CN105341361A - Nanoscale liquid compound premixed feed and production technology thereof - Google Patents
Nanoscale liquid compound premixed feed and production technology thereof Download PDFInfo
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- CN105341361A CN105341361A CN201510937733.2A CN201510937733A CN105341361A CN 105341361 A CN105341361 A CN 105341361A CN 201510937733 A CN201510937733 A CN 201510937733A CN 105341361 A CN105341361 A CN 105341361A
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- premixed feed
- liquid compound
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Abstract
The invention relates to nanoscale liquid compound premixed feed and a production technology of the nanoscale liquid compound premixed feed. The nanoscale liquid compound premixed feed is prepared from the following raw materials in parts by weight: 800 to 1.00*1,030,000 IU (International Unit)/kg of vitamin A acetate, 3,500 to 8,000,000 IU/kg of vitamin D, more than or equal to 2.0*103 mg/kg of dl-alpha-tocopherol acetate, more than or equal to 250 mg/kg of 2-methylnaphthoquinone, more than or equal to 500 mg/kg of thiamine hydrochloride, more than or equal to 400 mg/kg of riboflavin, more than or equal to 1.0*103 mg/kg of pyridoxine hydrochloride, more than or equal to 2.0*103 mg/kg of nicotinamide, more than or equal to 1.0*103 mg/kg of D-calcium pantothenate, more than or equal to 120 mg/kg of nicotinic acid, more than or equal to 10mg/kg of folic acid and the like. The nanoscale liquid compound premixed feed disclosed by the invention has the advantages that the nutritive value is high, the nanoscale liquid compound premixed feed is in a liquid state and can be easily absorbed by animals, the production technology is simple, the operation is convenient, the produced mixed feed is uniform, and the quality is high.
Description
Technical field
The present invention relates to a kind of premixed feed, be specifically related to the liquid compound premixed feed of a kind of nanoscale and production technology thereof.
Background technology
Premixed feed refers to the mixture stirred with carrier or diluent by one or more additive raw material (or monomer), also known as additive premix or premix, object is that the raw material being conducive to trace is dispersed in a large amount of mixed feeds, and premixed feed can not Direct-fed animal.
Premixed feed can be considered the core of mixed feed, because its trace active component contained is often the decisive factor of mixed feed feeding effect.
1. individual event premixed feed: it is by the multiple feed addictive of single additive raw material or one species and carrier or the formulated homogeneous mixture of diluent, mainly because certain or certain class additive use amount are considerably less, need elementary premix ability evenly be distributed in bulk feed, normal by single vitamin in production, single trace element (selenium, iodine, cobalt), multivitamin, various trace elements is first carried out elementary premix separately and is made individual event premix respectively.
2. compound premixed feed: be the homogeneous mixture various different types of feed addictive and carrier or mixing diluents made by formula and actual requirement.As trace element, the premix that vitamin and other composition mix.
Summary of the invention
The object of this invention is to provide the liquid compound premixed feed of a kind of nanoscale and production technology thereof, feed nutritive value is high, presents liquid state, is easily absorbed by animal, and production technology is simple, and easy to operate, the mixed fodder of production is even, quality is high.
The liquid compound premixed feed of a kind of nanoscale of the present invention, with weight parts, raw material is composed as follows:
Vitamin A acetic acid fat 800 ~ 1.00 × 10
3ten thousand IU/kg, vitamin D
3500 ~ 8,000,000 IU/kg, dl-alpha-tocopherol acetic acid fat>=2.0 × 10
3mg/kg, first be quinone>=250mg/kg, Tyiamine Hd>=500mg/kg, riboflavin>=400mg/kg, puridoxine hydrochloride>=1.0 × 10 how
3mg/kg, niacinamide>=2.0 × 10
3mg/kg, D-VB5 calcium>=1.0 × 10
3mg/kg, nicotinic acid>=120mg/kg, folic acid>=10mg/kg, Bio>=10mg/kg, L-AA>=3.0 × 10
3mg/kg, amino acid, manna oligosacchride 150 ~ 300mg/kg, chitosan oligosaccharide 1.50 × 10
3~ 3.00 × 10
3mg/kg; Wherein, amino acid accounts for the 2.0-5.0% of the liquid compound premixed feed quality of nanoscale.
