CN105419396A - Carboxylated imidozoline phosphate activator for calcium carbonate - Google Patents

Carboxylated imidozoline phosphate activator for calcium carbonate Download PDF

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Publication number
CN105419396A
CN105419396A CN201510755810.2A CN201510755810A CN105419396A CN 105419396 A CN105419396 A CN 105419396A CN 201510755810 A CN201510755810 A CN 201510755810A CN 105419396 A CN105419396 A CN 105419396A
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China
Prior art keywords
parts
imidozoline
carboxylated
phosphate
calcium carbonate
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Pending
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CN201510755810.2A
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Chinese (zh)
Inventor
李安平
廖煜明
杨毅
黄景诚
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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/02—Compounds of alkaline earth metals or magnesium
    • C09C1/021—Calcium carbonates
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
    • C09C1/02—Compounds of alkaline earth metals or magnesium
    • C09C1/021—Calcium carbonates
    • C09C1/022—Treatment with inorganic compounds
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
    • C09C3/006—Combinations of treatments provided for in groups C09C3/04 - C09C3/12
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
    • C09C3/06—Treatment with inorganic compounds
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
    • C09C3/08—Treatment with low-molecular-weight non-polymer organic compounds
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
    • C09C3/10—Treatment with macromolecular organic compounds
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK  ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
    • C09C3/00—Treatment in general of inorganic materials, other than fibrous fillers, to enhance their pigmenting or filling properties
    • C09C3/12—Treatment with organosilicon compounds

Abstract

The invention discloses a carboxylated imidozoline phosphate activator for calcium carbonate. The carboxylated imidozoline phosphate activator for the calcium carbonate is prepared from, by weight, 5-8 parts of carboxylated imidozoline phosphate, 3-8 parts of pentaerythritol rosin resin, 25-30 parts of cocoanut fatty acid diethanolamide, 5-8 parts of sodium carbonate, 3-5 parts of poly(sodium acrylate-4-vinylpyridine), 5-6 parts of glycerol triacetate, 10-12 parts of dioctyltin oxide, 3-5 parts of polyvinyl acetal resin, 25-30 parts of gamma-glycidyloxypropyl trimethoxy silane, 3-5 parts of dodecyl dimethyl benzyl ammonium bromide, 20-30 parts of ethyl alcohol and 550-600 parts of water. The carboxylated imidozoline phosphate activator for the calcium carbonate has the advantages of scientific and reasonable design, technical simplicity, safety, reliability, easiness in control, convenience in operation, suitableness for large-scale production, low cost and the like.

