CN105362160B - A kind of clay mask and preparation method thereof containing Chinese herbal medicine extract - Google Patents
A kind of clay mask and preparation method thereof containing Chinese herbal medicine extract Download PDFInfo
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Abstract
The clay mask and preparation method thereof containing Chinese herbal medicine extract that the invention discloses a kind of, it is desirable to provide a kind of easy to apply containing natural products component, anti-inflammatory, antiallergy and the clay mask with white-skinned face function；Its each component content are as follows: cetostearyl alcohol 1.36~2.04%, stearine/PEG-100 stearate 3.36~5.04%, polysorbate -60 1.36~2.04%, zinc oxide 2~3%, green stone mud 5.76~8.04%, titanium dioxide 0.64~0.96%, kaolin 5.76~8.04%, allantoin 0.13~0.25%, EDETATE SODIUM 0.06~0.1%, propylene glycol 3.5~5.5%, hydroxyethyl cellulose 0.2~0.3%, glycerol 2.5~5.0%, montmorillonite 3.0~4.6%, aluminum magnesium silicate 0.6~1.0%, PEG-12 dimethyl silicone polymer 1.36~2.04%, olive oil PEG-7 esters 0.6~1 .0%, reed fragrant plant oil 2~3%, lactic acid 0.06~0.1%, stephania tetrandra extract 0.5~2.5%, Purslane extract 1~3%, menthol 0.02~0.04%, Pelargonium sunflower oil 0.10~0.15%, preservative 0.1~0.9%, water are surplus.
Description
Technical field
The invention discloses a kind of clay masks, specifically, being a kind of clay mask containing Chinese herbal medicine extract, the present invention is also
It is related to the preparation method of the clay mask powder；Belong to technical field of skin care.
Background technique
In recent years, facial mask is gradually from both effectiveness product to the product transformation that disappears fastly, while the type of facial mask is also being constantly updated,
Clay mask is favored by the majority of consumers as a kind of emerging facial mask dosage form.However, current clay mask on the market still can not
Avoid there are segmental defect, such as can not be successfully and push open in use, or even will appear and rolled into a ball a phenomenon, many consumers couple
This is very annoyed, therefore, solves problems and is of great significance.
As cosmetics develop to natural, safe, scientific direction, design and develop the clay mask containing natural component be must
Right trend.Many natural materials have oil-control, moisturizing, releive and other effects, and sensitization is small, this will change for clay mask formula
Into offer direction.Clay mask containing natural component will increasingly be liked by people, exploitation of the natural component in clay mask
It has broad application prospects in design.
Summary of the invention
In view of the above-mentioned problems, the purpose of the present invention is to provide one kind containing natural products component is easy to apply, anti-inflammatory, antiallergy
And the clay mask with white-skinned face function, the invention further relates to the preparation methods of the mud film powder.
In order to solve the above technical problems, first technical solution provided by the invention is such that
A kind of clay mask containing Chinese herbal medicine extract is calculated by gross mass 100%, including following each components, each group sub-prime
Measure percentage such as:
Preferably, the above-mentioned clay mask containing Chinese herbal medicine extract is calculated by gross mass 100%, and each component and content are such as
Under:
Preferably, the above-mentioned clay mask containing Chinese herbal medicine extract, the preservative be Phenoxyethanol, Chlorphenesin,
One of dehydroactic acid sodium, ethohexadiol, Sensiva SC50, dybenal/Phenoxyethanol or any combination.