The liquid compound premixed feed of a kind of nanoscale of the present invention, with weight parts, raw material composition is preferably as follows:
Vitamin A acetic acid fat 800 ~ 1.00 × 10
3ten thousand IU/kg, vitamin D
3500 ~ 8,000,000 IU/kg, dl-alpha-tocopherol acetic acid fat 2.0 × 10
3-5.0 × 10
3mg/kg, first how quinone 250-500mg/kg, Tyiamine Hd 600-800mg/kg, riboflavin 400-800mg/kg, puridoxine hydrochloride 1.0 × 10
3-3.0 × 10
3mg/kg, niacinamide 2.0 × 10
3-5.0 × 10
3mg/kg, D-VB5 calcium 2.0 × 10
3-5.0 × 10
3mg/kg, nicotinic acid 120-300mg/kg, folic acid 10-30mg/kg, Bio 20-50mg/kg, L-AA 3.0 × 10
3-5.0 × 10
3mg/kg, amino acid, manna oligosacchride 150 ~ 300mg/kg, chitosan oligosaccharide 1.50 × 10
3~ 3.00 × 10
3mg/kg; Wherein, amino acid accounts for the 2.0-5.0% of the liquid compound premixed feed quality of nanoscale.
Amino acid is DL-METHIONINE, L-threonine, glycine, glutamine.
L-Methionine, L-threonine, glycine, glutamine account for 0.8%, 0.1%, 0.3%, 0.4%, 0.5% of the liquid compound premixed feed quality of nanoscale respectively.
The production technology of the liquid compound premixed feed of described nanoscale, raw material is dissolved in organic solvent and purified water respectively and carries out dosing, filter with micropore filter element, filling, gland in 100,000 grades of toilets, then puts in storage after labeling, coding, packaging, inspection.
Filling disposable bottle, lid are temporary through de-outsourcing, sterilization: the disposable bottle that inner packing is qualified, lid, respectively with being put in pass-through box after 75% ethanolic solution wiping, imported into after between keeping in stand-by after ultraviolet radiation sterilization 3-6 minute.
Be 100,000 grades of control zones between disposable bottle is temporary, temperature 18-26 DEG C, humidity 30-65%, with general district pressure reduction>=10 handkerchief, 0.5 μm of airborne <3500000/m
3, 5 μm of airborne <20000/m
3.
Filling, gland: the container of splendid attire liquid should be airtight, the liquid prepared should be filling complete on the same day.
Before filling, gland first open drive machine all normal after, regulate loading amount with purified water douche can assembling system.
After filling, within every 25-40 minute, extract the quality condition of semi-finished product inspection clarity, loading amount, gland tight ness rating.
Liquid completed to filling from preparation in 5-7 hour.
Dosing: purified water or the organic solvent of 45-60L will be added in Agitation Tank, open Agitation Tank mixer, the raw material of precise recipe quantity, add in Agitation Tank, stirring 10-20 minute to dissolving completely, adding water, stir 8-15 minute, detect PH, content, the qualified rear filtration of color and luster, filtering liquid medicine packing after clarity passed examination.
Filter and adopt 0.45um miillpore filter.
Filling bottle is less than 24 hours standing time.
Organic solvent is ethanol.
Before weighing, the necessary each school zero of weigher, prescription must be checked, and the use amount of raw material should convert according to the actual content of raw material, water content factor, feeds intake by 100% of recipe quantity.
After drug solution preparing, carry out intermediates content, PH checks.
Must use the flow flush 10-20 minute of 250L/h before filtering liquid medicine, maximum working pressure (MWP) is 0.5Mpa, maximum differential pressure 0.3Mpa.
In filter process, as found, filter pressure declines suddenly or the rate of filtration is accelerated suddenly, then should retest the integrity of filter core.
After utensil used uses, be immersed in the bromogeramine solution of 0.5%, lower 5 minutes of necessary pressurize 0.05Mpa before filter uses.
In production process, surrounding environment is 100000 grades of clean areas, should meet 100000 grades of clean area levels necessitate.
Compared with prior art, the present invention has following beneficial effect:
The liquid compound premixed feed of nanoscale of the present invention and production technology thereof, feed nutritive value is high, presents liquid state, is easily absorbed by animal, and production technology is simple, and easy to operate, the mixed fodder of production is even, quality is high.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described further.
