate
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- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
The invention discloses a coconut oil-calcium carbonate activating agent. The coconut oil-calcium carbonate activating agent is characterized by being prepared from, by weight, 5-8 parts of glycol ether, 3-8 parts of pentaerythritol rosin europium resin, 25-30 parts of cocoanut fatty acid diethanolamide, 5-8 parts of sodium carbonate, 3-5 parts of sodium acrylate-4-vinylpyridine copolymers, 5-6 parts of fungacetin, 10-12 parts of di-n-octyltin oxide, 3-5 parts of polyvinyl acetal resin, 25-30 parts of gamma-glycidoxy propyl trimethoxy silane, 3-5 parts of dodecyl dimethyl benzyl ammonium bromide, 20-30 parts of ethyl alcohol and 550-600 parts of water. The coconut oil-calcium carbonate activating agent has the advantages of being scientific and reasonable in design, simple in technology, safe, reliable, easy to control, convenient to operate, suitable for mass production, low in production cost and the like.
Description
Technical field
The invention belongs to a kind of auxiliary agent producing non-metallic powder.
Background technology
At present, calcium carbonate is widely used in papermaking, plastics, plastics film, chemical fibre, rubber, tackiness agent, sealing agent, daily-use chemical industry, makeup, building materials, coating, paint, ink, putty, sealing wax, putty, carpet veneer is packed, medicine, food is (as chewing gum, chocolate), in feed, its effect has: increase small product size, reduce costs, improve processing characteristics (as adjusting viscosity, rheological property, curability), improve dimensional stability, reinforcement or half reinforcement, improve printing performance, improve physicals (as thermotolerance, extinction, wear resistance, flame retardant resistance, whiteness, glossiness) etc., for obtaining more superior performance, auxiliary agent is all adopted to carry out activation treatment.
Summary of the invention
The object of the invention is to; A kind of Oleum Cocois calcium carbonate activator and preparation method thereof is proposed.
Oleum Cocois calcium carbonate activator calcium carbonate activator of the present invention, it is characterized in that: by weight, its formula is by ethylene glycol ethyl ether 5-8 part, rosin pentaerythritol ester europium resin 3-8 part, cocoanut fatty acid diethanolamide 25-30 part, sodium carbonate 5-8 part, sodium acrylate-4-vinylpridine multipolymer 3-5 part, Vanay 5-6 part, di-n-octyltin oxide 10--12 part, polyvinyl acetal resin 3-5 part, γ-glycidyl ether oxygen propyl trimethoxy silicane 25-30 part, dodecyl dimethyl benzyl ammonium bromide 3-5 part, ethanol 20-30 part, water 550-600 part forms.
The preparation method of Oleum Cocois calcium carbonate activator calcium carbonate activator of the present invention, it is characterized in that: by weight, its formula is by ethylene glycol ethyl ether 5-8 part, rosin pentaerythritol ester europium resin 3-8 part, cocoanut fatty acid diethanolamide 25-30 part, sodium carbonate 5-8 part, sodium acrylate-4-vinylpridine multipolymer 3-5 part, Vanay 5-6 part, di-n-octyltin oxide 10--12 part, polyvinyl acetal resin 3-5 part, γ-glycidyl ether oxygen propyl trimethoxy silicane 25-30 part, dodecyl dimethyl benzyl ammonium bromide 3-5 part, ethanol 20-30 part, water 550-600 part forms, first with ethanol by rosin europium resin dissolves, after adding water 550-600 part, add whole raw material and mix, at 85 ~ 95 DEG C, stir 20-30 minute, obtain product.
The present invention compared with prior art its beneficial effect is: have design science reasonable, and technique is simple, safe reliability, is easy to control, easy to operate, is applicable to scale operation, the advantages such as production cost is low.
Embodiment
Below in conjunction with embodiment, the invention will be further described, but embodiments of the present invention are not limited thereto.