Description

Carboxylated imidozoline phosphate calcium carbonate activator
Technical field
The invention belongs to a kind of auxiliary agent producing non-metallic powder.
Background technology
At present, calcium carbonate is widely used in papermaking, plastics, plastics film, chemical fibre, rubber, tackiness agent, sealing agent, daily-use chemical industry, makeup, building materials, coating, paint, ink, putty, sealing wax, putty, carpet veneer is packed, medicine, food is (as chewing gum, chocolate), in feed, its effect has: increase small product size, reduce costs, improve processing characteristics (as adjusting viscosity, rheological property, curability), improve dimensional stability, reinforcement or half reinforcement, improve printing performance, improve physicals (as thermotolerance, extinction, wear resistance, flame retardant resistance, whiteness, glossiness) etc., for obtaining more superior performance, auxiliary agent is all adopted to carry out activation treatment.
Summary of the invention
The object of the invention is to; A kind of carboxylated imidozoline phosphate calcium carbonate activator and preparation method thereof is proposed.
Carboxylated imidozoline phosphate calcium carbonate activator of the present invention, it is characterized in that: by weight, its formula is by carboxylated imidozoline phosphate 5-8 part, rosin pentaerythritol ester europium resin 3-8 part, cocoanut fatty acid diethanolamide 25-30 part, sodium carbonate 5-8 part, sodium acrylate-4-vinylpridine multipolymer 3-5 part, Vanay 5-6 part, di-n-octyltin oxide 10--12 part, polyvinyl acetal resin 3-5 part, γ-glycidyl ether oxygen propyl trimethoxy silicane 25-30 part, dodecyl dimethyl benzyl ammonium bromide 3-5 part, ethanol 20-30 part, water 550-600 part forms.
The preparation method of carboxylated imidozoline phosphate calcium carbonate activator of the present invention, it is characterized in that: by weight, its formula is by carboxylated imidozoline phosphate 5-8 part, rosin pentaerythritol ester europium resin 3-8 part, cocoanut fatty acid diethanolamide 25-30 part, sodium carbonate 5-8 part, sodium acrylate-4-vinylpridine multipolymer 3-5 part, Vanay 5-6 part, di-n-octyltin oxide 10--12 part, polyvinyl acetal resin 3-5 part, γ-glycidyl ether oxygen propyl trimethoxy silicane 25-30 part, dodecyl dimethyl benzyl ammonium bromide 3-5 part, ethanol 20-30 part, water 550-600 part forms, first with ethanol by rosin europium resin dissolves, after adding water 550-600 part, add whole raw material and mix, at 85 ~ 95 DEG C, stir 20-30 minute, obtain product.
The present invention compared with prior art its beneficial effect is: have design science reasonable, and technique is simple, safe reliability, is easy to control, easy to operate, is applicable to scale operation, the advantages such as production cost is low.
Embodiment
Below in conjunction with embodiment, the invention will be further described, but embodiments of the present invention are not limited thereto.
All raw materials of the present invention can buy acquisition.
Embodiment 1
The preparation method of carboxylated imidozoline phosphate calcium carbonate activator of the present invention, it is characterized in that: by weight, its formula is by carboxylated imidozoline phosphate 5-8 part, rosin pentaerythritol ester europium resin 3-8 part, cocoanut fatty acid diethanolamide 25-30 part, sodium carbonate 5-8 part, sodium acrylate-4-vinylpridine multipolymer 3-5 part, Vanay 5-6 part, di-n-octyltin oxide 10--12 part, polyvinyl acetal resin 3-5 part, γ-glycidyl ether oxygen propyl trimethoxy silicane 25-30 part, dodecyl dimethyl benzyl ammonium bromide 3-5 part, ethanol 20-30 part, water 550-600 part forms, first with ethanol by rosin europium resin dissolves, after adding water 550-600 part, add whole raw material and mix, at 85 ~ 95 DEG C, stir 20-30 minute, obtain product.
Embodiment 2
The preparation method of carboxylated imidozoline phosphate calcium carbonate activator of the present invention, it is characterized in that: by weight, its formula is by carboxylated imidozoline phosphate 5-8 part, rosin pentaerythritol ester europium resin 3 parts, cocoanut fatty acid diethanolamide 25 parts, 5 parts, sodium carbonate, sodium acrylate-4-vinylpridine multipolymer 3 parts, Vanay 5 parts, dioctyl tin 10 parts, polyvinyl acetal resin 3 parts, glycidyl ether oxygen propyl trimethoxy silicane 25 parts, ethanol 20-30 part, water 550-600 part forms; First with ethanol by rosin europium resin dissolves, after adding water 550-600 part, add whole raw material and mix, at 85 ~ 95 DEG C, stir 20-30 minute, obtain product.
Embodiment 3
The preparation method of carboxylated imidozoline phosphate calcium carbonate activator of the present invention, it is characterized in that: by weight, its formula is by carboxylated imidozoline phosphate 5-8 part, rosin pentaerythritol ester europium resin 8 parts, cocoanut fatty acid diethanolamide 30 parts, 8 parts, sodium carbonate, sodium acrylate-4-vinylpridine multipolymer 5 parts, Vanay 6 parts, dioctyl tin 12 parts, polyvinyl acetal resin 5 parts, glycidyl ether oxygen propyl trimethoxy silicane 30 parts, dodecyl dimethyl benzyl ammonium bromide 3-5 part, ethanol 20-30 part, water 550-600 part forms, first with ethanol by rosin europium resin dissolves, after adding water 550-600 part, add whole raw material and mix, at 85 ~ 95 DEG C, stir 20-30 minute, obtain product.
Embodiment 4
The preparation method of carboxylated imidozoline phosphate calcium carbonate activator of the present invention, it is characterized in that: by weight, its formula is by carboxylated imidozoline phosphate 5-8 part, rosin pentaerythritol ester europium resin 3 parts, cocoanut fatty acid diethanolamide 30 parts, 5 parts, sodium carbonate, sodium acrylate-4-vinylpridine multipolymer 5 parts, Vanay 5 parts, dioctyl tin 12 parts, polyvinyl acetal resin 3 parts, glycidyl ether oxygen propyl trimethoxy silicane 25 parts, dodecyl dimethyl benzyl ammonium bromide 3-5 part, ethanol 20-30 part, water 550-600 part forms, first with ethanol by rosin europium resin dissolves, after adding water 550-600 part, add whole raw material and mix, at 85 ~ 95 DEG C, stir 20-30 minute, obtain product.
Product of the present invention, uses through production firm, and produce modified superfine water-ground limestone product, reaction effect is fine.
Part material illustrates:
Described rosin pentaerythritol ester europium resin, the method that can be preferably ZL201410078259.8 by the Chinese patent patent No. obtains.
γ-glycidyl ether oxygen propyl trimethoxy silicane
No. Cas: 2530-83-8
Molecular formula: C9H20O5Si molecular weight: 236.34
Another name: 3-(2,3-epoxy third oxygen) propyl trimethoxy silicane, 3-glycydoxy Trimethoxy silane
γ-glycidyl ether oxygen propyl trimethoxy silicane.