Embodiment 1
The liquid compound premixed feed of a kind of nanoscale described in the present embodiment, with weight parts, raw material is composed as follows:
Vitamin A acetic acid fat 1.00 × 10
3ten thousand IU/kg, vitamin D
38000000 IU/kg, dl-alpha-tocopherol acetic acid fat 5.0 × 10
3mg/kg, first how quinone 250mg/kg, Tyiamine Hd 800mg/kg, riboflavin 800mg/kg, puridoxine hydrochloride 1.0 × 10
3mg/kg, niacinamide 5.0 × 10
3mg/kg, D-VB5 calcium 5.0 × 10
3mg/kg, nicotinic acid 120mg/kg, folic acid 30mg/kg, Bio 20mg/kg, L-AA 5.0 × 10
3mg/kg, amino acid, manna oligosacchride 300mg/kg, chitosan oligosaccharide 1.50 × 10
3mg/kg; Amino acid is DL-METHIONINE, L-threonine, glycine, glutamine, and DL-METHIONINE, L-threonine, glycine, glutamine account for 0.8%, 0.1%, 0.3%, 0.4%, 0.5% of the liquid compound premixed feed quality of nanoscale respectively.
The production technology of the liquid compound premixed feed of described nanoscale, raw material is dissolved in organic solvent and purified water respectively and carries out dosing, filter with micropore filter element, filling, gland in 100,000 grades of toilets, then puts in storage after labeling, coding, packaging, inspection.
Filling disposable bottle, lid are temporary through de-outsourcing, sterilization: the disposable bottle that inner packing is qualified, lid respectively with being put in pass-through box after 75% ethanolic solution wiping, through ultraviolet radiation sterilization import into after 3 minutes keep between after stand-by.
Be 100,000 grades of control zones between disposable bottle is temporary, temperature 18 DEG C, humidity 30-65%, with general district pressure reduction>=10 handkerchief, 0.5 μm of airborne <3500000/m
3, 5 μm of airborne <20000/m
3.
Filling, gland: the container of splendid attire liquid should be airtight, the liquid prepared should be filling complete on the same day.
Before filling, gland first open drive machine all normal after, regulate loading amount with purified water douche can assembling system.
After filling, within every 40 minutes, extract the quality condition of semi-finished product inspection clarity, loading amount, gland tight ness rating.
Liquid completed to filling from preparation in 7 hours.
Dosing: purified water or the organic solvent of 45L will be added in Agitation Tank, open Agitation Tank mixer, the raw material of precise recipe quantity, add in Agitation Tank, stirring 20 minutes to dissolving completely, adding water, stirring 15 minutes, detect PH, content, the qualified rear filtration of color and luster, filtering liquid medicine packing after clarity passed examination.
Filter and adopt 0.45um miillpore filter.
Filling bottle is less than 24 hours standing time.
Organic solvent is ethanol.
Before weighing, the necessary each school zero of weigher, prescription must be checked, and the use amount of raw material should convert according to the actual content of raw material, water content factor, feeds intake by 100% of recipe quantity.
After drug solution preparing, carry out intermediates content, PH checks.
Must use the flow flush 10-20 minute of 250L/h before filtering liquid medicine, maximum working pressure (MWP) is 0.5Mpa, maximum differential pressure 0.3Mpa.
In filter process, as found, filter pressure declines suddenly or the rate of filtration is accelerated suddenly, then should retest the integrity of filter core.
After utensil used uses, be immersed in the bromogeramine solution of 0.5%, lower 5 minutes of necessary pressurize 0.05Mpa before filter uses.
In production process, surrounding environment is 100000 grades of clean areas, should meet 100000 grades of clean area levels necessitate.
Embodiment 2
The liquid compound premixed feed of a kind of nanoscale described in the present embodiment, with weight parts, raw material composition is preferably as follows:
Vitamin A acetic acid fat 8,000,000 IU/kg, vitamin D
35000000 IU/kg, dl-alpha-tocopherol acetic acid fat 2.0 × 10
3mg/kg, first how quinone 500mg/kg, Tyiamine Hd 600mg/kg, riboflavin 400mg/kg, puridoxine hydrochloride 3.0 × 10
3mg/kg, niacinamide 2.0 × 10
3mg/kg, D-VB5 calcium 2.0 × 10
3mg/kg, nicotinic acid 300mg/kg, folic acid 10mg/kg, Bio 20mg/kg, L-AA 3.0 × 10
3mg/kg, amino acid, manna oligosacchride 150mg/kg, chitosan oligosaccharide 3.00 × 10
3mg/kg;
Amino acid be DL ?methionine, L ?threonine, glycine, glutamine, DL ?methionine, L ?threonine, glycine, glutamine account for 0.8%, 0.4%, 0.3%, 0.8%, 0.5% of the liquid compound premixed feed quality of nanoscale respectively.