Latter solution provided by the invention is such that
1) each component is weighed；
2) dissolution is added into 1/5~1/4 vol propylene glycol in the weighed hydroxyethyl cellulose of step 1) and is denoted as prefabrication
1；
3) by the weighed zinc oxide of step 1), chlorite, titanium dioxide, glycerol, the remaining propylene glycol of step 2) with 1/4~
1/2 volume of water after mixing evenly, crosses colloid mill and is denoted as prefabrication 2；
4) the weighed menthol of step 1) is added in Pelargonium sunflower oil, stirs evenly and is denoted as prefabrication 3；
5) the remaining water of step 4) is added in emulsion pot, then emulsion pot is added in kaolin, montmorillonite, aluminum magnesium silicate,
Homogeneous stirs evenly；
6) by the prefabrication 1 of step 1) preparation, EDETATE SODIUM, allantoin, PEG-12 dimethyl silicone polymer, olive oil
PEG-7 esters, reed fragrant plant oil, Purslane extract are added into the emulsion pot of step 5) and stir evenly, and add prefabrication 2, stir
It mixes and is heated to 83~87 DEG C, keep the temperature 10~15min；
7) by cetostearyl alcohol, oily phase pot is added in stearine/PEG-100 stearate, polysorbate -60,
80~85 DEG C are heated with stirring to, 10~15min is kept the temperature；
8) oil phase thing prepared by step 7) is crossed 200 mesh suction emulsion pot to vacuumize at 83~88 DEG C, is kept the temperature after homogeneous
30min；Lactic acid, stephania tetrandra extract, preservative, prefabrication 3 is added when being cooled to 50~55 DEG C, vacuumizes, homogeneous, stirring 10
~15min discharges after detection is qualified.
The prior art is compared, and technical solution provided by the invention has following technological merit:
1) clay mask provided by the invention, which easily pushes away, smears, and skin sense is soft, formula select reed fragrant plant oil, olive oil PEG-7 esters,
The components such as PEG-12 dimethyl silicone polymer have good lubricant effect, and the particles such as base-material, filler can be uniformly dispersed；Glycerol
Mud particle can further be uniformly dispersed by stearate/PEG-100 stearate, polysorbate -60, increase particle in body
Suspension stability in system keeps clay mask more stable；
2) using green stone mud, montmorillonite, kaolin as clay mask base-material in technical solution provided by the invention, have excellent
The effect of cleaning and absorption；Addition allantoin can promote chrotoplast generation, anti-inflammatory of releiving；Stephania tetrandra extract, horse are added simultaneously
Bitterroot extracting solution has good anti-inflammatory, antiallergy, acne-removing；There is Pelargonium sunflower oil whitening, balance skin to secrete
Effect.
3) powder of base-material is first stirred grinding in preparation method provided by the invention, disperses powder in advance
It is even, it is ensured that powder is uniformly dispersed in finished product, makes it have more preferably to push away and smears effect.
Specific embodiment
With reference to embodiment, claim of the invention is described in further detail, but do not constituted pair
Any restrictions of the invention, the modification of anyone limited times made in the claims in the present invention protection scope, still in this hair
Within bright claims.
Embodiment 1
A kind of clay mask containing Chinese herbal medicine extract provided by the invention is calculated by gross mass 100g, contains following mass numbers
Component: cetostearyl alcohol 2.04g, stearine/PEG-100 stearate 3.36g, polysorbate -602.04g, oxygen
Change zinc 2g, green stone mud 8.04g, titanium dioxide 0.64g, kaolin 8.04g, allantoin 0.13g, EDETATE SODIUM 0.1g, propylene glycol
3.5g, hydroxyethyl cellulose 0.3g, glycerol 2.5g, montmorillonite 4.6g, aluminum magnesium silicate 0.6g, PEG-12 dimethyl silicone polymer
2.04g, olive oil PEG-7 esters 0.6g, reed fragrant plant oil 3g, lactic acid 0.06g, stephania tetrandra extract 2.5g, Purslane extract 1g,
Menthol 0.02g, Pelargonium sunflower oil 0.15g, Chlorphenesin 0.2g, surplus is deionized water.
Embodiment 2
Clay mask of the another kind containing Chinese herbal medicine extract provided by the invention each component and is contained by gross mass 100g calculating
It measures as follows: cetostearyl alcohol 1.36g, stearine/PEG-100 stearate 5.04g, polysorbate -601.36g,
Zinc oxide 3g, green stone mud 5.76g, titanium dioxide 0.96g, kaolin 5.76g, allantoin 0.25g, EDETATE SODIUM 0.06g, the third two
Alcohol 5.5g, hydroxyethyl cellulose 0.2g, glycerol 5.0g, montmorillonite 3.0g, aluminum magnesium silicate 1.0g, PEG-12 dimethyl silicone polymer
1.36g, olive oil PEG-7 esters 1.0g, reed fragrant plant oil 2g, lactic acid 0.1g, stephania tetrandra extract 0.5g, Purslane extract 3g,
Menthol 0.04g, Pelargonium sunflower oil 0.10g, Sensiva SC50 0.3g, surplus is deionized water.