Claims (2)

1. a carboxylated imidozoline phosphate calcium carbonate activator, it is characterized in that: by weight, its formula is by carboxylated imidozoline phosphate 5-8 part, rosin pentaerythritol ester europium resin 3-8 part, cocoanut fatty acid diethanolamide 25-30 part, sodium carbonate 5-8 part, sodium acrylate-4-vinylpridine multipolymer 3-5 part, Vanay 5-6 part, di-n-octyltin oxide 10--12 part, polyvinyl acetal resin 3-5 part, γ-glycidyl ether oxygen propyl trimethoxy silicane 25-30 part, dodecyl dimethyl benzyl ammonium bromide 3-5 part, ethanol 20-30 part, water 550-600 part forms.
2. the preparation method of a carboxylated imidozoline phosphate calcium carbonate activator, it is characterized in that: by weight, its formula is by carboxylated imidozoline phosphate 5-8 part, rosin pentaerythritol ester europium resin 3-8 part, cocoanut fatty acid diethanolamide 25-30 part, sodium carbonate 5-8 part, sodium acrylate-4-vinylpridine multipolymer 3-5 part, Vanay 5-6 part, di-n-octyltin oxide 10--12 part, polyvinyl acetal resin 3-5 part, γ-glycidyl ether oxygen propyl trimethoxy silicane 25-30 part, dodecyl dimethyl benzyl ammonium bromide 3-5 part, ethanol 20-30 part, water 550-600 part forms, first with ethanol by rosin europium resin dissolves, after adding water 550-600 part, add whole raw material and mix, at 85 ~ 95 DEG C, stir 20-30 minute, obtain product.
CN201510755810.2A 2015-11-07 2015-11-07 Carboxylated imidozoline phosphate activator for calcium carbonate Pending CN105419396A (en)

Priority Applications (1)

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Application Number Priority Date Filing Date Title
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Publications (1)

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CN105419396A true CN105419396A (en) 2016-03-23