The low-carbon environment-friendly production technology of nanometer micro emulsion B B-complex is identical with embodiment 1, and difference is:
Liquid completes to being potted in 5 hours from preparation.
Dosing: purified water or the organic solvent of 60L will be added in Agitation Tank, and open Agitation Tank mixer, the raw material of precise recipe quantity, add in Agitation Tank, stirring 10 minutes to dissolving completely, adding water to full dose, stir 15 minutes, detect PH, content, the qualified rear filtration of color and luster.Filtering liquid medicine packing after clarity passed examination.
Must with the flow flush 20 minutes of 250L/h before filtering liquid medicine, maximum working pressure (MWP) is 0.5Mpa, maximum differential pressure 0.3Mpa.
Embodiment 3
The liquid compound premixed feed of a kind of nanoscale described in the present embodiment, with weight parts, raw material composition is preferably as follows:
Vitamin A acetic acid fat 9,000,000 IU/kg, vitamin D
37000000 IU/kg, dl-alpha-tocopherol acetic acid fat 4.0 × 10
3mg/kg, first how quinone 400mg/kg, Tyiamine Hd 700mg/kg, riboflavin 600mg/kg, puridoxine hydrochloride 2.0 × 10
3mg/kg, niacinamide 4.0 × 10
3mg/kg, D-VB5 calcium 4.0 × 10
3mg/kg, nicotinic acid 220mg/kg, folic acid 20mg/kg, Bio 30mg/kg, L-AA 4.0 × 10
3mg/kg, amino acid, manna oligosacchride 200mg/kg, chitosan oligosaccharide 2.00 × 10
3mg/kg.
Amino acid be DL ?methionine, L ?threonine, glycine, glutamine, DL ?methionine, L ?threonine, glycine, glutamine account for 0.9%, 0.3%, 0.5%, 0.6%, 0.5% of the liquid compound premixed feed quality of nanoscale respectively.
The low-carbon environment-friendly production technology of nanometer micro emulsion B B-complex is identical with embodiment 1, and difference is:
Liquid completes to being potted in 6 hours from preparation.
Dosing: purified water or the organic solvent of 50L will be added in Agitation Tank, and open Agitation Tank mixer, the raw material of precise recipe quantity, add in Agitation Tank, stirring 15 minutes to dissolving completely, adding water to full dose, stir 10 minutes, detect PH, content, the qualified rear filtration of color and luster.Filtering liquid medicine packing after clarity passed examination.
Must with the flow flush 15 minutes of 250L/h before filtering liquid medicine, maximum working pressure (MWP) is 0.5Mpa, maximum differential pressure 0.3Mpa.
Checking in production process of the present invention is as table 1.
Checking in table 1 production process of the present invention
The calculating of technical-economic index and the norm quota of consumption.
1 computational methods
1.1 yield rates: the ratio of actual output and theoretical yield.
Yield rate %=finished product warehouse-in number (bottle)/theoretical yield (bottle) × 100%
Theoretical yield (bottle)=total inventory (pure amount)/labelled amount
Regulation loading amount:
98 ~ 102ml/ bottle, average loading amount must not be less than 100ml/ bottle.
198 ~ 202ml/ bottle, average loading amount must not be less than 200ml/ bottle.
247 ~ 253ml/ bottle, average loading amount must not be less than 250ml/ bottle.
495 ~ 505ml/ bottle, average loading amount must not be less than 500ml/ bottle.
995 ~ 1005ml/ bottle, average loading amount must not be less than 1000ml/ bottle.
Yield rate 96-100%.
1.2 disposable bottles of utilization rate >=96%
Disposable bottle utilization rate %=finished product warehouse-in number (bottle)/(the disposable bottle number of number-cancelling stocks received by disposable bottle) × 100%.
1.3 every bottle of solution primary raw material consumptions
Unit consumption=total inventory (not pure)/finished product warehouse-in number.