Embodiment 3
Clay mask of the another kind containing Chinese herbal medicine extract provided by the invention each component and is contained by gross mass 100g calculating
It measures as follows: cetostearyl alcohol 1.8g, stearine/PEG-100 stearate 3.8g, polysorbate -601.8g, oxidation
Zinc 2.2g, green stone mud 7.5g, titanium dioxide 0.7g, kaolin 7.5g, allantoin 0.18g, EDETATE SODIUM 0.09g, propylene glycol 4g,
Hydroxyethyl cellulose 0.28g, glycerol 3.5g, montmorillonite 4.1g, aluminum magnesium silicate 0.7g, PEG-12 dimethyl silicone polymer 1.8g,
Olive oil PEG-7 esters 0.7g, reed fragrant plant oil .8g, lactic acid 0.07g, stephania tetrandra extract 2g, Purslane extract 1.5g, peppermint
Alcohol 0.04g, Pelargonium sunflower oil 0.10g, dehydroactic acid sodium 0.3g, surplus is deionized water.
Embodiment 4
Clay mask of the another kind containing Chinese herbal medicine extract provided by the invention, is calculated by gross mass 100g, contains following quality
Array point: cetostearyl alcohol 1.5g, stearine/PEG-100 stearate 4.5g, polysorbate -601.5g, oxidation
Zinc 2.8g, green stone mud 6.5g, titanium dioxide 0.8g, kaolin 6.5g, allantoin 0.20g, EDETATE SODIUM 0.07g, propylene glycol 5g,
Hydroxyethyl cellulose 0.22g, glycerol 4.5g, montmorillonite 3.5g, aluminum magnesium silicate 0.9g, PEG-12 dimethyl silicone polymer 1.5g,
Olive oil PEG-7 esters 0.8g, reed fragrant plant oil 2.2g, lactic acid 0.09g, stephania tetrandra extract 1g, Purslane extract 2.5g, peppermint
Alcohol 0.02g, Pelargonium sunflower oil 0.15g, Phenoxyethanol 0.4g, Sensiva SC50 0.2g, surplus is deionized water.
Embodiment 5
Clay mask of the another kind containing Chinese herbal medicine extract provided by the invention, is calculated by gross mass 100g, contains following quality
Array point: cetostearyl alcohol 1.7g, stearine/PEG-100 stearate 4.2g, polysorbate -601.7g, oxidation
Zinc 2.5g, green stone mud 7.2g, titanium dioxide 0.8g, kaolin 7.2g, allantoin 0.17g, EDETATE SODIUM 0.08g, propylene glycol
4.6g, hydroxyethyl cellulose 0.25g, glycerol 4.2g, montmorillonite 3.8g, aluminum magnesium silicate 0.8g, PEG-12 dimethyl silicone polymer
1.7g, olive oil PEG-7 esters 0.84g, reed fragrant plant oil 2.5g, lactic acid 0.08g, stephania tetrandra extract 0.5g, Purslane extract
1.7g, menthol 0.034g, Pelargonium sunflower oil 0.13g, Phenoxyethanol 0.7g, surplus is deionized water.
Any clay mask containing Chinese herbal medicine extract in embodiment 1 to 5, preparation method successively include following steps
It is rapid:
1) any one group of mass number weighs each component in embodiment 1 to 5；
2) dissolution is added into 1/5~1/4 vol propylene glycol in the weighed hydroxyethyl cellulose of step 1) and is denoted as prefabrication
1；
3) by the weighed zinc oxide of step 1), chlorite, titanium dioxide, glycerol, the remaining propylene glycol of step 2) with 1/4~
1/2 volume of water after mixing evenly, crosses colloid mill and is denoted as prefabrication 2；
4) the weighed menthol of step 1) is added in Pelargonium sunflower oil, stirs evenly and is denoted as prefabrication 3；
5) the remaining water of step 4) is added in emulsion pot, then emulsion pot is added in kaolin, montmorillonite, aluminum magnesium silicate,
Homogeneous stirs evenly；
6) by the prefabrication 1 of step 1) preparation, EDETATE SODIUM, allantoin, PEG-12 dimethyl silicone polymer, olive oil
PEG-7 esters, reed fragrant plant oil, Purslane extract are added into the emulsion pot of step 5) and stir evenly, and add prefabrication 2, stir
It mixes and is heated to 83~87 DEG C, keep the temperature 10~15min；
7) by cetostearyl alcohol, oily phase pot is added in stearine/PEG-100 stearate, polysorbate -60,
80~85 DEG C are heated with stirring to, 10~15min is kept the temperature；
8) oil phase thing prepared by step 7) is crossed 200 mesh suction emulsion pot to vacuumize at 83~88 DEG C, is kept the temperature after homogeneous
30min；Lactic acid, stephania tetrandra extract, preservative, prefabrication 3 is added when being cooled to 50~55 DEG C, vacuumizes, homogeneous, stirring 10
~15min discharges after detection is qualified.