All raw materials of the present invention can buy acquisition.
Embodiment 1
The preparation method of Oleum Cocois calcium carbonate activator calcium carbonate activator of the present invention, it is characterized in that: by weight, its formula is by ethylene glycol ethyl ether 5-8 part, rosin pentaerythritol ester europium resin 3-8 part, cocoanut fatty acid diethanolamide 25-30 part, sodium carbonate 5-8 part, sodium acrylate-4-vinylpridine multipolymer 3-5 part, Vanay 5-6 part, di-n-octyltin oxide 10--12 part, polyvinyl acetal resin 3-5 part, γ-glycidyl ether oxygen propyl trimethoxy silicane 25-30 part, dodecyl dimethyl benzyl ammonium bromide 3-5 part, ethanol 20-30 part, water 550-600 part forms, first with ethanol by rosin europium resin dissolves, after adding water 550-600 part, add whole raw material and mix, at 85 ~ 95 DEG C, stir 20-30 minute, obtain product.
Embodiment 2
The preparation method of Oleum Cocois calcium carbonate activator calcium carbonate activator of the present invention, is characterized in that: by weight, and its formula is by ethylene glycol ethyl ether 5-8 part, rosin pentaerythritol ester europium resin 3 parts, cocoanut fatty acid diethanolamide 25 parts, 5 parts, sodium carbonate, sodium acrylate-4-vinylpridine multipolymer 3 parts, Vanay 5 parts, dioctyl tin 10 parts, polyvinyl acetal resin 3 parts, glycidyl ether oxygen propyl trimethoxy silicane 25 parts, ethanol 20-30 part, water 550-600 part forms; First with ethanol by rosin europium resin dissolves, after adding water 550-600 part, add whole raw material and mix, at 85 ~ 95 DEG C, stir 20-30 minute, obtain product.
Embodiment 3
The preparation method of Oleum Cocois calcium carbonate activator calcium carbonate activator of the present invention, it is characterized in that: by weight, its formula is by ethylene glycol ethyl ether 5-8 part, rosin pentaerythritol ester europium resin 8 parts, cocoanut fatty acid diethanolamide 30 parts, 8 parts, sodium carbonate, sodium acrylate-4-vinylpridine multipolymer 5 parts, Vanay 6 parts, dioctyl tin 12 parts, polyvinyl acetal resin 5 parts, glycidyl ether oxygen propyl trimethoxy silicane 30 parts, dodecyl dimethyl benzyl ammonium bromide 3-5 part, ethanol 20-30 part, water 550-600 part forms; First with ethanol by rosin europium resin dissolves, after adding water 550-600 part, add whole raw material and mix, at 85 ~ 95 DEG C, stir 20-30 minute, obtain product.
Embodiment 4
The preparation method of Oleum Cocois calcium carbonate activator calcium carbonate activator of the present invention, it is characterized in that: by weight, its formula is by ethylene glycol ethyl ether 5-8 part, rosin pentaerythritol ester europium resin 3 parts, cocoanut fatty acid diethanolamide 30 parts, 5 parts, sodium carbonate, sodium acrylate-4-vinylpridine multipolymer 5 parts, Vanay 5 parts, dioctyl tin 12 parts, polyvinyl acetal resin 3 parts, glycidyl ether oxygen propyl trimethoxy silicane 25 parts, dodecyl dimethyl benzyl ammonium bromide 3-5 part, ethanol 20-30 part, water 550-600 part forms; First with ethanol by rosin europium resin dissolves, after adding water 550-600 part, add whole raw material and mix, at 85 ~ 95 DEG C, stir 20-30 minute, obtain product.
Product of the present invention, uses through production firm, and produce modified superfine water-ground limestone product, reaction effect is fine.
Part material illustrates:
Described rosin pentaerythritol ester europium resin, the method that can be preferably ZL201410078259.8 by the Chinese patent patent No. obtains.