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Citations (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101883485A (en) * 2007-10-02 2010-11-10 世界矿物公司 Enhanced retention capabilities through methods comprising surface treatment of functional particulate carrier materials, and functional particulate carrier materials made therefrom
CN101987927A (en) * 2009-08-05 2011-03-23 任绍志 Method for preparing modified nano-silica from polysilane
CN102911441A (en) * 2012-09-18 2013-02-06 铜陵市铜都特种线缆厂 High-temperature-resistant moisture-proof mould-proof environment-friendly cable material and preparation method thereof
CN103045106A (en) * 2012-12-12 2013-04-17 滁州市鑫彩印务有限公司 Adhesive containing modified PVC (polyvinyl chloride) resin for packaging materials
CN103059721A (en) * 2012-12-18 2013-04-24 芜湖恒坤汽车部件有限公司 Metal surface silicane treating agent containing polyethylene glycol and preparing method thereof
CN103088327A (en) * 2012-12-18 2013-05-08 芜湖恒坤汽车部件有限公司 Metal surface silane treatment agent containing water-soluble phenolic resin and preparation method thereof
CN103102724A (en) * 2012-12-18 2013-05-15 芜湖恒坤汽车部件有限公司 Metal surface silane treating agent containing acrylic acid and preparation method of metal surface silane treating agent
CN103131374A (en) * 2013-03-21 2013-06-05 黑龙江省科学院石油化学研究院 Inorganic/organic nano particle compound modification epoxy resin adhesive and preparation method thereof
CN103173140A (en) * 2013-02-26 2013-06-26 安徽明珠颜料科技有限公司 Neoprene adhesive for woodworking
CN103820032A (en) * 2014-03-05 2014-05-28 张雅静 Preparation method of pentaerythrite colophony europium resin
CN103923593A (en) * 2014-04-16 2014-07-16 杭州之江有机硅化工有限公司 One-component silane-modified polyurethane sealant and preparation method thereof
CN104371376A (en) * 2014-10-31 2015-02-25 陈显鹏 Glycidol ether superfine calcium carbonate powder assistant
CN104403367A (en) * 2014-10-31 2015-03-11 廖文成 Calcium carbonate gamma-aminopropyl triethoxy silane modifier
CN104403266A (en) * 2014-10-31 2015-03-11 廖文成 Amino resin-containing calcium carbonate powder modifier
CN104403246A (en) * 2014-10-31 2015-03-11 廖文成 Ultrafine calcium carbonate powder acetal modifier
CN104479412A (en) * 2014-11-26 2015-04-01 甘振辉 Preparation method of polydimethyl siloxane ground limestone superfine powder

Patent Citations (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101883485A (en) * 2007-10-02 2010-11-10 世界矿物公司 Enhanced retention capabilities through methods comprising surface treatment of functional particulate carrier materials, and functional particulate carrier materials made therefrom
CN101987927A (en) * 2009-08-05 2011-03-23 任绍志 Method for preparing modified nano-silica from polysilane
CN102911441A (en) * 2012-09-18 2013-02-06 铜陵市铜都特种线缆厂 High-temperature-resistant moisture-proof mould-proof environment-friendly cable material and preparation method thereof
CN103045106A (en) * 2012-12-12 2013-04-17 滁州市鑫彩印务有限公司 Adhesive containing modified PVC (polyvinyl chloride) resin for packaging materials
CN103059721A (en) * 2012-12-18 2013-04-24 芜湖恒坤汽车部件有限公司 Metal surface silicane treating agent containing polyethylene glycol and preparing method thereof
CN103088327A (en) * 2012-12-18 2013-05-08 芜湖恒坤汽车部件有限公司 Metal surface silane treatment agent containing water-soluble phenolic resin and preparation method thereof
CN103102724A (en) * 2012-12-18 2013-05-15 芜湖恒坤汽车部件有限公司 Metal surface silane treating agent containing acrylic acid and preparation method of metal surface silane treating agent
CN103173140A (en) * 2013-02-26 2013-06-26 安徽明珠颜料科技有限公司 Neoprene adhesive for woodworking
CN103131374A (en) * 2013-03-21 2013-06-05 黑龙江省科学院石油化学研究院 Inorganic/organic nano particle compound modification epoxy resin adhesive and preparation method thereof
CN103820032A (en) * 2014-03-05 2014-05-28 张雅静 Preparation method of pentaerythrite colophony europium resin
CN103923593A (en) * 2014-04-16 2014-07-16 杭州之江有机硅化工有限公司 One-component silane-modified polyurethane sealant and preparation method thereof
CN104371376A (en) * 2014-10-31 2015-02-25 陈显鹏 Glycidol ether superfine calcium carbonate powder assistant
CN104403367A (en) * 2014-10-31 2015-03-11 廖文成 Calcium carbonate gamma-aminopropyl triethoxy silane modifier
CN104403266A (en) * 2014-10-31 2015-03-11 廖文成 Amino resin-containing calcium carbonate powder modifier
CN104403246A (en) * 2014-10-31 2015-03-11 廖文成 Ultrafine calcium carbonate powder acetal modifier
CN104479412A (en) * 2014-11-26 2015-04-01 甘振辉 Preparation method of polydimethyl siloxane ground limestone superfine powder

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