CN105336261A - Pyromellitic dianhydride teaching factory for teaching and training - Google Patents

Pyromellitic dianhydride teaching factory for teaching and training Download PDF

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Publication number
CN105336261A
CN105336261A CN201410383489.5A CN201410383489A CN105336261A CN 105336261 A CN105336261 A CN 105336261A CN 201410383489 A CN201410383489 A CN 201410383489A CN 105336261 A CN105336261 A CN 105336261A
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China
Prior art keywords
chemical
teaching
chemical plant
instruments
area
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Pending
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CN201410383489.5A
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Chinese (zh)
Inventor
吴永贵
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Nanjing College of Chemical Technology
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Nanjing College of Chemical Technology
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Priority to CN201410383489.5A priority Critical patent/CN105336261A/en
Publication of CN105336261A publication Critical patent/CN105336261A/en
Pending legal-status Critical Current

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Abstract

The invention discloses a pyromellitic dianhydride teaching factory for teaching and training. The teaching factory comprises a chemical plant production area, a chemical plant control area and a teaching discussion area, wherein a small-size pyromellitic dianhydride production device is constructed inside the chemical plant production area; the small-sized pyromellitic dianhydride production device comprises chemical equipment, chemical instruments and a device frame; the device frame is a steel platform; the chemical equipment and the chemical instruments are arranged on the steel platform; and the chemical instruments and the chemical equipment are connected by virtue of pipelines and cables. The chemical device control area is composed of a control cabinet and an industrial personal computer; and the chemical device control area is connected to the small-sized pyromellitic dianhydride production device by virtue of a signal cable. The teaching discussion area comprises student computers, multimedia teaching facilities and simulation operation software. The teaching factory disclosed by the invention can solve the problems of an industrial device which is large in occupied area, high in investment and high in operating cost, and the problem on safety factors. The teaching factory disclosed by the invention, when used for implementing teaching, enables students to operate an actual chemical production device, so that students' understanding of chemical equipment and devices is enhanced.