γ-glycidyl ether oxygen propyl trimethoxy silicane
No. Cas: 2530-83-8
Molecular formula: C9H20O5Si molecular weight: 236.34
Another name: 3-(2,3-epoxy third oxygen) propyl trimethoxy silicane, 3-glycydoxy Trimethoxy silane
γ-glycidyl ether oxygen propyl trimethoxy silicane.
Claims (2)
1. an Oleum Cocois calcium carbonate activator calcium carbonate activator, it is characterized in that: by weight, its formula is by ethylene glycol ethyl ether 5-8 part, rosin pentaerythritol ester europium resin 3-8 part, cocoanut fatty acid diethanolamide 25-30 part, sodium carbonate 5-8 part, sodium acrylate-4-vinylpridine multipolymer 3-5 part, Vanay 5-6 part, di-n-octyltin oxide 10--12 part, polyvinyl acetal resin 3-5 part, γ-glycidyl ether oxygen propyl trimethoxy silicane 25-30 part, dodecyl dimethyl benzyl ammonium bromide 3-5 part, ethanol 20-30 part, water 550-600 part forms.
2. the preparation method of an Oleum Cocois calcium carbonate activator calcium carbonate activator, it is characterized in that: by weight, its formula is by ethylene glycol ethyl ether 5-8 part, rosin pentaerythritol ester europium resin 3-8 part, cocoanut fatty acid diethanolamide 25-30 part, sodium carbonate 5-8 part, sodium acrylate-4-vinylpridine multipolymer 3-5 part, Vanay 5-6 part, di-n-octyltin oxide 10--12 part, polyvinyl acetal resin 3-5 part, γ-glycidyl ether oxygen propyl trimethoxy silicane 25-30 part, dodecyl dimethyl benzyl ammonium bromide 3-5 part, ethanol 20-30 part, water 550-600 part forms, first with ethanol by rosin europium resin dissolves, after adding water 550-600 part, add whole raw material and mix, at 85 ~ 95 DEG C, stir 20-30 minute, obtain product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510755915.8A CN105384966A (en) | 2015-11-07 | 2015-11-07 | Coconut oil-calcium carbonate activating agent |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510755915.8A CN105384966A (en) | 2015-11-07 | 2015-11-07 | Coconut oil-calcium carbonate activating agent |
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| Publication Number | Publication Date |
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| CN105384966A true CN105384966A (en) | 2016-03-09 |
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| CN201510755915.8A Pending CN105384966A (en) | 2015-11-07 | 2015-11-07 | Coconut oil-calcium carbonate activating agent |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103820032A (en) * | 2014-03-05 | 2014-05-28 | 张雅静 | Preparation method of pentaerythrite colophony europium resin |
| CN104371375A (en) * | 2014-10-31 | 2015-02-25 | 陈显鹏 | Vinyltris(methylethylketoximino)silane superfine calcium carbonate powder assistant |
| CN104403246A (en) * | 2014-10-31 | 2015-03-11 | 廖文成 | Ultrafine calcium carbonate powder acetal modifier |
| CN104403266A (en) * | 2014-10-31 | 2015-03-11 | 廖文成 | Amino resin-containing calcium carbonate powder modifier |
-
2015
- 2015-11-07 CN CN201510755915.8A patent/CN105384966A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103820032A (en) * | 2014-03-05 | 2014-05-28 | 张雅静 | Preparation method of pentaerythrite colophony europium resin |
| CN104371375A (en) * | 2014-10-31 | 2015-02-25 | 陈显鹏 | Vinyltris(methylethylketoximino)silane superfine calcium carbonate powder assistant |
| CN104403246A (en) * | 2014-10-31 | 2015-03-11 | 廖文成 | Ultrafine calcium carbonate powder acetal modifier |
| CN104403266A (en) * | 2014-10-31 | 2015-03-11 | 廖文成 | Amino resin-containing calcium carbonate powder modifier |
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Application publication date: 20160309 |