Embodiment 6
Clay mask of the another kind containing Chinese herbal medicine extract provided by the invention each component and is contained by gross mass 100g calculating
It measures as follows: cetostearyl alcohol 1.8g, stearine/PEG-100 stearate 3.8g, polysorbate -601.8g, oxidation
Zinc 2.2g, green stone mud 7.5g, titanium dioxide 0.7g, kaolin 7.5g, allantoin 0.18g, EDETATE SODIUM 0.09g, propylene glycol 4g,
Hydroxyethyl cellulose 0.28g, glycerol 3.5g, montmorillonite 4.1g, aluminum magnesium silicate 0.7g, PEG-12 dimethyl silicone polymer 1.8g,
Olive oil PEG-7 esters 0.7g, reed fragrant plant oil .8g, lactic acid 0.07g, stephania tetrandra extract 2g, Purslane extract 1.5g, gold thread
Prunus mume extract 1.5g, peony extract 1.5g, extract of cinnamomum cassia bark 1.5g, menthol 0.04g, Pelargonium sunflower oil 0.10g,
Dehydroactic acid sodium 0.3g, surplus are deionized water.
Embodiment 7
Clay mask of the another kind containing Chinese herbal medicine extract provided by the invention, is calculated by gross mass 100g, contains following quality
Array point: cetostearyl alcohol 1.5g, stearine/PEG-100 stearate 4.5g, polysorbate -601.5g, oxidation
Zinc 2.8g, green stone mud 6.5g, titanium dioxide 0.8g, kaolin 6.5g, allantoin 0.20g, EDETATE SODIUM 0.07g, propylene glycol 5g,
Hydroxyethyl cellulose 0.22g, glycerol 4.5g, montmorillonite 3.5g, aluminum magnesium silicate 0.9g, PEG-12 dimethyl silicone polymer 1.5g,
Olive oil PEG-7 esters 0.8g, reed fragrant plant oil 2.2g, lactic acid 0.09g, stephania tetrandra extract 1g, Purslane extract 2.5g, gold thread
Prunus mume extract 2.5g, peony extract 2.5g, extract of cinnamomum cassia bark 2.5g, menthol 0.02g, Pelargonium sunflower oil 0.15g,
Phenoxyethanol 0.4g, Sensiva SC50 0.2g, surplus are deionized water.
Embodiment 8
Clay mask of the another kind containing Chinese herbal medicine extract provided by the invention, is calculated by gross mass 100g, contains following quality
Array point: cetostearyl alcohol 1.7g, stearine/PEG-100 stearate 4.2g, polysorbate -601.7g, oxidation
Zinc 2.5g, green stone mud 7.2g, titanium dioxide 0.8g, kaolin 7.2g, allantoin 0.17g, EDETATE SODIUM 0.08g, propylene glycol
4.6g, hydroxyethyl cellulose 0.25g, glycerol 4.2g, montmorillonite 3.8g, aluminum magnesium silicate 0.8g, PEG-12 dimethyl silicone polymer
1.7g, olive oil PEG-7 esters 0.84g, reed fragrant plant oil 2.5g, lactic acid 0.08g, stephania tetrandra extract 0.5g, Purslane extract
1.7g, hamamelis extract 1.7g, peony extract 1.7g, extract of cinnamomum cassia bark 1.7g, menthol 0.034g, Pelargonium roseum
Caul-fat 0.13g, Phenoxyethanol 0.7g, surplus are deionized water.