Description

A kind of pyromellitic acid anhydride school workshop for teaching, training
Technical field
The present invention relates to a kind of school workshop of chemical field, belong to education, chemical process and equipment technical field, for the teaching of universities and colleges of enterprise chemical and relevant speciality, training, practice, and carry out the training of chemical technician and senior technician.
Background technology
Due to singularity (inflammable, explosive, poisonous, harmful and high temperature etc. of chemical industry.), be not suitable for carrying out on commercial plant carrying out practising, in practice-training teaching training.Expense and safety be also must consider factor (its raw materials consumption, energy consumption etc., does is key that how a large amount of product processes in repetition training?).And chemical products are of a great variety, its synthetic method is not quite similar.Same raw material can produce different chemicals, and identical product can be produced by different raw materials, and its technique of the product line of same raw material is also incomplete same.So the teaching of universities and colleges, training, practice generally adopt a certain categorizing selection to carry out, as fixed bed reactors, fluidized-bed reactor, tank reactor etc.; Or themopositive reaction, thermonegative reaction etc.Following three kinds are roughly had at present: the first goes chemical enterprise to practise exactly for chemical teaching, training, student can be familiar with chemical plant, instrument at this and be familiar with chemical production technology flow process, but student can only see inactive, be also just far from being and improve operative skill; The second is exactly popular completely virtual chemical plant installations (i.e. simulation software) for many years, in kind without any chemical plant, only can carry out pseudo operation on computers, it is less to drop into little operating cost, and safety energy-conserving environment protection, all there are this teaching software in most of universities and colleges; The third is the chemical plant installations built in lyceum, has real chemical plant, simulation instrument and simulation operations software, does not throw industrial chemicals, do not produce chemical products.Student can be familiar with chemical plant, instrument and be familiar with chemical production technology flow process on this device, can also carry out simulation operations.Except input ratio the first greatly except, its operating cost etc. are close with the second.Owing to being at simulation operation apparatus, student train in such circumstances just have false sensation (with play games the same, mistake rebegins, and can not produce the consequence that true chemical plant installations is such, that is so training is difficult to drop into, and does not have the sense of duty on the spot in person.)。There is very large difference in actual device and analogue means, if the emulation of its abnormal occurrence is that people presets, and actual device is produced by many reasons, is difficult to practise real skill.
Summary of the invention
The object of this invention is to provide a kind of pyromellitic acid anhydride school workshop for teaching, training, to solve falseness, real not problem that existing analogue means exists.
For achieving the above object, the present invention is by the following technical solutions:
For a pyromellitic acid anhydride school workshop for teaching, training, it is characterized in that: comprise chemical plant installations production area, chemical plant installations control zone, teaching Discussion district;
Wherein, small-sized pyromellitic acid anhydride process units is had in chemical plant installations production area, small-sized pyromellitic acid anhydride process units comprises chemical plant, chemical instruments and device frame, device frame is steel platform, chemical plant, chemical instruments are arranged on steel platform, and chemical instruments are connected by pipeline and cable with chemical plant.
Chemical plant installations control zone is made up of switch board, industrial computer, is connected by signal cable with above-mentioned small-sized pyromellitic acid anhydride process units.
Teaching Discussion district comprises student's computer, multimedia teaching facility and simulated operation software.
Described chemical plant comprises: electromagnetical blower fan, air cushioning tank, carburetor, air preheater, reactor, drip catcher, water absorber, flowmeter, pressure unit, solenoid valve, electric control valve etc.
Further, flowmeter comprises mass flowmeter and wet test meter.
Further, switch board is made up of domestic instruments, comprises intelligent regulator, flow integrator, multichannel measurement alarm etc.
Further, industrial computer is by the control procedure of domestic configuration software configuration implement device, there is the Three Dimensional Interface of animated function, also there is real-time data acquisition, function that data history preservation, realtime curve, the inquiry of historical data, report query, Drawing of Curve, form curve printing, pid parameter are adjusted.
Further, simulated operation software is the same with device function software to be realized by domestic configuration software configuration, and operation interface and active station interface phase are together.
To the invention has the beneficial effects as follows: its structure designs by commercial plant, and making and installation, true to embody, be only the difference of output size, solve that commercial plant floor area is large, investment is large, operating cost is high and the problem of safety factor.Utilize the invention process to impart knowledge to students, student can be allowed to operate real chemical production device, improve the understanding of student to chemical plant and device, the operant level of student can be improved, cultivate collaboration capabilities and the sense of community of student.Effectively can alleviate the ubiquitous one-house show of current school, find the problem of the drawback of enterprise's real training difficulty.Trainee carries out the checking of the driving of device, parking, accident treatment operation and technological parameter in the school, and this is the training condition that industrial enterprise can not provide.
