CN105353061B - 用于食品中手性农药残留检测的气相色谱柱的制作方法 - Google Patents
用于食品中手性农药残留检测的气相色谱柱的制作方法 Download PDFInfo
- Publication number
- CN105353061B CN105353061B CN201510641699.4A CN201510641699A CN105353061B CN 105353061 B CN105353061 B CN 105353061B CN 201510641699 A CN201510641699 A CN 201510641699A CN 105353061 B CN105353061 B CN 105353061B
- Authority
- CN
- China
- Prior art keywords
- cyclodextrin
- chromatographic column
- gas chromatographic
- reaction
- food
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/60—Construction of the column
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N2030/022—Column chromatography characterised by the kind of separation mechanism
- G01N2030/025—Gas chromatography
Abstract
Description
Claims (1)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201510641699.4A CN105353061B (zh) | 2015-09-30 | 2015-09-30 | 用于食品中手性农药残留检测的气相色谱柱的制作方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201510641699.4A CN105353061B (zh) | 2015-09-30 | 2015-09-30 | 用于食品中手性农药残留检测的气相色谱柱的制作方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN105353061A CN105353061A (zh) | 2016-02-24 |
CN105353061B true CN105353061B (zh) | 2017-07-14 |
Family
ID=55329065
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201510641699.4A Active CN105353061B (zh) | 2015-09-30 | 2015-09-30 | 用于食品中手性农药残留检测的气相色谱柱的制作方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN105353061B (zh) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108398506B (zh) * | 2018-04-11 | 2020-02-04 | 国家烟草质量监督检验中心 | 一种超高效合相色谱-串联质谱技术拆分、测定手性农药喹禾灵和吡氟禾草灵对映体的方法 |
Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE4317139A1 (de) * | 1993-05-21 | 1994-11-24 | Volker Prof Dr Schurig | Verfahren zur präparativen gaschromatographischen Enantiomerentrennung von Inhalationsanästhektika (Enfluran) an Cyclodextrinderivaten in Polysiloxanlösung |
JP2005031091A (ja) * | 2004-08-05 | 2005-02-03 | T Hasegawa Co Ltd | ガスクロマトグラフィー用光学活性カラム充填剤 |
JP2005298574A (ja) * | 2004-04-07 | 2005-10-27 | T Hasegawa Co Ltd | 置換シクロデキストリンおよびその製法 |
JP2005344034A (ja) * | 2004-06-04 | 2005-12-15 | National Institute Of Advanced Industrial & Technology | シクロデキストリンを結合させた吸着材 |
CN101015789A (zh) * | 2007-01-05 | 2007-08-15 | 中国农业大学 | 新型β-环糊精衍生物毛细管气相色谱手性固定相及其制备方法 |
CN102649049A (zh) * | 2011-02-23 | 2012-08-29 | 中国农业科学院植物保护研究所 | 2,3-二-O-甲氧甲基-6-O-苄基-β-环糊精气相色谱手性固定相及其制备方法 |
CN102768250A (zh) * | 2012-07-23 | 2012-11-07 | 中国农业大学 | 毛细管气相色谱手性分离测定乳酸甲酯光学异构体的方法 |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20050106068A1 (en) * | 2003-11-18 | 2005-05-19 | Abdul Malik | Sol-gel dendron separation and extraction capillary column |
-
2015
- 2015-09-30 CN CN201510641699.4A patent/CN105353061B/zh active Active
Patent Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE4317139A1 (de) * | 1993-05-21 | 1994-11-24 | Volker Prof Dr Schurig | Verfahren zur präparativen gaschromatographischen Enantiomerentrennung von Inhalationsanästhektika (Enfluran) an Cyclodextrinderivaten in Polysiloxanlösung |
JP2005298574A (ja) * | 2004-04-07 | 2005-10-27 | T Hasegawa Co Ltd | 置換シクロデキストリンおよびその製法 |
JP2005344034A (ja) * | 2004-06-04 | 2005-12-15 | National Institute Of Advanced Industrial & Technology | シクロデキストリンを結合させた吸着材 |