Wherein:
Stephania tetrandra extract the preparation method is as follows:
10g Fourstamen Stephania Root root medicine materical crude slice is taken, is placed in flask, 70wt% ethanol solution 100g is added, after impregnating 0.5h, at 80 DEG C
Refluxing extraction 1h under water bath condition, extraction fluid, the dregs of a decoction continuously add 70wt% ethanol solution 100g, flow back and mention at 80 DEG C
1h is taken, secondary raffinate is obtained, merges two batches extracting solution.Fourstamen Stephania Root extracting solution is filtered using Buchner funnel, is obtained clear
Clear stephania tetrandra extract.
Purslane extract the preparation method is as follows:
10g purslane medicine materical crude slice is taken, is placed in flask, 60wt% ethanol solution 100g is added, after impregnating 0.5h, in 70 DEG C of water
Refluxing extraction 1h under the conditions of bath, extraction fluid, the dregs of a decoction continuously add 60wt% ethanol solution 100g, the refluxing extraction at 70 DEG C
1h obtains secondary raffinate, merges two batches extracting solution.Purslane extract is filtered using Buchner funnel, is clarified
Liquid Purslane extract.
The preparation formula of hazel extract is as follows:
10g witch hazel is taken, is placed in flask, water 100g is added, after impregnating 0.5h, the refluxing extraction under 60 DEG C of water bath conditions
1h, extraction fluid, the dregs of a decoction continuously add water 100g, the refluxing extraction 1h at 60 DEG C, obtain secondary raffinate, merge two batches and mention
Take liquid.Hazel extract is filtered using Buchner funnel, obtains clarification hazel extract.
Extract of cinnamomum cassia bark the preparation method is as follows:
10g cassia medicine materical crude slice is taken, is placed in flask, 70wt% ethanol solution 100g is added, after impregnating 0.5h, in 80 DEG C of water
Refluxing extraction 1h under the conditions of bath, extraction fluid, the dregs of a decoction continuously add 70wt% ethanol solution 100g, the refluxing extraction at 80 DEG C
1h obtains secondary raffinate, merges two batches extracting solution.Cassia extracting solution is filtered using Buchner funnel, is clarified
Extract of cinnamomum cassia bark.
Peony extract the preparation method is as follows:
10g Chinese herbaceous peony medicine materical crude slice is taken, is placed in flask, 70wt% ethanol solution 100g is added, after impregnating 0.5h, in 80 DEG C of water-baths
Under the conditions of refluxing extraction 1h, extraction fluid, the dregs of a decoction continuously add 70wt% ethanol solution 100g, the refluxing extraction at 80 DEG C
1h obtains secondary raffinate, merges two batches extracting solution.Chinese herbaceous peony extracting solution is filtered using Buchner funnel, obtains clarification Chinese herbaceous peony
Medicament extract.
In order to illustrate effect of the invention, clay mask provided by the invention and conventional clay mask friction in the market is given below
Coefficient test data:
The coefficient of friction data of 1 each sample of table
Note: sample 1 is clay mask of the invention, and sample 2 is the clay mask of certain famous brand name on the market, and sample 3 is market
The clay mask of upper another famous brand name.
Since the coefficient of friction of clay mask is smaller, smooth degree is higher, and the easier smearing of sample is pushed open.As shown in Table 1,
The size of dynamic friction coefficient are as follows: 1 < sample of sample, 3 < sample 2, therefore, the smooth degree of sample 1 are all higher than sample 2 and sample 3,
That is clay mask of the invention is easier to smear and push open.