Accompanying drawing explanation
Fig. 1 is schematic diagram of the present invention.
Fig. 2 is the composition schematic diagram of chemical plant installations of the present invention.
1-chemical plant installations production area in figure, 2-chemical plant installations control zone, 3-teaching Discussion district.11-electromagnetical blower fan, 12-air cushioning tank, 13-carburetor, 14, first, second air preheater of 15-, 16-reactor, 17, first, second drip catcher of 18-, 19-water absorbs to be inhaled, 20-wet type air-flow gauge, 21,22-mass flowmeter, 23,24-electric control valve, 25,26-solenoid valve.
Specific embodiment
Below in conjunction with accompanying drawing, the present invention will be further described.
As shown in Figure 1, a kind of pyromellitic acid anhydride school workshop for teaching, training, comprises chemical plant installations production area 1, chemical plant installations control zone 2, teaching Discussion district 3.
Wherein, small-sized pyromellitic acid anhydride process units is had in chemical plant installations production area, small-sized pyromellitic acid anhydride process units comprises chemical plant, chemical instruments and device frame, device frame is steel platform, chemical plant, chemical instruments are arranged on steel platform, and chemical instruments are connected by pipeline and cable with chemical plant.
Chemical plant installations control zone is made up of switch board, industrial computer, is connected by signal cable with above-mentioned small-sized pyromellitic acid anhydride process units.
Teaching Discussion district comprises student's computer, multimedia teaching facility and simulated operation software.
As shown in Figure 2, above-mentioned chemical plant installations comprises: electromagnetical blower fan, air cushioning tank, carburetor, air preheater, reactor, drip catcher, water absorber, flowmeter, pressure unit, solenoid valve, electric control valve etc.
Described chemical plant comprises: electromagnetical blower fan, air cushioning tank, carburetor, air preheater, reactor, drip catcher, water absorber, flowmeter, pressure unit, solenoid valve, electric control valve etc.
Further, flowmeter comprises mass flowmeter and wet test meter.
Further, switch board is made up of domestic intelligent instrument, comprises intelligent regulator, flow integrator, measurement alarm etc.
Further, industrial computer is by the control procedure of domestic configuration software configuration implement device, there is the Three Dimensional Interface of animated function, also there is real-time data acquisition, function that data history preservation, realtime curve, the inquiry of historical data, report query, Drawing of Curve, form curve printing, pid parameter are adjusted.
Simulated operation software is the same with device function software to be realized by domestic configuration software configuration, and operation interface and active station interface phase are together.
Operating process of the present invention is as follows:
(1) weighed by the carburetor 3 being added with durene, the weight of the first drip catcher 7, second drip catcher 8 of simultaneously weighing, wherein two catches and will weigh with interior filling together with cotton; (2) contrast process chart and each several part instrument is installed, adapter and adapter junction be paid special attention to, closely in order to avoid gas leakage; (3) check water absorber 9 liquid level, supplementing water, to assigned position, has supplemented timely closedown water intaking valve; (4) check whether air cushioning tank 2 bottom blow-down valve closes; (5) engaging means power supply, by login interface requirement input personal information; (6) check that whether the display of each instrument is correct, as there is error message, looking up the fault is also repaired; (7) confirm that device starts to heat up without error starting heating; (8) when the first air preheater 4, second air preheater 5 temperature rises to 150 DEG C, open electromagnetic valve 16.If variable valve 13,14 aperture, start electromagnetical blower fan 1, carry out system warm-up; (9) when temperature of reaction reaches lower than predetermined temperature of reaction about 20 ~ 30 DEG C, solenoid valve 15 is opened, and shut electromagnetic valve 16, connection carburetor 3 and reactor 6 carry out oxidation reaction; (10) every 10 minutes, record primary air flow 11, secondary air flow 12, exhaust flow 10, temperature, phenomenon etc.; (11) when determining to terminate reaction, open electromagnetic valve 16, closes solenoid valve 15, cuts off the connection of reactor and carburetor, continues logical warm air blowoff 15 minutes, stops heating; (12) Blowing stopper 1, drives surge tank 2 blowoff valve; (13) variable valve 13,14 aperture be set to 0 and close power supply, closing solenoid valve 16; (14) log off, system automatic shutdown; (15) taking-up carburetor 3, is caught 7 and two and is caught 8, takes the weight of carburetor 3 and drip catcher 7,8 respectively, draws the consumption consumption of durene and the general assembly (TW) of thick acid anhydride by the method for reducing.Thick product is through the content of stratographic analysis wherein dianhydride; (16) cleaning supplies and workspace.Can check real time data on active station at any time in operating process, the inquiry of historical data, report query, Drawing of Curve, form curve printing and pid parameter are adjusted.