JP2005031091A (ja) * | 2004-08-05 | 2005-02-03 | T Hasegawa Co Ltd | ガスクロマトグラフィー用光学活性カラム充填剤 |
CN101015789A (zh) * | 2007-01-05 | 2007-08-15 | 中国农业大学 | 新型β-环糊精衍生物毛细管气相色谱手性固定相及其制备方法 |
CN102649049A (zh) * | 2011-02-23 | 2012-08-29 | 中国农业科学院植物保护研究所 | 2,3-二-O-甲氧甲基-6-O-苄基-β-环糊精气相色谱手性固定相及其制备方法 |
CN102768250A (zh) * | 2012-07-23 | 2012-11-07 | 中国农业大学 | 毛细管气相色谱手性分离测定乳酸甲酯光学异构体的方法 |
Non-Patent Citations (5)
Title |
---|
Developments in stationary phase technology for gas chromatography;Jaap de Zeeuw 等;《TrAC Trends in Analytical Chemistry》;20020910;第21卷(第9-10期);594–607 * |
Recent development of cyclodextrin chiral stationary phases and their applications in chromatography;Xiao Yin 等;《Journal of Chromatography A》;20120824;第1269卷;52-68 * |
七(2,3,6-三-O-甲氧甲基)-β-环糊精的合成及其在气相色谱分离中的应用;尹明明 等;《色谱》;20110131;第29卷(第1期);91-94 * |
吴秀红 等.溶胶-凝胶法制备2,6-二丁基-β-环糊精毛细管柱用于气相色谱.《理化检验》.2010,第46卷(第10期),1135-1137,1140. * |
环糊精衍生物在手性农药气相色谱分离中的应用;朱小波 等;《现代农药》;20090630;第8卷(第3期);5-10 * |
Also Published As
Publication number | Publication date |
---|---|
CN105353061A (zh) | 2016-02-24 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN104854135B (zh) | 聚α-1,3-葡聚糖醚的制备 | |
CN105241983B (zh) | 一种用于食品中农药残留检测的色谱柱 | |
Raileanu et al. | Sol-gel materials with pesticide delivery properties | |
CN102416313B (zh) | 双酚a伪模板分子印迹搅拌棒及其制备方法 | |
CN107469653A (zh) | 一种富集和分离诺氟沙星的分子印迹复合膜的合成方法 | |
CN104262496B (zh) | 一种键合直链淀粉衍生物的手性固定相及其制备方法 | |
CN104028007A (zh) | 一种咪唑离子液体毛细管整体柱及其制备和应用 | |
CN105353061B (zh) | 用于食品中手性农药残留检测的气相色谱柱的制作方法 | |
CN106243352B (zh) | 一种聚苯基三唑甲酸酯及其制备方法与应用 | |
CN104689807A (zh) | 咪唑双阳离子液体亲水作用色谱固定相及其制备和应用 | |
CN103706341B (zh) | 离子液体键合聚硅氧烷固定相及其制备方法 | |
CN106914227A (zh) | 新烟碱类农药荧光分子印迹聚合物微球的制备方法和性能评价方法 | |
CN106478980A (zh) | 基于巯基-环氧点击聚合反应的杂化多孔整体材料的制备方法 | |
CN106975522A (zh) | 一种磷钼钨杂多酸的制备及其在催化烯烃环氧化上的应用 | |
CN104910339B (zh) | 用于检测莱克多巴胺的磁性分子印迹聚离子液体及其制备方法和用途 | |
CN102527350A (zh) | 双酚a伪模板分子印迹搅拌棒及其制备方法 | |
CN105289523A (zh) | β-环糊精-氧化石墨烯-硅藻土复合材料的制备方法与应用 | |
CN105949472B (zh) | 一种苯二甲酰乙二胺衍生化β-环糊精键合硅胶及其用途 | |
CN104437438B (zh) | 树脂表面改性色谱填料及其制备方法和固相萃取柱 | |
CN109705273A (zh) | 一种弱酸性阳离子色谱柱填料的制备方法 | |
CN101497035B (zh) | 取代脲类农药分子印迹固相萃取小柱的制备方法 | |
CN103193898A (zh) | L-苯丙氨酸衍生β-环糊精键合硅胶的合成及其对丙氨酸对映体的分离应用 | |
CN102382074A (zh) | 二元酚型手性和外消旋苯并噁嗪及其制备方法 | |
CN107266627B (zh) | 一种可识别赤藓红的核-壳型分子印迹聚合物及制备方法 | |
CN101152624B (zh) | 一种醇羟基亲水色谱固定相及其制备方法 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
CB03 | Change of inventor or designer information |
Inventor after: Zhao Linping Inventor after: Su Yongheng Inventor after: Li Mengyu Inventor after: Jia Songtao Inventor after: Wang Jimei Inventor after: Kang Xuemei Inventor after: Li Xiaomin Inventor before: Zhao Linping |
|
CB03 | Change of inventor or designer information | ||
TA01 | Transfer of patent application right |
Effective date of registration: 20170613 Address after: 9, building 450000, building 1, National University Science Park, 11 Zhengzhou Road, hi tech Development Zone, Henan, China Applicant after: ZHONGBIAO TESTING HENAN SERVICE LTD. Applicant after: Henan Centers for Disease Control and Prevention Address before: 450000 science Avenue, Henan, Zhengzhou, No. 100 Applicant before: Zhao Linping |
|
TA01 | Transfer of patent application right | ||
GR01 | Patent grant | ||
GR01 | Patent grant |