Claims (4)
1. a kind of clay mask containing Chinese herbal medicine extract, which is characterized in that calculated by gross mass 100%, each component quality percentage
Than as described below:
Successively include the following steps obtained:
1) each component is weighed；
2) dissolution is added into 1/5~1/4 vol propylene glycol in the weighed hydroxyethyl cellulose of step 1) and is denoted as prefabrication 1；
3) by the weighed zinc oxide of step 1), chlorite, titanium dioxide, glycerol, the remaining propylene glycol of step 2) and 1/4~1/2
Volume of water after mixing evenly, crosses colloid mill and is denoted as prefabrication 2；
4) the weighed menthol of step 1) is added in Pelargonium sunflower oil, stirs evenly and is denoted as prefabrication 3；
5) the remaining water of step 4) is added in emulsion pot, then kaolin, montmorillonite, aluminum magnesium silicate is added emulsion pot, homogeneous,
It stirs evenly；
6) by the prefabrication 1 of step 1) preparation, EDETATE SODIUM, allantoin, PEG-12 dimethyl silicone polymer, olive oil PEG-7
Esters, reed fragrant plant oil, Purslane extract are added into the emulsion pot of step 5) and stir evenly, and add prefabrication 2, agitating and heating
To 83~87 DEG C, 10~15min is kept the temperature；
7) by cetostearyl alcohol, stearine/PEG-100 stearate, the oily phase pot of the addition of polysorbate -60, stirring
80~85 DEG C are heated to, 10~15min is kept the temperature；
8) oil phase thing prepared by step 7) is crossed 200 mesh suction emulsion pot to vacuumize at 83~88 DEG C, is kept the temperature after homogeneous
30min；Lactic acid, stephania tetrandra extract, preservative, prefabrication 3 is added when being cooled to 50~55 DEG C, vacuumizes, homogeneous, stirring 10
~15min discharges after detection is qualified.
2. a kind of clay mask containing Chinese herbal medicine extract, which is characterized in that calculated by gross mass 100%, each component and content are such as
It is lower described:
3. the clay mask according to claim 1 or 2 containing Chinese herbal medicine extract, which is characterized in that the preservative
For Phenoxyethanol.
4. the method for preparing the clay mask described in claim 1 containing Chinese herbal medicine extract, which is characterized in that successively include following
Step:
1) mass ratio according to claim 1 weighs each component；
2) dissolution is added into 1/5~1/4 vol propylene glycol in the weighed hydroxyethyl cellulose of step 1) and is denoted as prefabrication 1；
3) by the weighed zinc oxide of step 1), chlorite, titanium dioxide, glycerol, the remaining propylene glycol of step 2) and 1/4~1/2
Volume of water after mixing evenly, crosses colloid mill and is denoted as prefabrication 2；
4) the weighed menthol of step 1) is added in Pelargonium sunflower oil, stirs evenly and is denoted as prefabrication 3；
5) the remaining water of step 4) is added in emulsion pot, then kaolin, montmorillonite, aluminum magnesium silicate is added emulsion pot, homogeneous,
It stirs evenly；
6) by the prefabrication 1 of step 1) preparation, EDETATE SODIUM, allantoin, PEG-12 dimethyl silicone polymer, olive oil PEG-7
Esters, reed fragrant plant oil, Purslane extract are added into the emulsion pot of step 5) and stir evenly, and add prefabrication 2, agitating and heating
To 83~87 DEG C, 10~15min is kept the temperature；
7) by cetostearyl alcohol, stearine/PEG-100 stearate, the oily phase pot of the addition of polysorbate -60, stirring
80~85 DEG C are heated to, 10~15min is kept the temperature；
8) oil phase thing prepared by step 7) is crossed 200 mesh suction emulsion pot to vacuumize at 83~88 DEG C, is kept the temperature after homogeneous
30min；Lactic acid, stephania tetrandra extract, preservative, prefabrication 3 is added when being cooled to 50~55 DEG C, vacuumizes, homogeneous, stirring 10
~15min discharges after detection is qualified.
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| CN105997629A (en) * | 2016-05-24 | 2016-10-12 | 广州南雪药业有限公司 | Acne treatment cream and preparation method thereof |
| ES2685002B1 (en) * | 2017-03-31 | 2019-07-17 | Itf Res Pharma Slu | Lubricant formulations |
| CN107811885A (en) * | 2017-11-08 | 2018-03-20 | 诺斯贝尔化妆品股份有限公司 | A kind of cleaning pack containing renewable frosted composition |
| CN109646707A (en) * | 2018-12-14 | 2019-04-19 | 广州润虹医药科技股份有限公司 | A kind of rapid hemostatic material and preparation method thereof |
| CN110960458A (en) * | 2019-12-18 | 2020-04-07 | 苏州东方之宝生物药业有限公司 | Moisturizing essence emulsion and preparation method thereof |
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| CN104116701A (en) * | 2014-06-26 | 2014-10-29 | 张少维 | Herbal clay facial mask |
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