Claims (9)

1. for a pyromellitic acid anhydride school workshop for teaching, training, it is characterized in that: comprise chemical plant installations production area, chemical plant installations control zone, teaching Discussion district.
2. have small-sized pyromellitic acid anhydride process units in chemical plant installations production area described in claim 1, small-sized pyromellitic acid anhydride process units comprises chemical plant, chemical instruments and device frame.
3. device frame is steel platform, and chemical plant, chemical instruments are arranged on steel platform, and chemical instruments are connected by pipeline and cable with chemical plant.
4. described in claim 1, chemical plant installations control zone is made up of switch board, industrial computer, is connected by signal cable with above-mentioned small-sized pyromellitic acid anhydride process units.
5. teaching Discussion district described in claim 1 comprises student's computer, multimedia teaching facility and simulated operation software.
6. described in claim 2, chemical plant comprises: electromagnetical blower fan, air cushioning tank, carburetor, air preheater, reactor, drip catcher, water absorber, flowmeter, pressure unit, solenoid valve, electric control valve etc.
7. described in claim 3, switch board is made up of domestic instruments, comprises intelligent regulator, flow integrator, multichannel measurement alarm etc.
8. simulated operation software described in claim 4 is the same with device function software is realized by domestic configuration software configuration, and operation interface and active station interface phase are together.
9. flowmeter described in claim 5 comprises mass flowmeter and wet test meter.
CN201410383489.5A 2014-08-06 2014-08-06 Pyromellitic dianhydride teaching factory for teaching and training Pending CN105336261A (en)

Priority Applications (1)

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CN105336261A true CN105336261A (en) 2016-02-17

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110070791A (en) * 2019-04-16 2019-07-30 杭州百子尖科技有限公司 Based on wireless technology can design mode parsing intelligent simulation device and emulation mode

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101546489A (en) * 2009-04-30 2009-09-30 南京化工职业技术学院 Tetroxide prepared pmda device for practice-training teaching
CN201799265U (en) * 2010-09-19 2011-04-20 南京化工职业技术学院 Device for controlling hot spots in production of durene oxidation to PMDA (pyromellitic dianhydride)
CN102031883A (en) * 2011-01-10 2011-04-27 南京化工职业技术学院 Simulation teaching factory for preparing cyclohexane through benzene hydrogenation
CN201993979U (en) * 2010-12-13 2011-09-28 南京化工职业技术学院 Operation training device based on pyromellitic dianhydride industrial production
CN102881215A (en) * 2012-10-15 2013-01-16 南京化工职业技术学院 Simulation teaching factory for producing aniline by hydrogenating nitrobenzene
CN204029265U (en) * 2014-08-06 2014-12-17 南京化工职业技术学院 A kind of pyromellitic acid anhydride school workshop for teaching, training

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101546489A (en) * 2009-04-30 2009-09-30 南京化工职业技术学院 Tetroxide prepared pmda device for practice-training teaching
CN201799265U (en) * 2010-09-19 2011-04-20 南京化工职业技术学院 Device for controlling hot spots in production of durene oxidation to PMDA (pyromellitic dianhydride)
CN201993979U (en) * 2010-12-13 2011-09-28 南京化工职业技术学院 Operation training device based on pyromellitic dianhydride industrial production
CN102031883A (en) * 2011-01-10 2011-04-27 南京化工职业技术学院 Simulation teaching factory for preparing cyclohexane through benzene hydrogenation
CN102881215A (en) * 2012-10-15 2013-01-16 南京化工职业技术学院 Simulation teaching factory for producing aniline by hydrogenating nitrobenzene
CN204029265U (en) * 2014-08-06 2014-12-17 南京化工职业技术学院 A kind of pyromellitic acid anhydride school workshop for teaching, training

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110070791A (en) * 2019-04-16 2019-07-30 杭州百子尖科技有限公司 Based on wireless technology can design mode parsing intelligent simulation device and emulation mode
CN110070791B (en) * 2019-04-16 2021-08-10 杭州百子尖科技股份有限公司 Wireless technology-based designable analytic intelligent simulation device and simulation method

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