1.4 high-grade-goods rate
Top grade product amount/finished product warehouse-in number × 100% of high-grade-goods rate=finished product warehouse-in number;
1.5 carton utilization rate >=99%;
1.6 label utilization rate >=98%;
1.7 quality certification utilization rate >=98%.
Claims (10)
1. the liquid compound premixed feed of nanoscale, it is characterized in that, with weight parts, raw material is composed as follows:
Vitamin A acetic acid fat 800 ~ 1.00 × 10
3ten thousand IU/kg, vitamin D
3500 ~ 8,000,000 IU/kg, dl-alpha-tocopherol acetic acid fat>=2.0 × 10
3mg/kg, first be quinone>=250mg/kg, Tyiamine Hd>=500mg/kg, riboflavin>=400mg/kg, puridoxine hydrochloride>=1.0 × 10 how
3mg/kg, niacinamide>=2.0 × 10
3mg/kg, D-VB5 calcium>=1.0 × 10
3mg/kg, nicotinic acid>=120mg/kg, folic acid>=10mg/kg, Bio>=10mg/kg, L-AA>=3.0 × 10
3mg/kg, amino acid, manna oligosacchride 150 ~ 300mg/kg, chitosan oligosaccharide 1.50 × 10
3~ 3.00 × 10
3mg/kg; Wherein, amino acid accounts for the 2.0-5.0% of liquid compound premixed feed quality.
2. the liquid compound premixed feed of nanoscale according to claim 1, it is characterized in that, amino acid is DL-METHIONINE, L-threonine, glycine, glutamine.
3. the liquid compound premixed feed of nanoscale according to claim 2, it is characterized in that, DL-METHIONINE, L-threonine, glycine, glutamine account for 0.8%, 0.1%, 0.3%, 0.4%, 0.5% of the liquid compound premixed feed quality of nanoscale respectively.
4. the production technology of the liquid compound premixed feed of nanoscale according to claim 1, it is characterized in that, raw material is dissolved in organic solvent and purified water respectively and carries out dosing, filter with micropore filter element, filling, gland in 100,000 grades of toilets, then puts in storage after labeling, coding, packaging, inspection.
5. the production technology of the liquid compound premixed feed of nanoscale according to claim 4, it is characterized in that, filling disposable bottle, lid are temporary through de-outsourcing, sterilization: the disposable bottle that inner packing is qualified, lid, respectively with being put in pass-through box after 75% ethanolic solution wiping, imported into after between keeping in stand-by after ultraviolet radiation sterilization 3-6 minute.
6. the production technology of the liquid compound premixed feed of nanoscale according to claim 5, is characterized in that, is 100,000 grades of control zones between disposable bottle is temporary, temperature 18-26 DEG C, humidity 30-65%, with general district pressure reduction>=10 handkerchief, 0.5 μm of airborne <3500000/m
3, 5 μm of airborne <20000/m
3.
7. the production technology of the liquid compound premixed feed of nanoscale according to claim 4, it is characterized in that, filling, gland: the container of splendid attire liquid should be airtight, the liquid prepared should be filling complete on the same day.
8. the production technology of the liquid compound premixed feed of nanoscale according to claim 4, is characterized in that, before filling, gland first open drive machine all normal after, regulate loading amount with purified water douche can assembling system; After filling, within every 25-40 minute, extract the quality condition of semi-finished product inspection clarity, loading amount, gland tight ness rating; Liquid completed to filling from preparation in 5-7 hour.
9. the production technology of the liquid compound premixed feed of nanoscale according to claim 4, it is characterized in that, dosing: purified water or the organic solvent of 45-60L will be added in Agitation Tank, and open Agitation Tank mixer, the raw material of precise recipe quantity, add in Agitation Tank, stirring 10-20 minute to dissolving completely, adding water, stir 8-15 minute, detect PH, content, the qualified rear filtration of color and luster, filtering liquid medicine packing after clarity passed examination.
10. the production technology of the liquid compound premixed feed of nanoscale according to claim 9, is characterized in that, filter and adopt 0.45um miillpore filter.
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CN107347473A (en) * | 2017-07-04 | 2017-11-17 | 岭南园林股份有限公司 | A kind of trees drip solution production system and its production technology |
CN112674211A (en) * | 2020-12-15 | 2021-04-20 | 济南深蓝动物保健品有限公司 | Liquid livestock and poultry vitamin premixed feed and preparation method thereof |
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Application publication date: 20160224 |